WO2016155152A1 - Temperature-controllable double-gas channel spraying plate with the uniform gas spraying function - Google Patents

Temperature-controllable double-gas channel spraying plate with the uniform gas spraying function Download PDF

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Publication number
WO2016155152A1
WO2016155152A1 PCT/CN2015/084424 CN2015084424W WO2016155152A1 WO 2016155152 A1 WO2016155152 A1 WO 2016155152A1 CN 2015084424 W CN2015084424 W CN 2015084424W WO 2016155152 A1 WO2016155152 A1 WO 2016155152A1
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Prior art keywords
spray
plate
heat transfer
ring
temperature
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PCT/CN2015/084424
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French (fr)
Chinese (zh)
Inventor
吕光泉
吴凤丽
苏欣
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沈阳拓荆科技有限公司
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Publication of WO2016155152A1 publication Critical patent/WO2016155152A1/en

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    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/455Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for introducing gases into reaction chamber or for modifying gas flows in reaction chamber

Definitions

  • the invention relates to a spraying component used in a semiconductor device, in particular to a temperature-controlled double gas channel uniform jet shower plate, belonging to the technical field of semiconductor thin film deposition application and manufacturing.
  • the spray parts used in semiconductor equipment generally have densely arranged spray holes, and below the spray holes, heaters for heating wafers or other forms of film substrates, and spray nozzles of the spray parts The side is closest to the heater, and the heat radiation amount of the heater is the largest. If the liquid heat medium passage is disposed on the spray orifice side of the spray component, the cooling effect is optimal, but the densely arranged spray orifices limit The space required for friction welding or burying the pipeline forces the position of the liquid heat transfer medium passage away from the side of the spray orifice.
  • the spray member located at the upper end of the spray member that is forced to increase in volume away from the position of the near wafer or other form of the film substrate, when the spray member is located above the spray wafer or the proximity wafer or If the liquid heat transfer medium passage at the position of other forms of the film substrate is passed through the coolant, the cooling efficiency thereof is lowered. Even if the liquid heat transfer medium passage is disposed in the form of an interlayer on the side of the spray orifice closest to the heat source, the heat transfer effect is reduced by the liquid heat transfer medium forming a flow accumulation at the edge of the sandwich layer, if The heat absorbed by the spray component causes it to rise to near the melting point or even the melting point, which can cause the spray component to deform.
  • the main body of the spray component is loaded with a high-frequency voltage, so the method of forming a liquid heat transfer medium without friction welding and adopting a liquid heat transfer medium pipe which is different from the material of the spray component inside the spray component affects the spray component.
  • the electrical properties of the subject are the following.
  • the invention aims to solve the above problems, and mainly solves the side of the spray small hole existing in the structure of the existing spray component, that is, the heat source side is closest to the heat source side and the liquid heat transfer medium channel cannot be effectively approached due to space limitation.
  • the temperature is controllable by the heat transfer medium passage and the two gas independent flow passages disposed therein, and the two gases are isolated from each other inside the spray component to achieve temperature control and two gases. Process requirements for film deposition by switching supply or simultaneous supply and not mixing within the spray component.
  • the present invention adopts the following technical solution: a temperature-controlled dual gas passage uniform jet shower plate, wherein the spray plate is provided with two gas passages separated from each other and a serpentine liquid liquid with high heat transfer efficiency. Heat transfer medium passage.
  • the two isolated gas passages and one serpentine liquid heat transfer medium passage are combined by the spray upper plate, the diffusion baffle, the intake ring, the closed ring and the spray orifice plate included in the component. to make.
  • the spray upper plate has a circular plate shape, and an annular boss is arranged on the edge of the lower end surface, and a rectangular groove is formed on the end surface of the annular boss.
  • the intake positions of the two gas passages are respectively at the center and the edge of the spray upper plate, and the intake passage at the edge and the rectangular shape of the lower end surface of the spray upper plate
  • the slots are connected, and the intake passage at the center is a through hole at the center of the spray upper plate.
  • the plate-shaped spray orifice plate is formed by removing the material to form a gas-guiding column regularly distributed in the interlayer and the interlayer, and a through hole is drilled in the center of each gas guide column, and the gas guide column is arranged at the lower end surface of the spray hole plate.
  • the short groove should be combined with a row of long through holes drilled by the spray upper plate to drill the short groove and the spray upper plate. Some rows of long through holes combine to form a closed serpentine tube. a series of passages are provided in the circumferential direction of the upper end surface of the intake ring to avoid the position of the short groove .
  • the intake ring is welded to the spray orifice plate, and the closed loop converts the structure formed by the spray orifice plate and the intake ring into a two-channel gas path.
  • the spray upper plate welded with the diffusion baffle at the center is concentrically placed on the upper end of the sprayed orifice plate, the inlet ring and the closed ring to form a rectangular groove and the inlet at the edge of the lower end surface of the spray plate
  • a series of passages disposed at a position avoiding the position of the short groove in the circumferential direction of the upper end surface of the ring are communicated.
  • Two holes drilled in the end face of the spray upper plate respectively communicate with the head and tail of the serpentine pipe.
  • Each of the through holes in each of the air guide columns flows out of the shower member.
  • the second gas enters from the second gas inlet at the edge of the spray upper plate of the spray device, flows in a rectangular groove provided on the lower end surface of the spray plate, and passes through the upper end surface of the intake ring in the flow direction during the flow.
  • a series of passages are provided to avoid the position of the short groove and enter the interlayer of the spray orifice plate, and fill the spray part through the half through hole drilled between the gas guide columns while filling the interlayer space.
  • the two gases enter the reaction chamber simultaneously or in a switched manner depending on the process requirements.
