WO2018078199A1

WO2018078199A1 - Method and apparatus for producing the protein, dhp, from the blood of animals for slaughter

Info

Publication number: WO2018078199A1
Application number: PCT/ES2017/070695
Authority: WO
Inventors: Jose Luis Florido Rodriguez
Original assignee: Keratin España, S.L.
Priority date: 2016-10-26
Filing date: 2017-10-19
Publication date: 2018-05-03
Also published as: ES2665786R2; ES2665786B1; DE112017002444T5; ES2665786A2

Abstract

The invention relates to a method and apparatus for producing the decolourised hydrolysed blood protein (DHP) from the blood of animals for slaughter, for which an integral industrial treatment is carried out on said blood, which is stabilised from the point of collection or slaughter, forming a mixture of said blood with water in a single closed reactor, in which hydrochloric acid, sodium hydroxide and hydrogen peroxide are also added, measuring the pH in order to stabilise the mixture, recirculating said mixture with a colloid mill which can be controlled to finally forward said mixture to a pressure tank, prior to the steps of washing and filtering the product in a centrifugal pump, and the subsequent dehydration, milling, cooling and packaging in the dryer, and having integral computer control of both the measurements of pH and oxygen, as well as of the remaining variables necessary for the correct reactions and behaviour of the mixture.

Description

PROCEDURE AND EQUIPMENT FOR

OBTAINING PROTEIN P.H.D. FROM THE

BLOOD OF SUPPLY ANIMALS

DESCRIPTION

Procedure and equipment for obtaining the P.H.D. from the blood of supply animals.

OBJECT OF THE INVENTION The present specification defines a procedure and the equipment required to obtain the Hydrolyzed and Discolored Protein of the Blood P.H.D. from the blood of food animals. For this, an integral industrial treatment of said blood is carried out from the point of collection and storage until obtaining said protein with optimal levels of quality through a series of stages that require a small number of elements and equipment that make This procedure increases production compared to existing processes and allows the production costs to be much lower.

This invention aims to be applied within the biological elements treatment industry and specifically in the industrial sector of equipment and treatment of blood from slaughter centers for supply animals for later use.

BACKGROUND It is known in the industrial sector related to the use of blood from animals the problem existing in the different steps of its treatment. For example, the problem of achieving stability, sterility, and preservation of blood at the point of collection is raised; in the treatment of sterility it should be noted that the blood is susceptible to being contaminated with certain speed, so that stabilizing products are currently needed to protect for a while without determining said blood against contaminating elements, mainly during transport and storage; or the inconveniences related to the discoloration, since the strong and persistent pigmentation of the blood makes the final product difficult to use as an additive and therefore makes it difficult to commercialize. In this sense, the present invention defines an industrial process that improves conventional treatment systems consisting of a system of continuous collection of blood in the slaughterhouse, and the use of a hydrolyzing reactor and a settling system, all in ambient temperature conditions without the use of cold or heat.

In the face of these conventional systems, methodologies that improve said treatment will be heard, as defined in the ES8308478 registry that discloses a method of treatment of blood and other liquid products in which blood is treated with anticoagulant that slows coagulation , a compound of sulfur and oxygen, and a carbohydrate; or as defined in the EIS2154182 registry that discloses a procedure for the recovery and purification of blood from industrial slaughterhouses, especially globin, for which physical-chemical processes of extraction, precipitation and separation, which mainly highlights the addition of the aqueous solution of hemoglobin on acetone in such a way that precipitation of globin occurs. It should be noted that the present invention differs from this type of treatments in that it incorporates a differentiated physical-chemical treatment and in that it incorporates different stages of treatment in the collection and reception, separation, filtration, pasteurization, drying and final grinding for obtaining PHD protein under optimal conditions for later use.

