WO2022047835A1 - 一种煤自燃特征参数测定实验平台 - Google Patents

一种煤自燃特征参数测定实验平台 Download PDF

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WO2022047835A1
WO2022047835A1 PCT/CN2020/115781 CN2020115781W WO2022047835A1 WO 2022047835 A1 WO2022047835 A1 WO 2022047835A1 CN 2020115781 W CN2020115781 W CN 2020115781W WO 2022047835 A1 WO2022047835 A1 WO 2022047835A1
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gas
coal
spontaneous combustion
infrared thermal
characteristic parameters
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PCT/CN2020/115781
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English (en)
French (fr)
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朱红青
陆新晓
郭松
谭波
李峰
赵金龙
姚勇征
赵鸿儒
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中国矿业大学(北京)
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Publication of WO2022047835A1 publication Critical patent/WO2022047835A1/zh

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    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N25/00—Investigating or analyzing materials by the use of thermal means
    • G01N25/20—Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity
    • G01N25/22—Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity on combustion or catalytic oxidation, e.g. of components of gas mixtures
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01D—MEASURING NOT SPECIALLY ADAPTED FOR A SPECIFIC VARIABLE; ARRANGEMENTS FOR MEASURING TWO OR MORE VARIABLES NOT COVERED IN A SINGLE OTHER SUBCLASS; TARIFF METERING APPARATUS; MEASURING OR TESTING NOT OTHERWISE PROVIDED FOR
    • G01D21/00—Measuring or testing not otherwise provided for
    • G01D21/02—Measuring two or more variables by means not covered by a single other subclass
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/22—Fuels, explosives
    • G01N33/222—Solid fuels, e.g. coal

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  • the invention relates to the technical field of coal spontaneous combustion experiments, in particular to an experimental platform for measuring coal spontaneous combustion characteristic parameters.
  • Coal spontaneous combustion is a complex and dynamic physical and chemical reaction.
  • oxygen molecules first physically and chemically adsorb on the coal surface and release reaction heat, which promotes the temperature rise, and the temperature rise promotes deep oxidation and decomposition reactions between oxygen molecules and the active functional groups in the coal molecules, resulting in the formation of macromolecules in the coal.
  • the type of characteristic gas released and when the characteristic gas is released are the characteristic parameters of coal spontaneous combustion.
  • Comprehensive and accurate measurement of coal spontaneous combustion characteristic parameters can provide theoretical support and technical support for mine fire prediction and prediction, and effectively control and prevent the occurrence of coal spontaneous combustion.
  • 201310638108.9 describes a coal spontaneous combustion high temperature temperature programming device, through which the coal sample is heated by high temperature programming to establish a coal spontaneous combustion model, but this method cannot monitor the quality change and temperature change of the coal sample in real time.
  • the present invention provides an experimental platform for the determination of coal spontaneous combustion characteristic parameters.
  • the characteristic parameters such as the heating rate of each marked point inside the coal sample are monitored and measured in real time, and the heating process of coal can also be simulated, and the characteristic parameters such as the quality of coal, gas products, and heating rate of each marked point inside the coal sample can be measured in real time during the spontaneous combustion of coal.
  • the present invention provides the following scheme:
  • the invention provides an experimental platform for measuring the characteristic parameters of coal spontaneous combustion, comprising: an intelligent temperature control reaction box; a gas supply component, wherein the gas supply component includes a plurality of gas supply devices for containing gas; a gas distribution instrument, each of the gas supply components The devices are all communicated with the air inlet of the gas distribution instrument, and the air outlet of the gas distribution instrument is communicated with the inside of the intelligent temperature control reaction box; the hanging weighing device used for detecting the quality of coal samples, the A hanging weighing device is arranged on the top of the intelligent temperature control reaction box; a hanging basket is connected to the hanging weighing device through a connecting rope, and the coal sample is placed in the hanging basket; a chromatograph, the air inlet of the gas chromatograph is communicated with the inside of the intelligent temperature control reaction box; an infrared thermal imaging system, the infrared thermal imaging system includes an infrared thermal imaging camera and an infrared thermal imaging probe, the infrared thermal imaging system The instrument is connected in communication with the infrared
  • the experimental platform for measuring the characteristic parameters of coal spontaneous combustion further comprises a gas flow dispersing pipe, the first end of the gas flow dispersing pipe is arranged inside the intelligent temperature control reaction box, and the first end of the gas flow dispersing pipe is spherical structure, and the first end of the gas flow dispersing pipe is provided with a plurality of dispersing holes that communicate with the inside of the gas flow dispersing pipe, the second end of the gas flow dispersing pipe and the gas outlet of the gas distribution instrument connected.
  • the experimental platform for measuring the characteristic parameters of coal spontaneous combustion further includes a gas flow changing device
  • the gas flow changing device includes a sleeve and a top plate
  • a plurality of air holes are provided on the peripheral side wall of the sleeve
  • the top plate is disposed on the The top end of the sleeve is closed to block the top end of the sleeve
  • the bottom end of the sleeve is in contact with the bottom end of the intelligent temperature control reaction box
  • the first end of the gas flow dispersing pipe is arranged on the inside the sleeve.
  • the sleeve is made of gauze.
  • a box door is provided on one side of the intelligent temperature control reaction box, and a high temperature resistant transparent glass window is provided on the box door.
  • the suspension basket is an aluminum suspension basket, and the suspension basket is oxidized.
