WO2021057099A1 - Plantago ovata and konjak chips and preparation method therefor - Google Patents
Plantago ovata and konjak chips and preparation method therefor Download PDFInfo
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- WO2021057099A1 WO2021057099A1 PCT/CN2020/095608 CN2020095608W WO2021057099A1 WO 2021057099 A1 WO2021057099 A1 WO 2021057099A1 CN 2020095608 W CN2020095608 W CN 2020095608W WO 2021057099 A1 WO2021057099 A1 WO 2021057099A1
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- Prior art keywords
- powder
- parts
- konjac
- mesh sieve
- flakes
- Prior art date
Links
- 229920002752 Konjac Polymers 0.000 title claims abstract description 69
- 235000010485 konjac Nutrition 0.000 title claims abstract description 69
- 244000134552 Plantago ovata Species 0.000 title claims abstract description 33
- 235000003421 Plantago ovata Nutrition 0.000 title claims abstract description 33
- 238000002360 preparation method Methods 0.000 title description 8
- 239000000843 powder Substances 0.000 claims abstract description 191
- 244000247812 Amorphophallus rivieri Species 0.000 claims abstract description 65
- 235000001206 Amorphophallus rivieri Nutrition 0.000 claims abstract description 65
- 239000000252 konjac Substances 0.000 claims abstract description 65
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims abstract description 50
- XOAAWQZATWQOTB-UHFFFAOYSA-N taurine Chemical compound NCCS(O)(=O)=O XOAAWQZATWQOTB-UHFFFAOYSA-N 0.000 claims abstract description 50
- HQKMJHAJHXVSDF-UHFFFAOYSA-L magnesium stearate Chemical compound [Mg+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O HQKMJHAJHXVSDF-UHFFFAOYSA-L 0.000 claims abstract description 44
- 235000009917 Crataegus X brevipes Nutrition 0.000 claims abstract description 33
- 235000013204 Crataegus X haemacarpa Nutrition 0.000 claims abstract description 33
- 235000009685 Crataegus X maligna Nutrition 0.000 claims abstract description 33
- 235000009444 Crataegus X rubrocarnea Nutrition 0.000 claims abstract description 33
- 235000009486 Crataegus bullatus Nutrition 0.000 claims abstract description 33
- 235000017181 Crataegus chrysocarpa Nutrition 0.000 claims abstract description 33
- 235000009682 Crataegus limnophila Nutrition 0.000 claims abstract description 33
- 235000004423 Crataegus monogyna Nutrition 0.000 claims abstract description 33
- 235000002313 Crataegus paludosa Nutrition 0.000 claims abstract description 33
- 235000009840 Crataegus x incaedua Nutrition 0.000 claims abstract description 33
- 244000068988 Glycine max Species 0.000 claims abstract description 31
- 235000010469 Glycine max Nutrition 0.000 claims abstract description 31
- 235000013312 flour Nutrition 0.000 claims abstract description 30
- 239000005913 Maltodextrin Substances 0.000 claims abstract description 28
- 229920002774 Maltodextrin Polymers 0.000 claims abstract description 28
- 239000010903 husk Substances 0.000 claims abstract description 28
- 229940035034 maltodextrin Drugs 0.000 claims abstract description 28
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 claims abstract description 25
- 229920000168 Microcrystalline cellulose Polymers 0.000 claims abstract description 25
- 229930003268 Vitamin C Natural products 0.000 claims abstract description 25
- 239000004222 ferrous gluconate Substances 0.000 claims abstract description 25
- 229960001645 ferrous gluconate Drugs 0.000 claims abstract description 25
- 235000013924 ferrous gluconate Nutrition 0.000 claims abstract description 25
- VRIVJOXICYMTAG-IYEMJOQQSA-L iron(ii) gluconate Chemical compound [Fe+2].OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O.OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O VRIVJOXICYMTAG-IYEMJOQQSA-L 0.000 claims abstract description 25
- 239000008108 microcrystalline cellulose Substances 0.000 claims abstract description 25
- 235000019813 microcrystalline cellulose Nutrition 0.000 claims abstract description 25
- 229940016286 microcrystalline cellulose Drugs 0.000 claims abstract description 25
- 229960003080 taurine Drugs 0.000 claims abstract description 25
- 239000011718 vitamin C Substances 0.000 claims abstract description 25
- 235000019154 vitamin C Nutrition 0.000 claims abstract description 25
- 235000019359 magnesium stearate Nutrition 0.000 claims abstract description 22
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims abstract description 18
- FBPFZTCFMRRESA-KVTDHHQDSA-N D-Mannitol Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-KVTDHHQDSA-N 0.000 claims abstract description 12
- 229930195725 Mannitol Natural products 0.000 claims abstract description 12
- 239000000594 mannitol Substances 0.000 claims abstract description 12
- 235000010355 mannitol Nutrition 0.000 claims abstract description 12
- 239000002994 raw material Substances 0.000 claims abstract description 10
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 58
- 241001092040 Crataegus Species 0.000 claims description 31
- 239000008187 granular material Substances 0.000 claims description 29
- 239000009223 Psyllium Substances 0.000 claims description 28
- 229940070687 psyllium Drugs 0.000 claims description 28
- 239000011812 mixed powder Substances 0.000 claims description 25
- 238000002156 mixing Methods 0.000 claims description 17
- 239000007779 soft material Substances 0.000 claims description 17
- 238000001035 drying Methods 0.000 claims description 13
- 238000000034 method Methods 0.000 claims description 12
- 239000007788 liquid Substances 0.000 claims description 10
- 239000002245 particle Substances 0.000 claims description 10
- 238000003756 stirring Methods 0.000 claims description 10
- 229940057948 magnesium stearate Drugs 0.000 claims description 5
- 238000003801 milling Methods 0.000 claims description 5
- 230000008569 process Effects 0.000 claims description 5
- 239000007921 spray Substances 0.000 claims description 5
- 238000005507 spraying Methods 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 4
- 230000000694 effects Effects 0.000 abstract description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 9
- 210000000577 adipose tissue Anatomy 0.000 abstract description 7
- 238000000354 decomposition reaction Methods 0.000 abstract description 5
- 239000004615 ingredient Substances 0.000 abstract description 4
- 210000002784 stomach Anatomy 0.000 abstract description 2
- 240000000171 Crataegus monogyna Species 0.000 abstract 2
- 102000004190 Enzymes Human genes 0.000 abstract 1
- 108090000790 Enzymes Proteins 0.000 abstract 1
- 230000037406 food intake Effects 0.000 abstract 1
- 230000002366 lipolytic effect Effects 0.000 abstract 1
- 239000013585 weight reducing agent Substances 0.000 abstract 1
- 230000000052 comparative effect Effects 0.000 description 8
- 235000013305 food Nutrition 0.000 description 7
- 230000004580 weight loss Effects 0.000 description 7
- 239000004367 Lipase Substances 0.000 description 4
- 102000004882 Lipase Human genes 0.000 description 4
- 108090001060 Lipase Proteins 0.000 description 4
- 235000019421 lipase Nutrition 0.000 description 4
- 241001127637 Plantago Species 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 235000013325 dietary fiber Nutrition 0.000 description 2
- 235000001916 dieting Nutrition 0.000 description 2
- 230000037228 dieting effect Effects 0.000 description 2
- 230000029087 digestion Effects 0.000 description 2
- 238000007908 dry granulation Methods 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- 235000003642 hunger Nutrition 0.000 description 2
- 239000006187 pill Substances 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 206010067484 Adverse reaction Diseases 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- 208000002720 Malnutrition Diseases 0.000 description 1
- 235000003805 Musa ABB Group Nutrition 0.000 description 1
- 206010067482 No adverse event Diseases 0.000 description 1
- 208000008589 Obesity Diseases 0.000 description 1
- 235000015266 Plantago major Nutrition 0.000 description 1
- 230000006838 adverse reaction Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 235000005911 diet Nutrition 0.000 description 1
- 230000037213 diet Effects 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 230000037080 exercise endurance Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 210000000936 intestine Anatomy 0.000 description 1
- 230000001071 malnutrition Effects 0.000 description 1
- 235000000824 malnutrition Nutrition 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 235000012054 meals Nutrition 0.000 description 1
- 230000004630 mental health Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 231100000989 no adverse effect Toxicity 0.000 description 1
- 235000021590 normal diet Nutrition 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 208000015380 nutritional deficiency disease Diseases 0.000 description 1
- 235000020824 obesity Nutrition 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 235000019614 sour taste Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 235000019605 sweet taste sensations Nutrition 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L11/00—Pulses, i.e. fruits of leguminous plants, for production of food; Products from legumes; Preparation or treatment thereof
- A23L11/05—Mashed or comminuted pulses or legumes; Products made therefrom
- A23L11/07—Soya beans, e.g. oil-extracted soya bean flakes
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L19/00—Products from fruits or vegetables; Preparation or treatment thereof
- A23L19/09—Mashed or comminuted products, e.g. pulp, purée, sauce, or products made therefrom, e.g. snacks
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L19/00—Products from fruits or vegetables; Preparation or treatment thereof
- A23L19/10—Products from fruits or vegetables; Preparation or treatment thereof of tuberous or like starch containing root crops
- A23L19/115—Konjak; Konntaku
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/15—Vitamins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/16—Inorganic salts, minerals or trace elements
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/17—Amino acids, peptides or proteins
- A23L33/175—Amino acids
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
- A23P10/20—Agglomerating; Granulating; Tabletting
- A23P10/28—Tabletting; Making food bars by compression of a dry powdered mixture
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Definitions
- the invention relates to the field of food processing. More specifically, the present invention relates to the composition of a round bud konjac flakes and a preparation method thereof.