It also highlights the ES2289937 record that differs from the previously defined procedures and that incorporates blood treatment stages from the collection to the final drying, but that is based on the separation of blood in both hemoglobin and plasma, and after the separation of blood requires at least one reactor for plasma, and another reactor for the treatment of hemoglobin, that is, a minimum of two reactors, and also is based on a differential treatment after obtaining the PHD protein, in all cases being open reactors. The present invention differs from said methodology in that it does not require the separation of the blood, does not require different open reactors, but requires a single closed and sealed main reactor, and therefore the rest of the process steps differ from the methodology defined in that previous record, such as in the processes of filtering, hydrolyzing, discoloration and dehydration; and the present invention incorporates automation in all steps of the process. In addition, it should be noted that the registration methodology £ 2289937 has the problem that due to the high amount of reactor equipment, the cost required to carry out a lot is very high given that there are many hours needed, in particular, to complete A lot from when it is loaded until the end of it, a total of about 30 hours must pass, an excessive time that reduces profitability. The present invention reduces the number of necessary equipment and reactors, thereby reducing the investment cost, as well as reducing the time required to obtain a batch of product, for which less than half of the amount is required. time of the previous history.

That is why it is considered that the present invention, which is described in detail below, constitutes an innovative solution that differs from the equipment and steps of any type of animal blood treatment methodology up to the known date and presents A solution with the PHD protein is obtained with optimal results for later use, there is a considerable increase in production by reducing process times, production costs are much lower, the necessary economic investment in machinery is reduced and the corresponding amortizations, reduce the risks of contamination when passing through a closed and hermetic circuit; Hydraulic environmental pollution is reduced at the slaughterhouse level by taking advantage of the blood that it now does not have; a raw material of high nutritional power and high digestibility is achieved for both people and animals; and the water consumption for the process is reduced, which is a sensible improvement from an environmental point of view. DESCRIPTION OF THE INVENTION

The present invention defines a process for obtaining the P.H.D. from the blood of supply animals, which is an automated procedure and is composed of the stages defined below. Prior to the definition of the procedure, it is stated that the present invention defines stages that require special equipment that can be located in any location. That is, these equipment for the development of the procedure can be located in the same industrial plant or slaughterhouse, or they can be located in a centralized way at a point or location that requires the transport of blood by tank trucks or remote pumping by conductions In any case, the blood of the animals to be treated needs to be stabilized with conventional reagents.

Additionally, it should be noted that the procedure is automated, for which everything is controlled by a program that manages the production plant, and that it has a set of pre-set parameters for the correct operation of the procedure. In this regard, it must be taken into account that the program regulates the entry or addition into the reactor of the amount of stabilized blood from the slaughterhouse; water, the amount of which is proportional to the entry of blood; dilute hydrochloric acid; sodium hydroxide; and hydrogen peroxide or hydrogen peroxide; just as there are detectors in the reactor for free oxygen, sulphite and pH content. At this point it is emphasized that the reactor is closed and hermetic, which is new in any type of blood treatment.

Once the blood is stabilized and ready to be treated, the rest of the stages required to obtain the P.H.D. They are as follows: - Storage in an initial deposit of blood obtained in the industrial plant or slaughterhouse of animals.

- A fixed amount of stabilized blood is loaded into the reactor from the initial reservoir. This reactor has the peculiarity of being closed and being airtight. The reactor is loaded from the initial tank by a connection pipe with a peristaltic pump. The entry of blood into the reactor by the action of the peristaltic pump is slow, so that the liquid slides on the vertical walls to prevent foaming or that the pump delivers the blood in the lower part of the ferrule together With ami return valve. - After the incorporation of the amount of blood stabilized with the reagent from the slaughterhouse, the same amount of water is added to the reactor, using the same system as for the blood, that is, it slides through the vertical walls of the reactor to avoid foaming or down the reactor. - After the incorporation of the same amount of water and blood into the reactor, the stirring blades of the reactor are activated and stirring of the mixture begins at low power and slow speed, 15 Hz maximum, to achieve a uniformity of the liquid Without foaming. At this point it is emphasized that the important thing about the mixture of blood and water is that foams are not formed, being really indifferent that water is introduced before blood, or vice versa. The important thing is that it is not necessary to previously separate the blood into hemoglobin and plasma, but in the reactor itself the water dilutes the hemoglobin membrane and the proloplasm is released.