  • the gas supply device is a gas cylinder.
  • the ambient temperature sensing device is an ambient temperature sensing thermocouple
  • the coal sample temperature sensing device is a coal sample temperature sensing thermocouple
  • the infrared thermal imaging camera is a split infrared thermal imaging camera
  • the infrared thermal imaging probe is a high temperature resistant infrared thermal imaging probe.
  • the hanging weighing device is an electronic balance.
  • the experimental platform for measuring the characteristic parameters of coal spontaneous combustion includes: an intelligent temperature control reaction box; a gas supply component, wherein the gas supply component includes a plurality of gas supply devices for containing gas; a gas distribution instrument, each gas supply device is connected with the gas distribution device The air inlet of the instrument is connected, and the air outlet of the gas distribution instrument is communicated with the inside of the intelligent temperature control reaction box; the hanging weighing device used to detect the quality of the coal sample, the hanging weighing device is installed in the intelligent temperature control reaction box.
  • the infrared thermal imaging system includes an infrared thermal imaging camera and an infrared thermal imaging probe, the infrared thermal imaging camera is connected to the infrared thermal imaging probe in communication, and the infrared thermal imaging probe is set in the intelligent temperature control reaction box;
  • the temperature sensing component the temperature sensing component is set in the Inside the intelligent temperature control reaction box, the temperature sensing components include an ambient temperature sensing device for sensing the internal temperature of the temperature box and a coal sample temperature sensing device for sensing the temperature of coal samples; computer, hanging weighing device, gas chromatograph, infrared
  • the thermal imager, the ambient temperature sensing device and the coal sample temperature sensing device are all connected in communication with the computer.
  • the experimental platform for the determination of coal spontaneous combustion characteristic parameters can use the metal mesh basket intersection method to predict the critical temperature of coal spontaneous combustion in a constant temperature environment and different gas atmospheres.
  • the characteristic parameters such as rate are monitored and measured in real time. It can also simulate the heating process of coal under different gas atmospheres, and measure the characteristic parameters of coal quality, gas products, heating rate of each marked point inside the coal sample in real time during the spontaneous combustion of coal.
  • the platform is easy to use, has a comprehensive range of measurement, and is convenient to control the experimental conditions, which is of great significance for the measurement of coal spontaneous combustion characteristic parameters.
  • Fig. 1 is the structural representation of the coal spontaneous combustion characteristic parameter measurement experimental platform provided in the embodiment of the present invention
  • Fig. 2 is the internal structure schematic diagram of the intelligent temperature-controlled reaction box of the coal spontaneous combustion characteristic parameter measurement experimental platform provided in the embodiment of the present invention
  • FIG. 3 is a schematic structural diagram of a suspension basket of an experimental platform for measuring the characteristic parameters of coal spontaneous combustion provided in the embodiment of the present invention
  • FIG. 4 is a schematic structural diagram of the structure diagram of the fully automatic online analysis gas chromatograph of the experimental platform for the determination of coal spontaneous combustion characteristic parameters provided in the embodiment of the present invention.
  • Gas supply device 2. Gas distribution instrument; 3. Gas flow direction dispersion pipe; 4. Gas flow changing device; 5. Intelligent temperature control reaction box; 6. Infrared thermal imaging probe; 7. Infrared thermal imaging camera; 8. Hanging basket; 9. Coal sample temperature sensing device; 10. Ambient temperature sensing device; 11. Connecting rope; 12. Hanging weighing device; 13. Coal spontaneous combustion sign gas collection pipeline; 14. Automatic online analysis gas chromatograph 15. Data acquisition equipment; 16. Computer; 17. High temperature resistant transparent glass window; 18. Box door.
  • the purpose of the present invention is to provide an experimental platform for measuring coal spontaneous combustion characteristic parameters, which can simulate the underground environment of the mine and simultaneously measure characteristic parameters such as coal quality, gas product, and heating rate of each marked point inside the coal sample.
  • the experimental platform for the determination of coal spontaneous combustion characteristic parameters includes an intelligent temperature control reaction box 5, a gas supply assembly, a gas distribution instrument 2, a hanging weighing device 12, a hanging basket 8, a gas chromatograph Instrument, infrared thermal imaging system, temperature sensing components and computer 16, wherein, the intelligent temperature control reaction box 5 is used to control the ambient temperature in which the experiment is located, and a constant temperature program or a temperature rise program can be set according to the needs of the experiment.
  • the gas supply component includes a plurality of gas supply devices 1 for containing gas, and the gas supply component is generally supplied with N2, O2 and other commonly used gases for measuring coal spontaneous combustion characteristic parameters, and different gases are placed in different gas cylinders ; wherein, the air inlet of the gas distribution instrument 2 is communicated with each air supply device 1, and the air outlet of the gas distribution instrument 2 is communicated with the inside of the intelligent temperature control reaction box 5, and the gas distribution instrument 2 belongs to the prior art, and the gas distribution instrument 2.
  • the hanging weighing device 12 is used to measure the quality change of the coal sample during the coal spontaneous combustion experiment, and the hanging weighing device 12 is arranged at The top of the intelligent temperature control reaction box 5; wherein, the hanging basket 8 is connected with the hanging weighing device 12 through the connecting rope 11, the coal sample is placed in the hanging basket 8, and the coal sample is burned in the hanging basket 8; wherein, the gas chromatograph
  • the air inlet is communicated with the inside of the intelligent temperature control reaction box 5, and the gas chromatograph belongs to the prior art.
