WO2021046897A1 - 风味组合物及包含所述风味组合物的电子烟液 - Google Patents

风味组合物及包含所述风味组合物的电子烟液 Download PDF

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Publication number
WO2021046897A1
WO2021046897A1 PCT/CN2019/107112 CN2019107112W WO2021046897A1 WO 2021046897 A1 WO2021046897 A1 WO 2021046897A1 CN 2019107112 W CN2019107112 W CN 2019107112W WO 2021046897 A1 WO2021046897 A1 WO 2021046897A1
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Prior art keywords
cigarette liquid
electronic cigarette
parts
weight
flavor composition
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PCT/CN2019/107112
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English (en)
French (fr)
Inventor
许静
姜兴涛
熊赞华
李锐
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深圳雾芯科技有限公司
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Publication of WO2021046897A1 publication Critical patent/WO2021046897A1/zh

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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/16Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A24B15/167Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes

Definitions

  • This application relates to the field of electronic aerosols or electronic atomization devices, and in particular to a flavor composition and an electronic cigarette liquid containing the flavor composition.
  • the electronic cigarette or electronic atomizer atomizes the smoking material at low temperature to form an aerosol for the user to inhale, to replace the smoke generated by traditional tobacco burning at high temperature.
  • the electronic cigarette liquid has a certain influence on the user's experience and taste.
  • This application provides a flavor composition, also known as flavor additive, which can be used in e-cigarette liquid.
  • a flavor composition also known as flavor additive
  • the aerosol for user inhalation can be generated by the user.
  • the flavor of grapefruit does not produce harmful substances such as tar and suspended particles.
  • the e-cigarette liquid can form a uniform and strong aerosol when the user inhales, and the aerosol has a soft mouthfeel and does not have a residual sensation, thereby enhancing the user experience.
  • the present application provides a flavor composition, wherein the flavor composition comprises the following parts by weight: about 0.5 to about 1.5 parts of 1-to- Ene-8-thiol, about 0.01 to about 1 part of ocimene, about 0.1 to about 1.0 part of ⁇ -phellandrene, about 1 to about 10 parts of ⁇ -terpinene, about 0.1 to about 1.0 part of Neral, about 0.1 to about 1.0 parts of decanal, about 90 to about 95 parts of limonene, about 1 to about 5 parts of Valencia tangerine, about 0.1 to about 1.0 parts of n-octanol, about 0.1 to About 1.0 part of caprylic aldehyde, about 0.1 to about 1.0 part of phenethyl acetate, about 0.1 to about 1.0 part of neryl acetate, and about 0.1 to about 1.0 part of citron.
  • the flavor composition comprises the following parts by weight: about 0.5 to about 1.5 parts of 1-to- Ene-8-
  • the present application provides an electronic cigarette liquid, which comprises the above-mentioned flavor composition.
  • the present application provides an atomization device, which includes the above-mentioned electronic cigarette liquid.
  • the terms “substantially”, “substantially”, “substantially”, “substantially” and “about” are used to describe and illustrate small changes. When used in conjunction with an event or situation, the term can refer to an example in which the event or situation occurs precisely and an example in which the event or situation occurs very closely.
  • the term when used in conjunction with a value, can refer to a range of variation less than or equal to ⁇ 10% of the stated value, such as less than or equal to ⁇ 5%, less than or equal to ⁇ 4%, less than or equal to ⁇ 3%, Less than or equal to ⁇ 2%, less than or equal to ⁇ 1%, less than or equal to ⁇ 0.5%, less than or equal to ⁇ 0.1%, or less than or equal to ⁇ 0.05%.
  • the difference between two values is less than or equal to ⁇ 10% of the average value of the value (for example, less than or equal to ⁇ 5%, less than or equal to ⁇ 4%, less than or equal to ⁇ 3%, less than Or equal to ⁇ 2%, less than or equal to ⁇ 1%, less than or equal to ⁇ 0.5%, less than or equal to ⁇ 0.1%, or less than or equal to ⁇ 0.05%), then the two values can be considered "substantially" the same.
  • a list of items connected by the terms “at least one of”, “at least one of”, “at least one of” or other similar terms may mean the listed items Any combination of. For example, if items A and B are listed, then the phrase “at least one of A and B” means only A; only B; or A and B. In another example, if items A, B, and C are listed, then the phrase "at least one of A, B, and C” means only A; or only B; only C; A and B (excluding C); A and C (exclude B); B and C (exclude A); or all of A, B, and C.
  • Project A can contain a single element or multiple elements.
  • Project B can contain a single element or multiple elements.
  • Project C can contain a single element or multiple elements.