- Without stopping the movement of the stirring blades, a dilute hydrochloric acid addition pump adds said acid until it reaches an acidic pH point at which the entire mass coagulates, at which point the acid addition automatically stops hydrochloric but stirring continues.

- The stirring blades continue to work and, then, a sodium hydroxide addition pump, slowly begins to incorporate this alkali until a less acidic pH is obtained that corresponds to the moment when the coagulated mass loses its high viscosity to move to a liquid state .

- Once this level of pIL is reached, the movement of the stirring blades is stopped for a short period to ensure that said pH value remains stable and does not have alterations that destabilize the concentration of hydrogenions The pH measurement is performed using a pH meter that reaches the bottom, which is where the mixture is located.

- Proven mass stability, a hydrogen peroxide or hydrogen peroxide application pump, adds this component to the top of the reactor mass so that it begins with its bleaching work. This addition is carried out with the stirring blades stopped.

- After a long time counted from the first addition of hydrogen peroxide, the same amount of hydrogen peroxide is incorporated again with the same system and methodology. In this way, the standby installation is maintained and in which only the oxidative action of oxygen on the blood hemoglobin and the variation of the pH of the reactor content can be observed, all monitored by the reactor detectors.

• After a few hours after oxidation begins, and in view of the data indicated in the detectors, a series of calculations are carried out to carry out the precise modifications to achieve maximum effectiveness in the discoloration and for this purpose the pll is modified with the addition of hydrochloric acid and / or hydrogen peroxide, to create the optimal working conditions.

- Once time passes, the pH is neutralized. To achieve neutralization, the equipment adds these components and starts and stops the stirring blades only to stabilize and neutralize the mixture as many times as necessary, until the time comes that the pH stabilizes at the point where it is has left after the last neutralization. In turn, the mixture is gradually neutralized because each time the pH value is raised, the work of the oxygen is put into operation, until it reaches a pH value of around 7.

- Λ Then, a colloid mill is put into operation, whose function is to make the colloid smaller so that the oxygen works harder and the neutralization process is secured and so that lumps are not produced. The process of driving the colloid mill is such that the discharge port of the reactor is opened and a mono pump that extracts product from the reactor starts, enters it into the entrance of the colloid mill, the colloid mill acts on the mixture, and it conducts it again through conduits to the interior of the reactor generating a closed circuit.

After a few minutes of circulating the mixture, the system calculates the pH values in the reactor and adds sodium hydroxide to correct the acidity that the product may have.

When the content of the reactor is considered to be a yellowish-colored mass of micronized appearance, a bypass valve is opened so that the product is led to a lung reservoir that has stirring blades in operation. Similarly, when the reactor is empty, the product remains, which are recovered along with those of the pipes and the colloid mill, are dragged, and are led to the lung tank so that the entire mixture is in said lung deposit

After the emptying, the reactor agitator is stopped, while the pump and the colloid mill remain in operation. With a network water hose, the reactor is washed internally, so that in a single operation, the drag of all the hydrolyzed particles to the lung tank is carried out. Then the reactor discharge mouth is closed, so that later the interior of the reactor is washed under pressure to remove any remaining solid matter that may have adhered to the walls. The washing waters, together with others resulting from the process, are taken to a storage tank to be subjected to a water recovery action. Once the cleaning operation is finished, a pneumatic activator closes the discharge mouth of the reactor, which ends the hydrolysis and discoloration phase, and the previous steps can be started again to load another new reactor with new raw material or stabilized blood from the industrial slaughterhouse of supply animals.