  • the gas chromatograph is an automatic online analysis gas chromatograph 14, and an automatic online analysis gas chromatograph 14.
  • the coal spontaneous combustion flag gas collection pipeline 13 is communicated with the intelligent temperature control reaction box 5, and the coal spontaneous combustion flag gas acquisition pipeline 13 passes the gas in the intelligent temperature control reaction box 5 into the fully automatic online analysis gas chromatograph 14 for automatic gas analysis. analysis, so as to monitor the changes of the gas content in the process of coal spontaneous combustion in real time.
  • the specific structure of the coal spontaneous combustion mark gas collection pipeline 13 is substantially the same as that of the ordinary pipeline; wherein, the infrared thermal imaging system includes an infrared thermal imaging camera 7 and an infrared thermal imaging probe 6.
  • the infrared thermal imager 7 is connected in communication with the infrared thermal image probe 6, and the infrared thermal image probe 6 is arranged in the intelligent temperature control reaction box 5.
  • the infrared thermal image probe 6 monitors the changes of the infrared thermal image state of the coal sample in real time during the experiment, and then monitors the changes of the thermal image state of the coal sample in real time.
  • the detected information is transmitted to the infrared thermal imager 7; wherein, the temperature sensing component is arranged inside the intelligent temperature control reaction box 5, and the temperature sensing component includes an ambient temperature sensing device 10 for sensing the internal temperature of the temperature box and a coal sample for sensing the temperature.
  • the coal sample temperature sensing device 9 for temperature the purpose of detecting both the ambient temperature and the coal sample temperature is that there may be errors between the ambient temperature and the actual temperature of the coal sample.
  • the hanging weighing device 12, the gas chromatograph, the infrared thermal imager 7, the ambient temperature sensing device 10 and the coal sample temperature sensing device 9 are all connected in communication with the computer 16 to transmit the detected information to the computer. 16.
  • the computer 16 performs summary processing on the received information.
  • the data acquisition device 15 receives the ambient temperature sensing device 10 and the coal sample temperature sensing device 15.
  • the device 9, the hanging weighing device 12 and the fully automatic online analysis gas chromatograph 14 measure the temperature, mass and gas concentration data, and transmit the received temperature, mass and gas concentration data to the computer 16 for data processing.
  • the experimental platform for the determination of coal spontaneous combustion characteristic parameters has comprehensive measurement indicators, wide measurement range and remarkable measurement effect. Prevention of spontaneous combustion is important.
  • the existing coal spontaneous combustion characteristic parameter measurement process is intermittent, sampling and analysis are carried out separately, the operation is cumbersome, and gas leakage is prone to occur, resulting in a decrease in the accuracy of the experiment, and the coal spontaneous combustion characteristic parameter measurement experimental platform can continuously complete the coal spontaneous combustion Determination of characteristic parameters effectively overcomes the above-mentioned defects.
  • the experimental platform for measuring the characteristic parameters of coal spontaneous combustion further includes a gas flow direction dispersion pipe 3, the first end of the gas flow direction dispersion pipe 3 is arranged inside the intelligent temperature control reaction box 5, and the first end of the gas flow direction dispersion pipe 3 is closed.
  • the first end of the gas flow dispersion pipe 3 is a spherical structure, and the first end of the gas flow dispersion pipe 3 is provided with a plurality of dispersion holes that communicate with the inside of the gas flow dispersion pipe 3, and the gas flows to the second end of the dispersion pipe 3 It is communicated with the gas outlet of the gas distributor 2.
  • the experimental platform for measuring the characteristic parameters of coal spontaneous combustion also includes a gas flow changing device 4, and the gas flow changing device 4 includes a sleeve and a top plate, and the peripheral side wall of the sleeve is provided with a A plurality of air holes, the top plate is arranged on the top of the sleeve to block the top of the sleeve, the bottom end of the sleeve is in contact with the bottom end of the intelligent temperature control reaction box 5, and the first end of the gas flow dispersing pipe 3 is arranged on the sleeve Inside.
  • the gas flow changing device 4 cooperates with the gas flow dispersing pipe 3 to prevent the intake air flow from affecting the stable state of the gas in the intelligent temperature control reaction box 5 .
  • the sleeve is made of gauze.
  • the sleeve refers to a structure with a hollow interior and open ends at both ends.
  • a box door 18 is provided on one side of the intelligent temperature control reaction box 5 .
  • the intelligent temperature control reaction box is specifically a temperature control box.
  • the box door 18 is provided with a high temperature resistant transparent glass window 17 .
  • the suspension basket 8 is an aluminum suspension basket, and the suspension basket 8 is oxidized, so that the thermal conductivity is guaranteed to be similar to that of coal, thereby reducing the error effect of the material of the suspension basket 8 on the experiment.
  • the overall structure of the suspension basket 8 is substantially the same as that of the basket, and there are numerous pores thereon, which ensure that ambient gas can quickly enter the interior of the suspension basket 8 .
  • the volume of the hanging basket 8 is determined according to the quality requirements of the coal samples in different experiments.
  • the gas supply device 1 is a gas cylinder. It should be noted that the gas supply device 1 is not limited to the use of gas cylinders, and any structure capable of holding gas may be used.
  • the ambient temperature sensing device 10 is an ambient temperature sensing thermocouple
  • the coal sample temperature sensing device 9 is a coal sample temperature sensing thermocouple.