  • aerosol for user inhalation may include, but is not limited to, aerosols, suspended liquids, low-temperature vapors, and volatile gases.
  • the present application provides an e-cigarette liquid comprising a flavor composition
  • the flavor composition comprises the following parts by weight: about 0.5 to about 1.5 parts of 1-p-mengene-8- Mercaptan, about 0.01 to about 1 part of ocimene, about 0.1 to about 1.0 part of ⁇ -phellandrene, about 1 to about 10 parts of ⁇ -terpinene, about 0.1 to about 1.0 part of neral, About 0.1 to about 1.0 parts of decanal, about 90 to about 95 parts of limonene, about 1 to about 5 parts of Valencia orange, about 0.1 to about 1.0 parts of n-octanol, about 0.1 to about 1.0 parts of octanol Aldehydes, about 0.1 to about 1.0 parts of phenethyl acetate, about 0.1 to about 1.0 parts of neryl acetate, and about 0.1 to about 1.0 parts of citron.
  • the flavor composition comprises the following parts by weight: about 0.5 to
  • 1-to- The ene-8-thiol can be roughly composed of 0.5 parts, 0.6 parts, 0.7 parts, 0.8 parts, 0.9 parts, 1.0 parts, 1.1 parts, 1.2 parts, 1.3 parts, 1.4 parts, 1.5 parts or any two of these parts by weight
  • Ocimene can be roughly 0.01 part, 0.02 part, 0.03 part, 0.04 part, 0.05 part, 0.1 part, 0.5 part, 1.0 part or any two of these parts by weight
  • ⁇ -phellandrene can be roughly It is 0.1 part, 0.2 part, 0.3 part, 0.4 part, 0.5 part, 1.0 part or any two of these parts by weight
  • ⁇ -terpinene can be roughly 1 part, 2 parts, 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts, 9 parts, 10 parts or any two of these parts by weight
  • neral can be roughly 0.1 part, 0.2 part, 0.3 part, 0.4 part, 0.5 part, 1.0 part or the range of any two of these parts by weight
  • the flavor composition is an additive, and when it is added to the electronic cigarette liquid, it can make the user produce the taste and smell of grapefruit flavor when the electronic cigarette liquid is used.
  • the weight of the flavor composition in the e-cigarette liquid is approximately based on the total weight of the e-cigarette liquid, for example, 0.1%, 0.5%, 1%, 2%, 3%, 4%. %, 5%, 6%, 7%, 8%, 9%, 10% or any two of these weight percentages. In some embodiments, the weight of the flavor composition in the e-cigarette liquid is approximately about 1% to about 10%, so that the generated aerosol has a mild taste, thereby optimizing the user experience.
  • the e-cigarette liquid also includes a base solvent, wherein the base solvent includes propylene glycol and glycerol (glycerin).
  • the weight of propylene glycol in the e-liquid is approximately, for example, 15%, 20%, 25%, 30%, 35%, 40%, 50%, 60%, 70%, or any two of these weight percentages; and the weight of glycerol in the e-cigarette liquid is roughly, for example, 30%, 35%, 40%, 45%, 50%, 55% , 60%, 65%, 70% or any two of these weight percentages.
  • the weight of the propylene glycol in the e-cigarette liquid is about 20% to about 60%, and the weight of the glycerol in the e-cigarette liquid is about 40% to about 70%, so that the electronic cigarette The smoke liquid achieves the best atomization effect and improves the user experience.
  • the basic solvent can be any solvent known in the art, such as deionized water, propylene glycol, and glycerol, according to specific needs, without being limited.
  • the electronic cigarette liquid further includes a cooling agent.
  • Cooling agents are additives, which are chemicals that can give users a cooling effect when the product is in use and are not very irritating.
  • the cooling agent includes selected from the group consisting of menthol, menthone, isomenthone, 1-menthyl lactate, WS-23 (N,2,3-trimethyl-2-isopropylbutyl Amide), WS-3 (N-ethyl-p-menthyl-3-carboxamide), WS-5 (N-(ethoxycarbonylmethyl)-p-alkane-3-carboxamide), WS-12(N -(4-Methoxyphenyl)-p-menthyl-3-carboxamide) and combinations thereof.
  • the weight of the cooling agent in the e-cigarette liquid is approximately, for example, 0.1%, 0.2%, 0.3%, 0.5%, 1.0%, 1.5% , 2.0%, 2.5%, 5%, 10% or any two of these weight percentages. In some embodiments, the weight of the cooling agent in the e-cigarette liquid is about 1.0% to about 10% based on the total weight of the e-cigarette liquid, so as to improve the user-friendliness of the e-cigarette liquid. The taste of the inhaled aerosol.
