WO2016015451A1 - 煤矿极性气体红外检测装置及检测方法 - Google Patents

煤矿极性气体红外检测装置及检测方法 Download PDF

Info

Publication number
WO2016015451A1
WO2016015451A1 PCT/CN2015/000516 CN2015000516W WO2016015451A1 WO 2016015451 A1 WO2016015451 A1 WO 2016015451A1 CN 2015000516 W CN2015000516 W CN 2015000516W WO 2016015451 A1 WO2016015451 A1 WO 2016015451A1
Authority
WO
WIPO (PCT)
Prior art keywords
gas
fixed
tested
electric
valve
Prior art date
Application number
PCT/CN2015/000516
Other languages
English (en)
French (fr)
Inventor
梁运涛
孙勇
罗海珠
张德鹏
冯文彬
Original Assignee
煤科集团沈阳研究院有限公司
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 煤科集团沈阳研究院有限公司 filed Critical 煤科集团沈阳研究院有限公司
Publication of WO2016015451A1 publication Critical patent/WO2016015451A1/zh

Links

Images

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
    • G01N21/35—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
    • G01N21/3504—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light for analysing gases, e.g. multi-gas analysis
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/01—Arrangements or apparatus for facilitating the optical investigation
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/01—Arrangements or apparatus for facilitating the optical investigation
    • G01N21/11—Filling or emptying of cuvettes
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/0004—Gaseous mixtures, e.g. polluted air
    • G01N33/0009—General constructional details of gas analysers, e.g. portable test equipment
    • G01N33/0027—General constructional details of gas analysers, e.g. portable test equipment concerning the detector
    • G01N33/0036—General constructional details of gas analysers, e.g. portable test equipment concerning the detector specially adapted to detect a particular component
    • G01N33/0057—Warfare agents or explosives
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/01—Arrangements or apparatus for facilitating the optical investigation
    • G01N2021/0193—Arrangements or apparatus for facilitating the optical investigation the sample being taken from a stream or flow to the measurement cell
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/01—Arrangements or apparatus for facilitating the optical investigation
    • G01N21/03—Cuvette constructions
    • G01N2021/036—Cuvette constructions transformable, modifiable
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/01—Arrangements or apparatus for facilitating the optical investigation
    • G01N21/03—Cuvette constructions
    • G01N2021/0389—Windows

Definitions

  • the invention relates to the field of gas infrared spectrum analysis technology and device, and particularly relates to a coal mine polar gas infrared detection device and a detection method.
  • the indicators for detecting natural fires mainly include CO and its derivatives, olefin and olefin ratio indicators, alkyne gas indicators, and alkane ratio indicators.
  • the existing gas detection devices and methods in coal mines are sensor method and gas chromatography.
  • the sensor method has a large error due to the influence of the underground environment.
  • the existing portable explosive analyzer is equipped with a methane sensor with a low oxygen concentration.
  • gas chromatography analysis must have an adsorption and desorption cycle of the analyzed gas components for different time periods, and the whole process takes a long time to achieve rapid analysis and chromatographic analysis.
  • the column in the device needs frequent maintenance, and the analysis program of the chromatographic system generally requires standard test every time. The technology is complicated, and the analysis result is greatly affected by the skill level of the operator.
  • the infrared spectrum analyzer performs gas quantitative analysis through a gas cell. Affected by the structure of the gas pool, the background gas in the pool cannot be drained, which seriously affects the test results. For continuous sampling and monitoring of gas concentration, this effect can be gradually reduced by long-time purging, and finally the interference gas can not be completely eliminated: but for the investigation of fire accidents, the gas analysis conditions of coal mine gas sampling and sampling, in the gas During the analysis process, it is limited by the fixed structure of the gas pool. The background gas in the gas pool can only be eliminated by manual multiple purging to eliminate the interference. It is difficult to replace the gas in the gas pool with the gas to be tested, which seriously affects the quantitative analysis of gas by infrared spectroscopy. The accuracy of the results.
  • the coal mine polar gas infrared detection device and detection method such as German-made Bruker Tensor27, Bruker ALPHA, American-made Perkin Elmer Spectrum100.
  • the composition includes a central processor electrically connected to the power source, the light source, the detector, the alarm and the indicator light, the input and output module, the data acquisition and storage module, the power source is also electrically connected to the power switch, the power interface, and the input and output module is also connected to the computer communication interface.
  • the data acquisition and storage module is also electrically connected to the detector, and a gas pool mainly with an air outlet and an air inlet is disposed between the light source and the detector.
  • the detection method of the coal mine polar gas infrared detecting device of the structure is: when detecting the gas, first removing the gas pool, injecting 99.999% N 2 gas from the air inlet, and replacing the gas in the gas pool, first closing the gas outlet, After the pressure is balanced, the air inlet is closed, the gas pool is returned to the original position, and the background gas spectrum is scanned until the gas-free peak map appears.