- An object of the present invention is to solve at least the above-mentioned problems and provide at least the advantages described later.
- Another object of the present invention is to provide a round bud konjac flakes, which through the principle of swelling of konjac flour and psyllium husk powder in contact with water, the round bud konjac flakes are dispersed in the stomach and make people feel full and reduce The intake of other foods, and then achieve the goal of weight loss.
- a round bud konjac slice which includes the following raw materials in parts by weight:
- the said round bud konjac slices comprise the following raw materials in parts by weight:
- the said round bud konjac flakes further comprise the following raw materials by weight:
- maltodextrin powder 0.7-1.3 parts of maltodextrin powder, 0.2-0.5 parts of soybean powder, 0.5-0.9 parts of hawthorn powder.
- the present invention also provides a preparation method of round bud konjac flakes, which comprises the following steps:
- the vitamin C powder is pulverized, ground, and sieved through 60-70 mesh to obtain the vitamin C powder for use;
- Step two mixing powder: take the proportion of konjac powder, soybean powder, hawthorn powder, psyllium husk powder, vitamin C powder, ferrous gluconate powder, taurine powder, microcrystalline cellulose powder and 1 /2 ratio of maltodextrin powder is stirred and mixed evenly to obtain the mixed powder for use;
- Step 3 Making soft materials: Take an ethanol solution with a weight of 28-38% of the total weight of the mixed powder described in step 2, and add a proportion of mannitol to the ethanol solution, then heat and stir until it is dissolved and mixed. Liquid, and then spray the mixed liquid into the mixed powder in step two, while spraying, tumbling, stirring and mixing uniformly to obtain a soft material;
- the volume ratio of ethanol in the ethanol solution is 50-70%; mannitol is dissolved in hot ethanol, and the ethanol solution is heated to promote the complete dissolution of mannitol in ethanol;
- Step 4 Dry granules: The soft material obtained in step 3 is continuously tumbling and mixed to form stable spherical granules, and then wet granules are obtained through a 15-25 mesh sieve, and the wet granules are put into drying Drying in the box for 30-50min, the drying temperature is 50-55°C, and then pass through 60-70 mesh sieve and 15-25 mesh sieve to screen out ungranulated fine powder and qualified dry particles;
- Step 5 Tableting: Mix the dry granules prepared in Step 4 with the proportioned amount of magnesium stearate powder and 1/2 proportion of maltodextrin powder, and then press the tablet machine to obtain a round shape. Konjac flakes
- the specifications of the round bud konjac slices are 0.2-0.3 g/tablet.
- the preparation of the round bud konjac flakes in the present invention is completed in a 100,000-grade clean area.
- the konjac flour, the soybean flour and the round bud plantago husk powder are obtained by passing through a 60-mesh sieve;
- the hawthorn powder needs to be obtained through a 90-mesh sieve.
- the vitamin C powder, the ferrous gluconate powder and the taurine powder are obtained by passing through a 60-mesh sieve;
- microcrystalline cellulose powder, the maltodextrin powder and the magnesium stearate powder need to be obtained through an 80-mesh sieve.
- the soft material in the step 4 needs to pass through a 20-mesh sieve to make wet granules, and the wet granules need to pass through a 20-mesh sieve after drying to obtain dry granules.
- the volume ratio of ethanol in the ethanol solution is 60%, and the added amount of the ethanol solution is 33% of the weight of the mixed powder.
- konjac flour and Psyllium rotundifolia shell powder swell with water and increase in volume, which can enhance a person's sense of fullness, thereby controlling the intake of other foods, and achieving the effect of weight loss;
- the water-soluble konjac flour is in a colloidal state, which can delay the absorption of glucose and fat.
- the lipase in hawthorn can promote the decomposition of fat;
- konjac flour and plantain husk flour are rich in dietary fiber. Foods rich in dietary fiber take less time to empty from the intestines, which can greatly reduce the absorption of harmful substances;
- the present invention has a sweet and sour taste and rich nutrition.
- the simultaneous addition of soybean powder and hawthorn powder to the ingredients not only reduces the speed of food digestion, but also makes people less likely to feel hungry, and the effective ingredients in soybeans can strengthen the effect of lipase in hawthorn. Promote the decomposition of body fat more quickly, and achieve the effect of faster fat loss.
- the round bud konjac flakes of the present invention dissolve quickly in water and disperse within 1 min.
- microcrystalline cellulose, maltodextrin, and magnesium stearate to obtain microcrystalline cellulose powder, maltodextrin powder, and magnesium stearate powder for later use;
- Step two mixing powder: take the proportion of konjac powder, soybean powder, hawthorn powder, psyllium husk powder, vitamin C powder, ferrous gluconate powder, taurine powder, microcrystalline cellulose powder and 1 /2 ratio of maltodextrin powder is stirred and mixed evenly to obtain the mixed powder for use;
- the original powders in the mixed powder are in a proportion by weight: 0.3 parts of konjac powder, 0.03 parts of vitamin C powder, 0.005 parts of ferrous gluconate powder, 0.005 parts of taurine powder, and Psyllium sylvestris 3.5 parts of powder, 1.2 parts of microcrystalline cellulose powder, 0.7 parts of maltodextrin powder, 0.2 parts of soybean powder, 0.5 parts of hawthorn powder;
- Step three making soft materials: take 28% ethanol solution of the total weight of the mixed powder in step two, add 2.3 parts by weight of mannitol to the ethanol solution, then heat and stir until it is dissolved and mixed Liquid, and then spray the mixed liquid into the mixed powder in step two, while spraying, tumbling, stirring and mixing uniformly to obtain a soft material;
- the volume ratio of ethanol in the ethanol solution is 50%;
- Step 4 Dry granulation: The soft material prepared in step 3 is continuously tumbling and mixed until stable spherical granules are formed, and then wet granules are obtained through a 15-mesh sieve, and the wet granules are put into the drying box Dry for 30 minutes at a drying temperature of 50°C, and then pass through a 65-mesh sieve and 15-mesh sieve to screen out ungranulated fine powder and qualified dry particles;
- Step 5 Tableting: After mixing the dry granules obtained in Step 4 with 0.04 parts by weight of magnesium stearate powder and the remaining 1/2 proportion of maltodextrin powder, they are pressed by a tableting machine. The slices are round bud konjac slices;
- round bud konjac flakes The specification of the round bud konjac flakes is 0.2g/piece, and it dissolves quickly in water and disperses within 1 min.