  • the e-cigarette liquid further includes nicotine salt.
  • the weight of the nicotine salt in the e-cigarette liquid is approximately, for example, 0.1%, 0.2%, 0.5%, 1.0% , 1.5%, 2.0%, 2.5%, 5%, 7.5%, 10% or any two of these weight percentages.
  • the weight of the nicotine salt in the e-cigarette liquid is about 1.8% to about 10.0% based on the total weight of the e-cigarette liquid.
  • the e-cigarette liquid further includes nicotine.
  • the weight of the nicotine in the e-cigarette liquid is approximately, for example, 0.1%, 0.2%, 0.5%, 1.0%, A range composed of 1.5%, 2.0%, 2.5%, 5% or any two of these weight percentages.
  • the weight of the nicotine in the e-cigarette liquid is about 0.9% to about 5.0% based on the total weight of the e-cigarette liquid.
  • the e-cigarette liquid further includes a fragrance, wherein the fragrance is selected from 1,4-cineole, ethyl 2-methylbutyrate, 3-carene, ⁇ -pinene, and ⁇ -pinene.
  • the fragrance is selected from 1,4-cineole, ethyl 2-methylbutyrate, 3-carene, ⁇ -pinene, and ⁇ -pinene.
  • the weight of the flavor in the e-cigarette liquid is about 0.01% to about 5.0% based on the total weight of the e-cigarette liquid, so as to enhance the flavor of the e-cigarette liquid and optimize its production The taste of the aerosol.
  • the present application provides a method for preparing e-cigarette liquid, which includes the following steps: mixing the ingredients in the flavor composition in a specific ratio within the range provided in the examples, and then adding flavor, nicotine salt and cooling The flavoring agent is then added to the basic e-liquid and mixed uniformly to obtain the e-liquid.
  • the present application provides an atomization device, which includes the electronic cigarette liquid described in any of the foregoing embodiments.
  • the electronic cigarette liquid can be atomized by the atomizing device to generate aerosol for inhalation by the user.
  • the atomization device includes an electronic cigarette, an ultrasonic atomizer, or a mesh atomizer.
  • Propylene glycol and glycerol are blended according to the following weight ratio (32:56) and mixed uniformly to obtain a basic smoke liquid.
  • Flavor preparation :
  • Neryl and citronone were formulated and mixed in the following weight ratio (1:0.04:0.6:2.6:0.2:0.3:92:1.4:0.4:0.3:0.2:0.2:0.5) to obtain a flavor composition, and then 2.0 grams The flavor composition is added to 98 grams of basic e-cigarette liquid and stirred evenly to obtain an electronic cigarette liquid.
  • Neryl and citronone were formulated and mixed in the following weight ratio (1:0.04:0.6:2.6:0.2:0.3:92:1.4:0.4:0.3:0.2:0.2:0.5) to obtain a flavor composition, and then 2.0 grams The flavor composition, 3.0 grams of nicotine, 1.7 grams of benzoic acid, 0.8 grams of WS-23 and 0.5 grams of WS-3 are mixed and added to 92.0 grams of basic e-liquid and stirred evenly to obtain an e-cigarette liquid.
  • Neryl and citronone were formulated and mixed in the following weight ratio (1:0.04:0.6:2.6:0.2:0.3:92:1.4:0.4:0.3:0.2:0.2:0.5) to obtain a flavor composition, and then 2 grams
  • the flavor composition 3.0 grams of nicotine, 1.7 grams of benzoic acid, 0.8 grams of WS-23, 0.5 grams of WS-3 and 4 grams of flavor are mixed and then added to 88.0 grams of basic tobacco liquid, and stirred evenly to obtain electronic Smoke liquid.
  • Neryl and citronone were blended in the following weight ratio (1.2:0.5:0.5:5:0.5:0.8:94:3.0:0.8:0.2:0.6:0.6:0.5) to obtain a flavor composition, and then 1.5 grams The flavor composition, 2.0 grams of nicotine, 1.5 grams of benzoic acid, 0.5 grams of WS-23, 0.5 grams of WS-3, and 2.0 grams of flavor are mixed and added to 92.0 grams of basic tobacco liquid. Smoke liquid.
  • composition of the fragrance in the above-mentioned embodiment is shown in Table 1 below.
  • Example 1 Example 2
  • Example 3 Example 4 Exquisite degree of smoke 4.1 4.7 4.8 4.8
  • the scent is consistent, no segmentation or fault 4.3 4.4 4.5 4.8
  • Smoke and aroma concentration 4.2 4.6 4.7 Richness of aroma, long degree of smoke 4.1 4.2 4.7 4.4
  • Taste sweetness freshness 4.5 4.6 4.8 4.5 Irritation and burning sensation
  • 4.1 4.2 4.7 Cleanliness of the mouth after suction 4.1 4.3 4.4 4.5 Is there any bad breath? 3.9
  • Statistical method Randomly select 1000 users to test the use of the e-cigarette liquids of the above examples 1-4 through e-cigarettes, and evaluate their taste and mouthfeel after the use test.
