WO2021238043A1 - 一种测量液体混合滴加产生电信号的实验装置 - Google Patents
一种测量液体混合滴加产生电信号的实验装置 Download PDFInfo
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- WO2021238043A1 WO2021238043A1 PCT/CN2020/123791 CN2020123791W WO2021238043A1 WO 2021238043 A1 WO2021238043 A1 WO 2021238043A1 CN 2020123791 W CN2020123791 W CN 2020123791W WO 2021238043 A1 WO2021238043 A1 WO 2021238043A1
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- 239000007788 liquid Substances 0.000 title claims abstract description 101
- 238000002474 experimental method Methods 0.000 title claims abstract description 26
- 239000007787 solid Substances 0.000 claims abstract description 71
- 238000010248 power generation Methods 0.000 claims abstract description 12
- 238000006073 displacement reaction Methods 0.000 claims description 18
- 230000002572 peristaltic effect Effects 0.000 claims description 17
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 14
- 238000010438 heat treatment Methods 0.000 claims description 12
- 229910052742 iron Inorganic materials 0.000 claims description 7
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims description 6
- 239000003292 glue Substances 0.000 claims description 6
- 229910052709 silver Inorganic materials 0.000 claims description 6
- 239000004332 silver Substances 0.000 claims description 6
- 239000000758 substrate Substances 0.000 claims description 6
- 239000011521 glass Substances 0.000 claims description 5
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 4
- 239000000741 silica gel Substances 0.000 claims description 4
- 229910002027 silica gel Inorganic materials 0.000 claims description 4
- 238000002791 soaking Methods 0.000 claims description 3
- 239000002699 waste material Substances 0.000 claims description 3
- 230000032258 transport Effects 0.000 claims 1
- 238000011160 research Methods 0.000 abstract description 4
- 238000010586 diagram Methods 0.000 description 7
- 239000000463 material Substances 0.000 description 3
- -1 polytetrafluoroethylene Polymers 0.000 description 3
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 3
- 239000004810 polytetrafluoroethylene Substances 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 238000013519 translation Methods 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
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- 239000002356 single layer Substances 0.000 description 2
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Classifications
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01R—MEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
- G01R29/00—Arrangements for measuring or indicating electric quantities not covered by groups G01R19/00 - G01R27/00
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01R—MEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
- G01R29/00—Arrangements for measuring or indicating electric quantities not covered by groups G01R19/00 - G01R27/00
- G01R29/24—Arrangements for measuring quantities of charge
Definitions
- the invention relates to an experimental device for measuring electrical signals generated by liquid mixing and dripping, and belongs to the field of solid-liquid friction power generation research.
- Triboelectricity is ubiquitous in nature, such as combing hair, walking, dressing, etc. As long as two objects are in contact with each other, there will be an exchange of charges.
- triboelectricity such as self-driven sensing and collection of various forms of mechanical energy through solid-solid interface friction, wave energy collection and raindrop power generation through solid-liquid interface friction, etc. .
- Regarding the field of solid-liquid friction power generation especially the research on friction power generation between droplets and solids, there are still many issues to be explored. When the solution is in contact with the solid friction pair, it can generate instantaneous electrical signals.
- the present invention proposes an experimental device for measuring electrical signals generated by liquid mixing and dripping.
- the present invention mainly adopts the following technical solutions:
- An experimental device for measuring electrical signals generated by liquid mixing and dripping including:
- the box is used to place the various parts that make up the experimental device.
- the multi-channel liquid dripping unit is used to drip different solutions on the solid electrode plate.
- the experimental temperature control module is used to change the temperature conditions of the experiment.
- the triboelectric generating unit is used to generate electrical signals by rubbing against the different dripping solutions.
- the clamping device is used to fix and support solid electrode plates of different thicknesses and sizes, and can achieve a certain angle of inclination between the solid electrode plates and the horizontal plane.
- the liquid tank can be raised and lowered for collecting waste liquid or soaking solid electrode plates.
- the signal acquisition and display unit is used for real-time acquisition and display of electrical signals generated by solid-liquid friction.