  • the air inlet is connected to the gas bag to be tested, and after the air inlet valve is opened. Open the air outlet valve, manually press the gas to be tested until the N 2 gas is emptied, close the air outlet valve and the air inlet valve, scan the spectrum of the gas to be tested, and use it for gas analysis.
  • the object of the present invention is to address the insufficiency of the existing coal mine polar gas infrared detecting device and the detecting method, and propose a coal mine polar gas infrared detecting device and a detecting method.
  • a coal mine polar gas infrared detecting device which comprises a central processor in the outer casing electrically connecting a power source, a light source, a detector, an alarm device and an indicator light, an input/output module, and a data acquisition and storage.
  • the module, the power source is also electrically connected to the power switch and the power interface
  • the input and output module is also connected to the computer communication interface
  • the data acquisition and storage module is also electrically connected to the detector
  • the feature is that the light source and the detector are fixedly fixed on the device with the moving window. Gas pool assembly.
  • the gas pool assembly with the moving window comprises an air inlet with an air inlet valve on the fixed pool body, the front end fixed the fixed window with a fixed window protection cover, and the rear end is fixed in the fixed pool by a limiting back cover.
  • the fixed pool body is inserted into the front end of the moving pool body, and the moving window is fixed by the moving window cover, and the back end is provided with a manual push-pull handle.
  • the rear end of the fixed pool body is provided with an air outlet port with an air outlet valve tube connected to the micro air pump for continuous detection of the gas to be tested.
  • the gas pool assembly with the moving window comprises an air inlet with an air inlet electric plug valve on the fixed pool body, and the front end is fixed and fixed with a fixed window protection cover, and a limiting block is arranged in the fixed pool body.
  • the rear end is fixed on the fixed pool body by the limiting back cover, and the fixed pool body is inserted into the front end of the moving pool body, and the moving window is fixed by the moving window protection cover, and the rear end is fixed with a limited position, and the inner limit of the back cover is fixed on both sides of the limit back cover.
  • the position sensor and the outer limit sensor of the pool have a rack with a driving thread fixed at a lower end of the moving pool body, a rack control slot at a lower portion of the limiting back cover, and a driving gear driven by a driving motor at a lower end of the pool body, a central processor
  • the inner limit sensor of the gas pool assembly with the moving window and the limit sensor outside the pool are electrically connected, and the central processor is also electrically connected to the electric plug valve of the air inlet and the drive motor switch.
  • the rear end of the fixed pool body is provided with an air outlet electric plug valve tube connected to the air outlet of the micro air pump for continuous detection of the gas to be tested, and the central processor is electrically connected to the air outlet electric plug valve.
  • the limiting back cover is fixed on the fixed pool body, and the protruding locking buckle in the limiting back cover is fastened with the protruding latch of the fixed pool body.
  • the gas pool assembly with a moving window comprises an air inlet and an air outlet with an air inlet electric plug valve on the fixed pool body
  • the air outlet of the electric plug valve, the electric plug between the air inlet plug and the air inlet is connected with the electric three-way valve.
  • the electric three-way valve is one.
  • the electric three-way valve is connected between the electric plug valve and the air outlet.
  • the micro-pumping pump, the electric three-way valve four, the electric three-way valve four-tube connection electric three-way valve two, the electric three-way valve one tube is connected to the electric three-way valve three
  • the front end is fixed fixed window by the fixed window protection cover
  • the fixed pool body is provided with a limiting block, a front limit sensor and a rear limit sensor.
  • the rear end is fixed on the fixed pool body with a limit back cover, and the moving window cover is placed in the fixed pool to fix the moving window and the circle. support.
  • the moving window protection cover has a venting groove.
  • a method for detecting polar gas in coal mine by using the coal mine polar gas infrared detecting device which comprises manually opening the air inlet valve when manually detecting the gas, pushing the manual push-pull handle to the moving window protection cover to contact the fixed window, and entering After the gas port is connected to the gas collecting bag to be tested, the manual push-pull handle is pulled out to move the window protective cover to contact the limit back cover, the gas to be tested is injected into the fixed pool body, the air inlet valve is closed, and the spectrum of the gas to be tested is scanned. Used for gas analysis to be tested.
  • the micro-pump pump to pump the gas in the pipeline to the gas in the pipeline filled with the gas to be tested, close the valve on the pipeline, manually open the inlet valve, and push the manual push-pull handle to the moving window protection cover.
  • the valve on the pipeline is opened, and the manual push-pull handle is pulled out to move the window protection cover to contact the limit back cover, and the gas to be tested is injected into the fixed pool body to be opened.