- microcrystalline cellulose, maltodextrin, and magnesium stearate to obtain microcrystalline cellulose powder, maltodextrin powder, and magnesium stearate powder for later use;
- Step two mixing powder: take the proportion of konjac powder, soybean powder, hawthorn powder, psyllium husk powder, vitamin C powder, ferrous gluconate powder, taurine powder, microcrystalline cellulose powder and 1 /2 ratio of maltodextrin powder is stirred and mixed evenly to obtain the mixed powder for use;
- the original powder in the mixed powder is in a proportion by weight: 0.4 part of konjac powder, 0.038 part of vitamin C powder, 0.007 part of ferrous gluconate powder, 0.01 part of taurine powder, and psyllium husk. 3 parts of powder, 2 parts of microcrystalline cellulose powder, 1 part of maltodextrin powder, 0.4 part of soybean powder, 0.8 part of hawthorn powder;
- Step 3 Making soft material: Take 33% ethanol solution of the total weight of the mixed powder described in step 2, add 2.465 parts by weight of mannitol to the ethanol solution, then heat and stir until it is dissolved and mixed Liquid, and then spray the mixed liquid into the mixed powder in step two, while spraying, tumbling, stirring and mixing uniformly to obtain a soft material;
- volume ratio of ethanol in the ethanol solution is 60%;
- Step 4 Dry granulation: The soft material obtained in step 3 is continuously tumbling and mixed until stable spherical granules are formed, and then wet granules are obtained through a 20-mesh sieve, and the wet granules are put into the drying box Dry for 40 minutes at a drying temperature of 53°C, and then pass through a 60-mesh sieve and 20-mesh sieve to screen out ungranulated fine powder and qualified dry particles;
- Step 5 Tableting: Mix the dry granules prepared in Step 4 with 0.08 parts by weight of magnesium stearate powder and the remaining 1/2 proportion of maltodextrin powder, and then press the tablet machine.
- the slices are round bud konjac slices;
- round bud konjac flakes 0.25 g/tablet, and it dissolves quickly in water and disperses within 1 min.
- microcrystalline cellulose, maltodextrin, and magnesium stearate to obtain microcrystalline cellulose powder, maltodextrin powder, and magnesium stearate powder for later use;
- Step two mixing powder: take the proportion of konjac powder, soybean powder, hawthorn powder, psyllium husk powder, vitamin C powder, ferrous gluconate powder, taurine powder, microcrystalline cellulose powder and 1 /2 ratio of maltodextrin powder is stirred and mixed evenly to obtain the mixed powder for use;
- the original powder in the mixed powder is in a proportion by weight: 0.5 parts of konjac powder, 0.046 parts of vitamin C powder, 0.01 parts of ferrous gluconate powder, 0.015 parts of taurine powder, and psyllium husks 2.5 parts of powder, 2.8 parts of microcrystalline cellulose powder, 1.3 parts of maltodextrin powder, 0.5 parts of soybean powder, 0.9 parts of hawthorn powder;
- Step three making soft materials: take 38% ethanol solution of the total weight of the mixed powder in step two, add 2.7 parts by weight of mannitol to the ethanol solution, and heat and stir until it is dissolved and mixed Liquid, and then spray the mixed liquid into the mixed powder in step two, while spraying, tumbling, stirring and mixing uniformly to obtain a soft material;
- the volume ratio of ethanol in the ethanol solution is 70%
- Step 4 Dry granules: The soft material obtained in step 3 is continuously tumbling and mixed to form stable spherical granules, then wet granules are obtained through a 25-mesh sieve, and the wet granules are put into the drying box Dry for 50 minutes at a drying temperature of 55°C, and then pass through a 70-mesh sieve and a 25-mesh sieve to screen out ungranulated fine powder and qualified dry particles;
- Step 5 Tableting: After mixing the dry granules obtained in Step 4 with 0.12 parts by weight of magnesium stearate powder and the remaining 1/2 proportion of maltodextrin powder, they are pressed by a tableting machine. The slices are round bud konjac slices;
- round bud konjac flakes dissolves quickly in water, and disperses within 1 min.
- Example 2 Same as Example 2, the difference is that no soybean powder is added to the raw material.
- the use method of the round bud konjac tablet of the present invention is oral, taken before meals, and taken with warm water, 4-8g per day, 60 days is a course of treatment; the present invention can achieve good results with one course of treatment without side effects and reduced Fat fast, no rebound.
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- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Nutrition Science (AREA)
- Health & Medical Sciences (AREA)
- Mycology (AREA)
- Inorganic Chemistry (AREA)
- Agronomy & Crop Science (AREA)
- Botany (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- Medicines Containing Plant Substances (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
Disclosed are Plantago ovata and konjak chips, which are prepared from the following raw materials in parts by weight: 0.3-0.5 parts of konjac flour, 0.03-0.046 parts of vitamin C powder, 0.005-0.01 parts of ferrous gluconate powder, 0.005-0.015 parts of taurine powder, 2.5-3.5 parts of Plantago ovata seed husk powder, 1.2-2.8 parts of microcrystalline cellulose powder, 2.3-2.7 parts of mannitol, 0.04-0.12 parts of magnesium stearate powder, 0.7-1.3 parts of maltodextrin powder, 0.2-0.5 parts of soybean powder, and 0.5-0.9 parts of hawthorn powder. Formulated by taking advantage of the principle that konjak powder and Plantago ovata seed husk powder swell upon contact with water, the Plantago ovata and konjak chips can satiate a user upon entry into the stomach and reduce ingestion of other foodstuffs by the user, thus achieving a weight reduction effect. Moreover, effective ingredients in soybean can enhance the effect of a lipolytic enzyme in the hawthorn and facilitate rapid decomposition of body fat, thus achieving a faster fat reduction effect.
Description
本发明涉及食品加工领域。更具体地说,本发明涉及一种圆苞魔芋片的组成及其制备方法。The invention relates to the field of food processing. More specifically, the present invention relates to the composition of a round bud konjac flakes and a preparation method thereof.
随着人们生活水平不断提高,肥胖人群的比例不断增加,肥胖不仅影响形体美观,还会带来多种疾病,严重影响人们的身心健康。减肥方式有节食减肥、运动减肥、减肥药减肥,对于意志力不强的人靠运动减肥容易半途而废,节食减肥容易导致营养不良,吃减肥药减肥副作用大。With the continuous improvement of people's living standards, the proportion of obese people continues to increase. Obesity not only affects the physical appearance, but also brings a variety of diseases, which seriously affects people's physical and mental health. Ways to lose weight include dieting, exercise, and diet pills. For people with weak willpower, it is easy to lose weight by exercising to lose weight. Dieting to lose weight can easily lead to malnutrition, and eating weight loss pills has a large side effect.
发明内容Summary of the invention
本发明的一个目的是解决至少上述问题,并提供至少后面将说明的优点。An object of the present invention is to solve at least the above-mentioned problems and provide at least the advantages described later.
本发明还有一个目的是提供一种圆苞魔芋片,其通过魔芋粉和圆苞车前子壳粉遇水膨胀原理,使圆苞魔芋片进入胃里分散后使人有饱腹感而减少其他食物的摄入量,进而达到减肥的目的。Another object of the present invention is to provide a round bud konjac flakes, which through the principle of swelling of konjac flour and psyllium husk powder in contact with water, the round bud konjac flakes are dispersed in the stomach and make people feel full and reduce The intake of other foods, and then achieve the goal of weight loss.
为了实现根据本发明的这些目的和其它优点,提供了一种圆苞魔芋片,包括以下重量份的原料:In order to achieve these objectives and other advantages according to the present invention, a round bud konjac slice is provided, which includes the following raw materials in parts by weight:
魔芋粉0.3~0.5份、维生素C粉0.03~0.046份、葡萄糖酸亚铁粉0.005~0.01份、牛磺酸粉0.005~0.015份、圆苞车前子壳粉2.5~3.5份、微晶纤维素粉1.2~2.8份、甘露糖醇2.3~2.7份、硬脂酸镁粉0.04~0.12份。Konjac flour 0.3~0.5 parts, vitamin C powder 0.03~0.046 parts, ferrous gluconate powder 0.005~0.01 parts, taurine powder 0.005~0.015 parts, psyllium husk powder 2.5~3.5 parts, microcrystalline cellulose 1.2 to 2.8 parts of powder, 2.3 to 2.7 parts of mannitol, 0.04 to 0.12 parts of magnesium stearate powder.
优选的是,所述的圆苞魔芋片中,包括以下重量份的原料:Preferably, the said round bud konjac slices comprise the following raw materials in parts by weight:
魔芋粉0.4份、维生素C粉0.038份、葡萄糖酸亚铁粉0.007份、牛磺酸粉0.01份、圆苞车前子壳粉3份、微晶纤维素粉2份、甘露糖醇2.465份、硬脂酸镁粉0.08份。0.4 parts of konjac flour, 0.038 parts of vitamin C powder, 0.007 parts of ferrous gluconate powder, 0.01 parts of taurine powder, 3 parts of psyllium husk powder, 2 parts of microcrystalline cellulose powder, 2.465 parts of mannitol, 0.08 parts of magnesium stearate powder.