- the above-mentioned box body includes a shell and a door; the inner bottom surface of the box body has two guide rails on the left and right sides; the door is a glass door with a certain curvature.
- the above-mentioned multi-channel liquid dripping unit includes a multi-channel peristaltic pump, a container for liquid, a hose, and a liquid collection device; the hose is installed on the peristaltic pump, one end is connected to the liquid collection device, and the other end is placed
- the liquid container; the peristaltic pump and the liquid container are outside the box and placed on a horizontal surface; the liquid container is a beaker, and the number and specifications of the beaker are determined according to the type and volume of the solution required in the experiment
- the liquid collection device is a hollow shell structure, the upper part of the liquid collection device is cylindrical, and there are several small holes on the side of the cylinder.
- the diameter of the small holes is slightly larger than the diameter of the hose for connecting the hose; the liquid The lower part of the collecting device is conical with small holes on the top of the cone. The solution drips onto the solid electrode plate through the small holes and generates frictional charge with the solid electrode plate; the liquid collecting device is installed on an iron stand; the iron The iron rod of the stand is engraved with a height line, and the liquid collecting device can move up and down along the iron rod, and the height of the liquid collecting device can be adjusted according to the needs of the experiment.
- the above-mentioned experimental temperature control module includes a heater, a temperature controller, a temperature sensor, and a wire;
- the temperature controller has a digital display screen and a setting button, which can set the target temperature and display the actual temperature measured by the temperature sensor in real time , Placed outside of the box, installed on the top of the box, respectively connected with the heating plate and temperature sensor through wires, used to control the working state of the heating plate and transmit temperature signals;
- the temperature sensor is installed on the iron frame, the height and solid The height of the electrode plate is the same, and the temperature around the solid electrode plate is measured;
- the heating plate is a silicon rubber heating plate, and there are five pieces in total, which are attached to the top, bottom, left, right and back of the box. Three-dimensional heating is performed inside the experiment box.
- the above-mentioned friction power generation unit includes a solid electrode plate, conductive silver glue, silica gel, and wires; both ends of the solid electrode plate use conductive silver glue and wires to achieve ohmic connection; the silica gel is coated on the surface of the conductive silver glue to prevent electrical circuits Short circuit; the solid electrode plate includes a substrate and a friction pair; the substrate is polytetrafluoroethylene; the friction pair is a single-layer graphene attached to a polytetrafluoroethylene material.
- the above-mentioned clamping device includes an angular displacement stage bracket, an angular displacement stage, an upper splint, a lower splint, a spring, a tie rod, and a cantilever;
- the angular displacement stage bracket is installed on a guide rail at the bottom of the box and can move left and right along the guide rail;
- the angular displacement stage is installed on the angular displacement stage bracket, fixed by screws, and can move left and right under the drive of the angular displacement stage bracket;
- the cantilever is installed on the side of the angular displacement stage and connected by screws;
- the cantilever is installed
- the lower splint and the upper splint, the upper splint and the pull rod are fixed together, and the pull rod is sleeved with a spring to make the upper and lower splints in a closed state;
- the angular displacement table can rotate within a certain angle range, thereby driving the cantilever to tilt to a certain
- the above-mentioned liftable liquid tank includes a lifting platform and a liquid tank; the lifting platform is installed in the middle of the left and right guide rails at the bottom of the box; the liquid tank is freely placed on the lifting platform, and the liquid tank is controlled by adjusting the lifting platform.
- Height The liquid tank has different specifications, and a liquid tank with a size slightly larger than the size of the solid electrode plate is generally selected in the experiment.
- the above-mentioned signal acquisition unit is an oscilloscope or a precision multimeter or other electrical measuring equipment; the positive and negative leads of the oscilloscope or other electrical measuring equipment are respectively connected with the leads at both ends of the solid electrode plate to form a conductive path.
