WO2022176692A1 - Soft drink - Google Patents
Soft drink Download PDFInfo
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- WO2022176692A1 WO2022176692A1 PCT/JP2022/004819 JP2022004819W WO2022176692A1 WO 2022176692 A1 WO2022176692 A1 WO 2022176692A1 JP 2022004819 W JP2022004819 W JP 2022004819W WO 2022176692 A1 WO2022176692 A1 WO 2022176692A1
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- WO
- WIPO (PCT)
- Prior art keywords
- mass ppm
- malt
- soft drink
- less
- beverage
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- 235000014214 soft drink Nutrition 0.000 title claims abstract description 117
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims abstract description 69
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- 235000010323 ascorbic acid Nutrition 0.000 claims abstract description 34
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- 239000002994 raw material Substances 0.000 claims description 28
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
Definitions
- the present invention relates to soft drinks.
- Patent Document 1 describes a method for producing a non-alcoholic fermented beverage, which can reduce the alcohol concentration by about 40 to 55% compared to conventional methods by adding ⁇ -glucosidase before the fermentation process in beer production. has been disclosed.
- a typical non-alcoholic beer-taste beverage produced by the method described in Patent Document 1 often lacks the texture typical of a malt-taste beverage. Therefore, there is a demand for a soft drink with an improved texture that is typical of malt-taste beverages. There is also a demand for a soft drink that not only has an improved texture, but also has a refreshing aftertaste and a good bitter aftertaste, which are characteristic of malt-taste beverages.
- the present invention provides a soft drink having a sucralose content of 0.1 to 4.5 mass ppm and an ascorbic acid content of 70 to 190 mass ppm. That is, the present invention includes inventions of the following aspects.
- the content of sucralose is 0.1 to 4.5 mass ppm
- the content of ascorbic acid is 70 to 190 mass ppm
- Soft drink [2] [1], wherein the content ratio of the sucralose content (unit: mass ppm) and the ascorbic acid content (unit: mass ppm) [sucralose/ascorbic acid] is 0.005 to 0.04 soft drink.
- a soft drink according to a preferred embodiment of the present invention can be a drink with improved texture.
- the soft drink of one preferred embodiment of the present invention can be a drink with a good refreshing aftertaste and a good bitter aftertaste, which is typical of malt-taste drinks.
- soft drinks refer to juices, carbonated drinks, malt drinks, lactic acid drinks, health drinks, sports drinks, amino acid drinks, vitamin drinks, malt-taste drinks, hop-taste drinks and the like.
- malt-taste beverage means a beverage having the flavor of wort obtained from barley and/or malt, and includes beverages imparted with a refreshing sensation by carbon dioxide gas or the like.
- a malt-tasting beverage may contain less than 1 (v/v %) alcohol.
- alcohol-containing malt-taste beverages include fermented malt-taste beverages and alcohol-added beverages.
- Alcohol-free malt-taste beverages include beverages obtained by removing alcohol, other low-boiling-point components and low-molecular-weight components from fermented malt-taste beverages.
- the raw material for the malt-taste beverage may be any raw material having the flavor of wort obtained from wheat and/or malt, and grains other than wheat and malt may be used.
- Grains that can be used as raw materials for malt-taste beverages include, for example, barley, malt, non-malt (barley, wheat, rye, oats, oats, pigeons, oats, etc.), rice (polished rice, brown rice).
- wort obtained from barley and/or malt may be used for the production of malt-taste beverages, or flavoring agents having a flavor similar to that of wort obtained from barley and/or malt may be used.
- the term "hop-flavored beverage” means a beverage having a hop flavor, and the thirst-quenching feeling obtained when using hop-derived raw materials, etc., and the refreshing and richness of a floral scent.
- the beverage has a balance of flavor, and a taste that is easy to drink with good texture and smoothness in the mouth.
- the hop-taste beverages also include beverages imparted with a refreshing feeling by carbon dioxide gas or the like.
- a hop-tasting beverage may contain less than 1 (v/v %) alcohol.
- the alcohol-containing hop-taste beverages include hop-taste beverages obtained by fermentation and alcohol-added beverages.
- Alcohol-free hop-taste beverages include beverages obtained by removing alcohol, other low-boiling-point components and low-molecular-weight components from hop-taste beverages obtained by fermentation.
- a bittering agent or a bittering agent may be used instead of hops.
- Bittering agents and bittering agents that can be used in hop-taste beverages include, for example, Ganoderma lucidum, Ganoderma lucidum, Himejiko, Juniper nut, Sage, Astragalus, Ganoderma lucidum, Laurel, Quassin, Citrus extract, Nigaki extract, Coffee extract, tea extract, bitter gourd extract, lotus germ extract, aloe vera extract, stonecrop extract, litchi extract, laurel extract, sage extract, caraway extract, naringin, wormwood and wormwood extract, etc. are mentioned. These may be used alone or in combination of two or more.
- the alcohol content of the soft drink of one embodiment of the present invention may be less than 1 (v/v%), preferably less than 0.5 (v/v)%, more preferably less than 0.1 (v/v%). v) %, more preferably less than 0.01 (v/v) %, even more preferably less than 0.005 (v/v) %.
- alcohol content shall be shown by the percentage (v/v%) of a volume/volume basis.
- the alcohol content of a drink can be measured by any well-known method, it can be measured by a gas chromatography, for example.
- a soft drink of one aspect of the present invention is a fermented beverage obtained by removing alcohol produced in the fermentation process after undergoing a fermentation process using yeast (top-fermenting yeast or bottom-fermenting yeast) in the production process, Alternatively, it may be a non-fermented beverage prepared without undergoing such a fermentation process.
- esters When the soft drink of one aspect of the present invention is a non-fermented drink, esters, higher alcohols (e.g., isoamyl acetate, ethyl acetate, n-propanol, isobutanol, acetaldehyde, Ethyl caproate, linalool, 4-vinyl guaiacol, isoamyl propionate, etc.), acids (e.g., 2-methyl-2-pentenoic acid, 4-methyl-3-pentenoic acid), etc.
- Carbonated beverages adjusted to have flavor or hop flavor are also included in the non-fermented refreshing beverage, malt-taste beverage, and hop-taste beverage of one aspect of the present invention.
- the soft drinks, malt-taste beverages, and hop-taste beverages of one aspect of the present invention may be malt-containing soft drinks that use malt as an ingredient, or malt-free soft drinks that do not use malt.
- malted beverages are preferred, barley malted beverages are more preferred.
- Such common soft drinks have a low alcohol content, so they tend to be insufficiently satisfying to drink. If a sweetener is added in order to impart a satisfying feeling to the drink, the refreshing aftertaste tends to be reduced. Beverages containing a large amount of sweeteners tend to have an unbalanced bitter aftertaste typical of soft drinks.
- a beverage containing sucralose and ascorbic acid compared to conventional soft drinks, it is possible to improve the good feeling of drinking malt taste beverages or hop taste beverages. It was found that the refreshing aftertaste and bitterness typical of beverages can be improved in a well-balanced manner. The present invention has been made based on this finding.
- the content of sucralose in the soft drink of one embodiment of the present invention is 0.1 to 4.5 ppm by mass based on the total amount of the soft drink, but it imparts a soft drink-like feel and improves the bitterness of the aftertaste.
- 0.2 mass ppm or more preferably 0.3 mass ppm or more, more preferably 0.4 mass ppm or more, more preferably 0.5 mass ppm or more , more preferably 0.6 mass ppm or more, more preferably 0.7 mass ppm or more, still more preferably 0.8 mass ppm or more, still more preferably 0.9 mass ppm or more, particularly preferably 1.0 mass ppm ppm or more, 1.2 mass ppm or more, 1.4 mass ppm or more, 1.5 mass ppm or more, 1.7 mass ppm or more, 1.9 mass ppm or more, 2.0 mass ppm or more, 2 .2 mass ppm or more, 2.4 mass ppm or more,
- the content of ascorbic acid in the soft drink of one aspect of the present invention is 70 to 190 ppm by mass based on the total amount of the soft drink, but it imparts a chewy texture typical of a malt-taste or hop-taste drink and has a refreshing aftertaste.
- the soft drink is preferably 80 mass ppm or more, more preferably 90 mass ppm or more, more preferably 100 mass ppm or more, more preferably 110 mass ppm or more, based on the total amount of the soft drink, and further, It may be 120 mass ppm or more, 130 mass ppm or more, 140 mass ppm or more, preferably 185 mass ppm or less, more preferably 180 mass ppm or less, 175 mass ppm or less, 170 mass ppm or less, 165 It may be mass ppm or less, 160 mass ppm or less, 155 mass ppm or less, 150 mass ppm or less, or 145 mass ppm or less.
- the content of sucralose (unit: mass ppm) and The content ratio [sucralose/ascorbic acid] to the content of ascorbic acid (unit: mass ppm) is preferably 0.005 to 0.04, more preferably 0.006 or more, and 0.007 or more.
- 034 or less is more preferable, 0.033 or less is still more preferable, 0.032 or less is still more preferable, 0.031 or less is even more preferable, 0.030 or less is particularly preferable, and 0.028 or less, 0 It may be 0.026 or less, 0.025 or less, or 0.023 or less.
- the soft drink of one aspect of the present invention preferably further contains acesulfame potassium (acesulfame K).
- acesulfame K acesulfame K
- sucralose and ascorbic acid it is possible to obtain a soft drink with a more improved feel like a malt-taste beverage or a hop-taste beverage.
- the content of acesulfame potassium is preferably 1.0%, based on the total amount of the soft drink, from the viewpoint of making the beverage more satisfying to drink, which is typical of malt-taste beverages or hop-taste beverages.
- 0 mass ppm or more more preferably 3.0 mass ppm or more, still more preferably 5.0 mass ppm, even more preferably 7.0 mass ppm or more, particularly preferably 10 mass ppm or more, and further preferably 12 mass ppm
- it may be 14 mass ppm or more, 15 mass ppm or more, 17 mass ppm or more, 19 mass ppm or more, 20 mass ppm or more, or 22 mass ppm or more.
- the content of acesulfame potassium is preferably 700 ppm by mass or less, more preferably 600 ppm by mass, based on the total amount of the soft drink, from the viewpoint of making a beverage with a more improved feel like a malt-taste beverage or a hop-taste beverage.
- ppm or less more preferably 500 mass ppm or less, more preferably 450 mass ppm or less, still more preferably 400 mass ppm or less, still more preferably 350 mass ppm or less, even more preferably 300 mass ppm or less, particularly preferably 250 mass ppm 200 mass ppm or less, 150 mass ppm or less, 100 mass ppm or less, 90 mass ppm or less, 80 mass ppm or less, 70 mass ppm or less, 60 mass ppm or less, 50 mass ppm or less, or 40 mass ppm It may be below.
- the soft drink of one aspect of the present invention in addition to the sharp aftertaste that is typical of a malt-taste beverage or a hop-taste beverage, it imparts a chewiness that is typical of a malt-taste beverage or a hop-taste beverage, resulting in an unsuitable aftertaste for a malt-taste beverage or a hop-taste beverage.
- the ratio of the sucralose content (unit: mass ppm) and the acesulfame potassium content (unit: mass ppm) [sucralose/acesulfame potassium] is preferably 0.05 or more.
- preferably 0.1 or more still more preferably 0.15 or more, still more preferably 0.2 or more, still more preferably 0.25 or more, particularly preferably 0.3 or more, more particularly preferably 0.33 or more 0.5 or more, 0.7 or more, 1.0 or more, 2.0 or more, 3.0 or more, 4.0 or more, 5.0 or more, 6.0 or more, 7.0 or more, 8.0 or more, 9.0 or more, 10.0 or more, 15.0 or more, or 20.0 or more, preferably 700 or less, more preferably 650 or less, still more preferably 600 or less, and even more It is preferably 550 or less, particularly preferably 500 or less, more preferably 400 or less, and may be 350 or less, 300 or less, 250 or less, or 200 or less.
