WO2019100812A1 - 气体突破压力测试装置及方法 - Google Patents
气体突破压力测试装置及方法 Download PDFInfo
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- WO2019100812A1 WO2019100812A1 PCT/CN2018/104638 CN2018104638W WO2019100812A1 WO 2019100812 A1 WO2019100812 A1 WO 2019100812A1 CN 2018104638 W CN2018104638 W CN 2018104638W WO 2019100812 A1 WO2019100812 A1 WO 2019100812A1
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- Prior art keywords
- gas
- sample
- cylinder
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- testing device
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- 238000012360 testing method Methods 0.000 title claims abstract description 47
- 238000000034 method Methods 0.000 title description 5
- 238000007789 sealing Methods 0.000 claims abstract description 45
- 238000012806 monitoring device Methods 0.000 claims abstract description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 10
- 230000005540 biological transmission Effects 0.000 claims description 5
- 238000003825 pressing Methods 0.000 claims description 3
- 238000010998 test method Methods 0.000 claims description 2
- 239000002927 high level radioactive waste Substances 0.000 abstract description 10
- 239000007789 gas Substances 0.000 description 52
- 239000000440 bentonite Substances 0.000 description 7
- 229910000278 bentonite Inorganic materials 0.000 description 7
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 description 7
- 239000000463 material Substances 0.000 description 6
- 239000011435 rock Substances 0.000 description 6
- 238000010521 absorption reaction Methods 0.000 description 5
- 230000004888 barrier function Effects 0.000 description 5
- 239000002699 waste material Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000003673 groundwater Substances 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 238000012544 monitoring process Methods 0.000 description 2
- 229910000851 Alloy steel Inorganic materials 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000009375 geological disposal Methods 0.000 description 1
- 239000010438 granite Substances 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 230000002522 swelling effect Effects 0.000 description 1
- 238000013022 venting Methods 0.000 description 1
Images
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01L—MEASURING FORCE, STRESS, TORQUE, WORK, MECHANICAL POWER, MECHANICAL EFFICIENCY, OR FLUID PRESSURE
- G01L13/00—Devices or apparatus for measuring differences of two or more fluid pressure values
Definitions
- the invention relates to the technical field of high-level waste disposal, and particularly relates to a device and a method for testing a gas breakthrough pressure of a buffer material in a high-level waste disposal repository.
- the repository is often referred to as the “high-level waste geological repository”, hereinafter referred to as the “repository”.
- the design concept of the repository is generally a “multi-barrier system”, including a surrounding rock geological barrier, an artificial barrier based on bentonite as a buffer material, and a waste storage container barrier.
- the glass-cured high-level waste is packaged in a special container made of a highly corrosion-resistant high-grade alloy steel or copper; when disposed, the cured container is filled with a bentonite material with good adsorption properties. This constitutes a multi-channel "artificial barrier”; in addition, there is an excellent "natural barrier”.
- the high-level waste repository is built in a stable geological layer (such as granite, clay rock, salt rock, etc.) that is several hundred meters deep underground.
- gases will gradually be produced in the repository due to complex physical and chemical reactions. These gases come from the following aspects: (1) hydrogen produced by metal cans in the bentonite and groundwater environment; (2) The decomposition of microorganisms causes the carbon dioxide, methane, nitrogen and other gases generated by the decay of organic matter; (3) the hydrogen produced by the radiation. With the continuous generation of these gases, the air pressure in the repository gradually increases, and the accumulated gas will escape to the outside. For the gas breakthrough pressure test, it is usually carried out in a three-axis pressure chamber, but due to the sample and device. There is a relatively smooth contact surface between them, which leads to inaccurate measurement results.
- the present invention provides a gas breakthrough pressure testing device comprising a cylinder for holding a sample, the inner wall of the cylinder is formed with a sealing section, and the sealing section is provided for a sample having expansion property. After water absorption, the sample expands and blocks the sealing section to achieve sealing, so that the sample and the cylinder are no longer smooth contact surfaces in the vertical direction, avoiding gas breakthrough from the interface between the sample and the cylinder, effectively improving The gas breaks through the accuracy of the stress test results.