  • the air outlet valve continuously draws the gas to be tested, and continuously scans the spectrum of the gas to be tested for gas analysis.
  • a method for detecting polar gas in a coal mine by using the coal mine polar gas infrared detecting device including a manual gas detecting method, a computer accessing a computer communication interface, an air inlet electric plug valve, a driving motor switch opening command, and a driving motor working Pushing the mobile cell body to the rear fixed position limit contact sensor outside the limit sensor stop, after the air inlet is connected to the gas collection bag to be tested, the drive motor reverse running command is issued, and the driving motor works to move the moving pool body to the moving window
  • the limit protection sensor in the contact cover of the piece is stopped, the gas to be tested is injected into the fixed cell body, the electric plug valve of the air inlet is closed, and the spectrum of the gas to be tested is scanned for gas analysis.
  • the gas in the pipeline is pumped by the micro-pump pump to the gas in the pipeline filled with the gas to be tested, the valve on the pipeline is closed, and the computer is connected to the computer communication interface to send the electric plug valve of the air inlet and the drive motor switch.
  • a method for detecting polar gas in coal mine by using the coal mine polar gas infrared detecting device comprising: when the artificial gas detecting is performed, the computer is connected to the computer communication interface to send the air inlet electric plug valve to open, and the electric three-way valve on the pipeline is second.
  • the computer sends the electric three-way valve on the pipeline through the computer communication interface, the electric three-way valve three, the electric three-way valve four, the electric three-way valve
  • the second sequence is turned on, the micro-pumping pump is started, and the gas to be tested is pressed into the fixed pool body to stop the rear end limit sensor in the contact hole of the moving window protection cover, the gas to be tested is injected into the fixed pool body, and the electric plug valve of the air inlet is closed.
  • the gas in the pipeline is pumped by the micro-pump pump to the gas in the pipeline filled with the gas to be tested, the valve on the pipeline is closed, and the computer is connected to the computer communication interface to open the electric plug valve of the air inlet, and the pipeline is opened.
  • the valve 2 sequentially turns on the command, activates the micro-pumping pump, presses the gas to be tested into the fixed pool body to stop the rear end limit sensor of the moving window protection cover contact pool, injects the gas to be tested into the fixed pool body, and opens the air outlet electric plug valve
  • the micro-pumping pump continuously extracts the gas to be tested, and continuously scans the spectrum of the gas to be tested for analysis of the gas to be tested.
  • the beneficial effects of the invention are: a gas pool assembly with a moving window fixed on the device between the light source and the detector in the infrared detecting device of the coal mine polar gas, providing a manual or automatic vacuum gas washing structure of the gas pool, combined with the coal mine
  • the detection method of the polar gas infrared detecting device realizes the manual or automatic vacuum gas washing function of the gas pool, saves the N 2 gas for washing, eliminates the cost of the gas cleaning gas, simplifies the gas washing procedure, saves labor costs, and eliminates
  • the artificial error ensures the authenticity of the spectrum of the gas to be tested, ensures the accuracy of the gas to be tested, and provides a scientific basis for early warning of coal mine fires and danger identification of disaster relief. It can also be used in other fields such as chemical industry.
  • Figure 1 is a schematic diagram of the structure of the present invention
  • Figure 2 is a schematic structural view of a first embodiment of the present invention
  • Figure 3 is a schematic structural view of a second embodiment of the present invention.
  • Figure 4 is a structural schematic view of a third embodiment of the present invention.
  • Figure 5 is a structural schematic view of a fourth embodiment of the present invention.
  • Figure 6 is a structural schematic view of a fifth embodiment of the present invention.
  • Figure 7 is a schematic view of the partial structure of Figure 4 or Figure 5 of the present invention.
  • Figure 8 is a cross-sectional view along line A-A of the schematic view of the partial structure of Figure 4 or Figure 5 of the present invention.
  • moving window cover 250. air inlet valve, 251 Outlet electric plug valve, 300. Ventilation slot, 341. Outboard limit sensor, 342. Limit position, 351. Electric three-way valve one, 352. Electric three-way valve two, 353. Electric three-way valve three, 400. Restricted rear cover with raised latches, 401. Fixed pool external protruding latches, 1341. Rear end limit sensor, 2501. Outlet port valve.
  • a coal mine polar gas infrared detecting device comprises a central processing unit 3 electrically connected to a power source 2, a light source 4, a detector 6, an alarm device and an indicator lamp 9, an input/output module 8, and data.
  • the storage module 7 is further connected to the power switch 11 and the power interface 12, and the input/output module 8 is also connected to the computer communication interface 10.
  • the data acquisition storage module 7 is also electrically connected to the detector 6, which is characterized in that the light source 4 and the detector 6 are A gas pool assembly 5 secured to the apparatus with a moving window is disposed therebetween.