- the soft drink of one embodiment of the present invention may further contain lactic acid from the viewpoint of imparting a refreshing aftertaste typical of a malt-taste beverage or a hop-taste beverage and a bitter aftertaste typical of a malt-taste beverage or a hop-taste beverage in a well-balanced manner.
- the content of lactic acid is preferably 1.0 mass ppm or more, more preferably 10.0 mass ppm or more, still more preferably 30.0 mass ppm or more, and even more preferably 50.0 mass ppm, based on the total amount of the soft drink.
- mass ppm or more more preferably 100 mass ppm or more, still more preferably 150 mass ppm or more, particularly preferably 200 mass ppm or more, preferably 700 mass ppm or less, more preferably 600 mass ppm or less, and further It is preferably 500 mass ppm or less, more preferably 400 mass ppm or less, and particularly preferably 350 mass ppm or less.
- the content of tartaric acid is Based on the total amount (100% by mass) of the beverage, preferably less than 300 mass ppm, more preferably 200 mass ppm or less, even more preferably 100 mass ppm or less, even more preferably 50 mass ppm or less, still more preferably 30 mass ppm Below, more preferably 20 mass ppm or less, particularly preferably 10 mass ppm or less, 0 mass ppm or more, 0.01 mass ppm or more, 0.1 mass ppm or more, 0.5 mass ppm or more, 1 0 mass ppm or more, 2.0 mass ppm or more, 3.0 mass ppm or more, 4.0 mass ppm or more, or 5.0 mass ppm or more.
- the phosphoric acid content is Based on the total amount (100 mass%) of the soft drink, preferably less than 300 mass ppm, more preferably 200 mass ppm or less, even more preferably 100 mass ppm or less, even more preferably 50 mass ppm or less, still more preferably 30 mass ppm Mass ppm or less, more preferably 20 mass ppm or less, particularly preferably 10 mass ppm or less, and 0 mass ppm or more, 0.01 mass ppm or more, 0.1 mass ppm or more, 0.5 mass ppm or more , 1.0 mass ppm or more, 2.0 mass ppm or more, 3.0 mass ppm or more, 4.0 mass ppm or more, or 5.0 mass ppm or more.
- the contents of ascorbic acid, lactic acid, tartaric acid, and phosphoric acid in soft drinks can be measured by high performance liquid chromatography.
- the content of sucralose and acesulfame potassium in soft drinks can also be measured by high performance liquid chromatography.
- Calorie content of the soft drink of one aspect of the present invention is preferably less than 5 kcal per 100 mL.
- the calorie can be controlled by adjusting the blending composition, blending amount, etc. of raw materials (eg, grains such as malt, barley, hops, etc.).
- the calories of soft drinks are calculated by adding the energy conversion factors of each component (protein: 4 kcal/g, fat: 9 kcal/g, sugar: 4 kcal/g, dietary fiber: 2 kcal/g , alcohol: 7 kcal/g, organic acid: 3 kcal/g).
- the pH of the soft drink of one embodiment of the present invention is not particularly limited, but is preferably less than 4.0. 0 or more.
- the total extract amount of the soft drink of one embodiment of the present invention is not particularly limited, but is preferably 1.5% by weight or less, more preferably 1.1% by weight, from the viewpoint of making the beverage imparted with a light mouthfeel. Below, more preferably 0.80% by weight or less, still more preferably less than 0.50% by weight.
- total extract amount in this specification is a revised BCOJ beer analysis method edited by the Beer Brewers Association International Technical Committee (BCOJ) for degassed samples (published by the Brewing Association of Japan, expanded and revised in 2013).
- BCOJ Beer Brewers Association International Technical Committee
- the color of the soft drink of one embodiment of the present invention is not particularly limited. good too.
- the color of the beverage can be determined with the naked eye, but it may also be defined by total light transmittance, chromaticity, or the like.
- the soft drink of one embodiment of the present invention may be in any form as long as the beverage is packed in a container, and examples of the container include bottles, PET bottles, cans, and barrels. cans, bottles, or PET bottles are preferable.
- Water and malt may or may not be used as the main raw materials of soft drinks such as malt-taste beverages and hop-taste beverages of one embodiment of the present invention.
- hops may be used, and preservatives, sweeteners, water-soluble dietary fibers, bittering agents or bitterness-imparting agents, antioxidants, flavors, acidulants, salts, and the like may also be used.
- the malt refers to germinated seeds of barley, wheat, rye, oats, oats, pigeons, oats, etc., dried, and rooted. Any variety may be used.
- the malt to be used is preferably malted barley.
- Barley malt is one of the most commonly used malts as an ingredient in Japanese malt-taste and hop-taste beverages.
- barley such as two-rowed barley and six-rowed barley, and any of them may be used.
- colored malt can also be used. When using colored malt, different types of colored malt may be appropriately combined and used, or one type of colored malt may be used.
- Grains other than malt may also be used together with malt.
- examples of such grains include wheat (barley, wheat, rye, oats, oats, pigeons, oats, etc.) that do not fall under malt, rice (polished rice, brown rice, etc.), corn, koryan, potato, etc. , beans (soybeans, peas, etc.), buckwheat, sorghum, millet, barley, and starches obtained therefrom, extracts thereof (malt extract, etc.).
- malt extract means a concentrated extract obtained by saccharifying barley (preferably malt).
- liquid sugar containing a carbon source when malt is not used, liquid sugar containing a carbon source, and soft drinks using a nitrogen source as an amino acid-containing material (for example, soybean protein, etc.) other than malt, such as the above-mentioned grains, can be mentioned.
- a nitrogen source as an amino acid-containing material (for example, soybean protein, etc.) other than malt, such as the above-mentioned grains
- hops used in one aspect of the present invention include pellet hops, powdered hops, hop extracts, and the like.
- processed hops such as isoformed hops and reduced hops may be used.
- the amount of hops to be added is appropriately adjusted, but is preferably 0.0001 to 1% by mass relative to the total amount of the beverage.
- soft drinks such as malt-taste beverages and hop-taste beverages using hops as raw materials are beverages containing iso- ⁇ acids, which are components derived from hops.
- the iso- ⁇ -acid content of the soft drink using hops may be greater than 0.1 ppm by mass or greater than 1.0 ppm by mass based on the total amount of the soft drink.
- the content of iso- ⁇ -acids in a hop-free soft drink may be 0.1 mass ppm or less based on the total amount of the soft drink.
- the content of iso- ⁇ acids is described in the revised BCOJ beer analysis method (published by the Brewing Association of Japan, Beer Brewers Association International Technical Committee [Analysis Committee] edited 2013 supplementary revision). It means a value measured by high performance liquid chromatography (HPLC) analytical method.
- the soft drink of one aspect of the present invention may be a drink further containing a preservative.
- Preservatives used in one aspect of the present invention include, for example, benzoic acid; benzoates such as sodium benzoate; benzoate esters such as propyl parahydroxybenzoate and butyl parahydroxybenzoate; dimethyl dicarbonate; Moreover, as a preservative, a commercially available preparation such as Strong Samprezer (a mixture of sodium benzoate and butyl benzoate, manufactured by San-Eigen FFI Co., Ltd.) may be used. These preservatives may be used alone or in combination of two or more.
- the amount of the preservative is preferably 5 to 1200 mass ppm, more preferably 10 to 1100 mass ppm, still more preferably 15 to 1000 mass ppm, Even more preferably 20 to 900 mass ppm.
- the soft drink of the present invention contains sucralose and may further contain acesulfame potassium, and may contain other sweeteners in addition to these sweeteners.
- sweeteners include commercially available saccharified solutions obtained by decomposing grain-derived starch with acids or enzymes, sugars such as commercially available starch syrup, sugars of trisaccharides or higher, sugar alcohols, natural sweeteners such as stevia, and artificial sweeteners. mentioned. These sweeteners may be used alone or in combination of two or more. The form of these sugars may be liquid such as solution, or solid such as powder.
- sugars with a higher proportion of maltose may be used by appropriately setting conditions for hydrolysis with an enzyme or acid.
- sucrose, fructose, glucose, maltose, trehalose, maltotriose, solutions of these (sugar solutions), and the like can also be used.
- sucralose and acesulfame potassium artificial sweeteners include aspartame and the like.
- the soft drink of one embodiment of the present invention may be a drink further containing dietary fiber such as water-soluble dietary fiber.
- dietary fiber such as water-soluble dietary fiber.
- water-soluble dietary fibers include indigestible dextrin, polydextrose, guar gum decomposition products, pectin, glucomannan, alginic acid, laminarin, fucoidin, carrageenan, and the like, from the viewpoint of versatility such as stability and safety. , indigestible dextrin or polydextrose are preferred. These dietary fibers may be used alone or in combination of two or more.
- bitterness may be imparted by hops or a hop extract obtained by isolating ⁇ -acids. You may use the bittering agent or bitterness imparting agent shown below. Instead of using hops and hop extracts obtained by isolating ⁇ -acids, the following bitterness agents or bitterness-imparting agents may be used in place of hops.
- Bittering agents or bitterness-imparting agents include, for example, Ganoderma lucidum, Ganoderma lucidum, Ganoderma lucidum, Juniper berry, Sage, Astragalus membranus, Ganoderma lucidum, Bay laurel, Kuwasin, Citrus extract, bittern bitter extract, coffee extract, tea extract, Goya extract, lotus germ extract, aloe vera extract, stonecrop extract, litchi extract, laurel extract, sage extract, caraway extract, naringin, wormwood, wormwood extract and the like. These bittering agents or bitterness-imparting agents may be used alone or in combination of two or more.
- the soft drink of one aspect of the present invention may be a drink further containing an antioxidant.
- the antioxidant is not particularly limited, and those commonly used as antioxidants in soft drinks can be used, examples of which include ascorbic acid, erythorbic acid, and catechin. These antioxidants may be used alone or in combination of two or more.
- the soft drink of one embodiment of the present invention may be a drink further containing a flavor.
- Flavors are not particularly limited, and general malt-taste beverage flavors and hop-taste beverage flavors can be used.
- the malt-taste beverage flavoring is used for flavoring like a malt-taste beverage
- the hop-taste beverage flavoring is used for flavoring like a hop-taste beverage.
- Examples of malt-taste beverage flavors and hop-taste beverage flavors include esters and higher alcohols, and specific examples include isoamyl acetate, ethyl acetate, n-propanol, isobutanol, acetaldehyde, ethyl caproate, linalool, and 4-vinyl.
- guaiacol isoamylpropionate, 2-methyl-2-pentenoic acid, 4-methyl-3-pentenoic acid and the like.
- the soft drink of one embodiment of the present invention preferably contains lactic acid, but may be a drink that further contains an acidulant other than lactic acid, tartaric acid, and phosphoric acid.
- Acidulants other than these are not particularly limited as long as they have a sour taste, and examples thereof include citric acid, gluconic acid, malic acid, phytic acid, acetic acid, succinic acid, gluconodeltalactone, and salts thereof. .
- the soft drink of one embodiment of the present invention may be a drink that further contains salts.
- salts include sodium chloride, acidic potassium phosphate, acidic calcium phosphate, ammonium phosphate, magnesium sulfate, calcium sulfate, potassium metabisulfite, calcium chloride, magnesium chloride, potassium nitrate, and ammonium sulfate. These salts may be used alone or in combination of two or more.
- the soft drink of one embodiment of the present invention may be a drink containing an extract of one or more woods selected from beech, cedar, cherry, apple, and walnut, or may be a drink substantially free of the extract. Beverages that do not contain the extract may also be used.
- the soft drink of one embodiment of the present invention may be a beverage containing an extract of a plant belonging to the genus Quercus of the family Fagaceae, a beverage substantially free of the extract, or a beverage free of the extract. .
- the soft drink of one embodiment of the present invention may have a spiranthol content of 0.1 mass ppb or more, or may have a spiranthol content of less than 0.1 mass ppb.
- Carbon dioxide contained in the soft drink of one embodiment of the present invention may be added by mixing with carbonated water, or may be added directly to the raw material liquid.