- the gas breakthrough pressure testing device comprises a cylinder body for holding a sample, the cylinder body has an air inlet end at one end and an air outlet end at the other end, and the air inlet device is connected to the air inlet end.
- a gas monitoring device is connected to the gas outlet end, and an inner wall of the cylinder body is formed with a sealing section. During testing, the sample is in close contact with the inner wall of the cylinder to seal.
- the inlet end of the cylinder body is detachably and fixedly connected with a pressure head, and the pressure head is formed with an air inlet hole, and the air inlet hole is connected to the gas transmission device;
- the air outlet end of the cylinder body is detachably and fixedly connected a base, the base is formed with an air outlet, the air outlet is connected to the gas monitoring device;
- the cylinder is internally formed with a hollow cavity, the sample is contained in the hollow cavity, and the sealing section is formed in the cylinder and the test On the inner wall of the sample.
- the sealing section height H t is related to the sample height H sample , the cylinder inner diameter D t and the sample diameter D sample as follows:
- the sealing segments are a plurality of sets of grooves uniformly distributed along the axial direction of the cylinder block, and each set of grooves is arranged or segmented along the inner wall of the cylinder.
- each of the grooves has a depth of 0.3 mm and a width of 1 mm, and a spacing between adjacent sets of grooves is 4 mm.
- the indenter and the base are respectively formed with protrusions, and the protrusions are embedded in the cavity in the cylinder.
- a gas breakthrough pressure testing method adopts the above testing device, the testing device comprises a cylinder body, a pressing head and a base, wherein the cylinder body is internally formed with a hollow cavity, and the sample is contained in the hollow cavity, and the cylinder body and the test a sealing section is formed on the inner wall of the sample contact, an air inlet hole is formed on the pressure head, and an air outlet hole is formed on the base;
- the test method includes the following steps:
- Step 1 Place the prepared sample into the sealing section of the cavity in the cylinder.
- Step 2 Increase the humidity of the test space, and the sample absorbs water and expands to block the sealing section until it is sealed.
- Step 3 The indenter and the base are respectively fixed to the air inlet end and the air outlet end of the cylinder body by bolts, and the air inlet hole formed on the pressure head is connected with the gas conveying device, and the air outlet hole formed on the base is connected with the gas monitoring device.
- Step 4 Gradually increase the gas pressure of the air inlet from 0. When the continuous air flow is detected at the air outlet of the base, the pressure difference between the two ends is the gas breakthrough pressure of the sample.
- the test space temperature is 20 °C.
- the advantages of the device disclosed in the present invention for testing the breakthrough pressure of the buffer material of the high-level waste disposal repository are:
- the gas breakthrough pressure testing device disclosed in the present invention comprises a cylinder body containing a sample, the inner wall of the cylinder body is formed with a sealing section, and a sealing section is processed on the inner wall of the cylinder body, so that for the sample having swelling property, After water absorption, the sample expands and blocks the sealing section to achieve sealing, so that the sample and the cylinder are no longer smooth contact surfaces in the vertical direction, avoiding gas breakthrough from the interface between the sample and the cylinder, effectively improving the gas. Break the accuracy of the stress test results.
- Fig. 1 is a cross-sectional view 1 of the first embodiment.
- Figure 2 is a cross-sectional view 2 of the first embodiment.
- Figure 3 is a cross-sectional view 1 of the second embodiment.
- Figure 4 is a cross-sectional view 2 of Embodiment 2
- FIGS. 1 - 4 illustrate a preferred embodiment of the present invention, which are detailed in a detailed view of the structure.
- the gas breakthrough pressure testing device shown in FIG. 1-2 includes a cylinder 6 for containing the sample 5.
- the cylinder 6 has an intake end at one end and an air outlet at the other end, and a gas delivery device is connected to the intake end.
- the gas monitoring device is connected to the end, and the inner wall of the cylinder body 6 is formed with a sealing section, and the structure of the sealing section is not limited.