  • the liquid heat transfer medium is introduced into the hole drilled in the end surface of the spray upper plate into the serpentine pipe and flows back and forth through the serpentine pipe and flows out of the spray component to reach a specific flow rate by the liquid heat transfer medium.
  • the specific structure the diffusion baffle is concentrically welded at the center of the spray upper plate, and the diffusion baffle and the spray upper plate constitute the first part.
  • the intake ring is welded to the spray orifice plate, so that the short groove opened by the intake ring and the long through hole drilled by the spray orifice plate are combined into a closed serpentine pipe, and the welded closed ring will be sprayed.
  • the structure formed with the intake ring is converted into a two-channel gas path.
  • the spray orifice plate, the intake ring and the closed ring constitute a second portion.
  • the two parts after welding are brazed together to form a cavity, and the spray upper plate is provided with an air inlet A, an air inlet B, a liquid path inlet C, a liquid path outlet D, an air inlet A and two parts.
  • the formed cavities are connected, and the inlet B communicates with the interlayer of the spray orifice
  • the invention utilizes the form of two parts welded to form a liquid heat transfer medium channel, and the position of the convection heat transfer is set on the side of the spray hole to maximize the heat transfer efficiency, and realize the simultaneous operation of the two gases under the controllable temperature condition.
  • the process requirements of entering the cavity or switching into the cavity for reaction reduce the volume of the spray component, improve the heat transfer efficiency, and ensure the reliability of the spray component.
  • Figure 1 is a front elevational view of a shower orifice of the present invention.
  • Fig. 2 is a perspective view of Fig. 1;
  • Figure 3 is a schematic view showing the structure of the intake ring of the present invention.
  • Fig. 4 is an enlarged view of E at Fig. 3.
  • Figure 5 is a schematic view showing the structure of a closed loop of the present invention.
  • Figure 6 is a schematic view of the structure of the present invention.
  • Fig. 7 is a cross-sectional view taken along line G-G of Fig. 6;
  • Fig. 8 is a cross-sectional view taken along line FF of Fig. 6;
  • Fig. 9 is a cross-sectional view taken along line H-H of Fig. 8;
  • the spray orifice plate 1 in the temperature-controlled dual gas passage uniform jet shower plate is in the form of a circular plate, and the inside of the interlayer is formed into a sandwich space 15 by using a material removal method.
  • a plurality of cylinders 3 are evenly arrayed, one through hole 4 is drilled in the center of each cylinder 3, and a uniform array of semi-through holes 5 is drilled in the lower layer of the interlayer space 15, in the upper layer of the interlayer space 15, parallel to the spray orifice plate 1
  • a row of long through holes 2 are drilled, and the long through holes 2 avoid the through holes 4.
  • the intake ring 6 has a circular ring shape, and the inner diameter of the intake ring 6 is the same as the outer diameter of the spray orifice plate 1.
  • the lower end surface of the intake ring 6 defines a circumferential groove 7, and on the inner side wall of the intake ring 6, a plurality of openings are opened.
  • the groove 8 is opened at a position avoiding the groove 8 to form a radial groove 9 with a radial direction of the intake ring 6 in the radial direction of the intake ring 6.
  • One end of each radial groove 9 is drilled through the hole 10, and the groove 8 of two special positions is selected. Two holes 11 communicating therewith are formed in the slots 8 of the two special positions.
  • the temperature-controlled dual gas channel uniform jet shower upper end is provided with four inlets, respectively, a central air inlet A, an edge air inlet B, a liquid heat transfer medium inlet C, and a liquid heat transfer medium.
  • the liquid heat transfer medium inlet C and outlet D are interchangeable.
  • the welding relationship of the temperature-controlled dual gas passage uniform jet shower plate is: the diffusion baffle 14 is concentrically welded at the center of the spray upper plate 13, so that the diffusion baffle 14 and the spray upper plate 13 form a first portion, which will enter
  • the gas ring 6 is sleeved on the outer ring of the spray orifice plate 1 and the upper end surface of the intake ring 6 is coplanar with the upper end surface of the spray orifice plate 1, and the intake ring 6 is rotated to open a plurality of inner side walls of the intake ring 6.
  • the slot 8 communicates with the long through hole 2 of the spray orifice plate, and converts the long through hole 2 into a serpentine pipe, and the serpentine pipe is formed by combining the intake ring 6 and the spray orifice plate 1 to form a snake.
  • the holes 11 respectively formed in the grooves 8 at the beginning and the end of the pipe are used as the inlet and outlet of the liquid heat medium passage.
  • the intake ring 6 and the spray orifice plate 1 are fixed in the above position, and friction welding is respectively performed on the upper and lower end faces to close the serpentine pipe, and the spray orifice plate 1 and the intake ring 6 form a second portion.
  • the first gas enters the temperature-controlled dual gas passage uniform jet shower plate from the air inlet A at the center of the spray upper plate 13, and is filled with the temperature-controlled double gas passage uniform jet spray through the diffusion baffle 14.
  • the inner cavity of the plate is sprayed through the through hole 4 of the spray orifice plate 1 to discharge the temperature-controlled double gas passage uniform jet shower plate into the reaction chamber.
  • the second gas enters from the edge inlet B of the spray upper plate 13 and passes through the radial groove 9 of the intake ring 6 and the through hole 10 drilled at one end of each radial groove 9 into the interlayer of the spray plate 1
  • the space 15 sprays the temperature-controlled dual gas passage uniform jet shower plate into the reaction chamber from the semi-through hole 5 below the sandwich space 15, and at the same time, the temperature control function of the temperature-controlled dual gas passage uniform jet shower plate It is realized by the liquid heat transfer medium which is introduced into the component: the liquid heat transfer medium is introduced from the outside to the liquid heat medium passage inlet C (or D) provided on the spray upper plate 13, and the heat transfer through the serpentine pipeline is sufficient
  • the utility model realizes the function of simultaneously introducing or switching the two gases of the temperature-controlled double gas passage uniform jet shower plate into the cavity and controlling the temperature of the spray component.