- the carbon dioxide gas concentration of the soft drink of one embodiment of the present invention is preferably 0.30 (w/w)% or more, more preferably 0.35 (w/w)% or more, and still more preferably 0.40 (w/w)% or more.
- w)% or more more preferably 0.42 (w/w)% or more, particularly preferably 0.45 (w/w)% or more, and preferably 0.80 (w/w)% 0.70 (w/w)% or less, more preferably 0.60 (w/w)% or less, even more preferably 0.57 (w/w) or less, particularly preferably 0.55 (w/w)% or less.
- the carbon dioxide gas concentration is measured by immersing the container containing the target beverage in a water tank at 20°C for 30 minutes or longer while occasionally shaking the beverage to adjust the temperature of the beverage to 20°C, and then measuring the gas volume. It can be measured using an apparatus (eg, GVA-500 (manufactured by Kyoto Electronics Industry Co., Ltd.)).
- GVA-500 manufactured by Kyoto Electronics Industry Co., Ltd.
- the carbon dioxide gas pressure of the packaged beverage may be appropriately adjusted within the above range of the carbon dioxide gas concentration.
- gas pressure refers to gas pressure within a container, except in special cases. The pressure is measured by a method well known to those skilled in the art. For example, after fixing a sample heated to 20° C.
- additives may be added to the soft drink of one embodiment of the present invention as necessary as long as the effects of the present invention are not impaired.
- additives include coloring agents, foaming agents, fermentation promoters, yeast extracts, protein substances such as peptide-containing substances, and seasonings such as amino acids.
- a coloring agent is used to give color to a beverage, and caramel pigments and the like can be used.
- Foam-forming agents are used to form foam in beverages or to retain foam in beverages, and include saponin-based substances extracted from plants such as soybean saponin and quillaja saponin, vegetable proteins such as corn and soybeans, and , peptide-containing substances such as soybean peptides and collagen peptides, yeast extracts, and the like can be used as appropriate.
- Fermentation accelerators are used to promote fermentation by yeast. For example, yeast extract, bran ingredients such as rice and wheat, vitamins, minerals, etc. can be used alone or in combination.
- Method for producing soft drink The method for producing the soft drink of the present invention is not particularly limited, and examples thereof include a method comprising the following steps (1) to (3).
- - Step (1) Using various raw materials, performing at least one of the saccharification treatment, boiling treatment, and solid content removal treatment to obtain a pre-beverage liquid.
- - Process (2) The process of adding a carbon dioxide gas to the said pre-beverage liquid.
- - Step (3) A step of adjusting the content of at least one of sucralose and ascorbic acid.
- the production method of one embodiment of the present invention may further include the following step (4), if necessary.
- - Process (4) The process of adjusting content of acesulfame potassium.
- Step (5) a step of adjusting the content of lactic acid.
- Step (1) is a step of obtaining a pre-beverage liquid by subjecting various raw materials to at least one of saccharification treatment, boiling treatment, and solid content removal treatment.
- various raw materials including water and malt are put into a preparation pot or a preparation tank, and enzymes such as amylase are added as necessary.
- various raw materials other than malt hops, dietary fiber, sweeteners, antioxidants, bitterness-imparting agents, flavors, acidulants, pigments, and the like may be added.
- a mixture of various raw materials is subjected to a saccharification treatment by heating to saccharify the starch of the raw materials. The temperature and time of saccharification treatment are appropriately adjusted depending on the type of malt used, the ratio of malt, water and raw materials other than malt, and the like.
- filtration is performed to obtain a saccharified liquid.
- the saccharified liquid is preferably subjected to boiling treatment.
- hops, a bittering agent, etc. as raw materials when performing this boiling treatment, it is preferable to add these.
- Hops, bittering agents, etc. may be added between the start of boiling of the saccharified liquid and before the end of boiling.
- the boiling treatment is completed, it is preferably transferred to a whirlpool, cooled to 0 to 10° C. to obtain a cooling liquid, and then subjected to a solid content removal treatment to remove solid content such as solidified protein.
- a pre-drink liquid is obtained.
- the pre-beverage liquid may be prepared by adding hot water to the malt extract, adding hops, a bittering agent, etc., and subjecting the mixture to boiling treatment.
- liquid sugar containing carbon sources nitrogen sources as amino acid-containing raw materials other than wheat or malt
- hops dietary fiber
- sweeteners antioxidants
- bitterness imparting agents Flavor, acidulant, pigment, etc.
- they may be added before the boiling process, or may be added between the start of boiling the liquid sugar solution and before the end of boiling.
- a fermentation step using yeast top-fermenting yeast or bottom-fermenting yeast is performed to remove the alcohol generated in the fermentation step, and the alcohol content is reduced to 1 (v / v).
- % preferably less than 0.5 (v/v)%, more preferably less than 0.1 (v/v)%, still more preferably less than 0.01 (v/v)%, even more preferably 0. 005 (v/v)%) may be performed to produce a soft drink.
- the production method of one embodiment of the present invention may be a method in which the fermentation step and the step of removing alcohol are not performed.
- Step (2) is a step of adding carbon dioxide gas to the pre-beverage liquid.
- the method of adding carbon dioxide gas a known method that is applied in the production of carbonated beverages can be used. Carbon dioxide may be added directly to the pre-beverage solution. Using such a method, the carbon dioxide pressure is preferably adjusted to fall within the range described above.
- Step (3) is the step of adjusting the content of at least one of sucralose and ascorbic acid
- step (4) is the step of adjusting the content of acesulfame potassium
- step (5) is the step of adjusting the content of lactic acid. It is a process to do.
- Steps (3) to (5) may be performed before or after the saccharification treatment of step (1), before or after the boiling treatment, and before or after the solid content removal treatment, and after the completion of step (1). It may be performed before or after step (2). However, from the viewpoint of accurately adjusting the content in the finally produced beverage, it is preferable to carry out after the step (1) and before the start of the step (2).
- the order of steps (3) to (5) is not particularly limited, and either step may be performed first. Steps (3) to (5) may be carried out continuously or simultaneously, or may be carried out with other steps interposed therebetween.
- step (3) the content of either sucralose or ascorbic acid may be adjusted, or the content of both sucralose and ascorbic acid may be adjusted.
- sucralose and ascorbic acid after measuring the content of sucralose and ascorbic acid in the beverage before adjustment, based on the measured value, add sucralose and / or ascorbic acid, or add water or carbonated water to dilute, sucralose and You may adjust so that content of ascorbic acid may be in a predetermined range.
- the contents of sucralose and ascorbic acid are already within the desired ranges, the addition of sucralose, ascorbic acid, etc. and the dilution by adding water or carbonated water in this step are unnecessary.
- acesulfame potassium may be added to the beverage before preparation to adjust the content of acesulfame potassium.
- lactic acid may be added to the beverage before preparation to adjust the content of lactic acid.
- the content of lactic acid is added or diluted with water based on the measured value so that the content of lactic acid is within a predetermined range. You can adjust as follows. If the content is already within the desired range due to the presence of lactic acid derived from raw materials in the beverage before preparation, the addition of lactic acid in this step and the addition of water for dilution are unnecessary. .
- steps known to those skilled in the art in the production of soft drinks such as a storage step and a filtration step, may be performed.
- the soft drink of one embodiment of the present invention thus obtained is filled in a predetermined container and distributed on the market as a product.
- the method for packing the beverage into a container is not particularly limited, and a container packing method known to those skilled in the art can be used.
- the soft drink of the present invention is filled and sealed in a container by the container filling step.
- a container of any shape and material may be used in the container filling step, and examples of the container are as described above.
- the soft drink of one preferred embodiment of the present invention can be obtained by diluting a soft drink concentrate.
- the malt-taste beverage of one preferred aspect of the present invention can be obtained by diluting the malt-taste beverage concentrate
- the hop-taste beverage of one preferred aspect of the present invention is obtained by diluting the hop-taste beverage concentrate.
- Soft drink concentrates can be diluted with water or carbonated water. The dilution ratio for diluting the soft drink concentrate of the present invention may be appropriately set according to the preference of the drinker, but is preferably 1.1 times or more and 10 times or less based on the volume ratio.
- a 2-fold dilution ratio based on volume ratio refers to adding 1 volume of dilution medium to 1 volume of soft drink concentrate.
- dilution ratios are based on volume ratios.
- Soft drink concentrates can be produced similarly to soft drinks. Specifically, it is possible to produce a concentrated soft drink solution with an improved concentration according to the dilution ratio.
- the content of sucralose in the soft drink concentrate of one preferred aspect of the present invention is preferably 0.1 to 45 mass ppm, more preferably 0.5 to 40 mass ppm, still more preferably 1.0 to 30 mass ppm. ppm, more preferably 2.0 to 20 mass ppm, particularly preferably 3.0 to 10 mass ppm.
- the content of ascorbic acid in the soft drink concentrate of one preferred aspect of the present invention is preferably 70 to 1,900 ppm by mass, more preferably 90 to 1,700 ppm by mass, and still more preferably 110 to 1,500 ppm by mass. , Still more preferably 150 to 1300 mass ppm, more preferably 190 to 1000 mass ppm, and particularly preferably 230 to 700 mass ppm.
- Example/Comparative example Sucralose, ascorbic acid, lactic acid and acesulfame potassium were added to the raw beverage thus obtained so as to have the contents shown in Table 1.
- the beverages prepared in Examples and Comparative Examples were each adjusted to have a tartaric acid content of less than 300 mass ppm and a phosphoric acid content of 300 mass ppm.
- the calories per 100 mL of the beverages prepared in Examples and Comparative Examples were both less than 5 kcal.
- each malt-taste beverage was comprehensively evaluated according to the following evaluation criteria.
- the results were as shown in Table 1.
- ⁇ “A” The average score of each panelist for the three sensory evaluation items of “refreshing aftertaste like a malt taste drink”, “drinking response like a malt taste drink”, and “bitter aftertaste like a malt taste drink”. 2.5 or more and 3.5 or less.
- ⁇ “B” The average score of each panelist for the three sensory evaluation items of “refreshing aftertaste like a malt taste drink”, “drinking response like a malt taste drink”, and “bitter aftertaste like a malt taste drink”. It is 2.0 or more and 4.0 or less, and does not correspond to "A".
- - “C” Neither "A” nor "B” applies.
- the malt-taste beverages of Examples 1 to 13 had moderate chewiness and a refreshing feeling typical of malt-taste beverages, and had a good bitter aftertaste.
- beverages with a low ascorbic acid content tend to have a low refreshing aftertaste that is typical of malt-taste beverages
- beverages with a high ascorbic acid content the refreshing feeling of the aftertaste typical of malt-taste beverages was too strong, and the bitterness of the aftertaste typical of malt-taste beverages was felt weak.
Abstract
Description
例えば、特許文献1には、ビール製造における発酵工程前において、α-グルコシダーゼを添加することで、従来法に比べ生成アルコール濃度を約40~55%も低減させ得る、ノンアルコール発酵飲料の製造方法に関する技術が開示されている。 As beverages manufactured using water and malt as part of the raw materials, alcohol content is less than 1 (v / v) %, and soft drinks that are beer-flavored carbonated drinks are distributed on the market. development is taking place.
For example, Patent Document 1 describes a method for producing a non-alcoholic fermented beverage, which can reduce the alcohol concentration by about 40 to 55% compared to conventional methods by adding α-glucosidase before the fermentation process in beer production. has been disclosed.