优选的是,所述的圆苞魔芋片中,还包括以下重量份的原料:Preferably, the said round bud konjac flakes further comprise the following raw materials by weight:
麦芽糊精粉0.7~1.3份、大豆粉0.2~0.5份、山楂粉0.5~0.9份。0.7-1.3 parts of maltodextrin powder, 0.2-0.5 parts of soybean powder, 0.5-0.9 parts of hawthorn powder.
本发明还提供了一种圆苞魔芋片的制备方法,其包括以下步骤:The present invention also provides a preparation method of round bud konjac flakes, which comprises the following steps:
步骤一、制粉:Step 1. Flour milling:
将魔芋和大豆洗净、蒸煮3~5小时,然后经干燥、粉碎、磨粉、过60~80目筛得所述魔芋粉和所述大豆粉待用;Wash the konjac and soybeans, steam for 3 to 5 hours, then dry, crush, grind, and sieve through 60-80 mesh to obtain the konjac flour and the soybean flour for later use;
将圆苞车前子壳洗净、干燥、粉碎、磨粉、过60~80目筛得所述圆苞车前子壳粉待用;Wash, dry, pulverize, grind, and sieve the psyllium husks of Psyllium rotundifolia to obtain the husk powder of Psyllium rotundus for use;
将山楂洗净经干燥灭菌、粉碎、磨粉、过80~100目筛得所述山楂粉待用;Wash the hawthorn, dry, sterilize, pulverize, pulverize, and sieve through 80-100 mesh to obtain the hawthorn powder for use;
将维生素C经粉碎、磨粉、过60~70目筛得所述维生素C粉待用;The vitamin C powder is pulverized, ground, and sieved through 60-70 mesh to obtain the vitamin C powder for use;
将葡萄糖酸亚铁和牛磺酸经磨粉、过60~70目筛得所述葡萄糖酸亚铁粉、所述牛磺酸粉待用;Grind the ferrous gluconate and taurine through a 60-70 mesh sieve to obtain the ferrous gluconate powder and the taurine powder for use;
将微晶纤维素、麦芽糊精、硬脂酸镁经磨粉、过80~100目筛得所述微晶纤维素粉、所述麦芽糊精粉、所述硬脂酸镁粉待用;Grind microcrystalline cellulose, maltodextrin, and magnesium stearate to obtain the microcrystalline cellulose powder, the maltodextrin powder, and the magnesium stearate powder through a 80-100 mesh sieve;
步骤二、混粉:取配比量的魔芋粉、大豆粉、山楂粉、圆苞车前子壳粉、维生素C粉、葡萄糖酸亚铁粉、牛磺酸粉、微晶纤维素粉和1/2配比量的麦芽糊精粉搅拌混合均匀得混合粉体待用;Step two, mixing powder: take the proportion of konjac powder, soybean powder, hawthorn powder, psyllium husk powder, vitamin C powder, ferrous gluconate powder, taurine powder, microcrystalline cellulose powder and 1 /2 ratio of maltodextrin powder is stirred and mixed evenly to obtain the mixed powder for use;
步骤三、制软材:取重量为步骤二中所述混合粉体总重量的28~38%的乙醇溶液,在所述乙醇溶液中加入配比量的甘露糖醇后加热搅拌至溶解得混合液体,然后将所述混合液体喷洒至步骤二中的所述混合粉体中,边喷洒边翻滚搅拌混合均匀制得软材;Step 3. Making soft materials: Take an ethanol solution with a weight of 28-38% of the total weight of the mixed powder described in step 2, and add a proportion of mannitol to the ethanol solution, then heat and stir until it is dissolved and mixed. Liquid, and then spray the mixed liquid into the mixed powder in step two, while spraying, tumbling, stirring and mixing uniformly to obtain a soft material;
其中所述乙醇溶液中乙醇的体积占比为50~70%;甘露糖醇溶于热乙醇,加热乙醇溶液,促进甘露糖醇在乙醇中完全溶解;Wherein, the volume ratio of ethanol in the ethanol solution is 50-70%; mannitol is dissolved in hot ethanol, and the ethanol solution is heated to promote the complete dissolution of mannitol in ethanol;
步骤四、制干粒:将步骤三中制得的所述软材继续经过不断翻滚混合至形成稳定球状颗粒,然后过15~25目筛制得湿粒,将所述湿粒放入烘干箱内进行干燥30~50min,干燥温度为50~55℃,然后依次经过60~70目筛、15~25目筛筛选出未成粒的细粉和合格的干粒;Step 4. Dry granules: The soft material obtained in step 3 is continuously tumbling and mixed to form stable spherical granules, and then wet granules are obtained through a 15-25 mesh sieve, and the wet granules are put into drying Drying in the box for 30-50min, the drying temperature is 50-55℃, and then pass through 60-70 mesh sieve and 15-25 mesh sieve to screen out ungranulated fine powder and qualified dry particles;
将所述细粉回收利用,与所述混合粉体混合后重复制备干粒过程;Recycle the fine powder and repeat the process of preparing dry particles after mixing with the mixed powder;
步骤五、制片:将步骤四中制得的干粒与配比量的硬脂酸镁粉和1/2配比量的麦芽糊精粉混合均匀后,经压片机压片即得圆苞魔芋片;Step 5. Tableting: Mix the dry granules prepared in Step 4 with the proportioned amount of magnesium stearate powder and 1/2 proportion of maltodextrin powder, and then press the tablet machine to obtain a round shape. Konjac flakes
其中所述圆苞魔芋片的规格为0.2~0.3g/片。The specifications of the round bud konjac slices are 0.2-0.3 g/tablet.
本发明中圆苞魔芋片的制备是在十万级洁净区内完成。The preparation of the round bud konjac flakes in the present invention is completed in a 100,000-grade clean area.
优选的是,所述的圆苞魔芋片的制备方法中,所述魔芋粉、所述大豆粉和所述圆苞车 前子壳粉需过60目筛制得;Preferably, in the preparation method of the round bud konjac flakes, the konjac flour, the soybean flour and the round bud plantago husk powder are obtained by passing through a 60-mesh sieve;
所述山楂粉需过90目筛制得。The hawthorn powder needs to be obtained through a 90-mesh sieve.
优选的是,所述的圆苞魔芋片的制备方法中,所述维生素C粉、所述葡萄糖酸亚铁粉和所述牛磺酸粉需过60目筛制得;Preferably, in the preparation method of the round bud konjac flakes, the vitamin C powder, the ferrous gluconate powder and the taurine powder are obtained by passing through a 60-mesh sieve;
所述微晶纤维素粉、所述麦芽糊精粉和所述硬脂酸镁粉需过80目筛制得。The microcrystalline cellulose powder, the maltodextrin powder and the magnesium stearate powder need to be obtained through an 80-mesh sieve.
优选的是,所述的圆苞魔芋片的制备方法中,所述步骤四中软材需经过20目筛制湿粒,所述湿粒经干燥后需再经过20目筛得干粒。Preferably, in the preparation method of the round bud konjac flakes, the soft material in the step 4 needs to pass through a 20-mesh sieve to make wet granules, and the wet granules need to pass through a 20-mesh sieve after drying to obtain dry granules.
优选的是,所述的圆苞魔芋片的制备方法中,所述乙醇溶液中乙醇的体积占比为60%,所述乙醇溶液加入量为所述混合粉体重量的33%。Preferably, in the preparation method of the round bud konjac flakes, the volume ratio of ethanol in the ethanol solution is 60%, and the added amount of the ethanol solution is 33% of the weight of the mixed powder.