Once the blood has been subjected to the hydrolysis and decolorization phase, the resulting product in the form of a suspension of solid and liquid, which is in the lung tank agitating, is still treated since the possible bisulfite must still be oxidized That remains in the blood. - When the product is stabilized, the lung reservoir transmits a signal and the following steps are started:

* First, a low-speed centrifugal filter pump is loaded so that the solid is retained while the water is expelled. The maximum level of solids retained in the basket of the centrifugal filter pump is decided by a thickness gauge and when the maximum amount of cake has been achieved, said pump stops injecting hydrolyzate, and then, water is injected for washing network . The introduction of mains water is continued to extract and wash the contents until the salt detector indicates that these salts have been eliminated. At that time the inlet of the wash water is stopped and the filter centrifugal pump is automatically accelerated until it stops expelling water;

* Then the revolutions of the centrifugal filter pump descend to the discharge level and, then, a hydraulic blade descends inside the basket to release the product or compact cake, which falls into a hopper that is located at the bottom of the centrifugal filter pump; Y

* Finally, endless extraction collects the drained cake and moves it to a hopper designed to feed the dryer.

- The dryer receives the wet cake, which is dehydrated in a regular and continuous way.

- Started this drying process and after checking that the moisture of the fine product! It is adequate, 6% · 7% humidity maximum, and that the temperature does not exceed 40 * C, the product is sent to a feed hopper of the micronized mill where it is subjected to molding and cooling.

- The product or the P.H.D. Dehydrated and ground is collected at the exit of a pneumatic cyclone and there it is packaged under conditions that guarantee its perfect preservation in suitable containers.

An analysis of the final product obtained shows us values of:

This is a slightly yellowish product and with a semolina-like appearance of loose texture, as the aminogram achieved is excellent in general, tryptophan not being found to be a hydrolyzed product, and obtaining a molecular weight of the P.H.S. of about 366.50 Dalton.

The special and innovative equipment required for the development of the methodology previously described, and that at certain points has already been advanced, is:

1 A special reactor.

It is a closed and hermetic reactor, for the control of oxygen and the rest of the variables, preferably made of steel. The capacity is at least four times the volume of blood to be treated.

Said reactor has an inlet mouth with closure, an anchor-type stirrer at the bottom with extended ends upwards and inclined blades perpendicular to the axis and distributed in its height. The reduction motor has a frequency regulator for power regulation, preferably 30 rpm. and about 5 hp per 1,000 1 of blood. The shaft has a diameter preferably between 70mm and 100mm.

On the other hand, in the top cover, since the reactor is closed, it has a PII or pH meter, a nozzle for the entry of acid, a nozzle for the entry of alkali and a nozzle for the incorporation of hydrogen peroxide.

In the lower part there is an inlet for the blood load with a non-return valve, a sight glass in the ferrule to see the state of the product in reaction, an inlet in the upper part of the ferrule with a curve and a tube of discharge of the colloidal mill inside the reaction mass. It also has a lower discharge port, a mono-type pump, and following this pump a bypass so that the product goes to the colloid mill or to the lung tank that receives, maintains or feeds the centrifugal pump, filter me.

2. - An adjustable colloidal mill

As mentioned in the development of the methodology, the neutralization phase of the mixture undoes the blood mass and, the final result * is a manipulable product, of a blackish color with coarse particles. This product and its particle size, once the critical precipitation pH is regulated, hydrogen peroxide is added for discoloration, and you can see how there are many fine bleached particles while the thickest ones stand out for a dark color that is expensive to lose .

In order to solve this problem, a colloid mill with metal mills located at a controlled separation is used, which receives the product extracted from the pressure reactor. As a consequence of the friction between the strawberries, this mill reduces the particles to a particle size of less than 200 μ.

In the closed circuit generated from reactor to mill and to reactor again, after a short time, the whole genus is homogenized to a minimum particle size that the hydrogen peroxide oxidizes and discolors completely with great ease.

The final product is yellowish in an impalpable powder, and is referred to as P.H.D.

3. - A lung deposit.

Another equipment that facilitates the acceleration of the manufacturing process is the installation of a lung reservoir that, provided with low speed stirring blades, which allows to maintain a perfect suspension of the hydrolyzed and discolored product, as well as possible pH corrections. This tank has a mono type pump with a frequency inverter, which regulates the ideal feed flow to the centrifugal filter pump. In this way, while the filtering and dehydrating operation of the mixture is being carried out, the production of a new batch in the hydrolysis and oxidation reactor can be started having been empty and clean. With this it is possible to obtain a greater production and a lower cost per kg of commercial final product obtained is achieved.