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  • Chemical & Material Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
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Abstract

A temperature-controllable double-gas channel spraying plate with the uniform gas spraying function is provided with two gas channels isolated from each other and a snake-like liquid heat transfer medium channel with high heat transfer efficiency in the interior of the spraying plate. The two isolated gas channels and the snake-like liquid heat transfer medium channel are formed by combining five parts of an upper spraying plate (13), a diffusion baffle (14), a gas inlet ring (6), a closed ring (12) and a spraying pore plate (1). Process requirements on simultaneous charging of two gases into cavities or switching of the cavities for reaction under controllable temperature conditions are met, the size of a spraying part is reduced, and the heat transfer efficiency is improved.

Description

控温型双气体通道均匀喷气喷淋板  Temperature-controlled dual gas channel uniform jet shower plate 技术领域Technical field
本发明涉及一种半导体设备采用的喷淋部件,具体地说是一种控温型双气体通道均匀喷气喷淋板,属于半导体薄膜沉积应用及制造技术领域。 The invention relates to a spraying component used in a semiconductor device, in particular to a temperature-controlled double gas channel uniform jet shower plate, belonging to the technical field of semiconductor thin film deposition application and manufacturing.
背景技术Background technique
现有的半导体薄膜沉积设备,在工艺过程中,往往需要在特定的温度场内且两种或多种气体同时通入腔体或切换通入腔体进行反应。而且大多数情况下,此特定的温度场会直接以热辐射的形式影响喷淋部件,导致喷淋部件达到或接近其熔点变形失效,这时,喷淋部件的控温功能就转化为对喷淋部件主体的冷却。为达到目前的两种或多种气体同时通入腔体或切换通入腔体而且在特定的温度条件下反应的工艺要求,人们提出了多种形式的多气体通道液态介质对流传热类喷淋部件结构形式,这些喷淋部件多采用摩擦焊或埋设其他材料管路形成液态传热介质通道, 但是半导体设备采用的喷淋部件普遍设有密集排列的喷淋小孔,喷淋小孔下方即是为晶圆或其他形式的薄膜基底加热的加热器,则喷淋部件的喷淋小孔一侧最接近加热器,受到加热器的热辐射量最大,若液态传热介质通道设置在喷淋部件的喷淋小孔一侧则其冷却效果最佳,但密集排列的喷淋小孔限制了摩擦焊焊接或埋设管路所需空间,迫使液态传热介质通道的位置远离喷淋小孔一侧, 即远离所在的接近晶圆或其他形式的薄膜基底的位置而设置在了被迫增大体积的喷淋部件的上端,这时在喷淋部件上方即远离喷淋小孔所在的接近晶圆或其他形式的薄膜基底的位置的液态传热介质通道若通入冷却液,则其冷却效率会降低, 即使液态传热介质通道以夹层的形式设置在了最接近热源的喷淋小孔一侧,其传热效果也会因液态传热介质在夹层边缘形成绕流堆积而降低其传热效率,若喷淋部件所吸收的热量使其升温到接近熔点甚至熔点之上,会导致喷淋部件变形失效。此外,在等离子增强型化学气相沉积设备中, 喷淋部件主体会加载高频电压,所以不采用摩擦焊接来形成液态传热介质通道而采取喷淋部件内部埋设不同于喷淋部件材料的液态传热介质管路的方式则会影响喷淋部件主体的电性。 In the conventional semiconductor thin film deposition apparatus, in a process, it is often required to simultaneously enter a cavity or switch into a cavity for reaction in a specific temperature field. Moreover, in most cases, this specific temperature field directly affects the spray components in the form of heat radiation, causing the spray components to reach or near their melting point deformation failure. At this time, the temperature control function of the spray components is converted into a spray. Cooling of the main part of the shower. In order to achieve the current process requirements of two or more gases simultaneously entering the cavity or switching into the cavity and reacting under specific temperature conditions, various forms of multi-gas channel liquid medium convection heat transfer type spraying have been proposed. In the form of shower components, these spray components are often friction welded or buried with other material pipes to form a liquid heat transfer medium passage. However, the spray parts used in semiconductor equipment generally have densely arranged spray holes, and below the spray holes, heaters for heating wafers or other forms of film substrates, and spray nozzles of the spray parts The side is closest to the heater, and the heat radiation amount of the heater is the largest. If the liquid heat medium passage is disposed on the spray orifice side of the spray component, the cooling effect is optimal, but the densely arranged spray orifices limit The space required for friction welding or burying the pipeline forces the position of the liquid heat transfer medium passage away from the side of the spray orifice. That is, located at the upper end of the spray member that is forced to increase in volume away from the position of the near wafer or other form of the film substrate, when the spray member is located above the spray wafer or the proximity wafer or If the liquid heat transfer medium passage at the position of other forms of the film substrate is passed through the coolant, the cooling efficiency thereof is lowered. Even if the liquid heat transfer medium passage is disposed in the form of an interlayer on the side of the spray orifice closest to the heat source, the heat transfer effect is reduced by the liquid heat transfer medium forming a flow accumulation at the edge of the sandwich layer, if The heat absorbed by the spray component causes it to rise to near the melting point or even the melting point, which can cause the spray component to deform. In addition, in a plasma enhanced chemical vapor deposition apparatus, The main body of the spray component is loaded with a high-frequency voltage, so the method of forming a liquid heat transfer medium without friction welding and adopting a liquid heat transfer medium pipe which is different from the material of the spray component inside the spray component affects the spray component. The electrical properties of the subject.