本发明至少包括以下有益效果:The present invention includes at least the following beneficial effects:
第一、魔芋粉和圆苞车前子壳粉遇水膨胀,体积增加,可增强的人的饱腹感,进而控制其他食物的摄取,达到减肥效果;First, konjac flour and Psyllium rotundifolia shell powder swell with water and increase in volume, which can enhance a person's sense of fullness, thereby controlling the intake of other foods, and achieving the effect of weight loss;
第二、魔芋粉溶水呈胶态可延缓葡萄糖和脂肪的吸收,同时山楂中的解脂酶可促进脂肪分解;Second, the water-soluble konjac flour is in a colloidal state, which can delay the absorption of glucose and fat. At the same time, the lipase in hawthorn can promote the decomposition of fat;
第三、魔芋粉和圆苞车前子壳粉内富含有的食物纤维,富含食物纤维的食品需更少的时间从肠道中排空,可在大大减少有害物质的吸收;Third, konjac flour and plantain husk flour are rich in dietary fiber. Foods rich in dietary fiber take less time to empty from the intestines, which can greatly reduce the absorption of harmful substances;
第四、本发明口味酸甜、营养丰富,成分中同时添加大豆粉和山楂粉不仅降低食物消化速度,使人不易产生饥饿感,且大豆中有效成分可加强山楂中解脂酶的作用,可促进体内脂肪更快速分解,达到更快减脂的效果。Fourth, the present invention has a sweet and sour taste and rich nutrition. The simultaneous addition of soybean powder and hawthorn powder to the ingredients not only reduces the speed of food digestion, but also makes people less likely to feel hungry, and the effective ingredients in soybeans can strengthen the effect of lipase in hawthorn. Promote the decomposition of body fat more quickly, and achieve the effect of faster fat loss.
第五、本发明的圆苞魔芋片遇水速溶,1min之内散开。Fifth, the round bud konjac flakes of the present invention dissolve quickly in water and disperse within 1 min.
本发明的其它优点、目标和特征将部分通过下面的说明体现,部分还将通过对本发明的研究和实践而为本领域的技术人员所理解。Other advantages, objectives and features of the present invention will be partially embodied by the following description, and partly will be understood by those skilled in the art through the research and practice of the present invention.
下面结合具体实施例对本发明做进一步的详细说明,以令本领域技术人员参照说明书文字能够据以实施。The present invention will be further described in detail below in conjunction with specific embodiments, so that those skilled in the art can implement it with reference to the text of the description.
应当理解,本文所使用的诸如“具有”、“包含”以及“包括”术语并不排除一个或多个其它元件或其组合的存在或添加。It should be understood that terms such as "having", "including" and "including" used herein do not exclude the presence or addition of one or more other elements or combinations thereof.
需要说明的是,下述实施方案中所述实验方法,如无特殊说明,均为常规方法,所述试剂和材料,如无特殊说明,均可从商业途径获得;对于本领域的普通技术人员而言,可以具体情况理解上述术语在本发明中的具体含义。It should be noted that the experimental methods described in the following embodiments are conventional methods unless otherwise specified, and the reagents and materials, unless otherwise specified, can be obtained from commercial sources; for those of ordinary skill in the art In other words, the specific meaning of the above-mentioned terms in the present invention can be understood under specific circumstances.
实施例1Example 1
步骤一、制粉:Step 1. Flour milling:
将魔芋和大豆洗净、蒸煮3小时,然后经干燥、粉碎、磨粉、过70目筛得魔芋粉和大豆粉待用;Wash konjac and soybeans, steam for 3 hours, then dry, crush, grind, and sieve through 70 mesh to obtain konjac flour and soybean flour for later use;
将圆苞车前子壳洗净、干燥、粉碎、磨粉、过70目筛得圆苞车前子壳粉待用;Wash, dry, smash, grind, and sieve the husk of Psyllium rotundifolia to obtain husk powder of Psyllium rotundus for later use;
将山楂洗净经干燥灭菌、粉碎、磨粉、过80目筛得山楂粉待用;Wash the hawthorn, dry, sterilize, pulverize, pulverize, and sieve through 80 mesh to obtain hawthorn powder for later use;
将维生素C经粉碎、磨粉、过65目筛得维生素C粉待用;Crush vitamin C, pulverize, and sieve through 65 mesh to obtain vitamin C powder for use;
将葡萄糖酸亚铁和牛磺酸经磨粉、过65目筛得葡萄糖酸亚铁粉、牛磺酸粉待用;Grind ferrous gluconate and taurine through a 65-mesh sieve to obtain ferrous gluconate powder and taurine powder for later use;
将微晶纤维素、麦芽糊精、硬脂酸镁经磨粉、过90目筛得微晶纤维素粉、麦芽糊精粉、硬脂酸镁粉待用;Grind microcrystalline cellulose, maltodextrin, and magnesium stearate to obtain microcrystalline cellulose powder, maltodextrin powder, and magnesium stearate powder for later use;
步骤二、混粉:取配比量的魔芋粉、大豆粉、山楂粉、圆苞车前子壳粉、维生素C粉、葡萄糖酸亚铁粉、牛磺酸粉、微晶纤维素粉和1/2配比量的麦芽糊精粉搅拌混合均匀得混合粉体待用;Step two, mixing powder: take the proportion of konjac powder, soybean powder, hawthorn powder, psyllium husk powder, vitamin C powder, ferrous gluconate powder, taurine powder, microcrystalline cellulose powder and 1 /2 ratio of maltodextrin powder is stirred and mixed evenly to obtain the mixed powder for use;
其中,所述混合粉体中各原来粉按重量配比量为:魔芋粉0.3份、维生素C粉0.03份、葡萄糖酸亚铁粉0.005份、牛磺酸粉0.005份、圆苞车前子壳粉3.5份、微晶纤维素粉1.2份、麦芽糊精粉0.7份、大豆粉0.2份、山楂粉0.5份;Wherein, the original powders in the mixed powder are in a proportion by weight: 0.3 parts of konjac powder, 0.03 parts of vitamin C powder, 0.005 parts of ferrous gluconate powder, 0.005 parts of taurine powder, and Psyllium sylvestris 3.5 parts of powder, 1.2 parts of microcrystalline cellulose powder, 0.7 parts of maltodextrin powder, 0.2 parts of soybean powder, 0.5 parts of hawthorn powder;
步骤三、制软材:取重量为步骤二中所述混合粉体总重量的28%的乙醇溶液,在所述乙醇溶液中加入重量份为2.3份的甘露糖醇后加热搅拌至溶解得混合液体,然后将所述混合液体喷洒至步骤二中的所述混合粉体中,边喷洒边翻滚搅拌混合均匀制得软材;Step three, making soft materials: take 28% ethanol solution of the total weight of the mixed powder in step two, add 2.3 parts by weight of mannitol to the ethanol solution, then heat and stir until it is dissolved and mixed Liquid, and then spray the mixed liquid into the mixed powder in step two, while spraying, tumbling, stirring and mixing uniformly to obtain a soft material;
其中所述乙醇溶液中乙醇的体积占比为50%;Wherein, the volume ratio of ethanol in the ethanol solution is 50%;
步骤四、制干粒:将步骤三中制得的所述软材继续经过不断翻滚混合至形成稳定球状颗粒,然后过15目筛制得湿粒,将所述湿粒放入烘干箱内进行干燥30min,干燥温度为50℃,然后依次经过65目筛、15目筛筛选出未成粒的细粉和合格的干粒;Step 4. Dry granulation: The soft material prepared in step 3 is continuously tumbling and mixed until stable spherical granules are formed, and then wet granules are obtained through a 15-mesh sieve, and the wet granules are put into the drying box Dry for 30 minutes at a drying temperature of 50°C, and then pass through a 65-mesh sieve and 15-mesh sieve to screen out ungranulated fine powder and qualified dry particles;
将所述细粉回收利用,与所述混合粉体混合后重复制备干粒过程;Recycle the fine powder and repeat the process of preparing dry particles after mixing with the mixed powder;
步骤五、制片:将步骤四中制得的干粒与重量份为0.04份的硬脂酸镁粉和剩余的1/2配比量的麦芽糊精粉混合均匀后,经压片机压片即得圆苞魔芋片;Step 5. Tableting: After mixing the dry granules obtained in Step 4 with 0.04 parts by weight of magnesium stearate powder and the remaining 1/2 proportion of maltodextrin powder, they are pressed by a tableting machine. The slices are round bud konjac slices;
其中所述圆苞魔芋片的规格为0.2g/片,且遇水速溶,1min之内散开。The specification of the round bud konjac flakes is 0.2g/piece, and it dissolves quickly in water and disperses within 1 min.
