WO2020035256A1 - Système et procédé de mesure du niveau de remplissage d'un gaz dans un cylindre, procédé d'étalonnage dudit système et procédé de détection de défauts - Google Patents

Système et procédé de mesure du niveau de remplissage d'un gaz dans un cylindre, procédé d'étalonnage dudit système et procédé de détection de défauts Download PDF

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Publication number
WO2020035256A1
WO2020035256A1 PCT/EP2019/069384 EP2019069384W WO2020035256A1 WO 2020035256 A1 WO2020035256 A1 WO 2020035256A1 EP 2019069384 W EP2019069384 W EP 2019069384W WO 2020035256 A1 WO2020035256 A1 WO 2020035256A1
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WO
WIPO (PCT)
Prior art keywords
cylinder
fill level
response
acoustic impact
gas
Prior art date
Application number
PCT/EP2019/069384
Other languages
English (en)
Inventor
Wilhelm Bayerl
Jean Blondeau
Matthias Bohn
Original Assignee
Linde Aktiengesellschaft
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Linde Aktiengesellschaft filed Critical Linde Aktiengesellschaft
Publication of WO2020035256A1 publication Critical patent/WO2020035256A1/fr

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Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01F—MEASURING VOLUME, VOLUME FLOW, MASS FLOW OR LIQUID LEVEL; METERING BY VOLUME
    • G01F22/00—Methods or apparatus for measuring volume of fluids or fluent solid material, not otherwise provided for
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C13/00—Details of vessels or of the filling or discharging of vessels
    • F17C13/02—Special adaptations of indicating, measuring, or monitoring equipment
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C13/00—Details of vessels or of the filling or discharging of vessels
    • F17C13/02—Special adaptations of indicating, measuring, or monitoring equipment
    • F17C13/023—Special adaptations of indicating, measuring, or monitoring equipment having the mass as the parameter
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C13/00—Details of vessels or of the filling or discharging of vessels
    • F17C13/02—Special adaptations of indicating, measuring, or monitoring equipment
    • F17C13/028—Special adaptations of indicating, measuring, or monitoring equipment having the volume as the parameter
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01F—MEASURING VOLUME, VOLUME FLOW, MASS FLOW OR LIQUID LEVEL; METERING BY VOLUME
    • G01F23/00—Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm
    • G01F23/22—Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm by measuring physical variables, other than linear dimensions, pressure or weight, dependent on the level to be measured, e.g. by difference of heat transfer of steam or water
    • G01F23/28—Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm by measuring physical variables, other than linear dimensions, pressure or weight, dependent on the level to be measured, e.g. by difference of heat transfer of steam or water by measuring the variations of parameters of electromagnetic or acoustic waves applied directly to the liquid or fluent solid material
    • G01F23/296—Acoustic waves
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01F—MEASURING VOLUME, VOLUME FLOW, MASS FLOW OR LIQUID LEVEL; METERING BY VOLUME
    • G01F23/00—Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm
    • G01F23/22—Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm by measuring physical variables, other than linear dimensions, pressure or weight, dependent on the level to be measured, e.g. by difference of heat transfer of steam or water
    • G01F23/28—Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm by measuring physical variables, other than linear dimensions, pressure or weight, dependent on the level to be measured, e.g. by difference of heat transfer of steam or water by measuring the variations of parameters of electromagnetic or acoustic waves applied directly to the liquid or fluent solid material
    • G01F23/296—Acoustic waves
    • G01F23/2966—Acoustic waves making use of acoustical resonance or standing waves
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01F—MEASURING VOLUME, VOLUME FLOW, MASS FLOW OR LIQUID LEVEL; METERING BY VOLUME
    • G01F23/00—Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm
    • G01F23/22—Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm by measuring physical variables, other than linear dimensions, pressure or weight, dependent on the level to be measured, e.g. by difference of heat transfer of steam or water
    • G01F23/28—Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm by measuring physical variables, other than linear dimensions, pressure or weight, dependent on the level to be measured, e.g. by difference of heat transfer of steam or water by measuring the variations of parameters of electromagnetic or acoustic waves applied directly to the liquid or fluent solid material
    • G01F23/296—Acoustic waves
    • G01F23/2966—Acoustic waves making use of acoustical resonance or standing waves
    • G01F23/2967—Acoustic waves making use of acoustical resonance or standing waves for discrete levels
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01F—MEASURING VOLUME, VOLUME FLOW, MASS FLOW OR LIQUID LEVEL; METERING BY VOLUME
    • G01F23/00—Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm
    • G01F23/22—Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm by measuring physical variables, other than linear dimensions, pressure or weight, dependent on the level to be measured, e.g. by difference of heat transfer of steam or water
    • G01F23/28—Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm by measuring physical variables, other than linear dimensions, pressure or weight, dependent on the level to be measured, e.g. by difference of heat transfer of steam or water by measuring the variations of parameters of electromagnetic or acoustic waves applied directly to the liquid or fluent solid material
    • G01F23/296—Acoustic waves
    • G01F23/2968—Transducers specially adapted for acoustic level indicators
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01F—MEASURING VOLUME, VOLUME FLOW, MASS FLOW OR LIQUID LEVEL; METERING BY VOLUME
    • G01F25/00—Testing or calibration of apparatus for measuring volume, volume flow or liquid level or for metering by volume
    • G01F25/0084—Testing or calibration of apparatus for measuring volume, volume flow or liquid level or for metering by volume for measuring volume
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01F—MEASURING VOLUME, VOLUME FLOW, MASS FLOW OR LIQUID LEVEL; METERING BY VOLUME
    • G01F25/00—Testing or calibration of apparatus for measuring volume, volume flow or liquid level or for metering by volume
    • G01F25/20—Testing or calibration of apparatus for measuring volume, volume flow or liquid level or for metering by volume of apparatus for measuring liquid level
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N29/00—Investigating or analysing materials by the use of ultrasonic, sonic or infrasonic waves; Visualisation of the interior of objects by transmitting ultrasonic or sonic waves through the object
    • G01N29/04—Analysing solids
    • G01N29/045—Analysing solids by imparting shocks to the workpiece and detecting the vibrations or the acoustic waves caused by the shocks
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N29/00—Investigating or analysing materials by the use of ultrasonic, sonic or infrasonic waves; Visualisation of the interior of objects by transmitting ultrasonic or sonic waves through the object
    • G01N29/04—Analysing solids
    • G01N29/12—Analysing solids by measuring frequency or resonance of acoustic waves
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N29/00—Investigating or analysing materials by the use of ultrasonic, sonic or infrasonic waves; Visualisation of the interior of objects by transmitting ultrasonic or sonic waves through the object
    • G01N29/14—Investigating or analysing materials by the use of ultrasonic, sonic or infrasonic waves; Visualisation of the interior of objects by transmitting ultrasonic or sonic waves through the object using acoustic emission techniques
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2291/00—Indexing codes associated with group G01N29/00
    • G01N2291/02—Indexing codes associated with the analysed material
    • G01N2291/023—Solids
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2291/00—Indexing codes associated with group G01N29/00
    • G01N2291/02—Indexing codes associated with the analysed material
    • G01N2291/023—Solids
    • G01N2291/0234—Metals, e.g. steel
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2291/00—Indexing codes associated with group G01N29/00
    • G01N2291/02—Indexing codes associated with the analysed material
    • G01N2291/028—Material parameters
    • G01N2291/02836—Flow rate, liquid level
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2291/00—Indexing codes associated with group G01N29/00
    • G01N2291/02—Indexing codes associated with the analysed material
    • G01N2291/028—Material parameters
    • G01N2291/0289—Internal structure, e.g. defects, grain size, texture
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2291/00—Indexing codes associated with group G01N29/00
    • G01N2291/26—Scanned objects
    • G01N2291/269—Various geometry objects
    • G01N2291/2695—Bottles, containers