技术问题technical problem
本发明以解决上述问题为目的,主要解决现有喷淋部件结构中存在的喷淋小孔一侧,即最接近热源一侧与液态传热介质通道因空间所限不能有效接近导致传热效率低,喷淋部件体积大,以及喷淋部件中不宜埋设其他材料的液态传热介质管路的问题。在喷淋部件中,通过设置在其内部的传热介质通道、两种气体独立流动通道,来实现温度可控且两种气体在喷淋部件内部相互隔离流动,以达到控温、两种气体切换供给或同时供给且在喷淋部件内不能混合而进行薄膜沉积的工艺要求。 The invention aims to solve the above problems, and mainly solves the side of the spray small hole existing in the structure of the existing spray component, that is, the heat source side is closest to the heat source side and the liquid heat transfer medium channel cannot be effectively approached due to space limitation. Low, large size of the spray parts, and the problem of liquid heat transfer medium lines in other parts of the spray parts that are not suitable for embedding. In the spray component, the temperature is controllable by the heat transfer medium passage and the two gas independent flow passages disposed therein, and the two gases are isolated from each other inside the spray component to achieve temperature control and two gases. Process requirements for film deposition by switching supply or simultaneous supply and not mixing within the spray component.
技术解决方案Technical solution
为实现上述目的,本发明采用下述技术方案:控温型双气体通道均匀喷气喷淋板,所述喷淋板内部设有相互隔离的两个气体通道、一个传热效率高的蛇形液态传热介质通道。所述的相互隔离的两个气体通道及一个蛇形液态传热介质通道由该部件所包括的喷淋上板、扩散挡板、进气环、封闭环及喷淋孔板五个部分组合而成。所述的喷淋上板为圆形板状,其下端面边缘上设置环形凸台,在环形凸台的端面上开矩形槽。两种气体通道的进气位置分别在喷淋上板的中心处和边缘处,边缘处的进气通道与喷淋上板下端面的矩形 槽相通,中心处的进气通道为喷淋上板中心处的通孔。将板状喷淋孔板用去除材料的方式,使其内部形成夹层及夹层中规律分布导气柱,在每个导气柱中心钻一个通孔,在喷淋孔板下端面导气柱之间规律地钻至夹层中形成半通孔,在所钻的半通孔另一端,即喷淋孔板的上端面至夹层的材料上,沿板面方向上且避开导气柱中心所钻有的通孔钻一列长通孔,形成上述结构后再将板状的喷淋孔板加工成圆形。 将内径与喷淋孔板外径一致的进气环的内侧壁开一系列与喷淋上板所钻有的长通孔相对应的短槽,在进气环套在喷淋孔板外缘且进气环上端面与喷淋孔板上端面共面时,所述的短槽应与喷淋上板所钻有的一列长通孔结合使所述的短槽与喷淋上板所钻有的一列长通孔结合成为封闭的蛇形管路。 进气环的上端面圆周方向上避开短槽的位置设置一系列通道 。进气环焊接在喷淋孔板上,封闭环将喷淋孔板与进气环形成的结构转化成双通道气路。将中心处焊有扩散挡板的喷淋上板同心置于喷淋孔板、进气环、封闭环焊接好形成的零件的上端,使喷淋上板下端面边缘处的矩形槽与进气环的上端面圆周方向上避开短槽的位置设置的一系列通道相通。 在喷淋上板上端面钻两个孔分别与蛇形管路的头尾对应相通。这样,第一种气体由喷淋部件的喷淋上板中心处的第一气体入口进入,经过扩散挡板的作用充分扩散到整个喷淋部件的内腔中,经喷淋孔板上的设置在各导气柱中的各通孔流出喷淋部件。 第二种气体由喷淋装置的喷淋上板边缘处的第二气体入口进入,在喷头上板下端面上设置的矩形槽内流动,在流动过程中通过进气环的上端面圆周方向上避开短槽的位置所设置一系列通道进入到喷淋孔板的夹层中,充满夹层空间的同时通过导气柱之间所钻的半通孔流出喷淋部件。两种气体则根据工艺需要以同时或切换的方式进入反应腔中。 与此同时,将液态传热介质通入在喷淋上板上端面所钻的孔进入蛇形管路并经蛇形管路往复流动后流出喷淋部件,达到凭借液态传热介质特定的流速及温度对喷淋部件控温的目的。 具体结构:将扩散挡板同心地焊接在喷淋上板的中心处,上述扩散挡板与喷淋上板构成第一个部分。将进气环与喷淋孔板焊接,使进气环开有的短槽与喷淋孔板所钻有的一列长通孔结合成为封闭的蛇形管路,焊接封闭环将喷淋孔板与进气环形成的结构转化成双通道气路。上述喷淋孔板、进气环、封闭环构成第二个部分。将焊接后的两个部分钎焊在一起,形成空腔,喷淋上板上设置进气口A、进气口B、液路入口C,液路出口D,进气口A与两个部分形成的空腔相通,进气口B与喷淋孔板的夹层相通 In order to achieve the above object, the present invention adopts the following technical solution: a temperature-controlled dual gas passage uniform jet shower plate, wherein the spray plate is provided with two gas passages separated from each other and a serpentine liquid liquid with high heat transfer efficiency. Heat transfer medium passage. The two isolated gas passages and one serpentine liquid heat transfer medium passage are combined by the spray upper plate, the diffusion baffle, the intake ring, the closed ring and the spray orifice plate included in the component. to make. The spray upper plate has a circular plate shape, and an annular boss is arranged on the edge of the lower end surface, and a rectangular groove is formed on the end surface of the annular boss. The intake positions of the two gas passages are respectively at the center and the edge of the spray upper plate, and the intake passage at the edge and the rectangular shape of the lower end surface of the spray upper plate The slots are connected, and the intake passage at the center is a through hole at the center of the spray upper plate. The plate-shaped spray orifice plate is formed by removing the material to form a gas-guiding column regularly distributed in the interlayer and the interlayer, and a through hole is drilled in the center of each gas guide column, and the gas guide column is arranged at the lower end surface of the spray hole plate. Regularly drilled into the interlayer to form a semi-through hole, at the other end of the drilled half-through hole, that is, the upper end surface of the spray plate to the material of the interlayer, and drilled in the direction of the plate surface and avoiding the center of the gas guide column Some through holes drill a row of long through holes, and after forming the above structure, the plate-shaped spray orifice plates are processed into a circular shape. The inner side wall of the intake ring having the inner diameter and the outer diameter of the spray orifice plate is opened with a series of short grooves corresponding to the long through holes drilled by the spray upper plate, and the intake ring is sleeved on the outer edge of the spray orifice plate. When the upper end surface of the intake ring is coplanar with the end surface of the spray