- An experimental method for measuring electrical signals generated by liquid mixing and dripping includes the following steps:
- Adjust the height of the lifting platform If the experiment is in a liquid environment, the lifting platform rises until the solid electrode plate can be immersed in the liquid tank; if the experiment is an atmospheric environment, adjust the liquid tank not to contact the solid electrode plate;
- the invention can test the triboelectric signal between the liquid drop and the solid electrode, and at the same time combines the temperature control module and the multi-channel peristaltic pump, so as to realize that under different temperature conditions, when solid electrodes of different sizes and thicknesses are in an atmospheric environment or a liquid environment,
- the study of triboelectric signals generated by different solutions dropping and hitting the electrode plates has important value and significance for the study of micro-tribology.
- Fig. 1 is an overall appearance view of the present invention.
- Figure 2 is a schematic diagram of the overall internal structure of the box.
- Figure 3 is a schematic diagram of the overall structure from another perspective.
- Fig. 4 is a schematic diagram of the structure of the angular displacement stage and the angular displacement stage bracket.
- Fig. 5 is a schematic diagram of the structure of the clamping device.
- Figure 6 is a schematic diagram of the structure of a friction power generation unit.
- Figure 7 is a schematic diagram of the structure of a liquid tank that can be raised and lowered.
- Fig. 8 is a schematic diagram of the structure of a multi-channel liquid dropping unit.
- the system includes:
- the box is used to place the components that make up the experimental device.
- the multi-channel liquid dripping unit is used to drip different solutions on the solid electrode plate.
- the experimental temperature control module is used to change the temperature conditions of the experiment.
- the triboelectric generating unit is used to generate electrical signals by rubbing against the different dripping solutions.
- the clamping device is used to fix and support solid electrode plates of different thicknesses and sizes, and can achieve a certain angle of inclination between the solid electrode plates and the horizontal plane.
- the liquid tank can be raised and lowered for collecting waste liquid or soaking solid electrode plates.
- the signal acquisition and display unit is used for real-time acquisition and display of electrical signals generated by solid-liquid friction.
- an arc-shaped glass door 3-15 and an arc-shaped glass door 3-17 are installed on both sides of the box body 3, respectively, which can be rotated around its rotation axis. 90°, open to the outside of the box; there are four guide rails 3-1 on the bottom surface of the box 3, two on the left and right sides, every two guide rails are a group, and each group of guide rails is equipped with an angle displacement stage bracket 3- 3. It can be slid left and right along the guide rail.
- An angle translation stage 3-4 is installed on the angle translation stage bracket 3-3, which is connected together by screws; the side wall of the angle translation stage 3-4 is connected with a clamp 3-5, which is connected by screws Together; move the brackets 3-3 of the left and right angle stages so that the distance between the left and right clamps 3-5 can hold the solid electrode plate 3-10; adjust the rotation angle of the left and right angle stages 3-4 to 0°,
- the clamped solid electrode plates 3-10 are placed horizontally.
- the left and right angular platform can be adjusted to rotate from 0° to 60°, so that the solid electrode plates 3-10 are inclined at a certain angle.
- the upper splint 3-5-3 of the clamp 3-5 can slide up and down along the chute 3-5-4, and the opening size can be adjusted as needed to adapt to different Thickness of the electrode plate; the clamp 3-5 clamps the solid electrode plate 3-10 under the tension of the compressed spring 3-5-2; the size of the solid electrode plate 3-10 is 10cm ⁇ 10cm, and the thickness is 2mm
- the substrate of the solid electrode plate 3-10 is polytetrafluoroethylene, and the friction pair attached to the substrate is a single-layer graphene.
- solid electrode plates of different sizes and materials can be selected.
- the inner rear wall of the box 3 is attached with an additional heat sheet 3-9
- the inner left wall is attached with an additional heat sheet 3-2
- the inner right wall is attached with an additional heat sheet 3-11.
- the inner and lower walls are attached with additional heat sheets 3-14
- the inner and upper walls are attached with additional heat sheets 3-16.
- the heating sheets used are all silicon rubber heating sheets with a size of 10cm ⁇ 10cm.
- a temperature sensor 3-8 is installed on the internal iron stand 3-7 of the box 3, the height of which is the same as the height of the solid electrode plate; a temperature controller 4 and a temperature controller 4 are installed on the outside of the top of the box 3 It is connected with the heating plate and the temperature sensor through a wire; in this embodiment, the target temperature is set to 26°C, the actual ambient temperature measured by the temperature sensor 3-8 is 20°C, and the temperature controller controls 4 to turn on the heating plate circuit , Heat the box 3.