  • the detection end of the ambient temperature induction thermocouple is placed in the intelligent temperature control reaction box to sense the ambient temperature
  • the detection end of the coal sample temperature induction thermocouple is placed in the hanging basket 8 to sense the coal sample temperature.
  • the infrared thermal imager 7 is a split-type infrared thermal imager
  • the infrared thermal imager probe 6 is a high-temperature resistant infrared thermal imager probe, so as to prevent the infrared thermal imager probe 6 from being damaged in a high temperature environment.
  • the hanging weighing device 12 is an electronic balance. It should be noted that the hanging weighing device 12 is not limited to the use of electronic balances, and any device that can realize hanging weighing can be used.
  • the coal spontaneous combustion characteristic parameter measurement experimental platform is set up, and the intelligent temperature control reaction box 5 is filled with ambient gas;
  • the gas distribution instrument 2 is used for proportioning; the coal sample is put into the hanging basket 8; the various experimental devices are connected to ensure good air tightness of the experimental catheter and equipment;
  • the intelligent temperature control reaction box 5 is turned on, and the temperature program or constant temperature is set , the temperature rise can be carried out in stages and the time required for the temperature rise can be set; turn on the high temperature resistant infrared thermal imaging probe, the coal sample temperature induction thermocouple, and the ambient temperature induction thermocouple, and simultaneously turn on the data acquisition device and the computer 16 .
  • the temperature state image of the coal sample during the reaction process was collected by a split infrared thermal imager.
  • the temperature of the coal sample during the experiment is measured by a coal sample temperature induction thermocouple, and fed back to the data acquisition device 15 .
  • the ambient temperature during the experiment is measured by an ambient temperature induction thermocouple, and fed back to the data acquisition device 15 .
  • the experimental exhaust gas generated during the heating process is simultaneously collected through the coal spontaneous combustion mark gas collection pipeline 13, and the exhaust gas is transmitted to the fully automatic on-line analysis gas chromatograph 14 to measure the type and content of the exhaust gas, and combine the occurrence time of the exhaust gas and the coal sample , ambient temperature, and real-time monitoring of the characteristic parameters of coal spontaneous combustion.