4.- Computer control of the process.

All equipment is controlled and monitored by a computer control, whose main control is centered on the reactor.

A series of control equipment is available that assess the data that is produced, and transmit it at 4/20 mV to the computer center that controls the manufacturing process.

Different load cells are available, which are used to control the amount of ingredients that are introduced into the reactor to start the transformation process.

It also has a pH measuring electrode that is submerged in the liquid mass of the reactor, and sends the data obtained from existing pH and temperature to! transmitter of the equipment that ios shows on a control screen.

There is also an oxygen analyzer, which is another electrode that continuously measures the amount of free oxygen that is dispersed in the liquid mass and the measured data, as in the case of the pH meter, sends them to the transmitter that ios shows on the control screen.

A sulfyl detector is available, which is continually indicating how their content decreases as the reaction hours go by.

Additionally, there is a control of the water expelled by the centrifugal filter pump, which consists of a probe that transmits values in micro Siemens of the salt content of the water resulting from the washing phase, so that the washing of the cake is with the water pure. Load cells and an additional pH meter are available in the lung reservoir.

Finally, there is a computer program or software, which is introduced into the hard disk of the computer that controls the production plant, and that has a series of parameters that can be varied by the person authorized to access them, such as the quantity of blood to be loaded into a reactor, the amount of water to be added proportionally to the incoming blood or the amount of hydrogen peroxide to be added

Finally, and from an environmental point of view, it is worth noting the consumption of water used during the procedure. Specifically * it can be said that network water is used which is mixed with the stabilized blood itself from the slaughterhouse and with the different reagents previously described in the different stages of the procedure. Water is initially included in the reactor, hydrolysis occurs, then the discoloration, the colloidal phase of recirculation and pH stabilization is reached, for subsequent transfer and washing and filtering. At this time, dehydration, micronizing and packaging occur on the one hand, while on the other hand wastewater is produced after filtration and washing, said wastewater being passed through an active carbon column and an osmosis plant, producing brine on one side, and the water is taken to an evaporator with evaporated water being produced but reusable water is also obtained again throughout the process. Λ as an example, a slaughterhouse that collects about 5,000 l / day of blood requires 5,000 1 of water for the reaction; about 250 1 of water to dilute acids; 250 1 of gua to dilute alkalis; 250 1 of water to dilute the hydrogen peroxide; and about 7,000 1 of water for PHD washing; being a total of about 12,750 1. To them it is necessary to add about 4,000 1 of water contributed by the blood and about 950 1 of water to evaporate in the drying, that makes a total of water that arrives at the treatment plant of 16,750 1. The Salt content in these 16,750 1 of water to be purified has about 190 kg of sodium chloride and 90 kg of sodium sulfate, that is, a total of 280 kg of sodium salts. These 16,750 I of water to be treated treated in a reverse osmosis plant produce water until the rejected brines have a concentration of 35 grs / 1, which is equivalent to recovering daily as pure, osmotized water, without salts or other residues, 8,750 1 to incorporate to the head of the plant. The rest, 8,000 I containing a concentration of 35 grs / l can be dehydrated and recover the water if necessary and 280 kg of sodium salts are obtained which, dehydrated, can be compressed into blocks to be made available in extensive ruminant livestock . After this analysis, it can be seen that this procedure is very favorable from an environmental point of view.

In order to complete the description that is being made and in order to help a better understanding of the characteristics of the invention, a set of drawings is attached as an integral part thereof, where the following has been represented as an illustrative and non-limiting nature:

Figure 1 is a representation of the different equipment that allows obtaining the final product.

Figure 2 is a representation of the water cycle with the different phases and equipment of the procedure. Description of the drawings

Figure 1 shows the representation of the different equipment with which it is possible to develop the different steps, stages and phases of the process object of the invention. Specifically, and following the steps of the description, it can be observed that: - Stabilized blood (S) obtained in the industrial plant or slaughterhouse of animals is stored in the initial tank (1).