  • the gas pool assembly with the moving window comprises an air inlet 23 with an air inlet valve 250 on the fixed pool body 20, and the front end is fixed to the fixed window 21 by a fixed window protection cover 22, and the rear end is used after the limit position.
  • the cover 211 is fixed to the fixed pool body 20.
  • the front end of the fixed pool body 20 is inserted into the front end of the moving pool body 28.
  • the movable window panel 27 is fixed by the moving window cover 212, and the rear end is provided with a manual push-pull handle 29.
  • the moving window protection cover 212 is provided with a deflation groove 300.
  • a coal mine polar gas infrared detecting device comprises a central processing unit 3 electrically connected to a power source 2, a light source 4, a detector 6, an alarm device and an indicator lamp 9, an input/output module 8, and data.
  • the storage module 7 is further connected to the power switch 11 and the power interface 12, and the input/output module 8 is also connected to the computer communication interface 10.
  • the data acquisition storage module 7 is also electrically connected to the detector 6, which is characterized in that the light source 4 and the detector 6 are A gas pool assembly 5 secured to the apparatus with a moving window is disposed therebetween.
  • the gas pool assembly with the moving window comprises an air inlet 23 with an air inlet valve 250 on the fixed pool body 20, and the front end is fixed to the fixed window 21 by a fixed window protection cover 22, and the rear end is used after the limit position.
  • the cover 211 is fixed to the fixed pool body 20.
  • the front end of the fixed pool body 20 is inserted into the front end of the moving pool body 28.
  • the movable window panel 27 is fixed by the moving window cover 212, and the rear end is provided with a manual push-pull handle 29.
  • the rear end of the fixed pool body 20 is provided with an outlet port 24 with an outlet valve 2501 connected to the micro-pumping pump 26 for continuous detection of the gas to be tested.
  • the moving window protection cover 212 is provided with a deflation groove 300.
  • a coal mine polar gas infrared detecting device comprises a central processing unit 3 electrically connected to a power source 2, a light source 4, a detector 6, an alarm device and an indicator light 9, respectively.
  • the input and output module 8 and the data acquisition and storage module 7 are further electrically connected to the power switch 11 and the power interface 12, and the input/output module 8 is also connected to the computer communication interface 10.
  • the data acquisition and storage module 7 is also electrically connected to the detector 6, and the feature is: A gas pool assembly 5 with a moving window attached to the device is disposed between the light source 4 and the detector 6.
  • the gas pool assembly with the moving window comprises an air inlet 23 with an air inlet electric plug valve 25 on the fixed pool body 20, and the front end fixed the window 21 with a fixed window protection cover 22, and the fixed pool body 20
  • a limiting stopper 30 is disposed therein, and the rear end is fixed to the fixed pool body 20 by the limiting rear jaw 211.
  • the fixed pool body 20 is inserted into the front end of the moving pool body 28, and the moving window panel 27 is fixed by the moving window protection cover 212.
  • the fixed limit position 342 is fixed, and the inner limit sensor 34 and the outer limit sensor 341 are fixed on both sides of the limit back cover 211.
  • the lower end of the movable pool body 28 is fixed with a rack with a drive thread 33, and the lower limit cover 211 is provided at the lower end.
  • the central processing unit 3 electrically connects the in-tank limit sensor 34 of the gas pool assembly 5 with the moving window and the outer limit sensor 341.
  • the central processing unit 3 is also electrically connected to the air inlet electric plug valve 25 and the drive motor 31 switch, respectively.
  • the limit back cover 211 is fixed on the fixed pool body 20, and the protruding buckle 400 in the limiting back cover is fastened to the fixed cavity outer latch 401.
  • the moving window protection cover 212 is provided with a deflation groove 300.
  • a coal mine polar gas infrared detecting device comprises a central processing unit 3 electrically connected to a power source 2, a light source 4, a detector 6, an alarm device and an indicator lamp 9, respectively.
  • the input and output module 8 and the data acquisition and storage module 7 are further electrically connected to the power switch 11 and the power interface 12, and the input/output module 8 is also connected to the computer communication interface 10.
  • the data acquisition and storage module 7 is also electrically connected to the detector 6, and the feature is: A gas pool assembly 5 with a moving window attached to the device is disposed between the light source 4 and the detector 6.
  • the gas pool assembly with the moving window comprises an air inlet 23 with an air inlet electric plug valve 25 on the fixed pool body 20, and the front end fixed the window 21 with a fixed window protection cover 22, and the fixed pool body 20
  • a limiting stopper 30 is disposed therein, and a rear end limiting cover 211 is fixed on the fixed pool body 20, and the fixed pool body 20 is inserted into the front end of the moving pool body 28, and the moving window piece 27 is fixed by the moving window protection cover 212, and the rear end is fixed.