  • the characteristic parameters of coal spontaneous combustion under different gas environments can be evaluated.
  • the relevant temperature of the coal sample and the environmental thermocouple is measured, and the infrared thermal imager 7 is used to collect the coal sample during the heating process
  • the temperature change image of the sample is used to dynamically capture the characteristic parameters such as the quality of coal, gas products, and the heating rate of each marked point inside the coal sample during the coal spontaneous combustion process, so as to provide theoretical and technical support for mine fire prediction and prediction, and effectively control and prevent The occurrence of spontaneous combustion of coal.

Abstract

一种煤自燃特征参数测定实验平台，属于煤自燃实验技术领域，其包括：智能控温反应箱(5)；供气组件，其包括多个供气装置(1)；配气仪(2)，各供气装置(1)均与配气仪(2)相连通，配气仪(2)与智能控温反应箱(5)内部相连通；悬挂式称重装置(12)，其设置于智能控温反应箱(5)的顶端；悬篮(8)，悬篮(8)与悬挂式称重装置(12)相连；气相色谱仪(14)，其与智能控温反应箱(5)内部连通；红外热像系统；温度感应组件，其设置于智能控温反应箱(5)内部，其包括环境温度感应装置(10)和煤样温度感应装置(9)；计算机(16)。该实验平台能够模拟矿井下环境，且能够对煤自燃过程中煤的质量、气体产物、煤样内部各标志点升温速率等特征参数进行动态捕捉。

Description

一种煤自燃特征参数测定实验平台 技术领域
本发明涉及煤自燃实验技术领域，特别是涉及一种煤自燃特征参数测定实验平台。
背景技术
煤自燃是一个复杂的、动态的物理化学反应。该现象中氧分子首先在煤表面发生物理、化学吸附并放出反应热，促使温度上升，而温度的升高促使氧分子与煤分子中的活性官能团发生深度氧化分解反应使得煤中的大分子生成小分子并释放一定的特征气体和大量的反应热。这些热量在煤体内部积聚，最终导致煤自燃。而释放出的特征气体种类以及何时释放该种特征气体便是煤自燃特征参数。全面、准确地测量出煤自燃特征参数能够为矿井火灾预测预报提供理论支持和技术支撑，有效的控制和预防煤自燃的发生。
目前，针对煤自燃特征参数测定，主要是建立恒温箱，通过控制程序升温，测定煤自燃过程中特征气体出现的时间以及温度。201310638108.9描述了一种煤自燃高温程序升温装置，通过该实验装置对煤样进行高温程序升温，建立煤自燃模型，但这种方法无法对煤样质量变化及温度变化进行实时监测。
因此，如何克服上述缺陷成为本领域技术人员目前所亟待解决的问题。
发明内容
为解决以上技术问题，本发明提供一种煤自燃特征参数测定实验平台，该煤自燃特征参数测定实验平台能够在不同气体环境下对煤自燃特征参数测定，同时能够对煤的质量、气体产物、煤样内部各标志点升温速率等特征参数进行实时监控测定，亦可模拟煤升温过程，并实时测定煤自燃过程煤的质量、气体产物、煤样内部各标志点升温速率等特征参数。
为实现上述目的，本发明提供了如下方案：
本发明提供一种煤自燃特征参数测定实验平台包括：智能控温反应 箱；供气组件，所述供气组件包括多个用于盛装气体的供气装置；配气仪，各所述供气装置均与所述配气仪的进气口相连通，所述配气仪的出气口与所述智能控温反应箱内部相连通；用于检测煤样质量的悬挂式称重装置，所述悬挂式称重装置设置于所述智能控温反应箱的顶端；悬篮，所述悬篮通过连接绳与所述悬挂式称重装置相连，所述煤样置于所述悬篮内；气相色谱仪，所述气相色谱仪的进气口与所述智能控温反应箱内部连通；红外热像系统，所述红外热像系统包括红外热像仪和红外热像探头，所述红外热像仪与所述红外热像探头通信连接，所述红外热像探头设置于所述智能控温反应箱内；温度感应组件，所述温度感应组件设置于所述智能控温反应箱内部，所述温度感应组件包括用于感应所述温度箱内部温度的环境温度感应装置和用于感应所述煤样温度的煤样温度感应装置；计算机，所述悬挂式称重装置、所述气相色谱仪、所述红外热像仪、所述环境温度感应装置以及所述煤样温度感应装置均与所述计算机通信连接。
优选地，煤自燃特征参数测定实验平台还包括气体流向分散管，所述气体流向分散管的第一端设置于所述智能控温反应箱内部，所述气体流向分散管的第一端为球形结构，且所述气体流向分散管的第一端设置有多个与所述气体流向分散管内部相连通的分散孔，所述气体流向分散管的第二端与所述配气仪的出气口相连通。
优选地，煤自燃特征参数测定实验平台还包括气体变流装置，所述气体变流装置包括套筒和顶板，所述套筒的周侧壁上设置有多个气孔，所述顶板设置于所述套筒的顶端、以封堵所述套筒的顶端，所述套筒的底端与所述智能控温反应箱的底端相抵，所述气体流向分散管的第一端设置于所述套筒内。
优选地，所述套筒采用纱网制成。
优选地，所述智能控温反应箱的一侧设置有箱门，所述箱门上设置有耐高温透明玻璃窗。
优选地，所述悬篮为铝悬篮，且所述悬篮做氧化处理。
优选地，所述供气装置为气瓶。
优选地，所述环境温度感应装置为环境温度感应热电偶，所述煤样温度感应装置为煤样温度感应热电偶。