- the gas delivery device may be an inert gas
- the gas monitoring device may be a gas leak detector or a flow meter. Gas monitoring is performed at different time intervals when using a gas leak detector, and when the gas continuously overflows, the gas is continuously broken. When using a flow meter for gas monitoring, when the detected gas flow suddenly increases, it can be determined that the gas continues to break through.
- the inlet end of the cylinder 6 is bolted to the indenter 1 , and the indenter 1 is formed with an air inlet 9 , and the air inlet 9 is connected to the gas transmission device; the outlet end of the cylinder 6 is bolted to the base 8 , and the base 8 is mounted on the base 8 An air outlet 7 is formed, and the air outlet 7 is connected to the gas monitoring device.
- the cylinder 6 is internally formed with a hollow cavity 10, and the sample 5 is contained in the hollow cavity 10.
- the sealing section is formed on the inner wall of the cylinder 6 which is in contact with the sample 5.
- the sample 5 absorbs water and expands to block the sealing section for sealing.
- the arrangement of the ram 1 and the base 8 makes the sealing effect of the cylinder 6 better, and the connection manner of the cylinder 6 with the ram 1 and the bottom 8 is not limited, and the bolting is only a preferred embodiment.
- the height of the sealing section 5 and the sample height H t H sample, 6 the inner diameter of the cylinder diameter D t D sample and the sample 5 has the following relationship:
- sealing segments are a plurality of sets of grooves 4 uniformly distributed along the axial direction of the cylinder block 6, and each set of the grooves 4 is disposed or segmented along the inner wall of the cylinder block 6.
- each of the grooves 4 has a depth of 0.3 mm and a width of 1 mm, and the interval between the adjacent two sets of grooves 4 is 4 mm.
- the gas breakthrough pressure testing device shown in Figures 3-4 is the same as in Embodiment 1, except that:
- the ram 1 and the base 8 are respectively formed with projections 3 which are embedded in the cavity 10 in the cylinder 6.
- the protrusion 3 is used together with the indenter 1 and the base 8 to facilitate the installation of the sealing ring, so that the sealing effect of the whole device is better.
- the gas breakthrough pressure testing device disclosed in the present invention processes a sealing section on the inner wall of the cylinder block 6.
- the sample 5 having expansion property, after the water absorption, the sample 5 expands and blocks the sealing section to achieve sealing, thereby making the sample 5 and the cylinder 6 is no longer a smooth contact surface in the vertical direction, avoiding gas breakthrough from the interface between the sample 5 and the cylinder 6, effectively improving the accuracy of the gas breakthrough stress test result.
- the present invention also provides a gas breakthrough pressure testing method, which is implemented by using the device of the above embodiment, and the testing method comprises the following steps:
- Step 1 Place the prepared sample 5 into the sealing section of the cavity 10 in the cylinder 6.
- Step 2 Increase the humidity of the test space, and sample 5 expands to block the seal section until it is sealed.
- Step 3 The indenter 1 and the base 8 are respectively fixed to the intake end and the outlet end of the cylinder 6 by bolts 2.
- the air inlet 9 formed on the indenter 1 is connected with the gas transmission device, and the air outlet formed on the base 8 is formed. 7 Connect to the gas monitoring device.
- Step 4 Gradually increase the gas pressure of the air inlet hole 9 from 0.
- the pressure difference between the two ends is the gas breakthrough pressure of the sample.
- test space temperature was 20 °C.
- the gas breakthrough pressure testing device disclosed in the present invention comprises a cylinder body for holding a sample, the inner wall of the cylinder body is formed with a sealing section, and the sealing section is processed on the inner wall of the cylinder body, so that the sample having the expansion property is In the case of water absorption, the sample expands and blocks the sealing section to achieve sealing, so that the sample and the cylinder are no longer smooth contact surfaces in the vertical direction, thereby avoiding gas breakthrough from the interface between the sample and the cylinder. Effectively improve the accuracy of gas breakthrough stress test results.