[1]
スクラロースの含有量が、0.1~4.5質量ppmであり、
アスコルビン酸の含有量が、70~190質量ppmである、
清涼飲料。
[2]
スクラロースの含有量(単位:質量ppm)とアスコルビン酸の含有量(単位:質量ppm)との含有量比〔スクラロース/アスコルビン酸〕が、0.005~0.04である、[1]に記載の清涼飲料。
[3]
さらにアセスルファムカリウムを含有する、[1]又は[2]に記載の清涼飲料。
[4]
さらに乳酸を含有する、[1]~[3]のいずれかに記載の清涼飲料。
[5]
酒石酸の含有量が、300質量ppm未満である、[1]~[4]のいずれか1つに記載の清涼飲料。
[6]
リン酸の含有量が、300質量ppm未満である、[1]~[5]のいずれか1つに記載の清涼飲料。
[7]
原材料としてモルトエキスを用いた飲料である、[1]~[6]のいずれか1つに記載の清涼飲料。
[8]
前記清涼飲料のカロリーが、100mL当たり5kcal未満である、[1]~[7]のいずれか1つに記載の清涼飲料。
[9]
容器詰め飲料である、[1]~[8]のいずれか1つに記載の清涼飲料。
[10]
前記容器詰め飲料の炭酸ガス圧が、0.20kgf/cm2以上5.0kgf/cm2以下である、[9]に記載の清涼飲料。
[11]
1.1倍以上10倍以下の希釈倍率で希釈して得られる[1]~[10]のいずれか1つに記載の清涼飲料を製造するための清涼飲料濃縮液。
[12]
水又は炭酸水で希釈される[11]に記載された濃縮液。
[13]
スクラロースの含有量が、0.1~45質量ppmであり、アスコルビン酸の含有量が、70~1900質量ppmである、[11]又は[12]に記載の濃縮液。
[14]
清涼飲料がモルトテイスト飲料又はホップテイスト飲料である、[1]~[10]のいずれかに記載された飲料。
[15]
清涼飲料濃縮液がモルトテイスト飲料濃縮液又はホップテイスト飲料濃縮液である、[11]~[13]のいずれかに記載された濃縮液。 The present invention provides a soft drink having a sucralose content of 0.1 to 4.5 mass ppm and an ascorbic acid content of 70 to 190 mass ppm. That is, the present invention includes inventions of the following aspects.
[1]
The content of sucralose is 0.1 to 4.5 mass ppm,
The content of ascorbic acid is 70 to 190 mass ppm,
Soft drink.
[2]
[1], wherein the content ratio of the sucralose content (unit: mass ppm) and the ascorbic acid content (unit: mass ppm) [sucralose/ascorbic acid] is 0.005 to 0.04 soft drink.
[3]
The soft drink of [1] or [2], further containing acesulfame potassium.
[4]
The soft drink according to any one of [1] to [3], further containing lactic acid.
[5]
The soft drink according to any one of [1] to [4], which has a tartaric acid content of less than 300 mass ppm.
[6]
The soft drink according to any one of [1] to [5], having a phosphoric acid content of less than 300 mass ppm.
[7]
The soft drink according to any one of [1] to [6], which uses malt extract as a raw material.
[8]
The soft drink according to any one of [1] to [7], wherein the soft drink has less than 5 kcal per 100 mL.
[9]
The soft drink according to any one of [1] to [8], which is a packaged drink.
[10]
The soft drink according to [9], wherein the packaged beverage has a carbon dioxide pressure of 0.20 kgf/cm 2 or more and 5.0 kgf/cm 2 or less.
[11]
1. A soft drink concentrate for producing a soft drink according to any one of [1] to [10], which is obtained by diluting at a dilution ratio of 1-fold or more and 10-fold or less.
[12]
A concentrate according to [11] diluted with water or carbonated water.
[13]
The concentrated liquid according to [11] or [12], wherein the content of sucralose is 0.1 to 45 mass ppm and the content of ascorbic acid is 70 to 1900 mass ppm.
[14]
The beverage according to any one of [1] to [10], wherein the soft drink is a malt-taste beverage or a hop-taste beverage.
[15]
The concentrate according to any one of [11] to [13], wherein the soft drink concentrate is a malt-taste beverage concentrate or a hop-taste beverage concentrate.
本発明において、「清涼飲料」とは、ジュース、炭酸飲料、麦芽飲料、乳酸菌飲料、健康飲料、スポーツ飲料、アミノ酸飲料、ビタミン飲料、モルトテイスト飲料、ホップテイスト飲料等をいうが、これらに限られない。
また、本発明において、「モルトテイスト飲料」とは、麦及び/又は麦芽から得られた麦汁の風味を有する飲料を意味し、炭酸ガス等により清涼感が付与された飲料も含まれる。モルトテイスト飲料は1(v/v%)未満のアルコールを含有してもよい。このアルコール含有モルトテイスト飲料としては、発酵して得られたモルトテイスト飲料とアルコールが添加された飲料が挙げられる。アルコール非含有モルトテイスト飲料としては、発酵して得られたモルトテイスト飲料からアルコール、その他の低沸点成分や低分子成分を除去して得られた飲料が挙げられる。なお、モルトテイスト飲料の原料は、麦及び/又は麦芽から得られた麦汁の風味を有する原料であればよく、麦及び麦芽以外の穀物を用いてもよい。モルトテイスト飲料の原料に使用できる穀物としては、例えば、麦、麦芽、麦芽には該当しない麦(大麦、小麦、ライ麦、カラス麦、オート麦、ハト麦、エン麦等)、米(白米、玄米等)、とうもろこし、こうりゃん、ばれいしょ、豆(大豆、えんどう豆等)、そば、ソルガム、粟、ひえ、及びそれらから得られたデンプン、これらの抽出物等(モルトエキス等)などが挙げられるが、これらに限定されない。また、モルトテイスト飲料の製造には麦及び/又は麦芽から得られた麦汁を使用しても、麦及び/又は麦芽から得られた麦汁に近い風味を持つ香料を使用してもよい。
また、本発明において、「ホップテイスト飲料」とは、ホップの風味を有する飲料を意味し、ホップ由来の原材料等を用いた場合に得られる止渇感、フローラルな香りのような爽快感や芳醇さを有する飲料が好ましく、香味のバランスや、口当たりや喉ごしが良く飲みやすい味覚をさらに有することが好ましい。また、ホップテイスト飲料には炭酸ガス等により清涼感が付与された飲料も含まれる。ホップテイスト飲料は1(v/v%)未満のアルコールを含有してもよい。このアルコール含有ホップテイスト飲料としては、発酵して得られたホップテイスト飲料とアルコールが添加された飲料が挙げられる。アルコール非含有ホップテイスト飲料としては、発酵して得られたホップテイスト飲料からアルコール、その他の低沸点成分や低分子成分を除去して得られた飲料が挙げられる。また、ホップ及びα酸をイソ化したホップエキスを用いずに、ホップに代えて苦味料又は苦味付与剤を用いてもよい。ホップテイスト飲料に用いることができる苦味料および苦味付与剤としては、例えば、マンネンロウ、レイシ、姫茴香、杜松実、セージ、迷迭香、マンネンタケ、月桂樹、クワシン、柑橘抽出物、ニガキ抽出物、コーヒー抽出物、茶抽出物、ゴーヤ抽出物、ハス胚芽抽出物、キダチアロエ抽出物、マンネンロウ抽出物、レイシ抽出物、ローレル抽出物、セージ抽出物、キャラウェイ抽出物、ナリンギン、ニガヨモギ及びニガヨモギ抽出物等が挙げられる。これらは、単独で用いてもよく、2種以上を併用してもよい。
本発明の一態様の清涼飲料のアルコール度数としては、1(v/v%)未満であればよいが、好ましくは0.5(v/v)%未満、より好ましくは0.1(v/v)%未満、更に好ましくは0.01(v/v)%未満、より更に好ましくは0.005(v/v)%未満である。
なお、本明細書において、アルコール度数は、体積/体積基準の百分率(v/v%)で示されるものとする。また、飲料のアルコール含有量は、公知のいずれの方法によっても測定することができるが、例えば、ガスクロマトグラフィーによって測定することができる。 1. Soft drinks In the present invention, "soft drinks" refer to juices, carbonated drinks, malt drinks, lactic acid drinks, health drinks, sports drinks, amino acid drinks, vitamin drinks, malt-taste drinks, hop-taste drinks and the like. Not limited.
In the present invention, the term "malt-taste beverage" means a beverage having the flavor of wort obtained from barley and/or malt, and includes beverages imparted with a refreshing sensation by carbon dioxide gas or the like. A malt-tasting beverage may contain less than 1 (v/v %) alcohol. Examples of alcohol-containing malt-taste beverages include fermented malt-taste beverages and alcohol-added beverages. Alcohol-free malt-taste beverages include beverages obtained by removing alcohol, other low-boiling-point components and low-molecular-weight components from fermented malt-taste beverages. The raw material for the malt-taste beverage may be any raw material having the flavor of wort obtained from wheat and/or malt, and grains other than wheat and malt may be used. Grains that can be used as raw materials for malt-taste beverages include, for example, barley, malt, non-malt (barley, wheat, rye, oats, oats, pigeons, oats, etc.), rice (polished rice, brown rice). etc.), corn, koryan, potato, beans (soybeans, peas, etc.), buckwheat, sorghum, millet, barnyard millet, and starch obtained therefrom, extracts thereof (malt extract, etc.), etc. but not limited to these. In addition, wort obtained from barley and/or malt may be used for the production of malt-taste beverages, or flavoring agents having a flavor similar to that of wort obtained from barley and/or malt may be used.
In the present invention, the term "hop-flavored beverage" means a beverage having a hop flavor, and the thirst-quenching feeling obtained when using hop-derived raw materials, etc., and the refreshing and richness of a floral scent. It is preferable that the beverage has a balance of flavor, and a taste that is easy to drink with good texture and smoothness in the mouth. The hop-taste beverages also include beverages imparted with a refreshing feeling by carbon dioxide gas or the like. A hop-tasting beverage may contain less than 1 (v/v %) alcohol. The alcohol-containing hop-taste beverages include hop-taste beverages obtained by fermentation and alcohol-added beverages. Alcohol-free hop-taste beverages include beverages obtained by removing alcohol, other low-boiling-point components and low-molecular-weight components from hop-taste beverages obtained by fermentation. Instead of using hops and hop extract obtained by isolating α-acid, a bittering agent or a bittering agent may be used instead of hops. Bittering agents and bittering agents that can be used in hop-taste beverages include, for example, Ganoderma lucidum, Ganoderma lucidum, Himejiko, Juniper nut, Sage, Astragalus, Ganoderma lucidum, Laurel, Quassin, Citrus extract, Nigaki extract, Coffee extract, tea extract, bitter gourd extract, lotus germ extract, aloe vera extract, stonecrop extract, litchi extract, laurel extract, sage extract, caraway extract, naringin, wormwood and wormwood extract, etc. are mentioned. These may be used alone or in combination of two or more.
The alcohol content of the soft drink of one embodiment of the present invention may be less than 1 (v/v%), preferably less than 0.5 (v/v)%, more preferably less than 0.1 (v/v%). v) %, more preferably less than 0.01 (v/v) %, even more preferably less than 0.005 (v/v) %.
In addition, in this specification, alcohol content shall be shown by the percentage (v/v%) of a volume/volume basis. Moreover, although the alcohol content of a drink can be measured by any well-known method, it can be measured by a gas chromatography, for example.
本発明の一態様の清涼飲料が非発酵飲料である場合、モルト様又はホップ様の風味を持つように、エステル、高級アルコール(例えば、酢酸イソアミル、酢酸エチル、n-プロパノール、イソブタノール、アセトアルデヒド、カプロン酸エチル、リナロール、4-ビニルグアイアコール、イソアミルプロピオネート等)、酸(例えば、2-メチル-2-ペンテン酸、4-メチル-3-ペンテン酸)等を含む香料を添加して、モルト風味又はホップ風味を有するように調整した炭酸飲料も、本発明の一態様の非発酵清涼テイスト飲料、モルトテイスト飲料、及び、ホップテイスト飲料に包含される。 A soft drink of one aspect of the present invention is a fermented beverage obtained by removing alcohol produced in the fermentation process after undergoing a fermentation process using yeast (top-fermenting yeast or bottom-fermenting yeast) in the production process, Alternatively, it may be a non-fermented beverage prepared without undergoing such a fermentation process.