优选地，所述红外热像仪为分体式红外热像仪，所述红外热像探头为耐高温红外热像探头。
优选地，所述悬挂式称重装置为电子天平。
本发明相对于现有技术取得了以下技术效果：
本发明提供的煤自燃特征参数测定实验平台包括：智能控温反应箱；供气组件，供气组件包括多个用于盛装气体的供气装置；配气仪，各供气装置均与配气仪的进气口相连通，配气仪的出气口与智能控温反应箱内部相连通；用于检测煤样质量的悬挂式称重装置，悬挂式称重装置设置于智能控温反应箱的顶端；悬篮，悬篮通过连接绳与悬挂式称重装置相连，煤样置于悬篮内；气相色谱仪，气相色谱仪的进气口与智能控温反应箱内部连通；红外热像系统，红外热像系统包括红外热像仪和红外热像探头，红外热像仪与红外热像探头通信连接，红外热像探头设置于智能控温反应箱内；温度感应组件，温度感应组件设置于智能控温反应箱内部，温度感应组件包括用于感应温度箱内部温度的环境温度感应装置和用于感应煤样温度的煤样温度感应装置；计算机，悬挂式称重装置、气相色谱仪、红外热像仪、环境温度感应装置以及煤样温度感应装置均与计算机通信连接。该煤自燃特征参数测定实验平台，能在恒温环境、不同气体氛围下，运用金属网篮交叉点法对煤自燃临界温度进行预测，同时对煤的质量、气体产物、煤样内部各标志点升温速率等特征参数进行实时监控测定。亦可在不同气体氛围下，模拟煤升温过程，实时测定煤自燃过程煤的质量、气体产物、煤样内部各标志点升温速率等特征参数。该平台使用方法简便，测定范围全面，实验条件方便调控，对煤自燃特征参数测定实验具有重要意义。
附图说明
为了更清楚地说明本发明实施例或现有技术中的技术方案，下面将对实施例中所需要使用的附图作简单地介绍，显而易见地，下面描述中的附图仅仅是本发明的一些实施例，对于本领域普通技术人员来讲，在不付出创造性劳动的前提下，还可以根据这些附图获得其他的附图。
图1为本发明实施例中提供的煤自燃特征参数测定实验平台的结构示意图；
图2为本发明实施例中提供的煤自燃特征参数测定实验平台智能控 温反应箱的内部结构示意图；
图3为本发明实施例中提供的煤自燃特征参数测定实验平台悬篮的结构示意图；
图4为本发明实施例中提供的煤自燃特征参数测定实验平台全自动在线分析气象色谱仪结构图的结构示意图。
附图标记说明：
1、供气装置；2、配气仪；3、气体流向分散管；4、气体变流装置；5、智能控温反应箱；6、红外热像探头；7、红外热像仪；8、悬篮；9、煤样温度感应装置；10、环境温度感应装置；11、连接绳；12、悬挂式称重装置；13、煤自燃标志气体采集管路；14、全自动在线分析气相色谱仪；15、数据采集设备；16、计算机；17、耐高温透明玻璃窗；18、箱门。
具体实施方式
下面将结合本发明实施例中的附图，对本发明实施例中的技术方案进行清楚、完整地描述，显然，所描述的实施例仅仅是本发明一部分实施例，而不是全部的实施例。基于本发明中的实施例，本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例，都属于本发明保护的范围。
本发明的目的是提供一种能够模拟矿井下环境，且能够同时测定煤的质量、气体产物、煤样内部各标志点升温速率等特征参数的煤自燃特征参数测定实验平台。
为使本发明的上述目的、特征和优点能够更加明显易懂，下面结合附图和具体实施方式对本发明作进一步详细的说明。
如图1-4所示，本实施例提供的煤自燃特征参数测定实验平台包括智能控温反应箱5、供气组件、配气仪2、悬挂式称重装置12、悬篮8、气相色谱仪、红外热像系统、温度感应组件以及计算机16，其中，智能控温反应箱5用于控制实验所处环境温度，可根据实验需要设定恒温程序或升温程序，能够实现该功能的结构均可；其中，供气组件包括多个用于盛装气体的供气装置1，供气组件一般供气种类为N2、O2等测定煤自燃特征参数常用气体，不同的气体置于不同的气瓶中；其中，配气仪2的进气口与各供气装置1均连通，配气仪2的出气口与智能控温反应箱5内部相 连通，配气仪2属于现有技术，配气仪2控制各实验气体进气比例，从而研究不同气体氛围下煤自燃特征参数；其中，悬挂式称重装置12用于测定煤自燃实验过程中煤样的质量变化，悬挂式称重装置12设置于智能控温反应箱5的顶端；其中，悬篮8通过连接绳11与悬挂式称重装置12相连，煤样置于悬篮8内，煤样在悬篮8内燃烧；其中，气相色谱仪的进气口与智能控温反应箱5内部连通，气相色谱仪属于现有技术，本实施例中具体地，气相色谱仪为全自动在线分析气相色谱仪14，全自动在线分析气相色谱仪14通过煤自燃标志气体采集管路13与智能控温反应箱5相连通，煤自燃标志气体采集管路13将智能控温反应箱5内的气体通入全自动在线分析气相色谱仪14进行自动气体分析，从而实时监测煤自燃过程中各气体含量变化，煤自燃标志气体采集管路13具体结构与普通管路实质相同；其中，红外热像系统包括红外热像仪7和红外热像探头6，红外热像仪7与所述红外热像探头6通信连接，红外热像探头6设置于智能控温反应箱5内，红外热像探头6实时监控实验过程中煤样红外热像状态变化并将检测到的信息传递至红外热像仪7；其中，温度感应组件设置于智能控温反应箱5内部，温度感应组件包括用于感应温度箱内部温度的环境温度感应装置10和用于感应煤样温度的煤样温度感应装置9，既检测环境温度又检测煤样温度的目的是环境温度与煤样实际温度可能存在误差，如果仅检测环境温度，以环境温度作为煤样温度，则可能导致实验精确度降低；悬挂式称重装置12、气相色谱仪、红外热像仪7、环境温度感应装置10以及煤样温度感应装置9均与计算机16通信连接、以将各自检测到的信息传递至计算机16，计算机16对接收的信息进行汇总处理，本实施例中具体地，数据采集设备15接收环境温度感应装置10、煤样温度感应装置9、悬挂式称重装置12和全自动在线分析气相色谱仪14测定的温度、质量，气体浓度数据，并将其接收到的温度、质量，气体浓度数据传输到计算机16进行数据处理。
该煤自燃特征参数测定实验平台测定指标全面，测定范围广，测定效果显著，能对煤自燃过程中煤的质量、气体产物、煤样内部各标志点升温速率等特征参数进行动态捕捉，对煤自燃预防具有重要意义。另外，现有煤自燃特征参数测定过程是间断的，采样和分析分开进行，操作繁琐，且 容易发生漏气，导致实验精准度降低，而该煤自燃特征参数测定实验平台能够连续完成该煤自燃特征参数测定，有效克服了上述缺陷。