  • the evaluation standard is based on a total score of 10 points. The better or the better the taste, the higher the score.
  • this application provides an e-cigarette liquid, through which the flavor composition contained in the e-cigarette liquid can allow users to produce the flavor of grapefruit without producing tar, suspended particles, etc. Harmful Substance.
  • the e-cigarette liquid can form a uniform and strong aerosol when the user inhales, and the aerosol has a soft mouthfeel and does not have a residual sensation, thereby enhancing the user experience.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Fats And Perfumes (AREA)
  • Manufacture Of Tobacco Products (AREA)

Abstract

一种风味组合物及包含该风味组合物的电子烟液,该风味组合物包含以下重量份的物质:0.5至1.5份的1-对- 烯-8-硫醇、0.01至1份的罗勒烯、0.1至1.0份的α-水芹烯、1至10份的γ-松油烯、0.1至1.0份的橙花醛、0.1至1.0份的癸醛、90至95份的柠檬烯、1至5份的巴伦西亚橘烯、0.1至1.0份的正辛醇、0.1至1.0份的辛醛、0.1至1.0份的乙酸苯乙酯、0.1至1.0份的乙酸橙花酯及0.1至1.0份的圆柚酮。该电子烟液在吸取时产生西柚风味的口感,且能够形成气味均匀且浓郁的气雾,有效提升使用者体验。

Description

风味组合物及包含所述风味组合物的电子烟液 技术领域
本申请涉及电子气雾剂或电子雾化装置的领域,尤其涉及一种风味组合物及包含所述风味组合物的电子烟液。
背景技术
由于对于个人健康、环境保护以及使用便利性的追求,电子烟作为传统烟草的取代品越来越受到消费者的青睐。电子烟或电子雾化器通过将发烟材料低温雾化形成用于使用者吸入的气雾,来取代传统烟草以高温燃烧的方式所产生的烟气。其中,电子烟液对于使用者的体验及口感具有一定的影响。
因此,有必要对电子烟液的组成做进一步的改进与研究。
发明内容
本申请通过提供一种风味组合物又称为风味添加剂,其可用于电子烟液中,该风味组合物通过雾化装置雾化后所形成的用于使用者吸入的气雾能够让使用者产生西柚的风味,且不产生焦油与悬浮微粒等有害物质。同时,该电子烟液在使用者抽吸时能够形成气味均匀且浓郁的气雾,而该气雾口感柔顺且不具有残留感,从而提升使用者体验。
根据本申请的一个层面,本申请提供了一种风味组合物,其中所述风味组合物包含以下重量份的物质:约0.5至约1.5份的1-对-
Figure PCTCN2019107112-appb-000001
烯-8-硫醇、约0.01至约1份的罗勒烯、约0.1至约1.0份的α-水芹烯、约1至约10份的γ-松油烯、约0.1至约1.0份的橙花醛、约0.1至约1.0份的癸醛、约90至约95份的柠檬烯、约1至约5份的巴伦西亚橘烯、约0.1至约1.0份的正辛醇、约0.1至约1.0份的辛醛、约0.1至约1.0份的乙酸苯乙酯、约0.1至约1.0份的乙酸橙花酯及约0.1至约1.0份的圆柚酮。
根据本申请的另一层面,本申请提供了一种电子烟液,其包含上述风味组合物。