Definitions

  • the present invention is directed to a system for measuring the fill level of gas inside a cylinder and corresponding method of use and method calibration.
  • a mobile gas vessel such as a gas cylinder
  • under-pressure liquefied gas has been to weigh the full cylinder and subtract the pre-measured weight of the cylinder when it was empty (tare weight).
  • tare weight the pre-measured weight of the cylinder when it was empty.
  • the weight could be miscalculated as any cylinder fixation would impact upon the measured weight.
  • Each connection and disconnection of the cylinder is an additional task involved in the measuring process and will allow an amount of gas to be lost to the atmosphere.
  • Some systems do allow a cylinder with connected piping to be weighed. However, this means that the tare weight of the cylinder must also be determined in an identical configuration. This can be altered by any remaining pressure or tension in the connection pipes which still leads to erroneous results.
  • the content of permanent gasses in gas vessels has typically been measured by using a pressure sensor.
  • a temperature sensor can also be included to account for the effect of temperature of the gas on the exerted pressure.
  • Each of these sensors requires a direct media contact to the pressurised gas. Accordingly, they will need to be inserted into the cylinder which introduces an additional step and allows for potential losses.
  • the materials used in the sensor must also be carefully selected to ensure that they are compatible with the gas within the cylinder. Furthermore, it is not possible to measure the remaining content in a gas vessel filled with under pressure liquefied gasses simply by measuring the pressure in this manner.
  • the head-pressure in such a cylinder is
  • a system for measuring the fill level of gas inside a cylinder according to the present invention is provided according to claim 1.
  • This system allows the fill level to be reliably measured without having to insert any probes into physical contact with the vessel’s contents.
  • the system can also be used in-situ with a gas cylinder.
  • the system can operate remotely without the need for an operator to physically access the system.
  • the computer readable storage medium may further include data representative of a second response from the cylinder to an acoustic impact when the cylinder is at a second fill level, different to the first fill level; and the processor may be further configured to:
  • the first fill level may be between 0% and 10%.
  • the first fill level may be between 0% and 10%; and the second fill level may be between 90% and 100%.
  • a method for measuring the fill level of gas inside a cylinder according to the present invention is provided according to claim 5.
  • the system can also be used in-situ with a gas cylinder.
  • the system can operate remotely without the need for an operator to physically access the system.
  • the method may further comprise the steps of: comparing the response to a second stored response at a second fill level; and determining the fill level of the cylinder based upon the comparison.
  • the first fill level may be between 0% and 10%.
  • the first fill level may be between 0% and 10%; and the second fill level may be between 90% and 100%.
  • a method of calibrating a system for measuring the fill level of gas inside a cylinder according to the present invention is provided according to claim 9.
  • the first fill level may be between 0% and 10%; and the second fill level may be between 90% and 100%.
  • a method of detecting defects in a cylinder according to the present invention is provided according to claim 11. This method allows defects in the cylinder to be remotely detected without requiring inspection of the cylinder. The defects are also detected without requiring any physical contact between a sensor and the contents of the cylinder.
  • Figure 1 shows a schematic cross-section of a system according to the present invention.
  • Figure 1 shows a system 100 for measuring the fill level of gas inside a cylinder 200. While the present invention is described with respect to a cylinder 200, this is merely exemplary and the gas container could be any shape.
  • the gas is preferably an under- pressure liquefied gas or a permanent gas.
  • the system 100 comprises an impactor 12 which is in physical contact with an outer surface of the cylinder 200.
  • the impactor 12 may be arranged to physically strike the cylinder 200. Alternatively, the impactor 12 may use some other method to generate vibrations in the cylinder 200.
  • the impactor 12 may be an actuator, in particular a piezoelectric actuator, a solenoid actuator, a spring powered actuator or a simple mechanical (hammer) actuator.
  • the impactor 12 is configured to apply an acoustic impact to the cylinder 200. This acoustic impact will travel through the cylinder 200 and the characteristics thereof will be determined by the fill level of the cylinder 200.
  • a sensor 14 is further provided in communication with an outer surface of the cylinder 200.
  • the sensor 14 may be any suitable sensor which is capable of determining the response of the cylinder 200 to the acoustic impact.