orifice, the short groove should be combined with a row of long through holes drilled by the spray upper plate to drill the short groove and the spray upper plate. Some rows of long through holes combine to form a closed serpentine tube. a series of passages are provided in the circumferential direction of the upper end surface of the intake ring to avoid the position of the short groove . The intake ring is welded to the spray orifice plate, and the closed loop converts the structure formed by the spray orifice plate and the intake ring into a two-channel gas path. The spray upper plate welded with the diffusion baffle at the center is concentrically placed on the upper end of the sprayed orifice plate, the inlet ring and the closed ring to form a rectangular groove and the inlet at the edge of the lower end surface of the spray plate A series of passages disposed at a position avoiding the position of the short groove in the circumferential direction of the upper end surface of the ring are communicated. Two holes drilled in the end face of the spray upper plate respectively communicate with the head and tail of the serpentine pipe. Thus, the first gas enters from the first gas inlet at the center of the spray plate of the spray member, and is diffused into the inner cavity of the entire spray member through the diffusion baffle, and is disposed through the spray plate. Each of the through holes in each of the air guide columns flows out of the shower member. The second gas enters from the second gas inlet at the edge of the spray upper plate of the spray device, flows in a rectangular groove provided on the lower end surface of the spray plate, and passes through the upper end surface of the intake ring in the flow direction during the flow. A series of passages are provided to avoid the position of the short groove and enter the interlayer of the spray orifice plate, and fill the spray part through the half through hole drilled between the gas guide columns while filling the interlayer space. The two gases enter the reaction chamber simultaneously or in a switched manner depending on the process requirements. At the same time, the liquid heat transfer medium is introduced into the hole drilled in the end surface of the spray upper plate into the serpentine pipe and flows back and forth through the serpentine pipe and flows out of the spray component to reach a specific flow rate by the liquid heat transfer medium. And the purpose of temperature control of the spray parts. The specific structure: the diffusion baffle is concentrically welded at the center of the spray upper plate, and the diffusion baffle and the spray upper plate constitute the first part. The intake ring is welded to the spray orifice plate, so that the short groove opened by the intake ring and the long through hole drilled by the spray orifice plate are combined into a closed serpentine pipe, and the welded closed ring will be sprayed. The structure formed with the intake ring is converted into a two-channel gas path. The spray orifice plate, the intake ring and the closed ring constitute a second portion. The two parts after welding are brazed together to form a cavity, and the spray upper plate is provided with an air inlet A, an air inlet B, a liquid path inlet C, a liquid path outlet D, an air inlet A and two parts. The formed cavities are connected, and the inlet B communicates with the interlayer of the spray orifice
有益效果Beneficial effect
本发明利用两个零件焊接形成液态传热介质通道的形式将对流传热的位置设置在喷淋小孔一侧,将传热效率最大化,实现了在可控的温度条件下两种气体同时通入腔体或切换通入腔体进行反应的工艺要求,减小了喷淋部件的体积,提高了传热效率,使喷淋部件的可靠性得以保证。 The invention utilizes the form of two parts welded to form a liquid heat transfer medium channel, and the position of the convection heat transfer is set on the side of the spray hole to maximize the heat transfer efficiency, and realize the simultaneous operation of the two gases under the controllable temperature condition. The process requirements of entering the cavity or switching into the cavity for reaction reduce the volume of the spray component, improve the heat transfer efficiency, and ensure the reliability of the spray component.
附图说明DRAWINGS
图1是本发明的喷淋孔板主视图。 BRIEF DESCRIPTION OF THE DRAWINGS Figure 1 is a front elevational view of a shower orifice of the present invention.
图2是图1的立体图。 Fig. 2 is a perspective view of Fig. 1;
图3是本发明的进气环结构示意图。 Figure 3 is a schematic view showing the structure of the intake ring of the present invention.
图4是图3的E处放大图。 Fig. 4 is an enlarged view of E at Fig. 3.
图5是本发明的封闭环结构示意图。 Figure 5 is a schematic view showing the structure of a closed loop of the present invention.
图6是本发明的结构示意图。 Figure 6 is a schematic view of the structure of the present invention.