根据本申请的又一层面,本申请提供了一种雾化装置,其包含上述电子烟液。
本申请实施例的额外层面及优点将部分地在后续说明中描述、显示、或是经由本申请实施例的实施而阐释。
具体实施方式
本申请的实施例将会被详细的描示在下文中。本申请的实施例不应所述被解释为对本申请的限制。
另外,有时在本文中以范围格式呈现量、比率和其它数值。应理解,此类范围格式是用于便利及简洁起见,且应灵活地理解,不仅包含明确地指定为范围限制的数值,而且包含涵盖于所述范围内的所有个别数值或子范围,如同明确地指定每一数值及子范围一般。
如本文中所使用,术语“大致”、“大体”、“大体上”、“实质”及“约”用以描述及说明小的变化。当与事件或情形结合使用时,所述术语可指代其中事件或情形精确发生的例子以及其中事件或情形极近似地发生的例子。举例来说,当结合数值使用时,术语可指代小于或等于所述数值的±10%的变化范围,例如小于或等于±5%、小于或等于±4%、小于或等于±3%、小于或等于±2%、小于或等于±1%、小于或等于±0.5%、小于或等于±0.1%、或小于或等于±0.05%。举例来说,如果两个数值之间的差值小于或等于所述值的平均值的±10%(例如小于或等于±5%、小于或等于±4%、小于或等于±3%、小于或等于±2%、小于或等于±1%、小于或等于±0.5%、小于或等于±0.1%、或小于或等于±0.05%),那么可认为所述两个数值“大体上”相同。
在具体实施方式及权利要求书中,由术语“中的至少一者”、“中的至少一个”、“中的至少一种”或其他相似术语所连接的项目的列表可意味着所列项目的任何组合。例如,如果列出项目A及B,那么短语“A及B中的至少一者”意味着仅A;仅B;或A及B。在另一实例中,如果列出项目A、B及C,那么短语“A、B及C中的至少一者”意味着仅A;或仅B;仅C;A及B(排除C);A及C(排除B);B及C(排除A);或A、B及C的全部。项目A可包含单个元件或多个元件。项目B可包含单个元件或多个元件。项目C可包含单个元件或多个元件。
在本文中,用语“用于使用者吸入的气雾”或“气雾”可以包括,但不限于,气溶胶、悬浮液体、低温蒸气及挥发性气体。
根据本申请的一个方面,本申请提供一种电子烟液,其包含风味组合物,其中所述 风味组合物包含以下重量份的物质:约0.5至约1.5份的1-对孟烯-8-硫醇、约0.01至约1份的罗勒烯、约0.1至约1.0份的α-水芹烯、约1至约10份的γ-松油烯、约0.1至约1.0份的橙花醛、约0.1至约1.0份的癸醛、约90至约95份的柠檬烯、约1至约5份的巴伦西亚橘、约0.1至约1.0份的正辛醇、约0.1至约1.0份的辛醛、约0.1至约1.0份的乙酸苯乙酯、约0.1至约1.0份的乙酸橙花酯及约0.1至约1.0份的圆柚酮。在一些实施例中,本申请的风味组合物可由以上重量份的物质组成。
在一些实施例的风味组合物中,1-对-
Figure PCTCN2019107112-appb-000002
烯-8-硫醇可大致为0.5份、0.6份、0.7份、0.8份、0.9份、1.0份、1.1份、1.2份、1.3份、1.4份、1.5份或这些重量份中任意两者组成的范围;罗勒烯可大致为0.01份、0.02份、0.03份、0.04份、0.05份、0.1份、0.5份、1.0份或这些重量份中任意两者组成的范围;α-水芹烯可大致为0.1份、0.2份、0.3份、0.4份、0.5份、1.0份或这些重量份中任意两者组成的范围;γ-松油烯可大致为1份、2份、3份、4份、5份、6份、7份、8份、9份、10份或这些重量份中任意两者组成的范围;橙花醛可大致为0.1份、0.2份、0.3份、0.4份、0.5份、1.0份或这些重量份中任意两者组成的范围;癸醛可大致为0.1份、0.2份、0.3份、0.4份、0.5份、1.0份或这些重量份中任意两者组成的范围;柠檬烯可大致为90份、91份、92份、93份、94份、95份或这些重量份中任意两者组成的范围;巴伦西亚橘烯可大致为1份、2份、3份、4份、5份或这些重量份中任意两者组成的范围;正辛醇可大致