实施例2Example 2
步骤一、制粉:Step 1. Flour milling:
将魔芋和大豆洗净、蒸煮4小时,然后经干燥、粉碎、磨粉、过60目筛得魔芋粉和大豆粉待用;Wash and steam the konjac and soybeans for 4 hours, then dry, crush, grind, and sieve through 60 mesh to obtain konjac flour and soybean flour for later use;
将圆苞车前子壳洗净、干燥、粉碎、磨粉、过60目筛得圆苞车前子壳粉待用;Wash, dry, smash, grind, and sieve the husks of Psyllium rotundifolia to obtain husks of Psyllium rotundifolia for use;
将山楂洗净经干燥灭菌、粉碎、磨粉、过90目筛得山楂粉待用;Wash the hawthorn, dry, sterilize, pulverize, pulverize, and pass through a 90-mesh sieve to obtain hawthorn powder for later use;
将维生素C经粉碎、磨粉、过60目筛得维生素C粉待用;Crush the vitamin C, pulverize, and sieve through 60 mesh to obtain vitamin C powder for use;
将葡萄糖酸亚铁和牛磺酸经磨粉、过60目筛得葡萄糖酸亚铁粉、牛磺酸粉待用;Grind ferrous gluconate and taurine through a 60-mesh sieve to obtain ferrous gluconate powder and taurine powder for later use;
将微晶纤维素、麦芽糊精、硬脂酸镁经磨粉、过80目筛得微晶纤维素粉、麦芽糊精粉、硬脂酸镁粉待用;Grind microcrystalline cellulose, maltodextrin, and magnesium stearate to obtain microcrystalline cellulose powder, maltodextrin powder, and magnesium stearate powder for later use;
步骤二、混粉:取配比量的魔芋粉、大豆粉、山楂粉、圆苞车前子壳粉、维生素C粉、葡萄糖酸亚铁粉、牛磺酸粉、微晶纤维素粉和1/2配比量的麦芽糊精粉搅拌混合均匀得混合粉体待用;Step two, mixing powder: take the proportion of konjac powder, soybean powder, hawthorn powder, psyllium husk powder, vitamin C powder, ferrous gluconate powder, taurine powder, microcrystalline cellulose powder and 1 /2 ratio of maltodextrin powder is stirred and mixed evenly to obtain the mixed powder for use;
其中,所述混合粉体中各原来粉按重量配比量为:魔芋粉0.4份、维生素C粉0.038份、葡萄糖酸亚铁粉0.007份、牛磺酸粉0.01份、圆苞车前子壳粉3份、微晶纤维素粉2份、麦芽糊精粉1份、大豆粉0.4份、山楂粉0.8份;Wherein, the original powder in the mixed powder is in a proportion by weight: 0.4 part of konjac powder, 0.038 part of vitamin C powder, 0.007 part of ferrous gluconate powder, 0.01 part of taurine powder, and psyllium husk. 3 parts of powder, 2 parts of microcrystalline cellulose powder, 1 part of maltodextrin powder, 0.4 part of soybean powder, 0.8 part of hawthorn powder;
步骤三、制软材:取重量为步骤二中所述混合粉体总重量的33%的乙醇溶液,在所述乙醇溶液中加入重量份为2.465份的甘露糖醇后加热搅拌至溶解得混合液体,然后将所述混合液体喷洒至步骤二中的所述混合粉体中,边喷洒边翻滚搅拌混合均匀制得软材;Step 3. Making soft material: Take 33% ethanol solution of the total weight of the mixed powder described in step 2, add 2.465 parts by weight of mannitol to the ethanol solution, then heat and stir until it is dissolved and mixed Liquid, and then spray the mixed liquid into the mixed powder in step two, while spraying, tumbling, stirring and mixing uniformly to obtain a soft material;
其中所述乙醇溶液中乙醇的体积占比为60%;Wherein the volume ratio of ethanol in the ethanol solution is 60%;
步骤四、制干粒:将步骤三中制得的所述软材继续经过不断翻滚混合至形成稳定球状颗粒,然后过20目筛制得湿粒,将所述湿粒放入烘干箱内进行干燥40min,干燥温度为53℃,然后依次经过60目筛、20目筛筛选出未成粒的细粉和合格的干粒;Step 4. Dry granulation: The soft material obtained in step 3 is continuously tumbling and mixed until stable spherical granules are formed, and then wet granules are obtained through a 20-mesh sieve, and the wet granules are put into the drying box Dry for 40 minutes at a drying temperature of 53°C, and then pass through a 60-mesh sieve and 20-mesh sieve to screen out ungranulated fine powder and qualified dry particles;
将所述细粉回收利用,与所述混合粉体混合后重复制备干粒过程;Recycle the fine powder and repeat the process of preparing dry particles after mixing with the mixed powder;
步骤五、制片:将步骤四中制得的干粒与重量份为0.08份的硬脂酸镁粉和剩余的1/2配比量的麦芽糊精粉混合均匀后,经压片机压片即得圆苞魔芋片;Step 5. Tableting: Mix the dry granules prepared in Step 4 with 0.08 parts by weight of magnesium stearate powder and the remaining 1/2 proportion of maltodextrin powder, and then press the tablet machine. The slices are round bud konjac slices;
其中所述圆苞魔芋片的规格为0.25g/片,且遇水速溶,1min之内散开。The specification of the round bud konjac flakes is 0.25 g/tablet, and it dissolves quickly in water and disperses within 1 min.
实施例3Example 3
步骤一、制粉:Step 1. Flour milling:
将魔芋和大豆洗净、蒸煮5小时,然后经干燥、粉碎、磨粉、过80目筛得魔芋粉和大豆粉待用;Wash and steam the konjac and soybeans for 5 hours, then dry, smash, grind, and pass through an 80-mesh sieve to obtain konjac flour and soybean flour for later use;
将圆苞车前子壳洗净、干燥、粉碎、磨粉、过80目筛得圆苞车前子壳粉待用;Wash, dry, smash, grind, and sieve the husk of Psyllium rotundifolia to obtain husk powder of Psyllium rotundifolia for later use;
将山楂洗净经干燥灭菌、粉碎、磨粉、过100目筛得山楂粉待用;Wash the hawthorn, dry, sterilize, pulverize, pulverize, and sieve through a 100-mesh sieve to obtain hawthorn powder for use;
将维生素C经粉碎、磨粉、过70目筛得维生素C粉待用;Crush the vitamin C, pulverize, and sieve through 70 mesh to obtain vitamin C powder for later use;
将葡萄糖酸亚铁和牛磺酸经磨粉、过70目筛得葡萄糖酸亚铁粉、牛磺酸粉待用;Grind ferrous gluconate and taurine through a 70-mesh sieve to obtain ferrous gluconate powder and taurine powder for later use;
将微晶纤维素、麦芽糊精、硬脂酸镁经磨粉、过100目筛得微晶纤维素粉、麦芽糊精粉、硬脂酸镁粉待用;Grind microcrystalline cellulose, maltodextrin, and magnesium stearate to obtain microcrystalline cellulose powder, maltodextrin powder, and magnesium stearate powder for later use;
步骤二、混粉:取配比量的魔芋粉、大豆粉、山楂粉、圆苞车前子壳粉、维生素C粉、葡萄糖酸亚铁粉、牛磺酸粉、微晶纤维素粉和1/2配比量的麦芽糊精粉搅拌混合均匀得混合粉体待用;Step two, mixing powder: take the proportion of konjac powder, soybean powder, hawthorn powder, psyllium husk powder, vitamin C powder, ferrous gluconate powder, taurine powder, microcrystalline cellulose powder and 1 /2 ratio of maltodextrin powder is stirred and mixed evenly to obtain the mixed powder for use;
其中,所述混合粉体中各原来粉按重量配比量为:魔芋粉0.5份、维生素C粉0.046份、葡萄糖酸亚铁粉0.01份、牛磺酸粉0.015份、圆苞车前子壳粉2.5份、微晶纤维素粉2.8份、麦芽糊精粉1.3份、大豆粉0.5份、山楂粉0.9份;Wherein, the original powder in the mixed powder is in a proportion by weight: 0.5 parts of konjac powder, 0.046 parts of vitamin C powder, 0.01 parts of ferrous gluconate powder, 0.015 parts of taurine powder, and psyllium husks 2.5 parts of powder, 2.8 parts of microcrystalline cellulose powder, 1.3 parts of maltodextrin powder, 0.5 parts of soybean powder, 0.9 parts of hawthorn powder;
步骤三、制软材:取重量为步骤二中所述混合粉体总重量的38%的乙醇溶液,在所述乙醇溶液中加入重量份为2.7份的甘露糖醇后加热搅拌至溶解得混合液体,然后将所述混合液体喷洒至步骤二中的所述混合粉体中,边喷洒边翻滚搅拌混合均匀制得软材;Step three, making soft materials: take 38% ethanol solution of the total weight of the mixed powder in step two, add 2.7 parts by weight of mannitol to the ethanol solution, and heat and stir until it is dissolved and mixed Liquid, and then spray the mixed liquid into the mixed powder in step two, while spraying, tumbling, stirring and mixing uniformly to obtain a soft material;
其中所述乙醇溶液中乙醇的体积占比为70%;Wherein, the volume ratio of ethanol in the ethanol solution is 70%;
步骤四、制干粒:将步骤三中制得的所述软材继续经过不断翻滚混合至形成稳定球状颗粒,然后过25目筛制得湿粒,将所述湿粒放入烘干箱内进行干燥50min,干燥温度为55℃,然后依次经过70目筛、25目筛筛选出未成粒的细粉和合格的干粒;Step 4. Dry granules: The soft material obtained in step 3 is continuously tumbling and mixed to form stable spherical granules, then wet granules are obtained through a 25-mesh sieve, and the wet granules are put into the drying box Dry for 50 minutes at a drying temperature of 55°C, and then pass through a 70-mesh sieve and a 25-mesh sieve to screen out ungranulated fine powder and qualified dry particles;
将所述细粉回收利用,与所述混合粉体混合后重复制备干粒过程;Recycle the fine powder and repeat the process of preparing dry particles after mixing with the mixed powder;
步骤五、制片:将步骤四中制得的干粒与重量份为0.12份的硬脂酸镁粉和剩余的1/2配比量的麦芽糊精粉混合均匀后,经压片机压片即得圆苞魔芋片;Step 5. Tableting: After mixing the dry granules obtained in Step 4 with 0.12 parts by weight of magnesium stearate powder and the remaining 1/2 proportion of maltodextrin powder, they are pressed by a tableting machine. The slices are round bud konjac slices;
其中所述圆苞魔芋片的规格为0.3g/片,且遇水速溶,1min之内散开。The specification of the round bud konjac flakes is 0.3g/piece, and it dissolves quickly in water, and disperses within 1 min.