图7是图6的G-G剖视图。 Fig. 7 is a cross-sectional view taken along line G-G of Fig. 6;
图8是图6的F-F剖视图。 Fig. 8 is a cross-sectional view taken along line FF of Fig. 6;
图9是图8的H-H剖视图。 Fig. 9 is a cross-sectional view taken along line H-H of Fig. 8;
本发明的最佳实施方式BEST MODE FOR CARRYING OUT THE INVENTION
本发明的实施方式Embodiments of the invention
实施例 Example
参照图1-图2,控温型双气体通道均匀喷气喷淋板中的喷淋孔板1为圆形板状,应用去除材料的加工方式,将其内部形成夹层空间15,夹层空间15内部均匀阵列若干柱体3,在每个柱体3中心处钻一个通孔4,在夹层空间15的下层钻均匀阵列的半通孔5,在夹层空间15的上层,平行于喷淋孔板1板面的方向上,钻一列长通孔2,所述的长通孔2避开通孔4。 Referring to Figures 1-2, the spray orifice plate 1 in the temperature-controlled dual gas passage uniform jet shower plate is in the form of a circular plate, and the inside of the interlayer is formed into a sandwich space 15 by using a material removal method. A plurality of cylinders 3 are evenly arrayed, one through hole 4 is drilled in the center of each cylinder 3, and a uniform array of semi-through holes 5 is drilled in the lower layer of the interlayer space 15, in the upper layer of the interlayer space 15, parallel to the spray orifice plate 1 In the direction of the board surface, a row of long through holes 2 are drilled, and the long through holes 2 avoid the through holes 4.
参照图3-图4, 控温型双气体通道均匀喷气喷淋板中的 进气环6为圆形环状,进气环6内径与喷淋孔板1外径相同,进气环6的下端面开设圆周槽7,在进气环6的内侧壁上,开有若干槽8,避开槽8所在位置开设一系列对称轴方向为进气环6径向的径向槽9,每个径向槽9的一端钻通孔10,选取两个特殊位置的槽8,在所述的两个特殊位置的槽8上开设与之相通的两个孔11。 Referring to Figures 3 to 4, the temperature-controlled dual gas channel uniform jet shower plate The intake ring 6 has a circular ring shape, and the inner diameter of the intake ring 6 is the same as the outer diameter of the spray orifice plate 1. The lower end surface of the intake ring 6 defines a circumferential groove 7, and on the inner side wall of the intake ring 6, a plurality of openings are opened. The groove 8 is opened at a position avoiding the groove 8 to form a radial groove 9 with a radial direction of the intake ring 6 in the radial direction of the intake ring 6. One end of each radial groove 9 is drilled through the hole 10, and the groove 8 of two special positions is selected. Two holes 11 communicating therewith are formed in the slots 8 of the two special positions.
参照图5,封闭环12的结构如图所示。 Referring to Figure 5, the structure of the closed loop 12 is as shown.
参照图6-图9,控温型双气体通道均匀喷气喷淋板上端,设置四个入口,分别是中心进气口A,边缘进气口B,液态传热介质进口C,液态传热介质出口D,液态传热介质进口C和出口D可互换。控温型双气体通道均匀喷气喷淋板的焊接关系是:将扩散挡板14同心焊接在喷淋上板13的中心处,使扩散挡板14与喷淋上板13形成第一部分,将进气环6套在喷淋孔板1外圈且使进气环6的上端面与喷淋孔板1的上端面共面,旋转进气环6使进气环6内侧壁上开有的若干槽8与喷淋孔板的长通孔2相通,将所述的长通孔2转化成蛇形管路,所述的蛇形管路由进气环6与喷淋孔板1组合形成,蛇形管路首尾处的槽8分别开设的孔11就作为液态传热介质通道的进出口。将进气环6与喷淋孔板1按照上述位置固定,在上、下端面分别进行摩擦焊,将蛇形管路封闭,喷淋孔板1与进气环6形成第二部分。将第一部分与第二部分同心纤焊,使喷淋上板13的边缘进气口B与进气环6的径向槽9及每个径向槽9一端所钻通孔10相通,使喷淋上板13设置的液态传热介质通道进出口C、D分别与蛇形管路首尾处的槽8分别开设的两个孔11相通。最后将封闭环12的外沿嵌入到进气环6下端面开设圆周槽7中,在在封闭环12边沿与进气环6接缝处及封闭环12下端与喷淋孔板1下端的接缝处摩擦焊接封闭整个部件。这样,第一种气体从喷淋上板13中心处的进气口A进入到控温型双气体通道均匀喷气喷淋板中,通过扩散挡板14充满控温型双气体通道均匀喷气喷淋板内腔并通过喷淋孔板1的通孔4喷淋出控温型双气体通道均匀喷气喷淋板进入反应腔。第二种气体从喷淋上板13边缘进气口B进入并经过进气环6的径向槽9及每个径向槽9一端所钻的通孔10进入到喷淋孔板1的夹层空间15,从夹层空间15下方的半通孔5喷淋出控温型双气体通道均匀喷气喷淋板进入反应腔,与此同时,控温型双气体通道均匀喷气喷淋板的控温功能由通入到该部件的液态传热介质实现:液态传热介质从外界通入到喷淋上板13设置的液态传热介质通道进口C(或D),经过蛇形管路的充分传热作用,实现控温型双气体通道均匀喷气喷淋板的双气体同时通入或先后切换进入腔体并控制喷淋部件温度的功能。 Referring to Figures 6-9, the temperature-controlled dual gas channel uniform jet shower upper end is provided with four inlets, respectively, a central air inlet A, an edge air inlet B, a liquid heat transfer medium inlet C, and a liquid heat transfer medium. At outlet D, the liquid heat transfer medium inlet C and outlet D are interchangeable. The welding relationship of the temperature-controlled dual gas passage uniform jet shower plate is: the diffusion baffle 14 is concentrically welded at the center of the spray upper plate 13, so that the diffusion baffle 14 and the spray upper plate 13 form a first portion, which will enter The gas ring 6 is sleeved on the outer ring of the spray orifice plate 1 and the upper end surface of the intake ring 6 is coplanar with the upper end surface of the spray orifice plate 1, and the intake ring 6 is rotated to open a plurality of inner side walls of the intake ring 6. The slot 8 communicates with the long through hole 2 of the spray orifice plate, and converts the long through hole 2 into a serpentine pipe, and the serpentine pipe is formed by combining the intake ring 6 and the spray orifice plate 1 to form a snake. The holes 11 respectively formed in the grooves 8 at the beginning and the end of the pipe are used as the inlet and outlet of the liquid heat medium passage. The intake ring 6 and the spray orifice plate 1 are fixed in the above position, and friction welding is respectively performed on the upper and lower end faces to close the serpentine pipe, and the spray orifice plate 1 and the intake ring 6 form a second portion. Concentrically brazing the first portion and the second portion such that the edge inlet B of the spray upper plate 13 communicates with the radial groove 9 