When the soft drink of one aspect of the present invention is a non-fermented drink, esters, higher alcohols (e.g., isoamyl acetate, ethyl acetate, n-propanol, isobutanol, acetaldehyde, Ethyl caproate, linalool, 4-vinyl guaiacol, isoamyl propionate, etc.), acids (e.g., 2-methyl-2-pentenoic acid, 4-methyl-3-pentenoic acid), etc. Carbonated beverages adjusted to have flavor or hop flavor are also included in the non-fermented refreshing beverage, malt-taste beverage, and hop-taste beverage of one aspect of the present invention.
乳酸の含有量は、前記清涼飲料の全量基準で、好ましくは1.0質量ppm以上、より好ましくは10.0質量ppm以上、更に好ましくは30.0質量ppm以上、より更に好ましくは50.0質量ppm以上、より更に好ましくは100質量ppm以上、より更に好ましくは150質量ppm以上、特に好ましくは200質量ppm以上であり、また、好ましくは700質量ppm以下、より好ましくは600質量ppm以下、更に好ましくは500質量ppm以下、より更に好ましくは400質量ppm以下、特に好ましくは350質量ppm以下である。 The soft drink of one embodiment of the present invention may further contain lactic acid from the viewpoint of imparting a refreshing aftertaste typical of a malt-taste beverage or a hop-taste beverage and a bitter aftertaste typical of a malt-taste beverage or a hop-taste beverage in a well-balanced manner. preferable.
The content of lactic acid is preferably 1.0 mass ppm or more, more preferably 10.0 mass ppm or more, still more preferably 30.0 mass ppm or more, and even more preferably 50.0 mass ppm, based on the total amount of the soft drink. mass ppm or more, more preferably 100 mass ppm or more, still more preferably 150 mass ppm or more, particularly preferably 200 mass ppm or more, preferably 700 mass ppm or less, more preferably 600 mass ppm or less, and further It is preferably 500 mass ppm or less, more preferably 400 mass ppm or less, and particularly preferably 350 mass ppm or less.
また、本明細書において、清涼飲料のスクラロース及びアセスルファムカリウムの含有量の含有量も同様に、高速液体クロマトグラフィーによって測定することができる。 As used herein, the contents of ascorbic acid, lactic acid, tartaric acid, and phosphoric acid in soft drinks can be measured by high performance liquid chromatography.
In this specification, the content of sucralose and acesulfame potassium in soft drinks can also be measured by high performance liquid chromatography.
なお、清涼飲料のカロリーは、定量した各種栄養成分の量に、それぞれの成分のエネルギー換算係数(タンパク質:4kcal/g、脂質:9kcal/g、糖質:4kcal/g、食物繊維:2kcal/g、アルコール:7kcal/g、有機酸:3kcal/g)を乗じたものの総和として算出することができる。 Calorie content of the soft drink of one aspect of the present invention is preferably less than 5 kcal per 100 mL. By making such a low-calorie beverage, it is possible to provide a beverage that is easily acceptable to health-conscious consumers. The calorie can be controlled by adjusting the blending composition, blending amount, etc. of raw materials (eg, grains such as malt, barley, hops, etc.).
In addition, the calories of soft drinks are calculated by adding the energy conversion factors of each component (protein: 4 kcal/g, fat: 9 kcal/g, sugar: 4 kcal/g, dietary fiber: 2 kcal/g , alcohol: 7 kcal/g, organic acid: 3 kcal/g).
なお、本明細書における「総エキス量」は、脱ガスしたサンプルをビール酒造組合国際技術委員会(BCOJ)が編集する改訂BCOJビール分析法(公益財団法人日本醸造協会発行、2013年増補改訂)の「ビール分析法 7.2 エキス」に従い測定したエキス値(質量%)を意味する。 The total extract amount of the soft drink of one embodiment of the present invention is not particularly limited, but is preferably 1.5% by weight or less, more preferably 1.1% by weight, from the viewpoint of making the beverage imparted with a light mouthfeel. Below, more preferably 0.80% by weight or less, still more preferably less than 0.50% by weight.
It should be noted that the "total extract amount" in this specification is a revised BCOJ beer analysis method edited by the Beer Brewers Association International Technical Committee (BCOJ) for degassed samples (published by the Brewing Association of Japan, expanded and revised in 2013). "Beer Analysis Method 7.2 Extract" means the extract value (% by mass) measured in accordance with
本発明の一態様のモルトテイスト飲料及びホップテイスト飲料等の清涼飲料の主な原材料は、水と共に麦芽を用いてもよく、また、麦芽を用いなくてもよい。さらにホップを用いてもよく、その他に、保存料、甘味料、水溶性食物繊維、苦味料又は苦味付与剤、酸化防止剤、香料、酸味料、塩類等を用いてもよい。 1.1 Raw Materials Water and malt may or may not be used as the main raw materials of soft drinks such as malt-taste beverages and hop-taste beverages of one embodiment of the present invention. Furthermore, hops may be used, and preservatives, sweeteners, water-soluble dietary fibers, bittering agents or bitterness-imparting agents, antioxidants, flavors, acidulants, salts, and the like may also be used.
本発明の一態様においては、用いる麦芽としては、大麦麦芽が好ましい。大麦麦芽は、日本のモルトテイスト飲料及びホップテイスト飲料の原料として最も一般的に用いられる麦芽の1つである。大麦には、二条大麦、六条大麦などの種類があるが、いずれを用いてもよい。さらに、通常麦芽のほか、色麦芽なども用いることができる。なお、色麦芽を用いる際には、種類の異なる色麦芽を適宜組み合わせて用いてもよいし、一種類の色麦芽を用いてもよい。 When malt is used as a raw material, the malt refers to germinated seeds of barley, wheat, rye, oats, oats, pigeons, oats, etc., dried, and rooted. Any variety may be used.
In one aspect of the present invention, the malt to be used is preferably malted barley. Barley malt is one of the most commonly used malts as an ingredient in Japanese malt-taste and hop-taste beverages. There are two kinds of barley, such as two-rowed barley and six-rowed barley, and any of them may be used. In addition to normal malt, colored malt can also be used. When using colored malt, different types of colored malt may be appropriately combined and used, or one type of colored malt may be used.
そのような穀物としては、例えば、麦芽には該当しない麦(大麦、小麦、ライ麦、カラス麦、オート麦、ハト麦、エン麦等)、米(白米、玄米等)、とうもろこし、こうりゃん、ばれいしょ、豆(大豆、えんどう豆等)、そば、ソルガム、粟、ひえ、及びそれらから得られたデンプン、これらの抽出物等(モルトエキス等)が挙げられる。
本発明の一態様において、原材料としてモルトエキスを用いることが好ましい。なお、本発明において、「モルトエキス」とは、大麦(好ましくは麦芽)を糖化して、濃縮した抽出物を意味する。 Grains other than malt may also be used together with malt.
Examples of such grains include wheat (barley, wheat, rye, oats, oats, pigeons, oats, etc.) that do not fall under malt, rice (polished rice, brown rice, etc.), corn, koryan, potato, etc. , beans (soybeans, peas, etc.), buckwheat, sorghum, millet, barley, and starches obtained therefrom, extracts thereof (malt extract, etc.).
In one aspect of the present invention, it is preferred to use malt extract as the raw material. In the present invention, "malt extract" means a concentrated extract obtained by saccharifying barley (preferably malt).
ホップの添加量としては、適宜調製されるが、飲料全量に対して、好ましくは0.0001~1質量%である。 Examples of forms of hops used in one aspect of the present invention include pellet hops, powdered hops, hop extracts, and the like. As the hops to be used, processed hops such as isoformed hops and reduced hops may be used.
The amount of hops to be added is appropriately adjusted, but is preferably 0.0001 to 1% by mass relative to the total amount of the beverage.
一方で、ホップを用いない清涼飲料におけるイソα酸の含有量は、当該清涼飲料の全量基準で、0.1質量ppm以下であってもよい。
なお、本明細書において、イソα酸の含有量は、改訂BCOJビール分析法(公益財団法人日本醸造協会発行、ビール酒造組合国際技術委員会〔分析委員会〕編集2013年増補改訂)に記載の高速液体クロマトグラフィー(HPLC)分析法により測定された値を意味する。 In addition, soft drinks such as malt-taste beverages and hop-taste beverages using hops as raw materials are beverages containing iso-α acids, which are components derived from hops. The iso-α-acid content of the soft drink using hops may be greater than 0.1 ppm by mass or greater than 1.0 ppm by mass based on the total amount of the soft drink.
On the other hand, the content of iso-α-acids in a hop-free soft drink may be 0.1 mass ppm or less based on the total amount of the soft drink.
In this specification, the content of iso-α acids is described in the revised BCOJ beer analysis method (published by the Brewing Association of Japan, Beer Brewers Association International Technical Committee [Analysis Committee] edited 2013 supplementary revision). It means a value measured by high performance liquid chromatography (HPLC) analytical method.
本発明の一態様で用いる保存料としては、例えば、安息香酸;安息香酸ナトリウム等の安息香酸塩;パラオキシ安息香酸プロピル、パラオキシ安息香酸ブチル等の安息香酸エステル;二炭酸ジメチル;等が挙げられる。また、保存料としては、強力サンプレザー(三栄源エフ・エフ・アイ株式会社製、安息香酸ナトリウムと安息香酸ブチルの混合物)等の市販の製剤を用いてもよい。
これらの保存料は、単独で用いてもよく、2種以上を併用してもよい。 The soft drink of one aspect of the present invention may be a drink further containing a preservative.
Preservatives used in one aspect of the present invention include, for example, benzoic acid; benzoates such as sodium benzoate; benzoate esters such as propyl parahydroxybenzoate and butyl parahydroxybenzoate; dimethyl dicarbonate; Moreover, as a preservative, a commercially available preparation such as Strong Samprezer (a mixture of sodium benzoate and butyl benzoate, manufactured by San-Eigen FFI Co., Ltd.) may be used.
These preservatives may be used alone or in combination of two or more.
甘味料としては、穀物由来のデンプンを酸又は酵素等で分解した市販の糖化液、市販の水飴等の糖類、三糖類以上の糖、糖アルコール、ステビア等の天然甘味料、人工甘味料等が挙げられる。
これらの甘味料は、単独で用いてもよく、2種以上を併用してもよい。
これらの糖類の形態は、溶液等の液体であってもよく、粉末等の固体であってもよい。
また、デンプンの原料穀物の種類、デンプンの精製方法、及び酵素や酸による加水分解等の処理条件についても特に制限はない。例えば、酵素や酸による加水分解の条件を適宜設定することにより、マルトースの比率を高めた糖類を用いてもよい。その他、スクロース、フルクトース、グルコース、マルトース、トレハロース、マルトトリオース及びこれらの溶液(糖液)等を用いることもできる。
また、人工甘味料としては、スクラロース及びアセスルファムカリウムの他に、アスパルテーム等が挙げられる。 The soft drink of the present invention contains sucralose and may further contain acesulfame potassium, and may contain other sweeteners in addition to these sweeteners.
Examples of sweeteners include commercially available saccharified solutions obtained by decomposing grain-derived starch with acids or enzymes, sugars such as commercially available starch syrup, sugars of trisaccharides or higher, sugar alcohols, natural sweeteners such as stevia, and artificial sweeteners. mentioned.
These sweeteners may be used alone or in combination of two or more.
The form of these sugars may be liquid such as solution, or solid such as powder.
In addition, there are no particular restrictions on the type of starch raw material grains, the method of purifying starch, and the treatment conditions such as hydrolysis with enzymes or acids. For example, sugars with a higher proportion of maltose may be used by appropriately setting conditions for hydrolysis with an enzyme or acid. In addition, sucrose, fructose, glucose, maltose, trehalose, maltotriose, solutions of these (sugar solutions), and the like can also be used.
In addition to sucralose and acesulfame potassium, artificial sweeteners include aspartame and the like.
水溶性食物繊維としては、例えば、難消化性デキストリン、ポリデキストロース、グアーガム分解物、ペクチン、グルコマンナン、アルギン酸、ラミナリン、フコイジン、カラギーナン等が挙げられ、安定性や安全性等の汎用性の観点から、難消化性デキストリン又はポリデキストロースが好ましい。
これらの食物繊維は、単独で用いてもよく、2種以上を併用してもよい。 The soft drink of one embodiment of the present invention may be a drink further containing dietary fiber such as water-soluble dietary fiber.