  • the fixed limit position 342 is fixed, and the inner limit sensor 34 and the outer limit sensor 341 are fixed on both sides of the limit back cover 211.
  • the lower end of the movable pool body 28 is fixed with a rack with a drive thread 33, and the lower limit cover 211 is provided at the lower end. There is a rack control slot 36.
  • the lower end of the pool body is provided with a drive gear 32 driven by a driving motor 31.
  • the central processing unit 3 electrically connects the in-tank limit sensor 34 of the gas pool assembly 5 with the moving window and the outer limit sensor 341.
  • the central processing unit 3 is also electrically connected The air inlet electric plug valve 25 and the drive motor 31 are switched.
  • the rear end of the fixed pool body 20 is provided with an air outlet electric plug valve 251 tube connected to the air outlet port 24 of the micro air pump 26 for continuous detection of the gas to be tested, and the central processing unit 3 is electrically connected to the air outlet electric plug valve 251.
  • the limit back cover 211 is fixed on the fixed pool body 20, and the protruding buckle 400 in the limiting back cover is fastened to the fixed cavity outer latch 401.
  • the moving window protection cover 212 is provided with a deflation groove 300.
  • a coal mine polar gas infrared detecting device comprises a central processing unit 3 electrically connected to a power source 2, a light source 4, a detector 6, an alarm device and an indicator lamp 9, respectively.
  • the input and output module 8 and the data acquisition and storage module 7 are further electrically connected to the power switch 11 and the power interface 12, and the input/output module 8 is also connected to the computer communication interface 10.
  • the data acquisition and storage module 7 is also electrically connected to the detector 6, and the feature is: A gas pool assembly 5 with a moving window attached to the device is disposed between the light source 4 and the detector 6.
  • the gas pool assembly with the moving window comprises an air inlet 23 with an air inlet electric plug valve 25 on the fixed pool body 20 and an air outlet 24 of the air outlet electric plug valve 251.
  • the air inlet electric plug valve 25 The electric three-way valve two 352, the electric three-way valve one 351, the air outlet electric plug valve 251 and the air outlet 24 are connected between the air inlet 23 and the air outlet port 24, and the electric three-way valve three 353, the micro air pump 26, the electric motor Three-way valve four 35, electric three-way valve four 35 tube connection electric three-way valve two 352, electric three-way valve one 351 tube connected electric three-way valve three 353, front fixed window cover 22 fixed fixed window 21,
  • the fixed pool body 20 is provided with a limiting stopper 30, a front end limit sensor 134, and a rear end limit sensor 1341.
  • the rear end limit back cover 211 is fixed on the fixed pool body 20, and the movable window body 20 is placed in the fixed pool body 20
  • the protective cover 212 fixes the moving window 27 and the circular bracket 38
  • the moving window protection cover 212 is provided with a deflation groove 300.
  • a method for detecting polar gas in a coal mine by using the coal mine polar gas infrared detecting device which comprises manually opening the air inlet valve 250 and pushing the manual push-pull handle 29 when the artificial gas detecting is performed.
  • the moving window protection cover 212 contacts the fixed window 21, and after the air inlet 23 is connected to the gas collecting bag to be tested, the manual sliding handle 29 is pulled out until the moving window protection cover 212 contacts the limiting rear cover 211, and the fixed pool is fixed.
  • the gas to be tested is injected into the body 20, the inlet valve 250 is closed, and the spectrum of the gas to be tested is scanned for gas analysis.
  • the gas in the pipeline is drained by the micro-pump pump until the gas in the pipeline is filled with the gas to be tested, the valve on the pipeline is closed, the inlet valve 250 is manually opened, and the manual push-pull handle 29 is pushed to the moving window.
  • the protective cover 212 contacts the fixed window 21, and after the air inlet 23 is connected to the gas pipeline to be tested, the valve on the pipeline is opened, and the manual push-pull handle 29 is pulled out to move the window protection cover 212 to contact the limit back cover 211, and then fixed.
  • the gas to be tested is injected into the cell body 20, and the gas outlet valve 2501 is opened.
  • the micro-pumping pump 26 continuously extracts the gas to be tested, and continuously scans the spectrum of the gas to be tested for analysis of the gas to be tested.
  • a method for detecting polar gas in a coal mine by using the coal mine polar gas infrared detecting device wherein when the artificial gas detecting is performed, the computer accesses the computer communication interface 10 to issue an air inlet electric cock
  • the valve 25 and the driving motor 31 open and close the command, and the driving motor 31 works to push the moving pool body 28 to the rear fixed position limit position 342 to contact the outer limit sensor 341 of the pool, and the air inlet 23 is connected to the gas collecting bag to be tested.