对比例1Comparative example 1
同实施例2,不同之处为原料中未添加山楂粉。Same as Example 2, except that hawthorn powder is not added to the raw materials.
对比例2Comparative example 2
同实施例2,不同之处为原料中未添加大豆粉。Same as Example 2, the difference is that no soybean powder is added to the raw material.
对比例3Comparative example 3
同实施例2,不同之处为原料中未添加山楂粉和大豆粉。Same as Example 2, the difference is that hawthorn powder and soybean powder are not added to the raw materials.
本发明的圆苞魔芋片的使用方法为口服,餐前服用,温开水送服,每日4-8g,60天为一个疗程;本发明使用一个疗程即可取得良好效果,且无副作用,减脂快,不反弹。The use method of the round bud konjac tablet of the present invention is oral, taken before meals, and taken with warm water, 4-8g per day, 60 days is a course of treatment; the present invention can achieve good results with one course of treatment without side effects and reduced Fat fast, no rebound.
召集300名肥胖志愿者,男女各150名:男性体脂率高于25%,女性体脂率高于30%,随机分为6组,每组50人,男女各25人,各组成员分别服用实施例1~3和对比例1~3中的圆苞魔芋片60天,正常饮食,测量并记录每位志愿者的体脂率和体重情况在如下统计表中。Convene 300 obese volunteers, 150 men and women: male body fat rate is higher than 25%, female body fat rate is higher than 30%, randomly divided into 6 groups, each group has 50 people, male and female 25 people, each group has its own members Take the round bud konjac tablets in Examples 1 to 3 and Comparative Examples 1 to 3 for 60 days with a normal diet, and measure and record the body fat rate and weight of each volunteer in the following statistical table.
To | 服用本品3h后有无饥饿感Whether there is hunger after taking this product for 3 hours | 体脂率下降Decreased body fat rate | 体重下降weight loss | 不良反应Adverse reactions | 人数Number of people |
实施例1Example 1 | 无no | 3.3%3.3% | 10~12斤10~12 kg | 无no | 4545 |
实施例2Example 2 | 无no | 3.6%3.6% | 12~14斤12~14 kg | 无no | 4747 |
实施例3Example 3 | 无no | 3.5%3.5% | 10~12斤10~12 kg | 无no | 4848 |
对比例1Comparative example 1 | 无no | 2.5%2.5% | 7~9斤7~9 kg | 无no | 4444 |
对比例2Comparative example 2 | 有Have | 2.8%2.8% | 9~10斤9~10 kg | 无no | 4545 |
对比例3Comparative example 3 | 无no | 2.5%2.5% | 7~8斤7~8 kg | 无no | 4646 |
从表中数据看出,服用本发明中的圆苞魔芋片进行减肥的志愿者中,服用一个疗程后减重10~14斤的人数为140人,占比93.3%,且服用本发明中圆苞魔芋片减肥期间不易产生饥饿感,不会分散患者精力,且患者运动耐力不会下降,无不良反应;魔芋粉和圆苞车前子壳粉遇水膨胀,体积增加,可增强的人的饱腹感,进而控制其他食物的摄取,达到减肥效果;山楂中的解脂酶能加快脂肪分解;本发明对患者健康无不良影响;对比实施例1~3和对比例1~3的实验结果发现,本发明同时添加大豆粉和山楂粉,大豆中成分抑制山楂的促消化作用,降低食物消化速度,使人不易产生饥饿感;且大豆中有效成分可加强山 楂中解脂酶的作用,可促进体内脂肪更快速分解,达到更快减脂的效果。It can be seen from the data in the table that among the volunteers who took the round bud konjac tablets of the present invention for weight loss, 140 people lost 10 to 14 kilograms after taking a course of treatment, accounting for 93.3%. During weight loss, konjac flakes are not easy to produce hunger, will not distract the patient, and the patient’s exercise endurance will not decrease, and there will be no adverse reactions; konjac flour and psyllium husk powder will swell in water and increase in volume, which can enhance people’s health Satisfaction, and control the intake of other foods to achieve weight loss; the lipase in hawthorn can accelerate the decomposition of fat; the present invention has no adverse effect on the health of patients; compare the experimental results of Examples 1 to 3 and Comparative Examples 1 to 3 It is found that the present invention adds soybean powder and hawthorn powder at the same time, and the components in soybean inhibit the digestion-promoting effect of hawthorn, reduce the speed of food digestion, and make people less hungry; and the effective ingredients in soybean can strengthen the effect of lipase in hawthorn. Promote the decomposition of body fat more quickly, and achieve the effect of faster fat loss.
这里说明的设备数量和处理规模是用来简化本发明的说明的。对本发明的应用、修改和变化对本领域的技术人员来说是显而易见的。The number of equipment and processing scale described here are used to simplify the description of the present invention. The applications, modifications and changes to the present invention are obvious to those skilled in the art.
尽管本发明的实施方案已公开如上,但其并不仅仅限于说明书和实施方式中所列运用,它完全可以被适用于各种适合本发明的领域,对于熟悉本领域的人员而言,可容易地实现另外的修改,因此在不背离权利要求及等同范围所限定的一般概念下,本发明并不限于特定的细节和这里示出与描述的实施例。Although the embodiments of the present invention have been disclosed as above, they are not limited to the applications listed in the specification and embodiments. It can be applied to various fields suitable for the present invention. For those skilled in the art, it can be easily Therefore, without departing from the general concept defined by the claims and equivalent scope, the present invention is not limited to the specific details and the embodiments shown and described herein.
Claims (8)
- 圆苞魔芋片,其特征在于,包括以下重量份的原料:The round bud konjac flakes are characterized in that they comprise the following raw materials by weight:魔芋粉0.3~0.5份、维生素C粉0.03~0.046份、葡萄糖酸亚铁粉0.005~0.01份、牛磺酸粉0.005~0.015份、圆苞车前子壳粉2.5~3.5份、微晶纤维素粉1.2~2.8份、甘露糖醇2.3~2.7份、硬脂酸镁粉0.04~0.12份。Konjac flour 0.3~0.5 parts, vitamin C powder 0.03~0.046 parts, ferrous gluconate powder 0.005~0.01 parts, taurine powder 0.005~0.015 parts, psyllium husk powder 2.5~3.5 parts, microcrystalline cellulose 1.2 to 2.8 parts of powder, 2.3 to 2.7 parts of mannitol, 0.04 to 0.12 parts of magnesium stearate powder.