- The amount of stabilized blood (S) from the initial reservoir is loaded into the reactor (3)

(one). The blood load (S) is carried out by means of a connection pipe (21) with a peristaltic pump (2), with an inlet valve (22) at the reactor inlet (3). The entry of blood (S) into the reactor by the action of the peristaltic pump (2) is in slow mode.

- After the incorporation of the amount of blood (S) into the reactor (3), the same amount of water (A) is added to the reactor. For this the same system is used as for blood, that is, from the initial deposit (1) and by By means of the peristaltic pump (2) and the connecting pipe (21), water (A) is introduced into the reactor (3).

- After the incorporation of the same amount of water (Λ) and blood (S) into the reactor (3), the stirring blades (31) of the reactor are activated and stirring of the mixture begins at low power and slow speed , to achieve a uniformity of the liquid without the formation of lumps.

- Without stopping the movement of the stirring blades (31), the diluted hydrochloric acid addition pump (4) adds said acid in the reactor (3) until it reaches the acidic pH point to coagulate the entire mass, whose value is around 1, 5 to 3 as strong acid.

- The stirring blades (31) and then the sodium hydroxide addition pump (5) continue to operate. Slowly begin to incorporate this alkali in the reactor (3) until the pH level rises, to a value around 4.5 to 5.5, approaching neutrality. - Once the previous pH value is reached, the movement of the stirring blades (31) stops for a short period to verify that the pH remains stable. The pH measurement is carried out by means of a pH meter (32) that reaches the bottom of the reactor.

- Checked the stability time of the dough, the hydrogen peroxide application pump or hydrogen peroxide (6). add this component in the reactor (3) to begin the bleaching work, with the stirring blades (31) being stopped.

- After a prolonged time counted from the first addition of hydrogen peroxide, the same amount of hydrogen peroxide (6) is incorporated back into the reactor (3) with the same system and methodology. In this way the installation is kept on hold.

- After a few hours after the oxidation begins, and in view of the data indicated in the reactor detectors (3), a series of calculations are carried out to carry out the precise modifications to achieve maximum effectiveness in the decolorization and for this you must modify the pH with the addition of hydrochloric acid (4) and / or hydrogen peroxide (6), to create the optimal working conditions.

Once time passes and the pH is corrected and neutralized, the equipment adds these components and starts and stops the stirring blades (31) only to stabilize and neutralize the mixture as many times as necessary, so that the mixture is neutralized little by little until it reaches a pH value of around 7.

Λ then the colloid mill (7) is put into operation. The process of driving the colloid mill (7) is such that the discharge port (33) of the reactor is opened and a mono pump (34) that extracts product from the reactor starts, enters it into the inlet mouth (72) of the colloidal mill, the colloidal mill acts on the mixture, and this one conducts it again by means of conduits (71) to the interior of the reactor (3) generating a closed circuit.

After a few minutes of "circulating the mixture, the pH values in the reactor are calculated with the meter (32) and the compound necessary to correct the acidity that the product may have is added.

When the content of the reactor (3) is a yellowish-colored mass of micronized appearance, which is observed with a sight glass (35), the bypass valve (73) is opened so that the product is led to the lung reservoir ( 8) that the agitator (82) is running. Similarly, when the reactor (3) is empty, the product remains are carried away, which are recovered together with those of the pipes (71) and the colloid mill (7), and are driven and introduced through its mouth input (81) in said lung tank (8).

- After emptying, the stirring blades (31) of the reactor, the mono pump (34), the colloid mill (7) are stopped and the discharge mouth (33) of the reactor is closed, so that later all this is washed with mains water to drag solid matter remains that may have adhered to the walls. Again, the discharge port (33) of the reactor is opened and the colloidal mill (7) and the mono pump (34) are put into operation. These first wash waters They drag all remains of PHD solids that exist in the reactor, mono pump, colloid mill and conduits to the lung reservoir. Once this operation is finished, you can proceed to the deep cleaning of the equipment whose washing water is channeled to a treatment plant. Once the cleaning is finished, the previous steps can be started again to load another new reactor with new raw material or stabilized blood from the slaughterhouse of supply animals.