- the liquid tank 3-12 is placed on the lifting platform 3-13, and the liquid tank is adjusted by the lifting platform 3-13
- the height of 3-12 makes the solid electrode plate 3-10 directly above the liquid tank 3-12.
- the height of the lifting platform 3-13 can be increased so that the solid electrode plate 3-10 is immersed in the liquid tank 3.
- the size of the liquid tank 3-12 used is 12cm ⁇ 12cm.
- a liquid tank whose size is slightly larger than the size of the solid electrode plate can be selected as required.
- the multi-channel liquid dripping unit includes a multi-channel peristaltic pump 6, a container 7, a hose 5, and a liquid collection device 3-6; the hose 5 is installed in On the peristaltic pump 6, one end is connected to the liquid collection device 3-6, and the other end is placed in the container 7 containing the liquid. Under the action of the peristaltic pump 6, the solution flows to the liquid collection device 3-6 through the hose 5, and is collected by the liquid.
- the outlet of the lower end of the device 3-6 flows out and drips to the solid electrode plate 3-10; the peristaltic pump 6 and the liquid container 7 are placed on the right outside the box 3 on a horizontal surface; in this embodiment, the liquid container 7 is Two small beakers, different solutions are placed in the two small beakers, the peristaltic pump 6 uses two channels, sets the dripping rate of the peristaltic pump, and draws the solution in the two beakers to the solid electrode plate 3-10 dropwise.
- the signal acquisition and display unit is an oscilloscope 1, which is placed on the left outside of the cabinet 3;
- the oscilloscope 1 displays an instantaneous electrical signal, and records the electrical signals generated by different solutions dropping onto the solid electrode plate 3-10.
- solid electrode plates of different sizes can be clamped by the clamps, and the solid electrode plates can be tilted at a certain angle.
- the temperature control module, the multi-channel liquid dropping unit, the signal acquisition and display unit, and the The lifting tank realizes the measurement of the triboelectric signal generated by the liquid droplet and the solid electrode plate under different experimental conditions.
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Abstract
Description
Claims (10)