为0.1份、0.2份、0.3份、0.4份、0.5份、1.0份或这些重量份中任意两者组成的范围;辛醛可大致为0.1份、0.2份、0.3份、0.4份、0.5份、1.0份或这些重量份中任意两者组成的范围;乙酸苯乙酯可大致为0.1份、0.2份、0.3份、0.4份、0.5份、1.0份或这些重量份中任意两者组成的范围;乙酸橙花酯可大致为0.1份、0.2份、0.3份、0.4份、0.5份、1.0份或这些重量份中任意两者组成的范围;及圆柚酮可大致为0.1份、0.2份、0.3份、0.4份、0.5份、1.0份或这些重量份中任意两者组成的范围。
风味组合物为添加剂,其添加于电子烟液中时,能够使该电子烟液在使用时让使用者产生西柚风味的味觉及嗅觉感受。
在一些实施例中,所述风味组合物在所述电子烟液中的重量以所述电子烟液总重计大致为,例如,0.1%、0.5%、1%、2%、3%、4%、5%、6%、7%、8%、9%、10%或这些重量百分比中任意两者组成的范围。在一些实施例中,所述风味组合物在电子烟液中的重量份大致为约1%至约10%,以使其生成的气雾味道温和,从而优化使用者体验。
电子烟液还包含基础溶剂,其中所述基础溶剂包含丙二醇及丙三醇(甘油)。在一些实施例中,以所述电子烟液总重计,丙二醇在电子烟液中的重量大致为,例如,15%、20%、25%、30%、35%、40%、50%、60%、70%或这些重量百分比中任意两者组成的范围;及丙三醇在电子烟液中的重量大致为,例如,30%、35%、40%、45%、50%、55%、60%、65%、70%或这些重量百分比中任意两者组成的范围。在一些实施例中,所述丙二醇在电子烟液中的重量为约20%至约60%,且所述丙三醇在电子烟液中的重量为约40%至约70%,以使电子烟液达到最佳的雾化效果,提高使用者体验。
本领域技术人员应理解,基础溶剂可以根据具体需求选择本领域任何已知的溶剂,例如,去离子水、丙二醇、丙三醇,而不受其限制。
在一些实施例中,所述电子烟液还进一步包含凉味剂。
凉味剂为添加剂,其为能够使产品在使用时让使用者产生清凉效果的感受且刺激性不强的化学物。在一些实施例中,所述凉味剂包括选自由薄荷脑、薄荷酮、异薄荷酮、乳酸l-薄荷酯、WS-23(N,2,3-三甲基-2-异丙基丁酰胺)、WS-3(N-乙基-对薄荷基-3-甲酰胺)、WS-5(N-(乙氧羰基甲基)-对烷-3-甲酰胺)、WS-12(N-(4-甲氧基苯基)-对薄荷基-3-羧酰胺)及其组合所组成的群组。
在一些实施例中,以所述电子烟液总重计,所述凉味剂在电子烟液中的重量大致为,例如,0.1%、0.2%、0.3%、0.5%、1.0%、1.5%、2.0%、2.5%、5%、10%或这些重量百分比中任意两者组成的范围。在一些实施例中,所述凉味剂在电子烟液中的重量以所述电子烟液总重计为约1.0%至约10%,以提高所述电子烟液所生成的用于使用者吸入的气雾的口感。
在一些实施例中,所述电子烟液还包括尼古丁盐。在一些实施例中,以所述电子烟液总重计,所述尼古丁盐在电子烟液中在所述电子烟液中的重量大致为,例如,0.1%、0.2%、0.5%、1.0%、1.5%、2.0%、2.5%、5%、7.5%、10%或这些重量百分比中任意两者组成的范围。在一些实施例中,所述尼古丁盐在所述电子烟液中的重量以所述电子烟液总重计为约1.8%至约10.0%。
在一些实施例中,所述电子烟液还包括尼古丁。在一些实施例中,以所述电子烟液总重计,所述尼古丁在电子烟液中在所述电子烟液中的重量大致为,例如,0.1%、0.2%、0.5%、1.0%、1.5%、2.0%、2.5%、5%或这些重量百分比中任意两者组成的范围。在一些实施例中,所述尼古丁在所述电子烟液中的重量以所述电子烟液总重计为约0.9 %至约5.0%。
在一些实施例中,所述电子烟液进一步包括香精,其中所述香精选自由1,4-桉叶素、2-甲基丁酸乙酯、3-蒈烯、α-蒎烯、α-松油醇、β-大马酮(β-突厥酮)、β-蒎烯、月桂烯、苯乙醇、丁酸、丁酸乙酯、二氢茉莉酮酸甲酯、芳樟醇、肉桂酸乙酯、己酸烯丙酯、柠檬醛、柠檬酸乙酯、三乙酸甘油酯、β-石竹烯、香兰素、香茅醇、香叶醇、乙基麦芽酚、乙基香兰素、乙酸苄酯、乙酸芳樟酯、乙酸香叶酯、乙酸乙酯、异戊酸乙酯及其组合所组成的群组。