of the intake ring 6 and the through hole 10 drilled at one end of each radial groove 9 to spray The liquid heat transfer medium passage inlets C and D provided on the upper plate 13 are respectively communicated with the two holes 11 respectively opened in the slots 8 at the beginning and the end of the serpentine line. Finally, the outer edge of the closed ring 12 is embedded in the lower end surface of the intake ring 6 to open the circumferential groove 7, at the edge of the closed ring 12 and the joint of the intake ring 6 and the lower end of the closed ring 12 and the lower end of the spray orifice plate 1 Friction welding at the seam closes the entire part. Thus, the first gas enters the temperature-controlled dual gas passage uniform jet shower plate from the air inlet A at the center of the spray upper plate 13, and is filled with the temperature-controlled double gas passage uniform jet spray through the diffusion baffle 14. The inner cavity of the plate is sprayed through the through hole 4 of the spray orifice plate 1 to discharge the temperature-controlled double gas passage uniform jet shower plate into the reaction chamber. The second gas enters from the edge inlet B of the spray upper plate 13 and passes through the radial groove 9 of the intake ring 6 and the through hole 10 drilled at one end of each radial groove 9 into the interlayer of the spray plate 1 The space 15 sprays the temperature-controlled dual gas passage uniform jet shower plate into the reaction chamber from the semi-through hole 5 below the sandwich space 15, and at the same time, the temperature control function of the temperature-controlled dual gas passage uniform jet shower plate It is realized by the liquid heat transfer medium which is introduced into the component: the liquid heat transfer medium is introduced from the outside to the liquid heat medium passage inlet C (or D) provided on the spray upper plate 13, and the heat transfer through the serpentine pipeline is sufficient The utility model realizes the function of simultaneously introducing or switching the two gases of the temperature-controlled double gas passage uniform jet shower plate into the cavity and controlling the temperature of the spray component.
工业实用性Industrial applicability
序列表自由内容Sequence table free content

Claims (1)

  1. 1 、一种控温型双气体通道均匀喷气喷淋板,其特征在于:所述喷淋板内部设有相互隔离的两个气体通道、一个传热效率高的蛇形液态传热介质通道,上述的相互隔离的两个气体通道及一个蛇形液态传热介质通道由该部件所包括的喷淋上板、扩散挡板、进气环、封闭环及喷淋孔板五个部分组合而成,将扩散挡板同心地焊接在喷淋上板的中心处,上述扩散挡板与喷淋上板构成第一个部分,将进气环与喷淋孔板焊接,使进气环开有的短槽与喷淋孔板所钻有的一列长通孔结合成为封闭的蛇形管路,焊接封闭环将喷淋孔板与进气环形成的结构转化成双通道气路,上述喷淋孔板、进气环、封闭环构成第二个部分,将焊接后的两个部分钎焊在一起,形成空腔,喷淋上板上设置进气口A、进气口B、液路入口C,液路出口D,进气口A与焊接后的两个部分钎焊在一起后形成的空腔相通,进气口B与喷淋孔板的夹层相通。1 a temperature-controlled dual gas passage uniform jet shower plate, characterized in that: the spray plate is provided with two gas passages separated from each other, and a serpentine liquid heat transfer medium passage with high heat transfer efficiency, The two isolated gas passages and one serpentine liquid heat transfer medium passage are composed of a spray upper plate, a diffusion baffle, an intake ring, a closed ring and a spray orifice plate. The diffusion baffle is concentrically welded at the center of the spray upper plate, and the diffusion baffle and the spray upper plate form a first portion, and the intake ring and the spray hole plate are welded to make the intake ring open short. The slot is combined with a row of long through holes drilled by the spray orifice plate to form a closed serpentine pipeline, and the welded closed loop converts the structure formed by the spray orifice plate and the intake ring into a two-channel gas passage, the spray orifice plate The intake ring and the closed ring form a second part, and the two parts after welding are brazed together to form a cavity, and the spray upper plate is provided with an air inlet A, an air inlet B, and a liquid path inlet C, Liquid circuit outlet D, after the air inlet A is brazed with the two parts after welding Into the cavity communicates with the intake port B communicates shower plate sandwich.
    2 、如权利要求1所述的控温型双气体通道均匀喷气喷淋板,其特征在于:所述喷淋孔板为圆形板状,应用去除材料的加工方式,将其内部形成夹层空间,夹层空间内部均匀阵列若干柱体,在每个柱体中心处钻一个通孔,在夹层空间的下层钻均匀阵列的半通孔,在夹层空间的上层,平行于喷淋孔板板面的方向上,钻一列长通孔,所述的长通孔避开通孔。2 The temperature-controlled dual gas passage uniform jet shower plate according to claim 1, wherein the spray orifice plate has a circular plate shape, and a processing method of removing the material is applied to form a sandwich space therein. A plurality of cylinders are evenly arranged inside the interlayer space, a through hole is drilled in the center of each cylinder, and a uniform array of semi-through holes is drilled in the lower layer of the interlayer space, in the upper layer of the interlayer space, parallel to the direction of the shower plate surface Up, drill a row of long through holes, and the long through holes avoid the through holes.