- 如权利要求1所述的圆苞魔芋片,其特征在于,包括以下重量份的原料:The round bud konjac flakes according to claim 1, characterized in that it comprises the following parts by weight of raw materials:魔芋粉0.4份、维生素C粉0.038份、葡萄糖酸亚铁粉0.007份、牛磺酸粉0.01份、圆苞车前子壳粉3份、微晶纤维素粉2份、甘露糖醇2.465份、硬脂酸镁粉0.08份。0.4 parts of konjac flour, 0.038 parts of vitamin C powder, 0.007 parts of ferrous gluconate powder, 0.01 parts of taurine powder, 3 parts of psyllium husk powder, 2 parts of microcrystalline cellulose powder, 2.465 parts of mannitol, 0.08 parts of magnesium stearate powder.
- 如权利要求1或2所述的圆苞魔芋片,其特征在于,还包括以下重量份的原料:The round bud konjac flakes according to claim 1 or 2, characterized in that it further comprises the following parts by weight of raw materials:麦芽糊精粉0.7~1.3份、大豆粉0.2~0.5份、山楂粉0.5~0.9份。0.7-1.3 parts of maltodextrin powder, 0.2-0.5 parts of soybean powder, 0.5-0.9 parts of hawthorn powder.
- 如权利要求3所述的圆苞魔芋片的制备方法,其特征在于,包括以下步骤:The method for preparing round bud konjac flakes according to claim 3, characterized in that it comprises the following steps:步骤一、制粉:Step 1. Flour milling:将魔芋和大豆洗净、蒸煮3~5小时,然后经干燥、粉碎、磨粉、过60~80目筛得所述魔芋粉和所述大豆粉待用;Wash the konjac and soybeans, steam for 3 to 5 hours, then dry, crush, grind, and sieve through 60-80 mesh to obtain the konjac flour and the soybean flour for later use;将圆苞车前子壳洗净、干燥、粉碎、磨粉、过60~80目筛得所述圆苞车前子壳粉待用;Wash, dry, pulverize, grind, and sieve the psyllium husks of Psyllium rotundifolia to obtain the husk powder of Psyllium rotundus for use;将山楂洗净经干燥灭菌、粉碎、磨粉、过80~100目筛得所述山楂粉待用;Wash the hawthorn, dry, sterilize, pulverize, pulverize, and sieve through 80-100 mesh to obtain the hawthorn powder for use;将维生素C经粉碎、磨粉、过60~70目筛得所述维生素C粉待用;The vitamin C powder is pulverized, ground, and sieved through 60-70 mesh to obtain the vitamin C powder for use;将葡萄糖酸亚铁和牛磺酸经磨粉、过60~70目筛得所述葡萄糖酸亚铁粉、所述牛磺酸粉待用;Grind the ferrous gluconate and taurine through a 60-70 mesh sieve to obtain the ferrous gluconate powder and the taurine powder for use;将微晶纤维素、麦芽糊精、硬脂酸镁经磨粉、过80~100目筛得所述微晶纤维素粉、所述麦芽糊精粉、所述硬脂酸镁粉待用;Grind microcrystalline cellulose, maltodextrin, and magnesium stearate to obtain the microcrystalline cellulose powder, the maltodextrin powder, and the magnesium stearate powder through a 80-100 mesh sieve;步骤二、混粉:取配比量的魔芋粉、大豆粉、山楂粉、圆苞车前子壳粉、维生素C粉、葡萄糖酸亚铁粉、牛磺酸粉、微晶纤维素粉和1/2配比量的麦芽糊精粉搅拌混合均匀得混合粉体待用;Step two, mixing powder: take the proportion of konjac powder, soybean powder, hawthorn powder, psyllium husk powder, vitamin C powder, ferrous gluconate powder, taurine powder, microcrystalline cellulose powder and 1 /2 ratio of maltodextrin powder is stirred and mixed evenly to obtain the mixed powder for use;步骤三、制软材:取重量为步骤二中所述混合粉体总重量的28~38%的乙醇溶液,在所述乙醇溶液中加入配比量的甘露糖醇后加热搅拌至溶解得混合液体,然后将所述混合液 体喷洒至步骤二中的所述混合粉体中,边喷洒边翻滚搅拌混合均匀制得软材;Step 3. Making soft materials: Take an ethanol solution with a weight of 28% to 38% of the total weight of the mixed powder described in step 2, and add a proportion of mannitol to the ethanol solution, then heat and stir until it is dissolved and mixed Liquid, and then spray the mixed liquid into the mixed powder in step two, while spraying, tumbling, stirring and mixing to obtain a soft material;其中所述乙醇溶液中乙醇的体积占比为50~70%;Wherein, the volume ratio of ethanol in the ethanol solution is 50-70%;步骤四、制干粒:将步骤三中制得的所述软材继续经过不断翻滚混合至形成稳定球状颗粒,然后过15~25目筛制得湿粒,将所述湿粒放入烘干箱内进行干燥30~50min,干燥温度为50~55℃,然后依次经过60~70目筛、15~25目筛筛选出未成粒的细粉和合格的干粒;Step 4. Dry granules: The soft material obtained in step 3 is continuously tumbling and mixed to form stable spherical granules, and then wet granules are obtained through a 15-25 mesh sieve, and the wet granules are put into drying Drying in the box for 30-50min, the drying temperature is 50-55℃, and then pass through 60-70 mesh sieve and 15-25 mesh sieve to screen out ungranulated fine powder and qualified dry particles;将所述细粉回收利用,与所述混合粉体混合后重复制备干粒过程;Recycle the fine powder and repeat the process of preparing dry particles after mixing with the mixed powder;步骤五、制片:将步骤四中制得的干粒与配比量的硬脂酸镁粉和1/2配比量的麦芽糊精粉混合均匀后,经压片机压片即得圆苞魔芋片;Step 5. Tableting: Mix the dry granules prepared in Step 4 with the proportioned amount of magnesium stearate powder and 1/2 proportion of maltodextrin powder, and then press the tablet machine to obtain a round shape. Konjac flakes其中所述圆苞魔芋片的规格为0.2~0.3g/片。The specifications of the round bud konjac slices are 0.2-0.3 g/tablet.
- 如权利要求4所述的圆苞魔芋片的制备方法,其特征在于,所述魔芋粉、所述大豆粉和所述圆苞车前子壳粉需过60目筛制得;The method for preparing konjac flakes with round buds according to claim 4, wherein the konjac flour, the soybean flour and the psyllium husk powder need to pass through a 60-mesh sieve;所述山楂粉需过90目筛制得。The hawthorn powder needs to be obtained through a 90-mesh sieve.
- 如权利要求4所述的圆苞魔芋片的制备方法,其特征在于,所述维生素C粉、所述葡萄糖酸亚铁粉和所述牛磺酸粉需过60目筛制得;The method for preparing konjac flakes with round buds according to claim 4, wherein the vitamin C powder, the ferrous gluconate powder and the taurine powder are obtained by passing through a 60-mesh sieve;所述微晶纤维素粉、所述麦芽糊精粉和所述硬脂酸镁粉需过80目筛制得。The microcrystalline cellulose powder, the maltodextrin powder and the magnesium stearate powder need to be obtained through an 80-mesh sieve.
- 如权利要求4所述的圆苞魔芋片的制备方法,其特征在于,所述步骤四中软材需经过20目筛制湿粒,所述湿粒经干燥后需再经过20目筛得干粒。The method for preparing konjac flakes with round buds according to claim 4, wherein the soft material in the step 4 needs to pass through a 20-mesh sieve to make wet granules, and the wet granules need to be dried through a 20-mesh sieve to obtain dry granules. .
- 如权利要求4所述的圆苞魔芋片的制备方法,其特征在于,所述乙醇溶液中乙醇的体积占比为60%,所述乙醇溶液加入量为所述混合粉体重量的33%。The method for preparing konjac flakes with round buds according to claim 4, wherein the volume ratio of ethanol in the ethanol solution is 60%, and the added amount of the ethanol solution is 33% of the weight of the mixed powder.
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