在一些实施例中,所述香精在所述电子烟液中的重量以所述电子烟液总重计为约0.01%至约5.0%,以增添所述电子烟液的风味及优化其所生成的气雾的口感。
根据本申请一些实施例,本申请提供电子烟液的制备方法,其包含以下步骤:将风味组合物中的各成份按实施例提供的范围中的特定比例混合,随后加入香精、尼古丁盐及凉味剂,然后加入至基础烟液中,使其均匀混合以获得电子烟液。
根据本申请的另一个方面,本申请提供一种雾化装置,其包含上述任一实施例所述的电子烟液。所述电子烟液可通过所述雾化装置雾化生成供使用者吸入的气雾。
在一些实施例中,所述雾化装置包括电子烟、超声雾化器或网式雾化器。
实施例
为便于更好地理解本申请,通过以下实例加以说明。这些实例属于本申请的保护范围,但不限制本申请的保护范围。
基础烟液的制备:
将丙二醇和丙三醇依照以下重量比(32:56)调配后混合均匀,以获得基础烟液。
香精的制备:
按照下表1中的重量比例配置,混合以获得香精。
实施例1
将1-对-
Figure PCTCN2019107112-appb-000003
烯-8-硫醇、罗勒烯、α-水芹烯、γ-松油烯、橙花醛、癸醛、柠檬烯、巴伦西亚橘烯、正辛醇、辛醛、乙酸苯乙酯、乙酸橙花酯及圆柚酮按以下重量比(1:0.04:0.6:2.6:0.2:0.3:92:1.4:0.4:0.3:0.2:0.2:0.5)调配混合以获得风味组合物,随后将2.0克的风味组合物加入98克的基础烟液中,搅拌均匀,得到电子烟液。
实施例2
将1-对-
Figure PCTCN2019107112-appb-000004
烯-8-硫醇、罗勒烯、α-水芹烯、γ-松油烯、橙花醛、癸醛、柠檬烯、巴伦西亚橘烯、正辛醇、辛醛、乙酸苯乙酯、乙酸橙花酯及圆柚酮按以下重量比(1:0.04:0.6:2.6:0.2:0.3:92:1.4:0.4:0.3:0.2:0.2:0.5)调配混合以获得风味组合物,随后将2.0克的风味组合物、3.0克的尼古丁、1.7克的苯甲酸、0.8克的WS-23与0.5克的WS-3混合后加入92.0克的基础烟液中,搅拌均匀,得到电子烟液。
实施例3
将1-对-
Figure PCTCN2019107112-appb-000005
烯-8-硫醇、罗勒烯、α-水芹烯、γ-松油烯、橙花醛、癸醛、柠檬烯、巴伦西亚橘烯、正辛醇、辛醛、乙酸苯乙酯、乙酸橙花酯及圆柚酮按以下重量比(1:0.04:0.6:2.6:0.2:0.3:92:1.4:0.4:0.3:0.2:0.2:0.5)调配混合以获得风味组合物,随后将2克的风味组合物、3.0克的尼古丁、1.7克的苯甲酸、0.8克的WS-23、0.5克的WS-3与4克的香精混合后加入88.0克的基础烟液中,搅拌均匀,得到电子烟液。
实施例4
将1-对-
Figure PCTCN2019107112-appb-000006
烯-8-硫醇、罗勒烯、α-水芹烯、γ-松油烯、橙花醛、癸醛、柠檬烯、巴伦西亚橘烯、正辛醇、辛醛、乙酸苯乙酯、乙酸橙花酯及圆柚酮按以下重量比(1.2:0.5:0.5:5:0.5:0.8:94:3.0:0.8:0.2:0.6:0.6:0.5)调配混合以获得风味组合物,随后将1.5克的风味组合物、2.0克的尼古丁、1.5克的苯甲酸、0.5克的WS-23、0.5克的WS-3与2.0克的香精混合后加入92.0克的基础烟液中,搅拌均匀,得到电子烟液。
上述实施例中香精的组成如下表1所示。
表1
Figure PCTCN2019107112-appb-000007
Figure PCTCN2019107112-appb-000008
上述实施例1-4的电子烟液完成后,随后进行口感评分测试。
口感评分测试方法1
请20位评析者按表2中的各个评价指标对上述实施例1-4的电子烟气溶胶体验打分。评测结果如下表3所示.