- 一种测量液体混合滴加产生电信号的实验装置,包括:箱体,用于放置组成实验装置的各部件;多通道液体滴加单元,用于将不同的溶液滴加在固体电极板上;实验温度控制模块,用于改变实验的温度条件;摩擦发电单元,用于与所述滴落的不同溶液发生摩擦并产生电信号;夹持装置,用于固定和支撑不同规格的固体电极板,并实现固体电极板与水平面之间呈一定角度的倾斜;可升降液槽,用于收集废液或浸泡固体电极板;信号采集显示单元,用于实时采集并显示固液摩擦所产生的电信号;多通道液体滴加单元放置在箱体外部,运输液体至箱体内部摩擦发电单元的正上方;实验温度控制模块分布在箱体的各内表面;夹持装置安装在箱体内底部的导轨上,夹持摩擦发电单元;摩擦发电单元的正下方箱底底面上固定连接可升降液槽;信号采集显示单元放置在箱体外部,通过导线与摩擦发电单元连接。
- 根据权利要求1所述的系统,其特征在于,所述箱体包括壳体和门;所述箱体内部底面左右两边各有两根导轨;所述门为具有一定弧度的玻璃门,扇叶安装在箱体的侧面,所述玻璃门关闭时能够将箱体封闭。
- 根据权利要求1所述的系统,其特征在于:所述多通道液体滴加单元包括多通道蠕动泵、盛装液体的容器、软管、和液体汇集装置;所述软管安装在蠕动泵上,一端与液体汇集装置相连,另一端置于盛装液体的容器内,溶液在蠕动泵的作用下,通过软管流向液体汇集装置,经液体汇集装置下端出口流出,滴向固体电极板;所述蠕动泵和盛装液体的容器在箱体外,放置在水平面上。
- 根据权利要求1所述的系统,其特征在于:所述实验温度控制模块包括加热片、温度控制器、温度传感器和导线;所述温度控制器通过导线分别与加热片和温度传感器相连,用于控制加热片的工作状态和传输温度信号。
- 根据权利要求1所述的系统,其特征在于:所述摩擦发电单元包括固体电极板、导电银胶、硅胶和导线;所述固体电极板两端使用导电银胶与导线实现欧姆连接;所述硅胶涂覆在导电银胶表面;所述固体电极板包括基材和摩擦副,摩擦副附着在基材上。
- 根据权利要求1所述的系统,其特征在于:所述夹持装置包括角位移台支架、角位移台、上夹板、下夹板、弹簧、拉杆和悬臂;所述角位移台支架安装在箱体底部的导轨上;所述角位移台安装在角位移台支架上,由螺钉固定;所述悬臂装在角位移台侧面;所述悬臂上安装有下夹板和上夹板,所述上夹板与所述拉杆固接在一起,拉杆上套有弹簧;所述角位移 台能够在一定角度范围内旋转,从而带动悬臂倾斜一定角度;所述夹持装置有两个,对称安装在箱体的导轨上,两个夹持装置共同夹住固体电极板的两边;所述夹持装置通过拉杆调节上下夹板张口的大小,夹持不同厚度的固体电极板。
- 根据权利要求1所述的系统,其特征在于:所述可升降液槽包括升降台和液槽;所述升降台安装在箱体底端左右导轨的中间;所述液槽自由放置在升降台上,通过调节升降台来控制液槽的高度;所述液槽有不同规格,实验时选择尺寸大于固体电极板尺寸的液槽。
- 根据权利要求1所述的系统,其特征在于:所述信号采集单元为示波器或精密万用表或其他测电设备;所述示波器的正负极导线分别与固体电极板两端的导线相连,形成一个导通的通路。
- 根据权利要求3所述的系统,其中,所述液体汇集装置为中空的壳体结构,液体汇集装置上半部分为圆柱形,圆柱侧面有若干个小孔,小孔的直径大于软管直径,用于连接软管;所述液体汇集装置的下半部分为圆锥形,圆锥形的顶部开有小孔,溶液经小孔滴到固体电极板上,与固体电极板产生摩擦电荷;所述液体汇集装置安装于铁架台上。
- 一种测量液体混合滴加产生电信号的实验方法,包括权利要求1至16任一所述系统,包括以下步骤:S1根据固体电极板实验所需的倾斜角度,将左右角位移台的旋转角度调成一致;S2调节左右夹持装置的间距,使间距能够适应固体电极板的宽度,并将固体电极板夹持住;S3将固体电极板两端的导线与示波器相连;S4调节升降台高度,若实验为液体环境,升降台上升至固体电极板能正好浸没在液槽内;若实验为大气环境,调节液槽不与固体电极板接触;S5向烧杯中放入实验所需的溶液;S6调节液体汇集装置的高度;S7设定多通道蠕动泵的流速;S8关闭箱门,打开温度控制器,设定实验所需温度;S9当温度传感器测得的温度达到实验所需温度时,打开示波器;S10启动多通道蠕动泵,使液滴以一定的流速撞击固体电极板,产生摩擦电信号;S11通过示波器实时观测电信号并记录电信号。
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US4869722A (en) * | 1988-01-20 | 1989-09-26 | Measurement Resources Inc. | Flow monitor of liquid drops |
CN108627707A (zh) * | 2018-08-16 | 2018-10-09 | 大连海事大学 | 一种液滴表面zeta电势检测装置及方法 |
CN110208614A (zh) * | 2019-05-22 | 2019-09-06 | 西安交通大学 | 一种基于固液混合液滴的摩擦发电测试系统及方法 |
CN110687146A (zh) * | 2019-10-14 | 2020-01-14 | 北京工业大学 | 一种电致变色薄膜的x衍射原位测试装置 |
CN111537804A (zh) * | 2020-05-23 | 2020-08-14 | 北京工业大学 | 一种测量液体混合滴加产生电信号的实验装置 |
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