  • the sensor 14 may be a vibrometer or microphone. As the acoustic impact travels through the cylinder 200 a response thereto will be generated by the cylinder 200. This sensor 14 is configured to detect this response and generate a signal indicative thereof.
  • the signal generated by the sensor 14 is transmitted to a processor 16.
  • the processor 16 is further in communication with a computer readable storage medium 18.
  • the computer readable storage medium 18 may be provided locally in proximity to the cylinder 200.
  • the computer readable storage medium may be a remote system which can be accessed by the system 100, such as via the internet (the“Cloud”).
  • the computer readable storage medium 18 includes data representative of at least a first response from the cylinder 200 to an acoustic impact when a cylinder 200 is at a first fill level Fi.
  • the processor 16 compares the received signal from the sensor 14 to the first response and based upon this comparison determines the fill level of the cylinder 200.
  • the number of responses stored in the computer readable storage medium 18 that the processor 16 is configured to determine the fill level depends upon the accuracy required. For simple operations, it may be sufficient to have a single stored response and the processor 16 simply configured to determine whether the contact fill level Fc is higher or lower than the fill level F, for this stored response. In particular, this fill level F, could be between 40% and 60%. In preferred embodiments this fill level F, may be approximately 50%. Accordingly, the processor 16 would be able to determine whether the cylinder 200 is above or below half-full. In further embodiments, this first fill level F, could be set at a lower bound, such as between 0 to 20%, in order to warn the user that the cylinder 200 is substantially empty and near replacement.
  • the computer readable storage medium 18 includes first and second responses from the cylinder to an acoustic impact when the cylinder is at first and second fill levels Fi, F 2 being different to one another.
  • the first and second fill levels Fi, F 2 may be selected to generally correspond to a full state of the cylinder 200 and an empty state of the cylinder 200 respectively. While it may not be possible to completely empty or completely fill the cylinder it is appreciated that within 10% thereof may be suitable for the present invention.
  • the processor 12 may extrapolate a reference for the entire range of fill-levels that the detected signal can be compared to. This allows the current fill level Fc of the cylinder 200 to be generally known at any level.
  • a calibration method may need to be carried out on the cylinder 200.
  • the cylinder 200 when empty can have the acoustic impact applied by the impactor 12 and the response detected by the sensor 14.
  • This response is then stored in the computer readable storage medium 18 (whether locally or remotely, as discussed above).
  • the cylinder 200 is then filled with the relevant gas and the impactor 12 applies a second acoustic impact to the now full cylinder 200. Again, the response thereto is detected by the sensor 14 and stored in the computer readable storage medium 18.
  • the system 100 is then configured to determine the current fill-level Fc of the cylinder 200. This configuration needs to be done only once for each combination of cylinder 200 and fill-gas.
  • the system 100 may then further comprise an input for the user to select which pre-stored calibration they desire without the need to locally re-calibrate.
  • the system 100 may further include a transmitter which is configured to send a signal when the cylinder 200 reaches a pre-determined low level.
  • This signal may be for example a warning signal which could be sent to a user’s device such as a smart phone.
  • the signal could automatically trigger an order for a replacement cylinder to be delivered.
  • the signal can be sent via any known transmission method with an appropriate transmitter selected. This includes, but is not limited to, via Bluetooth (RTM) and/or the internet.
  • RTM Bluetooth
  • a further use of the system 100 may be to detect damage in the cylinder 200 (cracks, corrosion, etc.).
  • the response of the cylinder 200 to the acoustic impact can be compared to a response at a known pressure stored on the computer readable storage medium 18 (whether locally or remotely, as discussed above).
  • the differences between the response of the cylinder 200 and the stored response can then be analysed in order to determine any defects in the cylinder 200. For example, cracks or corrosion may cause a reflection of the response to be generated, which can be detected.
  • the comparison may, in particular embodiments, take the form of a comparison of the acoustic spectrum of the responses.
  • system 100 depicted in the Figures is shown generally in the valve region of the cylinder 200 this is not necessarily the case.
  • the system 100 could be provided at any point on the cylinder 200. This may be in the form of a further attachable component which attaches to the cylinder. However, it is convenient if the system can be incorporated into the valve as there may already be further use for components therein.