表2
Figure PCTCN2019107112-appb-000009
Figure PCTCN2019107112-appb-000010
表3
评价指标 实施例1 实施例2 实施例3 实施例4
烟气细腻程度 4.1 4.7 4.8 4.8
香味前后一致,无分段或断层 4.3 4.4 4.5 4.8
烟气和香味浓度 4.2 4.2 4.6 4.7
香味丰富性,烟气悠长程度 4.1 4.2 4.7 4.4
口感甜润度、生津感 4.5 4.6 4.8 4.5
刺激性和灼烧感 4.0 4.1 4.2 4.7
抽吸后口腔干净程度 4.1 4.3 4.4 4.5
有无不良气息 3.9 4.2 4.3 4.2
击喉感 3.5 4.1 4.0 4.2
香味的还原度和辨识度 4.1 4.3 4.5 4.6
口感评分测试方式2;
统计方法:随机选取1000使用者通过电子烟对上述实施例1-4的电子烟液进行使用测试,待使用测试后对其口味及口感进行评价,其中评价标准以总分10分计,口味越佳或口感越好则分数越高。
实施例1-4的电子烟液经过口感评分测试的测试结果如下表4所示。
表4
Figure PCTCN2019107112-appb-000011
由表2-4中数据可知,本申请实施例1-4的电子烟液经雾化后能产生的具有西柚风 味的供使用者吸入的气雾,其不论在口感或是口味的表现上都能有效的提升客户的满意度。
通过本申请上述实施例应可了解,本申请提供了一种电子烟液,通过该电子烟液中包含的风味组合物,能够让使用者产生西柚的风味,且不产生焦油与悬浮微粒等有害物质。同时,该电子烟液在使用者抽吸时能够形成气味均匀且浓郁的气雾,而该气雾口感柔顺且不具有残留感,从而提升使用者体验。
虽然已参考本申请的特定实施例描述并说明本申请,但是这些描述和说明并不限制本申请。所属领域的技术人员可清晰地理解,在不脱离如由所附权利要求书定义的本申请的真实精神和范围的情况下,可进行各种改变(例如对本申请的风味组合物中的成分进行适当增加、减少和改变),以使特定情形、材料、物质组成、物质、方法或过程适宜于本申请的目标、精神和范围。所有此类修改都意图在此所附权利要求书的范围内。虽然已参考按特定次序执行的特定操作描述本文中所公开的方法,但应理解,可在不脱离本申请的教示的情况下组合、细分或重新排序这些操作以形成等效方法。因此,除非本文中特别指示,否则操作的次序和分组并非本申请的限制。

Claims (11)

  1. 一种风味组合物,其包含以下重量份的物质:
    0.5至1.5份的1-对-
    Figure PCTCN2019107112-appb-100001
    烯-8-硫醇、0.01至1份的罗勒烯、0.1至1.0份的α-水芹烯、1至10份的γ-松油烯、0.1至1.0份的橙花醛、0.1至1.0份的癸醛、90至95份的柠檬烯、1至5份的巴伦西亚橘烯、0.1至1.0份的正辛醇、0.1至1.0份的辛醛、0.1至1.0份的乙酸苯乙酯、0.1至1.0份的乙酸橙花酯及0.1至1.0份的圆柚酮。
  2. 一种电子烟液,其包含权利要求1所述的风味组合物。
  3. 根据权利要求2所述的电子烟液,其中所述风味组合物在所述电子烟液中的重量以所述电子烟液总重计为1%至10%。
  4. 根据权利要求2所述的电子烟液,其进一步包括凉味剂,其中所述凉味剂选自由薄荷脑、薄荷酮、异薄荷酮、乳酸l-薄荷酯、WS-23(N,2,3-三甲基-2-异丙基丁酰胺)、WS-3(N-乙基-对薄荷基-3-甲酰胺)、WS-5(N-(乙氧羰基甲基)-对烷-3-甲酰胺)、WS-12(N-(4-甲氧基苯基)-对薄荷基-3-羧酰胺)及其组合所组成的群组。
  5. 根据权利要求4所述的电子烟液,其中所述凉味剂在所述电子烟液中的重量以所述电子烟液总重计为1%至10%。
  6. 根据权利要求2所述的电子烟液,其进一步包括尼古丁盐,且所述尼古丁盐在所述电子烟液中的重量以所述电子烟液总重计为1.8%至10.0%。
  7. 根据权利要求2所述的电子烟液,其进一步包含尼古丁,且所述尼古丁在所述电子烟液中的重量以所述电子烟液总重计为0.9%至5.0%。
  8. 根据权利要求2所述的电子烟液,其进一步包括香精,其中所述香精选自由1,4-桉叶素、2-甲基丁酸乙酯、3-蒈烯、α-蒎烯、α-松油醇、β-大马酮(β-突厥酮)、β-蒎烯、月桂烯、苯乙醇、丁酸、丁酸乙酯、二氢茉莉酮酸甲酯、芳樟醇、肉桂酸乙酯、己酸烯丙酯、柠檬醛、柠檬酸乙酯、三乙酸甘油酯、β-石竹烯、香兰素、香茅醇、香叶醇、乙基麦芽酚、乙基香兰素、乙酸苄酯、乙酸芳樟酯、乙酸香叶酯、乙酸乙酯、异戊酸乙酯及其组合所组成的群组。
  9. 根据权利要求8所述的电子烟液,其中所述香精在所述电子烟液中的重量以所述电子烟液总重计为0.01%至5.0%。
  10. 一种雾化装置,其包含权利要求1所述的风味组合物或权利要求2至9中任 一权利要求所述的电子烟液。
  11. 根据权利要求10所述的雾化装置,其中所述雾化装置包括电子烟、超声雾化器或网式雾化器。
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