    3 、如权利要求1所述的控温型双气体通道均匀喷气喷淋板,其特征在于:所述进气环为圆形环状,进气环内径与喷淋孔板外径相同,进气环的下端面开设圆周槽,在进气环的内侧壁上,开有若干槽,避开槽所在位置开设一系列对称轴方向为进气环径向的径向槽,每个径向槽的一端钻通孔,选取两个位置的槽,在所述的两个位置的槽上开设与之相通的两个孔。3 The temperature-controlled dual gas passage uniform jet shower plate according to claim 1, wherein the intake ring has a circular ring shape, and the inner diameter of the intake ring is the same as the outer diameter of the spray orifice plate. a circular groove is formed in the lower end surface of the ring, and a plurality of grooves are formed in the inner side wall of the air inlet ring, and a series of radial grooves in the radial direction of the intake ring are opened at a position avoiding the groove, and each radial groove A through hole is drilled at one end, and a groove at two positions is selected, and two holes communicating with each other are formed in the groove at the two positions.
    4 、如权利要求1所述的控温型双气体通道均匀喷气喷淋板,其特征在于:所述喷淋板上端,设置四个入口,分别是中心进气口A,边缘进气口B,液态传热介质进口C,液态传热介质出口D,液态传热介质进口C和液态传热介质出口D可互换。4 The temperature-controlled dual gas passage uniform jet shower plate according to claim 1, wherein: at the shower plate end, four inlets are provided, which are a central air inlet A and an edge air inlet B, respectively. The liquid heat transfer medium inlet C, the liquid heat transfer medium outlet D, the liquid heat transfer medium inlet C and the liquid heat transfer medium outlet D are interchangeable.
    5 、如权利要求1所述的控温型双气体通道均匀喷气喷淋板,其特征在于:所述的蛇形管路由进气环与喷淋孔板组合形成,蛇形管路首尾处的槽分别开设的孔就作为液态传热介质通道的进出口,将进气环与喷淋孔板按照上述位置固定,在上、下端面分别进行摩擦焊,将蛇形管路封闭,喷淋孔板与进气环形成第二部分,将第一部分与第二部分同心纤焊,使喷淋上板的边缘进气口B与进气环的径向槽及每个径向槽一端所钻通孔相通,使喷淋上板设置的液态传热介质通道进出口C、D分别与蛇形管路首尾处的槽分别开设的两个孔相通,最后将封闭环的外沿嵌入到进气环下端面开设圆周槽中,在在封闭环边沿与进气环接缝处及封闭环下端与喷淋孔板下端的接缝处摩擦焊接封闭整个部件,这样,第一种气体从喷淋上板中心处的进气口A进入到控温型双气体通道均匀喷气喷淋板中,通过扩散挡板充满控温型双气体通道均匀喷气喷淋板内腔并通过喷淋孔板的通孔喷淋出控温型双气体通道均匀喷气喷淋板进入反应腔,第二种气体从喷淋上板边缘进气口B进入并经过进气环的径向槽及每个径向槽一端所钻的通孔进入到喷淋孔板的夹层空间,从夹层空间下方的半通孔喷淋出控温型双气体通道均匀喷气喷淋板进入反应腔,与此同时,控温型双气体通道均匀喷气喷淋板的控温功能由通入到该部件的液态传热介质实现:液态传热介质从外界通入到喷淋上板设置的液态传热介质通道进口C或D,经过蛇形管路的充分传热作用,实现双气体同时通入或先后切换进入腔体并控制喷淋部件温度。5 The temperature-controlled dual gas passage uniform jet shower plate according to claim 1, wherein the serpentine tube is formed by a combination of an intake ring and a spray orifice plate, and a groove at the beginning and the end of the serpentine pipe. The separately opened holes serve as the inlet and outlet of the liquid heat transfer medium passage, and the intake ring and the spray orifice plate are fixed according to the above positions, and the upper and lower end faces are respectively subjected to friction welding, and the serpentine pipeline is closed, and the spray orifice plate is closed. Forming a second portion with the intake ring, and welding the first portion and the second portion concentrically, so that the edge of the upper plate of the spray upper plate B and the radial groove of the intake ring and the through hole of one end of each radial groove In the same way, the liquid heat transfer medium passage inlets C and D provided on the spray upper plate are respectively communicated with the two holes respectively opened in the slots at the beginning and the end of the serpentine pipeline, and finally the outer edge of the closed loop is embedded under the intake ring. Opening the circumferential groove in the end face, frictionally welding the entire part at the seam of the closed ring edge and the joint of the intake ring and the lower end of the closed ring and the lower end of the spray orifice plate, so that the first gas is sprayed from the center of the upper plate At the inlet A, enter the temperature-controlled double gas passage evenly In the gas spray plate, the inner wall of the uniform jet shower plate is filled with the temperature-controlled double gas passage through the diffusion baffle, and the temperature-controlled double gas passage uniform jet shower plate is sprayed into the reaction chamber through the through hole of the spray orifice plate. The second gas enters from the inlet B of the upper edge of the spray plate and passes through the radial groove of the intake ring and the through hole drilled at one end of each radial groove to enter the interlayer space of the spray orifice plate, from the interlayer space The lower half-hole sprays out the temperature-controlled dual gas channel uniform jet shower plate into the reaction chamber, while the temperature control function of the temperature-controlled dual gas channel uniform jet shower plate is passed into the liquid state of the component. The heat transfer medium is realized: the liquid heat transfer medium is introduced from the outside to the liquid heat transfer medium passage inlet C or D provided on the spray upper plate, and the double heat gas is simultaneously introduced or successively switched through the sufficient heat transfer action of the serpentine pipeline. Enter the chamber and control the temperature of the spray unit.
PCT/CN2015/084424 2015-04-01 2015-07-20 Temperature-controllable double-gas channel spraying plate with the uniform gas spraying function WO2016155152A1 (en)

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