  • the driving motor 31 is issued with a reverse running command, and the driving motor 31 works to pull the moving pool body 28 to the moving window protection cover 212 to contact the in-cell limit sensor 34 to stop, the fixed pool body 20 is injected with the gas to be tested, and the air inlet electric plug valve is closed. 25. Scan the spectrum of the gas to be tested for gas analysis.
  • the gas in the pipeline is pumped by the micro-pump pump to the gas in the pipeline filled with the gas to be tested, the valve on the pipeline is closed, and the computer is connected to the computer communication interface 10 to send the air-port electric plug valve 25 and drive.
  • the motor 31 opens and closes the command, and the driving motor 31 works to push the moving pool body 28 to the rear fixed fixed position block 342 to contact the outer limit sensor 341 of the pool to stop.
  • the valve on the pipeline is opened.
  • the driving motor 31 works to pull the moving pool body 28 to the moving window protection cover 212 to contact the limit sensor 34 in the pool to stop, the gas to be tested is injected into the fixed pool body 20, the air outlet electric plug valve 251 is opened, and the micro suction pump 26 is continuously selected. The gas is measured, and the spectrum of the gas to be tested is continuously scanned for the gas analysis to be tested.
  • a method for detecting polar gas in a coal mine by using the coal mine polar gas infrared detecting device wherein when the artificial gas detecting is performed, the computer accessing the computer communication interface 10 issues an air inlet electric plug valve 25 to open.
  • the window protection cover 212 contacts the front end limit sensor 134 of the pool to stop, and after the air inlet 23 is connected to the gas collection bag to be tested, the computer sends a three-way electric valve 351 and an electric three-way valve 353 through the computer communication interface 10.
  • the electric three-way valve four 35, the electric three-way valve two 352 sequential turn-on command, start the micro-pumping pump 26, press the gas to be tested into the fixed pool body 20 to the moving window protection cover 212 contact pool inner end limit sensor 1341 Stop, inject the gas to be tested into the fixed cell body 20, close the air port electric plug valve 25, and scan the spectrum of the gas to be tested for gas analysis.
  • the gas in the pipeline is pumped by the micro-pumping pump until the gas in the pipeline is filled with the gas to be tested, the valve on the pipeline is closed, and the computer is connected to the computer communication interface 10 to open the electric plugcock 25 of the air inlet.