Examples of water-soluble dietary fibers include indigestible dextrin, polydextrose, guar gum decomposition products, pectin, glucomannan, alginic acid, laminarin, fucoidin, carrageenan, and the like, from the viewpoint of versatility such as stability and safety. , indigestible dextrin or polydextrose are preferred.
These dietary fibers may be used alone or in combination of two or more.
苦味料又は苦味付与剤としては、例えば、マンネンロウ、レイシ、姫茴香、杜松実、セージ、迷迭香、マンネンタケ、月桂樹、クワシン、柑橘抽出物、ニガキ抽出物、コーヒー抽出物、茶抽出物、ゴーヤ抽出物、ハス胚芽抽出物、キダチアロエ抽出物、マンネンロウ抽出物、レイシ抽出物、ローレル抽出物、セージ抽出物、キャラウェイ抽出物、ナリンギン、ニガヨモギ及びニガヨモギ抽出物等が挙げられる。
これらの苦味料又は苦味付与剤は、単独で用いてもよく、2種以上を併用してもよい。 In soft drinks such as malt-taste beverages and hop-taste beverages according to one embodiment of the present invention, bitterness may be imparted by hops or a hop extract obtained by isolating α-acids. You may use the bittering agent or bitterness imparting agent shown below. Instead of using hops and hop extracts obtained by isolating α-acids, the following bitterness agents or bitterness-imparting agents may be used in place of hops.
Bittering agents or bitterness-imparting agents include, for example, Ganoderma lucidum, Ganoderma lucidum, Ganoderma lucidum, Juniper berry, Sage, Astragalus membranus, Ganoderma lucidum, Bay laurel, Kuwasin, Citrus extract, bittern bitter extract, coffee extract, tea extract, Goya extract, lotus germ extract, aloe vera extract, stonecrop extract, litchi extract, laurel extract, sage extract, caraway extract, naringin, wormwood, wormwood extract and the like.
These bittering agents or bitterness-imparting agents may be used alone or in combination of two or more.
酸化防止剤としては、特に限定されず、通常の清涼飲料に酸化防止剤として用いられるものが使用でき、例えば、アスコルビン酸、エリソルビン酸、及びカテキン等が挙げられる。
これらの酸化防止剤は、単独で用いてもよく、2種以上を併用してもよい。 The soft drink of one aspect of the present invention may be a drink further containing an antioxidant.
The antioxidant is not particularly limited, and those commonly used as antioxidants in soft drinks can be used, examples of which include ascorbic acid, erythorbic acid, and catechin.
These antioxidants may be used alone or in combination of two or more.
香料としては、特に限定されず、一般的なモルトテイスト飲料香料及びホップテイスト飲料香料を用いることができる。モルトテイスト飲料香料は、モルトテイスト飲料様の風味付けのために用いるものであり、ホップテイスト飲料香料はホップテイスト飲料様の風味付けのために用いるものである。
モルトテイスト飲料香料及びホップテイスト飲料香料としては、エステルや高級アルコール等が挙げられ、具体的には、酢酸イソアミル、酢酸エチル、n-プロパノール、イソブタノール、アセトアルデヒド、カプロン酸エチル、リナロール、4-ビニルグアイアコール、イソアミルプロピオネート、2-メチル-2-ペンテン酸、4-メチル-3-ペンテン酸等が挙げられる。
これらの香料は、単独で用いてもよく、2種以上を併用してもよい。 The soft drink of one embodiment of the present invention may be a drink further containing a flavor.
Flavors are not particularly limited, and general malt-taste beverage flavors and hop-taste beverage flavors can be used. The malt-taste beverage flavoring is used for flavoring like a malt-taste beverage, and the hop-taste beverage flavoring is used for flavoring like a hop-taste beverage.
Examples of malt-taste beverage flavors and hop-taste beverage flavors include esters and higher alcohols, and specific examples include isoamyl acetate, ethyl acetate, n-propanol, isobutanol, acetaldehyde, ethyl caproate, linalool, and 4-vinyl. guaiacol, isoamylpropionate, 2-methyl-2-pentenoic acid, 4-methyl-3-pentenoic acid and the like.
These perfumes may be used alone or in combination of two or more.
これら以外の酸味料としては、酸味を有する物質であれば特に限定されないが、例えば、クエン酸、グルコン酸、リンゴ酸、フィチン酸、酢酸、コハク酸、グルコノデルタラクトン又はそれらの塩が挙げられる。 The soft drink of one embodiment of the present invention preferably contains lactic acid, but may be a drink that further contains an acidulant other than lactic acid, tartaric acid, and phosphoric acid.
Acidulants other than these are not particularly limited as long as they have a sour taste, and examples thereof include citric acid, gluconic acid, malic acid, phytic acid, acetic acid, succinic acid, gluconodeltalactone, and salts thereof. .
塩類としては、例えば、塩化ナトリウム、酸性リン酸カリウム、酸性リン酸カルシウム、リン酸アンモニウム、硫酸マグネシウム、硫酸カルシウム、メタ重亜硫酸カリウム、塩化カルシウム、塩化マグネシウム、硝酸カリウム、硫酸アンモニウム等が挙げられる。
これらの塩類は、単独で用いてもよく、2種以上を併用してもよい。 The soft drink of one embodiment of the present invention may be a drink that further contains salts.
Examples of salts include sodium chloride, acidic potassium phosphate, acidic calcium phosphate, ammonium phosphate, magnesium sulfate, calcium sulfate, potassium metabisulfite, calcium chloride, magnesium chloride, potassium nitrate, and ammonium sulfate.
These salts may be used alone or in combination of two or more.
本発明の一態様の清涼飲料に含まれる炭酸ガスは、炭酸水との混和によって加えてもよく、又は原料液に炭酸ガスを直接添加してもよい。 1.2 Carbon dioxide The carbon dioxide contained in the soft drink of one embodiment of the present invention may be added by mixing with carbonated water, or may be added directly to the raw material liquid.
なお、本明細書において、炭酸ガス濃度は、対象となる飲料が入った容器を時々振りながら20℃の水槽に30分間以上浸して、当該飲料が20℃になるよう調整した後に、ガスボリューム測定装置(例えば、GVA-500(京都電子工業株式会社製)等)を用いて測定することができる。 The carbon dioxide gas concentration of the soft drink of one embodiment of the present invention is preferably 0.30 (w/w)% or more, more preferably 0.35 (w/w)% or more, and still more preferably 0.40 (w/w)% or more. w)% or more, more preferably 0.42 (w/w)% or more, particularly preferably 0.45 (w/w)% or more, and preferably 0.80 (w/w)% 0.70 (w/w)% or less, more preferably 0.60 (w/w)% or less, even more preferably 0.57 (w/w) or less, particularly preferably 0.55 (w/w)% or less.
In this specification, the carbon dioxide gas concentration is measured by immersing the container containing the target beverage in a water tank at 20°C for 30 minutes or longer while occasionally shaking the beverage to adjust the temperature of the beverage to 20°C, and then measuring the gas volume. It can be measured using an apparatus (eg, GVA-500 (manufactured by Kyoto Electronics Industry Co., Ltd.)).
本明細書において、ガス圧とは、特別な場合を除き、容器内におけるガス圧をいう。
圧力の測定は、当業者によく知られた方法、例えば20℃にした試料をガス内圧計に固定した後、一度ガス内圧計の活栓を開いてガスを抜き、再び活栓を閉じ、ガス内圧計を振り動かして指針が一定の位置に達したときの値を読み取る方法を用いて、又は市販のガス圧測定装置を用いて測定することができる。 When the soft drink of one embodiment of the present invention is a packaged beverage, the carbon dioxide gas pressure of the packaged beverage may be appropriately adjusted within the above range of the carbon dioxide gas concentration. 0.5 kgf/cm 2 or less, or 4.0 kgf/cm 2 or less, or 0.20 kgf/cm 2 or more, 0.50 kgf/cm 2 or more, or 1.0 kgf/cm 2 or more. Any combination of these upper and lower limits may be used. cm 2 or less, or 1.0 kgf/cm 2 or more and 4.0 kgf/cm 2 or less.
In the present specification, gas pressure refers to gas pressure within a container, except in special cases.
The pressure is measured by a method well known to those skilled in the art. For example, after fixing a sample heated to 20° C. to a gas pressure gauge, open the stopcock of the gas pressure gauge once to release the gas, close the stopcock again, and can be measured using a method of reading the value when the pointer reaches a certain position by shaking the pointer, or using a commercially available gas pressure measuring device.
本発明の一態様の清涼飲料は、本発明の効果を妨げない範囲で、必要に応じて、様々な添加物を添加してもよい。
そのような添加物としては、例えば、着色料、泡形成剤、発酵促進剤、酵母エキス、ペプチド含有物等のタンパク質系物質、アミノ酸等の調味料が挙げられる。
着色料は、飲料に色を与えるために使用するものであり、カラメル色素などを用いることができる。泡形成剤は、飲料に泡を形成させるため、あるいは飲料の泡を保持させるために使用するものであり、大豆サポニン、キラヤサポニン等の植物抽出サポニン系物質、コーン、大豆などの植物タンパク、及び、大豆ペプチド、コラーゲンペプチド等のペプチド含有物、酵母エキスなどを適宜使用することができる。
発酵促進剤は、酵母による発酵を促進させるために使用するものであり、例えば、酵母エキス、米や麦などの糠成分、ビタミン、ミネラル剤などを単独又は組み合わせて使用することができる。 1.3 Other Additives Various additives may be added to the soft drink of one embodiment of the present invention as necessary as long as the effects of the present invention are not impaired.
Examples of such additives include coloring agents, foaming agents, fermentation promoters, yeast extracts, protein substances such as peptide-containing substances, and seasonings such as amino acids.
A coloring agent is used to give color to a beverage, and caramel pigments and the like can be used. Foam-forming agents are used to form foam in beverages or to retain foam in beverages, and include saponin-based substances extracted from plants such as soybean saponin and quillaja saponin, vegetable proteins such as corn and soybeans, and , peptide-containing substances such as soybean peptides and collagen peptides, yeast extracts, and the like can be used as appropriate.
Fermentation accelerators are used to promote fermentation by yeast. For example, yeast extract, bran ingredients such as rice and wheat, vitamins, minerals, etc. can be used alone or in combination.
本発明の清涼飲料の製造方法としては、特に制限は無く、例えば、下記工程(1)~(3)を有する方法が挙げられる。
・工程(1):各種原材料を用いて、糖化処理、煮沸処理、及び固形分除去処理のうち少なくとも1つの処理を行い、飲料前液を得る工程。
・工程(2):前記飲料前液に、炭酸ガスを加える工程。
・工程(3):スクラロース及びアスコルビン酸の少なくとも一方の含有量を調整する工程。
また、本発明の一態様の製造方法において、必要に応じて、さらに下記工程(4)を有してもよい。
・工程(4):アセスルファムカリウムの含有量を調整する工程。
・工程(5):乳酸の含有量を調整する工程。
以下、上記の各工程について説明する。 2. Method for producing soft drink The method for producing the soft drink of the present invention is not particularly limited, and examples thereof include a method comprising the following steps (1) to (3).
- Step (1): Using various raw materials, performing at least one of the saccharification treatment, boiling treatment, and solid content removal treatment to obtain a pre-beverage liquid.
- Process (2): The process of adding a carbon dioxide gas to the said pre-beverage liquid.
- Step (3): A step of adjusting the content of at least one of sucralose and ascorbic acid.
Further, the production method of one embodiment of the present invention may further include the following step (4), if necessary.
- Process (4): The process of adjusting content of acesulfame potassium.
• Step (5): a step of adjusting the content of lactic acid.
Each of the above steps will be described below.