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- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Sampling And Sample Adjustment (AREA)
- Measuring Fluid Pressure (AREA)
- Testing Resistance To Weather, Investigating Materials By Mechanical Methods (AREA)
- Filling Or Discharging Of Gas Storage Vessels (AREA)
Abstract
Description
Claims (8)
- 一种气体突破压力测试装置,其特征在于,包括用以盛装试样(5)的缸体(6),所述缸体(6)一端为进气端,另一端为出气端,所述进气端连接有输气装置,所述出气端连接有气体监测装置,所述缸体(6)的内壁成型有密封段,测试时,试样(5)与所述缸体(6)内壁间紧密接触以密封。
- 根据权利要求1所述的气体突破压力测试装置,其特征在于,所述缸体(6)进气端可拆卸固定连接有压头(1),所述压头(1)上成型有进气孔(9),所述进气孔(9)连接输气装置;所述缸体(6)出气端可拆卸固定连接有底座(8),所述底座(8)上成型有出气孔(7),所述出气孔(7)连接气体监测装置;所述缸体(6)内部成型有中空腔(10),所述试样(5)盛装于中空腔(10)内,所述密封段成型于缸体(6)与试样(5)接触的内壁上。
- 根据权利要求3所述的气体突破压力测试装置,其特征在于,所述密封段为沿缸体(6)的轴向均匀分布的多组凹槽(4),每组凹槽(4)沿缸体(6)内壁一周设置或分段设置。
- 根据权利要求4所述的气体突破压力测试装置,其特征在于,每一所述凹槽(4)的深度为0.3mm,宽度为1mm,相邻两组凹槽(4)之间的间距为4mm。
- 根据权利要求5所述的气体突破压力测试装置,其特征在于,所述压头(1)与底座(8)分别成型有凸出部(3),所述凸出部(3)嵌入缸体(6)中空腔(10)内。
- 一种气体突破压力测试方法,其特征在于,采用权利要求1-6任一项所述的测试装置,所述测试装置包括缸体(6)、压头(1)和底座(8),所述缸体(6)内部成型有中空腔(10),试样盛装于中空腔(10)内,所述缸体(6)与试样(5)接触的内壁上成型有密封段,所述压头(1)上成型有进气孔(9),底座(8)上成型有出气孔(7);所述测试方法包括以下步骤:步骤一:将制作好的试样(5)放入缸体(6)中空腔(10)内密封段处;步骤二:增加测试空间的湿度,试样(5)吸水膨胀堵塞密封段,直至密封;步骤三:将压头(1)与底座(8)通过螺栓(2)分别固定在缸体的进气端与出气端,压头(1)上成型的进气孔(9)与输气装置连接,底座(8)上成型的出气孔(7)与气体监测装置连接;步骤四:从0开始逐渐增加进气孔(9)的气体压力,待底座(8)出气孔(7)处监测到持续的气流时,则进气孔(9)与出气孔(7)的气体压力差即为试样(5)的气体突破压力。
- 根据权利要求7所述的气体突破压力测试方法,其特征在于,测试空间温度为20℃。
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
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RU2019118231A RU2723232C1 (ru) | 2017-11-23 | 2018-09-07 | Устройство и способ экспериментального определения давления прорыва газа |
AU2018372341A AU2018372341B2 (en) | 2017-11-23 | 2018-09-07 | Gas escape pressure testing device and method |
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CN201711182357.6A CN108168768B (zh) | 2017-11-23 | 2017-11-23 | 气体突破压力测试装置及方法 |
CN201711182357.6 | 2017-11-23 |
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AU (1) | AU2018372341B2 (zh) |
RU (1) | RU2723232C1 (zh) |
WO (1) | WO2019100812A1 (zh) |
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CN110132746A (zh) * | 2019-06-19 | 2019-08-16 | 四川大学 | 三轴测试仪进行地质断层力学行为的室内实验模拟装置及方法 |
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CN108168768B (zh) * | 2017-11-23 | 2019-03-01 | 中国矿业大学 | 气体突破压力测试装置及方法 |
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RU2723232C1 (ru) | 2020-06-09 |
CN108168768B (zh) | 2019-03-01 |
CN108168768A (zh) | 2018-06-15 |
AU2018372341A1 (en) | 2019-06-27 |
AU2018372341A2 (en) | 2019-07-25 |
AU2018372341B2 (en) | 2020-10-15 |
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