Once the blood (S) has been subjected to the hydrolysis and discoloration phase, the resulting product is in its entirety in the lung reservoir (8) with stirring until stabilization.

When the product is stabilized, the lung reservoir (8) transmits a signal and the following equipment is started: the centrifugal filter pump (9), a cake extraction and transport auger in an auger (93) and a mono pump (83) that feeds the centrifuge through the mouth (91). The centrifugal filter pump (9) is loaded at low speed so that the solid is retained while the reaction water is expelled; the introduction of mains water is continued to extract and wash the salt content; when the level of salts detected at the outlet of the wash water is low, the inlet of the wash water is stopped and the machine automatically accelerates until it stops expelling water; then the revolutions of the centrifugal filter pump descend to the discharge level and, then, a hydraulic blade descends inside that scratches to release the product or compact cake that falls into an internal hopper (92) that is located in the inner part of the centrifugal filter pump (9); and finally, the extraction auger (93) collects the drained cake and transfers it to a hopper (10) designed to feed the dryer (11) that continuously generates the final product.

£ 1 dryer (Π) receives the wet cake that is dehydrated in a regular and continuous way, where once the product is dehydrated, ground and cooled it is packaged under conditions that guarantee its perfect preservation in suitable containers. On the other hand, Figure 2 shows the representation of the water cycle with the different phases and equipment of the procedure, which is important from the environmental point of view. Specifically, it can be said that network water is used which is mixed with the stabilized blood itself from the slaughterhouse and with the different reagents previously described in the different stages of the process. Initially, both water (A) and blood (S) are included in the reactor (3), producing a mixture (I) without foaming, hydrochloric acid (4), sodium hydroxide (5) and hydrogen peroxide (5) are added. 6), so that the hydrolysis (II) takes place, then the discoloration (III), the colloidal phase of recirculation (IV) is reached with the mill (7) and of pH stabilization (V), for later transfer (VI) to the lung tank (8), washing and filtering (VII) in the centrifugal filter pump (9). At this time, dehydration (VIII), micronized (IX) and packaging (X) in the hopper (10) and dryer (11) occur on the one hand, while on the other hand wastewater (XI) is produced after filtration and washing (VI), said wastewater being passed through a column of active carbon (XII) and an osmosis plant (XIII), producing brine (XIV) on the one hand, and water taken to an evaporator (XV) with which produces evaporated water itself and reusable water (XVI) is also obtained again throughout the process.

Claims

1. Procedure for obtaining the PHD protein from the blood of supply animals, for which it is based on water (Λ) and stabilized blood (S) obtained in the industrial plant or slaughterhouse, which is characterized by: i) initially the same amount of blood (S) and water (A) is incorporated into a single reactor (3), both being introduced from an initial reservoir (1) by means of a peristaltic pump (2) and a connecting pipe (twenty-one); ti) stirring blades (31) located in the reactor (3) are actuated and stirring of the mixture begins to achieve uniformity of the liquid without foaming; iii) with the stirring blades (31) of the reactor (3) in motion, a dilute hydrochloric acid addition pump (4) adds said compound in the reactor (3), until it reaches an acid pH point around the environment. 1, 5 to 3; iv) following the blades (31) of the reactor (3) in operation, a sodium hydroxide addition pump (5) begins to slowly incorporate this alkali into the reactor (3); v) once a pH value in the environment of 4.5 to 5.5 is reached, the movement of the stirring pins (31) is stopped; vi) with the stirring blades stopped (31), a hydrogen peroxide application pump (6) adds this component to the reactor (3), repeating this action again; vii) after a few hours, the conditions of the mixture are checked and hydrochloric acid (4) and / or hydrogen peroxide (6) is incorporated, with stirring blades (31) being activated or stopped as necessary, until the mixture is corrects and neutralizes to a pH value of 7; viii) a colloid mill (7) is put into operation, for this a discharge port (33) of the reactor is opened and a mono pump (34) is started that Extract product from the reactor (3) by passing the product to said colloid mill (7), which after treating and reducing the size of the colloid, returns the product back to the inside of the reactor (3) by means of conduits (71) generating a closed circuit; ix) after a few minutes of being recirculating the mixture, the pH values in the reactor (3) are calculated and any of the above compounds necessary to correct the acidity of the mixture is added; x) when the reactor mixture (3) is neutralized and is a yellowish mass, a bypass valve (73) of the closed circuit is opened and the product is led to a lung reservoir (8) that has an agitator in operation (82), where the mixture stabilizes; xi) when the mixture in the lung tank (8) is fully stabilized, a signal is transmitted that starts a mono pump (83) that introduces the product through an inlet (91) into a centrifugal filter pump (9) continue, where the product is filtered and washed; xii) an auger (93) for extracting the centrifugal filter pump (9) takes the drained product cake to a hopper (10) designed to feed a dryer (11); and finally, xiii) in the dryer (11) the product is dehydrated in a regular and continuous manner, and the milled and cooled product is finally packaged.