工程(1)は、各種原材料を用いて、糖化処理、煮沸処理、及び固形分除去処理のうち少なくとも1つの処理を行い、飲料前液を得る工程である。
例えば、各種原材料として、麦芽を用いる場合には、水及び麦芽を含む各種原材料を仕込釜又は仕込槽に投入し、必要に応じてアミラーゼ等の酵素を添加する。麦芽以外の各種原材料としては、ホップ、食物繊維、甘味料、酸化防止剤、苦味付与剤、香料、酸味料、色素等を加えてもよい。
各種原材料の混合物は、加温し、原材料の澱粉質を糖化させて糖化処理を行う。糖化処理の温度及び時間は、使用する麦芽の種類や、麦芽比率、水及び麦芽以外の原材料等によって適宜調整する。糖化処理後に、濾過を行い、糖化液が得られる。 <Step (1)>
Step (1) is a step of obtaining a pre-beverage liquid by subjecting various raw materials to at least one of saccharification treatment, boiling treatment, and solid content removal treatment.
For example, when malt is used as various raw materials, various raw materials including water and malt are put into a preparation pot or a preparation tank, and enzymes such as amylase are added as necessary. As various raw materials other than malt, hops, dietary fiber, sweeteners, antioxidants, bitterness-imparting agents, flavors, acidulants, pigments, and the like may be added.
A mixture of various raw materials is subjected to a saccharification treatment by heating to saccharify the starch of the raw materials. The temperature and time of saccharification treatment are appropriately adjusted depending on the type of malt used, the ratio of malt, water and raw materials other than malt, and the like. After the saccharification treatment, filtration is performed to obtain a saccharified liquid.
この煮沸処理を行う際に、原材料としてホップや苦味料等を用いる場合には、これらを加えることが好ましい。ホップや苦味料等は、糖化液の煮沸開始から煮沸終了前の間で加えてもよい。
煮沸処理終了後には、ワールプールに移送し、0~10℃に冷却して冷却液とした後、凝固タンパク等の固形分を取り除くための固形分除去処理を行うことが好ましい。このようにして、飲料前液が得られる。
なお、上記の糖化液の代わりに、麦芽エキスに温水を加えたものに、ホップや苦味料等を加えて煮沸処理を行い、飲料前液を調製してもよい。 The saccharified liquid is preferably subjected to boiling treatment.
When using hops, a bittering agent, etc. as raw materials when performing this boiling treatment, it is preferable to add these. Hops, bittering agents, etc. may be added between the start of boiling of the saccharified liquid and before the end of boiling.
After the boiling treatment is completed, it is preferably transferred to a whirlpool, cooled to 0 to 10° C. to obtain a cooling liquid, and then subjected to a solid content removal treatment to remove solid content such as solidified protein. Thus, a pre-drink liquid is obtained.
Instead of the above saccharified liquid, the pre-beverage liquid may be prepared by adding hot water to the malt extract, adding hops, a bittering agent, etc., and subjecting the mixture to boiling treatment.
ホップを用いる場合には、煮沸処理前に加えてもよく、液糖溶液の煮沸開始から煮沸終了前の間で加えてもよい。 In addition, when malt is not used as various raw materials, liquid sugar containing carbon sources, nitrogen sources as amino acid-containing raw materials other than wheat or malt, hops, dietary fiber, sweeteners, antioxidants, bitterness imparting agents , Flavor, acidulant, pigment, etc. may be mixed with hot water to prepare a liquid sugar solution, and the liquid sugar solution may be subjected to boiling treatment to prepare a pre-drink liquid.
When hops are used, they may be added before the boiling process, or may be added between the start of boiling the liquid sugar solution and before the end of boiling.
一方で、本発明の一態様の製造方法において、上記の発酵工程及びアルコールを除去する工程を行わない方法であってもよい。 After step (1), a fermentation step using yeast (top-fermenting yeast or bottom-fermenting yeast) is performed to remove the alcohol generated in the fermentation step, and the alcohol content is reduced to 1 (v / v). % (preferably less than 0.5 (v/v)%, more preferably less than 0.1 (v/v)%, still more preferably less than 0.01 (v/v)%, even more preferably 0. 005 (v/v)%) may be performed to produce a soft drink.
On the other hand, the production method of one embodiment of the present invention may be a method in which the fermentation step and the step of removing alcohol are not performed.
工程(2)は、記飲料前液に、炭酸ガスを加える工程である。
炭酸ガスを加える方法について、炭酸飲料を製造する際に適用される公知の方法を用いることができ、例えば、工程(1)で得た飲料前液と炭酸水との混和によって加えてもよく、飲料前液に炭酸ガスを直接添加してもよい。このような方法を用いて、炭酸ガス圧が上述の範囲となるように調整されることが好ましい。 <Step (2)>
Step (2) is a step of adding carbon dioxide gas to the pre-beverage liquid.
As for the method of adding carbon dioxide gas, a known method that is applied in the production of carbonated beverages can be used. Carbon dioxide may be added directly to the pre-beverage solution. Using such a method, the carbon dioxide pressure is preferably adjusted to fall within the range described above.
工程(3)はスクラロース及びアスコルビン酸の少なくとも一方の含有量を調整する工程であり、工程(4)はアセスルファムカリウムの含有量を調整する工程であり、工程(5)は乳酸の含有量を調整する工程である。
工程(3)~工程(5)は、工程(1)の糖化処理の前後、煮沸処理の前後、及び固形分除去処理の前後のいずれに行ってもよく、また、工程(1)終了後の工程(2)の前後で行ってもよい。ただし、最終的に製造される飲料中の含有量を正確に調整する観点から、工程(1)終了後であって、工程(2)開始前に行うことが好ましい。
なお、工程(3)~工程(5)の順序は、特に制限は無く、どちらの工程から行ってもよい。また、工程(3)~工程(5)は連続又は同時に行ってもよく、他の工程を挟んで行われてもよい。 <Step (3), Step (4), Step (5)>
Step (3) is the step of adjusting the content of at least one of sucralose and ascorbic acid, step (4) is the step of adjusting the content of acesulfame potassium, and step (5) is the step of adjusting the content of lactic acid. It is a process to do.
Steps (3) to (5) may be performed before or after the saccharification treatment of step (1), before or after the boiling treatment, and before or after the solid content removal treatment, and after the completion of step (1). It may be performed before or after step (2). However, from the viewpoint of accurately adjusting the content in the finally produced beverage, it is preferable to carry out after the step (1) and before the start of the step (2).
The order of steps (3) to (5) is not particularly limited, and either step may be performed first. Steps (3) to (5) may be carried out continuously or simultaneously, or may be carried out with other steps interposed therebetween.
工程(3)において、調整前の飲料に、スクラロース、アスコルビン酸、スクラロース含有添加剤及びアスコルビン酸含有添加剤なる群から選ばれる1以上を添加して、又は、仕込工程もしくは発酵工程で得られるスクラロース及びアスコルビン酸の量を調整して、清涼飲料に含まれるスクラロース及びアスコルビン酸の量を調整してもよい。
また、調整前の飲料中のスクラロース及びアスコルビン酸の含有量を測定した上で、その測定値の基づき、スクラロース及び/又はアスコルビン酸を添加、もしくは水又は炭酸水を加えて希釈して、スクラロース及びアスコルビン酸の含有量が所定の範囲となるように調整を行ってもよい。なお、すでにスクラロース及びアスコルビン酸の含有量が所望の範囲内である場合には、本工程によるスクラロース、アスコルビン酸等の添加や水又は炭酸水を加えて希釈するといった操作は不要である。 In step (3), the content of either sucralose or ascorbic acid may be adjusted, or the content of both sucralose and ascorbic acid may be adjusted.
In step (3), sucralose obtained by adding one or more selected from the group consisting of sucralose, ascorbic acid, a sucralose-containing additive, and an ascorbic acid-containing additive to the beverage before preparation, or in a preparation process or a fermentation process and the amount of ascorbic acid may be adjusted to adjust the amount of sucralose and ascorbic acid in the soft drink.
In addition, after measuring the content of sucralose and ascorbic acid in the beverage before adjustment, based on the measured value, add sucralose and / or ascorbic acid, or add water or carbonated water to dilute, sucralose and You may adjust so that content of ascorbic acid may be in a predetermined range. When the contents of sucralose and ascorbic acid are already within the desired ranges, the addition of sucralose, ascorbic acid, etc. and the dilution by adding water or carbonated water in this step are unnecessary.
また、工程(3)と同様に、工程(5)においても、調整前の飲料に、乳酸を添加して、乳酸の含有量を調整してもよい。また、調整前の飲料中の乳酸の含有量を測定した上で、その測定値の基づき、乳酸の含有量を添加、もしくは水を加えて希釈して、乳酸の含有量が所定の範囲となるように調整を行ってもよい。なお、調整前の飲料中の原材料に由来する乳酸の存在によって、すでに含有量が所望の範囲内である場合には、本工程による乳酸の添加や水を加えて希釈するといった操作は不要である。 As in step (3), also in step (4), acesulfame potassium may be added to the beverage before preparation to adjust the content of acesulfame potassium.
Also in step (5), similarly to step (3), lactic acid may be added to the beverage before preparation to adjust the content of lactic acid. In addition, after measuring the content of lactic acid in the beverage before adjustment, the content of lactic acid is added or diluted with water based on the measured value so that the content of lactic acid is within a predetermined range. You can adjust as follows. If the content is already within the desired range due to the presence of lactic acid derived from raw materials in the beverage before preparation, the addition of lactic acid in this step and the addition of water for dilution are unnecessary. .
飲料の容器詰め方法としては、特に限定されず、当業者に周知の容器詰め方法を用いることができる。容器詰め工程によって、本発明の清涼飲料は容器に充填・密閉される。容器詰め工程には、いずれの形態・材質の容器を用いてもよく、容器の例としては、上述のとおりである。 The soft drink of one embodiment of the present invention thus obtained is filled in a predetermined container and distributed on the market as a product.
The method for packing the beverage into a container is not particularly limited, and a container packing method known to those skilled in the art can be used. The soft drink of the present invention is filled and sealed in a container by the container filling step. A container of any shape and material may be used in the container filling step, and examples of the container are as described above.
本発明の好適な一態様の清涼飲料は、清涼飲料濃縮液を希釈して得ることができる。また、本発明の好適な一態様のモルトテイスト飲料は、モルトテイスト飲料濃縮液を希釈して得ることができ、本発明の好適な一態様のホップテイスト飲料は、ホップテイスト飲料濃縮液を希釈して得ることができる。清涼飲料濃縮液は水又は炭酸水を用いて希釈できる。本発明の清涼飲料濃縮液を希釈するための希釈倍率は、飲用者の嗜好に合わせて適宜設定してよいが、体積比に基づいて1.1倍以上10倍以下とするのが好ましい。具体的には、たとえば体積比に基づいて2倍の希釈倍率とは、1体積の清涼飲料濃縮液に対して1体積の希釈媒体を加えることをいう。本明細書において、希釈倍率は体積比に基づくものとする。
清涼飲料濃縮液は、清涼飲料と同様に製造できる。具体的には、希釈倍率に合わせて、濃度を向上させた清涼飲料濃縮液を製造できる。
本発明の好適な一態様の清涼飲料濃縮液におけるスクラロースの含有量は好ましくは0.1~45質量ppmであり、より好ましくは0.5~40質量ppm、さらに好ましくは1.0~30質量ppm、よりさらに好ましくは2.0~20質量ppm、特に好ましくは3.0~10質量ppmである。本発明の好適な一態様の清涼飲料濃縮液におけるアスコルビン酸の含有量は好ましくは70~1900質量ppmであり、より好ましくは90~1700質量ppmであり、さらに好ましくは110~1500質量ppmであり、よりさらに好ましくは150~1300質量ppmであり、より好ましくは190~1000質量ppmであり、特に好ましくは230~700質量ppmである。 3. Soft Drink Concentrate and Production Method Thereof The soft drink of one preferred embodiment of the present invention can be obtained by diluting a soft drink concentrate. Further, the malt-taste beverage of one preferred aspect of the present invention can be obtained by diluting the malt-taste beverage concentrate, and the hop-taste beverage of one preferred aspect of the present invention is obtained by diluting the hop-taste beverage concentrate. can be obtained. Soft drink concentrates can be diluted with water or carbonated water. The dilution ratio for diluting the soft drink concentrate of the present invention may be appropriately set according to the preference of the drinker, but is preferably 1.1 times or more and 10 times or less based on the volume ratio. Specifically, for example, a 2-fold dilution ratio based on volume ratio refers to adding 1 volume of dilution medium to 1 volume of soft drink concentrate. In this specification, dilution ratios are based on volume ratios.