  • the electric three-way valve two 352, the electric three-way valve one 351, the electric three-way valve three 353, the electric three-way valve four 35 sequentially turn on the command, start the micro air pump 26, and extract the gas in the fixed pool body 20 to the moving window.
  • the sheet protection cover 212 contacts the front end limit sensor in the pool 134 stops, the air inlet 23 is connected to the gas pipeline to be tested, the valve on the pipeline is opened, and the computer sends an electric electric three-way valve 351, an electric three-way valve three 353, an electric three-way valve through the computer communication interface 10 Four 35, electric three-way valve two 352 sequential turn-on command, start the micro-pumping pump 26, press the gas to be tested into the fixed cell body 20 to the moving window protection cover 212 contact pool inner end limit sensor 1341 stop, fix the pool body 20 is injected into the gas to be tested, and the air outlet electric plug valve 251 is opened.
  • the micro-pumping pump 26 continuously extracts the gas to be tested, and continuously scans the spectrum of the gas to be tested for gas analysis.

Landscapes

  • Physics & Mathematics (AREA)
  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Medicinal Chemistry (AREA)
  • Combustion & Propulsion (AREA)
  • Investigating Or Analysing Materials By Optical Means (AREA)

Abstract

一种煤矿极性气体红外检测装置及其检测方法，该检测装置包括外壳内中央处理器（3）分别电连接电源（2）、光源（4）、检测器（6）、报警器及指示灯（9）、输入输出模块（8）、数据采集储存模块（7），电源（2）还电连接电源开关（11）、电源接口（12），输入输出模块（8）还连接计算机通信接口（10），数据采集储存模块（7）还电连接检测器（6），光源（4）与检测器（6）之间设置固定在装置上带移动窗片（27）的气体池组件（5）。通过气体池的手动或自动真空洗气结构及其检测方法，实现了气体池的手动或自动真空洗气功能，节省了洗气N 2气体，简化了洗气程序，节约了人工费用，消除了人工误差，确保了待测气体光谱的真实性，保证了待测气体分析准确性。

Description

煤矿极性气体红外检测装置及检测方法 技术领域
本发明涉及气体红外光谱分析技术及装置领域，具体涉及煤矿极性气体红外检测装置及检测方法。
背景技术
煤炭自然发火不同氧化阶段对应着不同的自燃温度范围和气体产物的种类和浓度，这些气体产物中通常用于预测预报自然发火进程的有CO、CO2、CH4、C2H6、C3H8、C4H10、C2H4、C3H8、C2H2等，根据氧化气体产物的构成、浓度及其变化速率等特性，可对煤炭自然发火做出准确的预测预报，用来指导煤矿的防灭火安全生产工作，检测自然发火的指标主要有CO及其派生指标、烯烃及烯烷比指标、炔烃气体指标、链烷比指标等；煤矿发生火灾事故以后，对封闭的火区管理和启封都需要监测火区内气体成分，此时监测的气体主要为CO、C2H2、C2H4；而煤矿发生瓦斯爆炸后，主要有毒气体为CO、C2H4、C2H6等，因此，在煤炭生产领域，无论是煤矿日常生产过程中预防煤炭自然发火、瓦斯爆炸事故，还是在灾害应急救援过程中，都需要对上述气体进行快速、精确定量分析，所以研究煤矿极性气体红外检测装置及检测方法是保证煤矿安全生产和保障矿工生命安全的重要手段之一。
煤矿现有的气体检测装置及方法是传感器法和气相色谱法，传感器方法由于受到井下环境影响，其检测结果存在较大误差，例如，现有便携式爆炸性测定仪配置的甲烷传感器在氧浓度较低时，结果会出现较大的偏差；气相色谱法分析时必须要有一个被分析气体组分不同时间段的吸附和脱附周期，整个过程需要较长的时间，无法实现快速分析，同时色谱分析装置中的色谱柱需要经常维护，并且色谱分析系统的分析程序一般要求每次先进行标样测试，技术复杂，分析结果受操作人员技术水平影响较大。