于本实施例中，煤自燃特征参数测定实验平台还包括气体流向分散管3，气体流向分散管3的第一端设置于智能控温反应箱5内部，气体流向分散管3的第一端封闭，气体流向分散管3的第一端为球形结构，且气体流向分散管3的第一端设置有多个与气体流向分散管3内部相连通的分散孔，气体流向分散管3的第二端与配气仪2的出气口相连通。
于本实施例中，为了保证进气气流多方向进入，煤自燃特征参数测定实验平台还包括气体变流装置4，气体变流装置4包括套筒和顶板，套筒的周侧壁上设置有多个气孔，顶板设置于套筒的顶端、以封堵套筒的顶端，套筒的底端与智能控温反应箱5的底端相抵，气体流向分散管3的第一端设置于套筒内。气体变流装置4与气体流向分散管3协同作用，防止进气气流影响智能控温反应箱5内气体稳定状态。
于本实施例中，套筒采用纱网制成。套筒指的是内部中空，且两端开口的结构。
于本实施例中，智能控温反应箱5的一侧设置有箱门18。本实施例中，智能温控反应箱具体选用控温箱。
于本实施例中，为了方便观察智能温控反应箱内部情况，箱门18上设置有耐高温透明玻璃窗17。
于本实施例中，悬篮8为铝悬篮，且悬篮8做氧化处理，如此，保证了热传导性能与煤相近，从而减小悬篮8材质对实验造成误差影响。悬篮8整体结构与篮子结构实质相同，其上具有众多孔隙，孔隙保证环境气体能够均有快速地进入悬篮8内部。悬篮8的容积根据不同实验中煤样质量的需求而定。
于本实施例中，供气装置1为气瓶。需要说明的是供气装置1并不仅限于采用气瓶，能够承装气体的结构均可。
于本实施例中，环境温度感应装置10为环境温度感应热电偶，煤样温度感应装置9为煤样温度感应热电偶。环境温度感应热电偶的检测端置于智能温控反应箱内、以感应环境温度，煤样温度感应热电偶的检测端置于悬篮8内、以感应煤样温度。
于本实施例中，具体地，红外热像仪7为分体式红外热像仪，同时红外热像探头6为耐高温红外热像探头，以避免红外热像探头6在高温环境下损坏。
于本实施例中，悬挂式称重装置12为电子天平。需要说明的是悬挂式称重装置12并不仅限于采用电子天平，能够实现悬挂称重的装置均可。
本实施例提供的煤自燃特征参数测定实验平台具体使用过程中：布设该煤自燃特征参数测定实验平台，向智能控温反应箱5内充入环境气体；环境气体根据实验需求由供气仪和配气仪2进行配比；向悬篮8中放入煤样；连接完整各项实验装置，保证实验导管、器材的气密性良好；开启智能控温反应箱5，设定程序升温或恒温，升温可分阶段进行升温且可设置升温所需时间；开启耐高温红外热像探头、煤样温度感应热电偶、环境温度感应热电偶，并同时打开数据采集装置和计算机16。实验开始，根据实验需求定时记录相关参数变化。通过分体式红外热像仪采集煤样在反应过程中的温度状态图像。通过煤样温度感应热电偶测定实验过程中煤样温度，并反馈给数据采集设备15。通过环境温度感应热电偶测定实验过程中环境温度，并反馈给数据采集设备15。通过煤自燃标志气体采集管路13同时采集升温过程中产生的实验尾气，并将尾气传输给所述全自动在线分析气相色谱仪14，测定尾气种类以及含量，并结合尾气出现的时间及煤样、环境温度，对煤自燃的特征参数进行实时监控。
本实施例中，可对不同气体环境下煤自燃特征参数进行测评，结合金属网篮交叉点法，通过煤样及环境热电偶测定相关温度，通过红外热像仪7采集煤样升温过程中煤样温度变化图像，对煤自燃过程中煤的质量、气体产物、煤样内部各标志点升温速率等特征参数进行动态捕捉，从而为矿井火灾预测预报提供理论支持和技术支撑，有效的控制和预防煤自燃的发生。
本说明书中应用了具体个例对本发明的原理及实施方式进行了阐述，以上实施例的说明只是用于帮助理解本发明的方法及其核心思想；同时，对于本领域的一般技术人员，依据本发明的思想，在具体实施方式及应用范围上均会有改变之处。综上所述，本说明书内容不应理解为对本发明的限制。

Claims (10)

  1. 一种煤自燃特征参数测定实验平台，其特征在于，包括：
    智能控温反应箱；
    供气组件，所述供气组件包括多个用于盛装气体的供气装置；
    配气仪，各所述供气装置均与所述配气仪的进气口相连通，所述配气仪的出气口与所述智能控温反应箱内部相连通；
    用于检测煤样质量的悬挂式称重装置，所述悬挂式称重装置设置于所述智能控温反应箱的顶端；
    悬篮，所述悬篮通过连接绳与所述悬挂式称重装置相连，所述煤样置于所述悬篮内；
    气相色谱仪，所述气相色谱仪的进气口与所述智能控温反应箱内部连通；
    红外热像系统，所述红外热像系统包括红外热像仪和红外热像探头，所述红外热像仪与所述红外热像探头通信连接，所述红外热像探头设置于所述智能控温反应箱内；
    温度感应组件，所述温度感应组件设置于所述智能控温反应箱内部，所述温度感应组件包括用于感应所述温度箱内部温度的环境温度感应装置和用于感应所述煤样温度的煤样温度感应装置；
    计算机，所述悬挂式称重装置、所述气相色谱仪、所述红外热像仪、所述环境温度感应装置以及所述煤样温度感应装置均与所述计算机通信连接。
  2. 根据权利要求1所述的煤自燃特征参数测定实验平台，其特征在于，还包括气体流向分散管，所述气体流向分散管的第一端设置于所述智能控温反应箱内部，所述气体流向分散管的第一端为球形结构，且所述气体流向分散管的第一端设置有多个与所述气体流向分散管内部相连通的分散孔，所述气体流向分散管的第二端与所述配气仪的出气口相连通。
  3. 根据权利要求2所述的煤自燃特征参数测定实验平台，其特征在于，还包括气体变流装置，所述气体变流装置包括套筒和顶板，所述套筒的周侧壁上设置有多个气孔，所述顶板设置于所述套筒的顶端、以封堵所述套筒的顶端，所述套筒的底端与所述智能控温反应箱的底端相抵，所述气体 流向分散管的第一端设置于所述套筒内。
  4. 根据权利要求3所述的煤自燃特征参数测定实验平台，其特征在于，所述套筒采用纱网制成。
  5. 根据权利要求1所述的煤自燃特征参数测定实验平台，其特征在于，所述智能控温反应箱的一侧设置有箱门，所述箱门上设置有耐高温透明玻璃窗。
  6. 根据权利要求1所述的煤自燃特征参数测定实验平台，其特征在于，所述悬篮为铝悬篮，且所述悬篮做氧化处理。