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  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Fluid Mechanics (AREA)
  • Acoustics & Sound (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Electromagnetism (AREA)
  • Thermal Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Filling Or Discharging Of Gas Storage Vessels (AREA)

Abstract

L'invention concerne un système de mesure du niveau de remplissage de gaz à l'intérieur d'un cylindre. Le système comprend un impacteur conçu pour appliquer un impact acoustique à un cylindre ; un capteur conçu pour détecter une réponse provenant du cylindre à l'impact acoustique et générer un signal indiquant ce dernier ; et un support d'informations lisible par ordinateur comprenant des données représentant une première réponse provenant du cylindre à un impact acoustique lorsque le cylindre est à un premier niveau de remplissage. Un processeur en communication avec le capteur et le support d'informations lisible par ordinateur est conçu pour : recevoir le signal en provenance du capteur ; comparer le signal aux données représentant la première réponse ; et déterminer un niveau de remplissage du cylindre en fonction de ladite comparaison.
PCT/EP2019/069384 2018-08-16 2019-07-18 Système et procédé de mesure du niveau de remplissage d'un gaz dans un cylindre, procédé d'étalonnage dudit système et procédé de détection de défauts WO2020035256A1 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GB1813406.4 2018-08-16
GB1813406.4A GB2576361A (en) 2018-08-16 2018-08-16 A system

Publications (1)

Publication Number Publication Date
WO2020035256A1 true WO2020035256A1 (fr) 2020-02-20

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Country Status (2)

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WO (1) WO2020035256A1 (fr)

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US20060021448A1 (en) * 2001-06-22 2006-02-02 Young Manufacturing & Engineering, Inc. Acoustic volume indicator
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US20130263657A1 (en) * 2012-04-09 2013-10-10 Ferrellgas, L.P. d/b/a Blue Rhino Apparatus and method for determining the liquid level in an un-modified tank
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