Soft drink concentrates can be produced similarly to soft drinks. Specifically, it is possible to produce a concentrated soft drink solution with an improved concentration according to the dilution ratio.
The content of sucralose in the soft drink concentrate of one preferred aspect of the present invention is preferably 0.1 to 45 mass ppm, more preferably 0.5 to 40 mass ppm, still more preferably 1.0 to 30 mass ppm. ppm, more preferably 2.0 to 20 mass ppm, particularly preferably 3.0 to 10 mass ppm. The content of ascorbic acid in the soft drink concentrate of one preferred aspect of the present invention is preferably 70 to 1,900 ppm by mass, more preferably 90 to 1,700 ppm by mass, and still more preferably 110 to 1,500 ppm by mass. , Still more preferably 150 to 1300 mass ppm, more preferably 190 to 1000 mass ppm, and particularly preferably 230 to 700 mass ppm.
水、麦芽及びホップを原料として用い、炭酸ガスを添加して原飲料を調製した。原飲料の調製では、酵母を用いた発酵工程を行わなかった。得られた原飲料の炭酸ガス圧は1.8kgf/cm2、pHは3.6、アルコール度数は0.0(v/v)%、Brixは0.6であった。 [Preparation of original drink]
Water, malt and hops were used as raw materials, and carbon dioxide gas was added to prepare an original beverage. No fermentation step using yeast was performed in the preparation of the original beverage. The original beverage obtained had a carbon dioxide pressure of 1.8 kgf/cm 2 , a pH of 3.6, an alcohol content of 0.0 (v/v)%, and a Brix of 0.6.
このようにして得られた原飲料に、スクラロース、アスコルビン酸、乳酸及びアセスルファムカリウムを表1に記載の含有量となるように添加した。なお、実施例及び比較例で調製した飲料は、いずれも、酒石酸の含有量は300質量ppm未満、リン酸の含有量は300質量ppmとなるように調整した。そして、実施例及び比較例で調製した飲料100mL当たりのカロリーは、いずれも5kcal未満であった。 [Example/Comparative example]
Sucralose, ascorbic acid, lactic acid and acesulfame potassium were added to the raw beverage thus obtained so as to have the contents shown in Table 1. The beverages prepared in Examples and Comparative Examples were each adjusted to have a tartaric acid content of less than 300 mass ppm and a phosphoric acid content of 300 mass ppm. The calories per 100 mL of the beverages prepared in Examples and Comparative Examples were both less than 5 kcal.
・「5.0」:モルトテイスト飲料らしい飲みごたえがかなり強く感じられる。
・「4.0」:モルトテイスト飲料らしい飲みごたえがやや強く感じられる。
・「3.0」:モルトテイスト飲料らしい良好な飲みごたえが適度に感じられる。
・「2.0」:モルトテイスト飲料らしい良好な飲みごたえがある程度感じられる。
・「1.0」:モルトテイスト飲料らしい良好な飲みごたえが感じられない。
[モルトテイスト飲料らしい後味のすっきり感のスコア基準]
・「5.0」:モルトテイスト飲料のすっきり感がかなり強く感じられる。
・「4.0」:モルトテイスト飲料のすっきり感がやや強く感じられる。
・「3.0」:モルトテイスト飲料らしいすっきり感が適度に感じられる。
・「2.0」:モルトテイスト飲料らしいすっきり感がある程度感じられる。
・「1.0」:モルトテイスト飲料らしいすっきり感が感じられない。
[モルトテイスト飲料らしい後味の苦味のスコア基準]
・「5.0」:モルトテイスト飲料の後味の苦味がかなり強く感じられる。
・「4.0」:モルトテイスト飲料の後味がやや強く感じられる。
・「3.0」:モルトテイスト飲料らしい良好な後味の苦味が適度に感じられる。
・「2.0」:モルトテイスト飲料らしい良好な後味の苦味がある程度感じられる。
・「1.0」:モルトテイスト飲料らしい良好な後味の苦味が感じられない。 [Score criteria for malt-taste-like drinkability]
- "5.0": Feels quite strong to drink like a malt-taste beverage.
- "4.0": A slightly strong feeling of a malt-taste drink.
- "3.0": Moderately good feeling of a malt-taste beverage.
- "2.0": A good feeling of drinking that seems to be a malt-taste beverage can be felt to some extent.
· “1.0”: A good feeling of drinking that is typical of malt-taste beverages is not felt.
[Score criteria for refreshing aftertaste typical of malt-taste beverages]
- "5.0": The refreshing feeling of the malt-taste beverage is felt quite strongly.
- "4.0": The refreshing feeling of the malt-taste beverage is slightly strong.
- "3.0": Moderate refreshing feeling typical of malt-taste beverages.
- "2.0": Refreshing feeling typical of malt-taste beverages can be felt to some extent.
- "1.0": A refreshing feeling typical of malt-taste beverages is not felt.
[Score criteria for bitterness of aftertaste typical of malt-taste beverages]
- "5.0": The bitter aftertaste of the malt-taste beverage is felt quite strongly.
- "4.0": The aftertaste of a malt-taste beverage is felt to be slightly strong.
- "3.0": Moderate bitterness of a good aftertaste typical of malt-taste beverages.
- "2.0": A good bitter aftertaste typical of malt-taste beverages can be sensed to some extent.
・“1.0”: A good bitter aftertaste typical of malt-taste beverages is not felt.
[総合評価]
・「A」:「モルトテイスト飲料らしい後味すっきり感」、「モルトテイスト飲料らしい飲みごたえ」及び「モルトテイスト飲料らしい後味の苦味」の3つの官能評価項目の各パネラーのスコアの平均値がいずれも2.5以上かつ3.5以下。
・「B」:「モルトテイスト飲料らしい後味すっきり感」、「モルトテイスト飲料らしい飲みごたえ」及び「モルトテイスト飲料らしい後味の苦味」の3つの官能評価項目の各パネラーのスコアの平均値がいずれも2.0以上かつ4.0以下であり、かつ、「A」に該当しない。
・「C」:「A」にも「B」にも該当しない。 In addition, from the average score of each panelist for the above three sensory evaluation items, each malt-taste beverage was comprehensively evaluated according to the following evaluation criteria. The results were as shown in Table 1.
[Comprehensive evaluation]
・ “A”: The average score of each panelist for the three sensory evaluation items of “refreshing aftertaste like a malt taste drink”, “drinking response like a malt taste drink”, and “bitter aftertaste like a malt taste drink”. 2.5 or more and 3.5 or less.
・ “B”: The average score of each panelist for the three sensory evaluation items of “refreshing aftertaste like a malt taste drink”, “drinking response like a malt taste drink”, and “bitter aftertaste like a malt taste drink”. It is 2.0 or more and 4.0 or less, and does not correspond to "A".
- "C": Neither "A" nor "B" applies.
Claims (15)
- スクラロースの含有量が、0.1~4.5質量ppmであり、
アスコルビン酸の含有量が、70~190質量ppmである、
清涼飲料。 The content of sucralose is 0.1 to 4.5 mass ppm,
The content of ascorbic acid is 70 to 190 mass ppm,
Soft drink. - スクラロースの含有量(単位:質量ppm)とアスコルビン酸の含有量(単位:質量ppm)との含有量比〔スクラロース/アスコルビン酸〕が、0.005~0.04である、請求項1に記載の清涼飲料。 2. The content ratio of the sucralose content (unit: mass ppm) and the ascorbic acid content (unit: mass ppm) [sucralose/ascorbic acid] is 0.005 to 0.04. soft drink.
- さらにアセスルファムカリウムを含有する、請求項1又は2に記載の清涼飲料。 The soft drink according to claim 1 or 2, further containing acesulfame potassium.
- さらに乳酸を含有する、請求項1~3のいずれかに記載の清涼飲料。 The soft drink according to any one of claims 1 to 3, further containing lactic acid.
- 酒石酸の含有量が、300質量ppm未満である、請求項1~4のいずれか1つに記載の清涼飲料。 The soft drink according to any one of claims 1 to 4, wherein the content of tartaric acid is less than 300 mass ppm.
- リン酸の含有量が、300質量ppm未満である、請求項1~5のいずれか1つに記載の清涼飲料。 The soft drink according to any one of claims 1 to 5, wherein the phosphoric acid content is less than 300 mass ppm.
- 原材料としてモルトエキスを用いた飲料である、請求項1~6のいずれか1つに記載の清涼飲料。 The soft drink according to any one of claims 1 to 6, which is a drink using malt extract as a raw material.
- 前記清涼飲料のカロリーが、100mL当たり5kcal未満である、請求項1~7のいずれか1つに記載の清涼飲料。 The soft drink according to any one of claims 1 to 7, wherein the soft drink has less than 5 kcal per 100 mL.
- 容器詰め飲料である、請求項1~8のいずれか1つに記載の清涼飲料。 The soft drink according to any one of claims 1 to 8, which is a packaged drink.
- 前記容器詰め飲料の炭酸ガス圧が、0.20kgf/cm2以上5.0kgf/cm2以下である、請求項9に記載の清涼飲料。 The soft drink according to claim 9, wherein the packaged beverage has a carbon dioxide pressure of 0.20 kgf/cm 2 or more and 5.0 kgf/cm 2 or less.
- 1.1倍以上10倍以下の希釈倍率で希釈して得られる請求項1~10のいずれか1つに記載の清涼飲料を製造するための清涼飲料濃縮液。 A soft drink concentrate for producing a soft drink according to any one of claims 1 to 10, which is obtained by dilution at a dilution ratio of 1.1 times or more and 10 times or less.
- 水又は炭酸水で希釈される請求項11に記載された濃縮液。 The concentrate according to claim 11, which is diluted with water or carbonated water.
- スクラロースの含有量が、0.1~45質量ppmであり、アスコルビン酸の含有量が、70~1900質量ppmである、請求項11又は12に記載の濃縮液。 The concentrate according to claim 11 or 12, wherein the content of sucralose is 0.1 to 45 ppm by mass and the content of ascorbic acid is 70 to 1900 ppm by mass.
- 清涼飲料がモルトテイスト飲料又はホップテイスト飲料である、請求項1~10のいずれかに記載された飲料。 The beverage according to any one of claims 1 to 10, wherein the soft drink is a malt-taste beverage or a hop-taste beverage.
- 清涼飲料濃縮液がモルトテイスト飲料濃縮液又はホップテイスト飲料濃縮液である、請求項11~13のいずれかに記載された濃縮液。
A concentrate according to any one of claims 11 to 13, wherein the soft drink concentrate is a malt-tasting beverage concentrate or a hop-tasting beverage concentrate.
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JP2011030512A (en) * | 2009-08-03 | 2011-02-17 | Suntory Holdings Ltd | Vitamin c-enriched beverage |
JP2015027309A (en) * | 2014-09-30 | 2015-02-12 | 太一 染谷 | Agent for imparting beer flavor, and beer-flavored beverage |
JP2016111964A (en) * | 2014-12-15 | 2016-06-23 | サントリーホールディングス株式会社 | Beer taste alcoholic beverage |
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Publication number | Priority date | Publication date | Assignee | Title |
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JP2011030512A (en) * | 2009-08-03 | 2011-02-17 | Suntory Holdings Ltd | Vitamin c-enriched beverage |
JP2015027309A (en) * | 2014-09-30 | 2015-02-12 | 太一 染谷 | Agent for imparting beer flavor, and beer-flavored beverage |
JP2016111964A (en) * | 2014-12-15 | 2016-06-23 | サントリーホールディングス株式会社 | Beer taste alcoholic beverage |
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