2. Procedure for obtaining the P.H.D. from the blood of supply animals, according to the characteristics of claim 1, characterized in that the different pH measurements are made with a pH meter (32) that reaches the bottom of the reactor (3).

3. Method for obtaining the PHD protein from the blood of supply animals, according to the characteristics of claim 1, which is It is characterized in that when the mixture passes into the lung tank (8), the product residues found in the reactor walls (3), the pipes of the pipes (71) and in the colloid mill (7) are carried away.

4. Procedure for obtaining the P.H.D. from the blood of supply animals, according to the characteristics of claims 1 and 3, characterized in that after the emptying of the reactor (3) and colloid mill (7) the entire circuit and washing waters are removed and washed They are taken to a tank with active carbon column treatment and reverse osmosis for reuse.

5. Procedure for obtaining the P.H.D. from the blood of supply animals, according to the characteristics of claims 1, 3 and 4, characterized in that after the cleaning of the circuit the load of! reactor (3) with new stabilized blood (S) and water (A).

6. Equipment for carrying out the procedure for obtaining the PHD protein from the blood of supply animals, said equipment comprising an initial storage tank (1) for both stabilized blood (S) and! water (A) and the initial tank (1) being connected to a peristaltic pump (2), having a centrifugal filter pump (9) continuous before the final product reaches a dryer (11) with its feed hopper ( 10), and characterized in that it has a single reactor (3), which is closed and hermetic, and has stirring blades (31), a lower discharge port (33) and a mono pump (34) extraction; a colloidal mill (7) adjustable and closed; a closed circuit of recirculation pipes (71) between the reactor (3) and the colloid mill (7), as well as a bypass valve (73) that allows the passage to a lung reservoir (8); a closed lung tank (8) that has a stirrer (82), a pH meter and a mono-type pump (83) that has a frequency inverter that regulates the feed flow to the centrifugal filter pump (9); and a computer control with its hardware and software that controls and tnonitoriza the values and different actions required for the correct functioning of the different stages.

7. Equipment for carrying out the procedure for obtaining the P.H.D. from the blood of supply animals, according to the characteristics of claim 6, characterized in that the reactor (3) has a PH or pH meter, a nozzle for the entry of acid, a nozzle for the entry of alkali and a nozzle for the incorporation of hydrogen peroxide.

8. Equipment for carrying out the procedure for obtaining the P.H.D. from the blood of supply animals, according to the characteristics of claim 6, characterized in that the colloid mill (7) has metal drills.

9. Equipment for carrying out the procedure for obtaining the P.H.D. from the blood of supply animals, according to the characteristics of claim 6, characterized in that the computer control has an electrode control of the different load cells of the compounds necessary for reactions within the reactor, an electrode for the analysis of the data of the pH meter, an oxygen analyzer electrode, a sulphite detector and a probe measuring the salt content from the water expelled by the centrifugal pump.