  7. 根据权利要求1所述的煤自燃特征参数测定实验平台，其特征在于，所述供气装置为气瓶。
  8. 根据权利要求1所述的煤自燃特征参数测定实验平台，其特征在于，所述环境温度感应装置为环境温度感应热电偶，所述煤样温度感应装置为煤样温度感应热电偶。
  9. 根据权利要求1所述的煤自燃特征参数测定实验平台，其特征在于，所述红外热像仪为分体式红外热像仪，所述红外热像探头为耐高温红外热像探头。
  10. 根据权利要求1所述的煤自燃特征参数测定实验平台，其特征在于，所述悬挂式称重装置为电子天平。
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CN112684100B (zh) * 2021-01-04 2021-10-29 大连理工大学 一种模拟井下密闭空间煤自燃过程的实验装置及使用方法
CN113049633A (zh) * 2021-03-05 2021-06-29 浙江省应急管理科学研究院 一种金属粉尘遇水自燃测试装置及方法
CN113092333B (zh) * 2021-03-10 2023-04-07 苏州工业园区蒙纳士科学技术研究院 一种对胶质层透气性进行实时测量的煤焦化过程实验方法
CN113252840B (zh) * 2021-05-19 2022-05-13 重庆大学 一种模拟煤自燃及灭火过程的测试装置
CN113720378A (zh) * 2021-07-29 2021-11-30 华北科技学院(中国煤矿安全技术培训中心) 一种采空区煤自燃灾害智能在线监测与联动处置装置
CN113654477B (zh) * 2021-08-16 2023-02-21 中国矿业大学 一种煤体变形测试装置、测试系统及测试方法
CN113960243B (zh) * 2021-11-02 2023-07-07 宁波工程学院 一种快速确定煤绝热自然发火期的对照实验系统与方法
CN115032325A (zh) * 2022-04-12 2022-09-09 北京理工大学 一种用于研究镁粉自燃的装置及方法
CN116608003B (zh) * 2023-05-25 2023-11-24 中国矿业大学 一种矿井煤与瓦斯共采复合灾害模拟试验系统及方法

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104483350A (zh) * 2014-11-21 2015-04-01 中国矿业大学(北京) 模拟煤升温及绝热氧化的装置
CN105807029A (zh) * 2016-05-20 2016-07-27 河南理工大学 基于热重的煤自燃特性测定装置
CN106124357A (zh) * 2016-07-05 2016-11-16 山东科技大学 一种自动取样的多功能煤样升温氧化规律测试平台
KR20180033882A (ko) * 2016-09-26 2018-04-04 한국전력공사 석탄의 자연발화 측정장치
CN207924864U (zh) * 2018-03-29 2018-09-28 中国神华能源股份有限公司 煤场自燃监测系统
JP2019066296A (ja) * 2017-09-29 2019-04-25 中国電力株式会社 石炭自然発熱性の評価装置及び評価方法
CN208818642U (zh) * 2018-09-07 2019-05-03 西安科技大学 一种测试煤自然发火全过程的实验系统
CN111311870A (zh) * 2020-02-25 2020-06-19 中国矿业大学(北京) 煤堆自燃监测方法及防控系统

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201700043U (zh) * 2009-12-02 2011-01-05 广州擎天实业有限公司 一种应急灯控制终端
CN205643334U (zh) * 2016-05-20 2016-10-12 河南理工大学 一种基于热重的煤自燃特性测定装置
CN108519403A (zh) * 2018-03-28 2018-09-11 辽宁工程技术大学 一种基于动态氧环境的油浴式煤程序升温实验装置
CN108896611A (zh) * 2018-08-23 2018-11-27 中原工学院 煤自燃倾向性的测定装置及测定方法
CN109632879B (zh) * 2018-11-16 2020-08-18 西安交通大学 一种用于型煤燃烧的可视化宏观热重分析仪
CN210534042U (zh) * 2019-07-24 2020-05-15 汇乐因斯福环保安全研究院（苏州）有限公司 一种测定堆积粉尘自燃特性的装置

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104483350A (zh) * 2014-11-21 2015-04-01 中国矿业大学(北京) 模拟煤升温及绝热氧化的装置
CN105807029A (zh) * 2016-05-20 2016-07-27 河南理工大学 基于热重的煤自燃特性测定装置
CN106124357A (zh) * 2016-07-05 2016-11-16 山东科技大学 一种自动取样的多功能煤样升温氧化规律测试平台
KR20180033882A (ko) * 2016-09-26 2018-04-04 한국전력공사 석탄의 자연발화 측정장치
JP2019066296A (ja) * 2017-09-29 2019-04-25 中国電力株式会社 石炭自然発熱性の評価装置及び評価方法
CN207924864U (zh) * 2018-03-29 2018-09-28 中国神华能源股份有限公司 煤场自燃监测系统
CN208818642U (zh) * 2018-09-07 2019-05-03 西安科技大学 一种测试煤自然发火全过程的实验系统
CN111311870A (zh) * 2020-02-25 2020-06-19 中国矿业大学(北京) 煤堆自燃监测方法及防控系统

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