红外光谱分析仪通过气体池实现对气体定量分析。受气体池结构影响，池内背景气体无法排净，严重影响测试结果。对于连续采样监测气体浓度时，这种影响可以通过长时间的吹扫逐渐降低，最终也无法彻底排除干扰气体：但对于火灾事故调查、煤矿井下气体人工采样送样的气体分析条件下，在气体分析过程中受气体池的固定结构限制，气体池内背景气体只能靠人工多次吹扫来消除其干扰，很难将气体池内气体置换成待测气体，严重影响了红外光谱法对气体定量分析结果的准确性。目前，煤矿极性气体红外检测装置及检测方法，检测装置如德国产Bruker Tensor27，Bruker ALPHA，美国产Perkin Elmer Spectrum100。其构成均包括中央处理器分别电连接电源、光源、检测器、报警器及指示灯、输入输出模块、数据采集储存模块，电源还电连接电源开关、电源接口，输入输出模块还连接计算机通信接口， 数据采集储存模块还电连接检测器，光源与检测器之间设置可取下的主要带有出气口和进气口的气体池。该结构的煤矿极性气体红外检测装置的检测方法为：在检测气体时，首先取下气体池，从进气口注入含量99.999％N2气体，置换气体池内的气体后，先关闭出气口，待压力平衡后关闭进气口，气体池放回原处，扫描背景气体光谱图至无气体峰值图出现后，人工采样时，进气口连接待测气体采气袋，打开进气口阀后打开出气口阀，人工压入待测气体至N2气体排空，关闭出气口阀和进气口阀，扫描待测气体光谱，用于待测气体分析。由于气体池内部两端存在死角，经常出现N2气体洗气不净和N2气体排空不净现象出现，造成待测气体光谱失真，致使待测气体分析失准。有造成煤矿安全事故的可能。该结构的煤矿极性气体红外检测装置的检测方法需拆卸气体池才能实现，使用很麻烦。
发明内容
本发明的目的是针对现有煤矿极性气体红外检测装置及检测方法的不足之处，提出一种煤矿极性气体红外检测装置及检测方法。
本发明解决问题所采用的技术方案是提供一种煤矿极性气体红外检测装置，包括外壳内中央处理器分别电连接电源、光源、检测器、报警器及指示灯、输入输出模块、数据采集储存模块，电源还电连接电源开关、电源接口，输入输出模块还连接计算机通信接口，数据采集储存模块还电连接检测器，特点在于：光源与检测器之间设置固定在装置上带移动窗片的气体池组件。
所述的带移动窗片的气体池组件包括固定池体上带有进气口阀的进气口，前端用固定窗片保护罩固定固定窗片，后端用限位后盖固定在固定池体上，固定池体内插入移动池体前端用移动窗片保护罩固定移动窗片，后端带有手动推拉把手。其中：固定池体后端设带有出气口阀管连接微型抽气泵的出气口，用于待测气体连续检测。
所述的带移动窗片的气体池组件包括固定池体上带有进气口电动旋塞阀的进气口，前端用固定窗片保护罩固定固定窗片，固定池体内设有限位挡片，后端用限位后盖固定在固定池体上，固定池体内插入移动池体前端用移动窗片保护罩固定移动窗片，后端固定有限位挡，限位后盖两侧固定有池内限位传感器、池外限位传感器，移动池体下端固定有带驱动螺纹的齿条，限位后盖下部设有齿条控位槽，池体下端设有驱动电机带动的驱动齿轮，中央处理器电连接带移动窗片的气体池组件的池内限位传感器、池外限位传感器，中央处理器还分别电连接进气口电动旋塞阀、驱动电机开关。其中：固定池体后端设带有出气口电动旋塞阀管连接微型抽气泵的出气口，用于待测气体连续检测，中央处理器电连接出气口电动旋塞阀。其中：限位后盖固定在固定池体上由限位后盖内凸起锁扣与固定池体外凸起锁扣扣接实现。
所述的带移动窗片的气体池组件包括固定池体上带有进气口电动旋塞阀的进气口和出气 口电动旋塞阀的出气口，进气口电动旋塞阀与进气口之间管连接电动三通阀二、电动三通阀一，出气口电动旋塞阀与出气口之间管连接电动三通阀三、微型抽气泵、电动三通阀四，电动三通阀四管连接电动三通阀二，电动三通阀一管连接电动三通阀三，前端用固定窗片保护罩固定固定窗片，固定池体内设有限位挡片、前端限位传感器、后端限位传感器，后端用限位后盖固定在固定池体上，固定池体内放置移动窗片保护罩固定移动窗片及圆形支架。
其中：移动窗片保护罩带有泄气槽。
一种利用所述煤矿极性气体红外检测装置检测煤矿极性气体的方法，包括人工采气检测时，手动打开进气口阀，推动手动推拉把手至移动窗片保护罩接触固定窗片，进气口接入待测气体采气袋后，拉出手动推拉把手至移动窗片保护罩接触限位后盖后，固定池体内注入待测气体，关闭进气口阀，扫描待测气体光谱，用于待测气体分析。其中：连续采样时，用微型抽气泵抽放管路中的气体至管路中气体充满待测气体，关闭管路上的阀门，手动打开进气口阀，推动手动推拉把手至移动窗片保护罩接触固定窗片，进气口接入待测气体管路后，打开管路上的阀门，拉出手动推拉把手至移动窗片保护罩接触限位后盖后，固定池体内注入待测气体，打开出气口阀，微型抽气泵连续抽取待测气体，连续扫描待测气体光谱，用于待测气体分析。
一种利用所述煤矿极性气体红外检测装置检测煤矿极性气体的方法，包括人工采气检测时，计算机接入计算机通信接口发出进气口电动旋塞阀、驱动电机开关打开指令，驱动电机工作推动移动池体至后端固定有限位挡接触池外限位传感器停止，进气口接入待测气体采气袋后，发出驱动电机反向运行指令，驱动电机工作拉动移动池体至移动窗片保护罩接触池内限位传感器停止，固定池体内注入待测气体，关闭进气口电动旋塞阀，扫描待测气体光谱，用于待测气体分析。其中：连续采样时，用微型抽气泵抽放管路中的气体至管路中气体充满待测气体，关闭管路上的阀门，计算机接入计算机通信接口发出进气口电动旋塞阀、驱动电机开关打开指令，驱动电机工作推动移动池体至后端固定有限位挡接触池外限位传感器停止，进气口接入待测气体管路后，打开管路上的阀门，驱动电机工作拉动移动池体至移动窗片保护罩接触池内限位传感器停止，固定池体内注入待测气体，打开出气口电动旋塞阀，微型抽气泵连续抽取待测气体，连续扫描待测气体光谱，用于待测气体分析。
一种利用所述煤矿极性气体红外检测装置检测煤矿极性气体的方法，包括人工采气检测时，计算机接入计算机通信接口发出进气口电动旋塞阀打开，管路上电动三通阀二、电动三通阀一、电动三通阀三、电动三通阀四顺序接通命令，启动微型抽气泵，抽取固定池体内气体至移动窗片保护罩接触池内前端限位传感器停止，进气口接入待测气体采气袋后，计算机通过计算机通信接口发出管路上电动三通阀一、电动三通阀三、电动三通阀四、电动三通阀 二顺序接通命令，启动微型抽气泵，将待测气体压入固定池体至移动窗片保护罩接触池内后端限位传感器停止，固定池体内注入待测气体，关闭进气口电动旋塞阀，扫描待测气体光谱，用于待测气体分析。其中：连续采样时，用微型抽气泵抽放管路中的气体至管路中气体充满待测气体，关闭管路上的阀门，计算机接入计算机通信接口发出进气口电动旋塞阀打开，管路上电动三通阀二、电动三通阀一、电动三通阀三、电动三通阀四顺序接通命令，启动微型抽气泵，抽取固定池体内气体至移动窗片保护罩接触池内前端限位传感器停止，进气口接入待测气体管路后，打开管路上的阀门，计算机通过计算机通信接口发出管路上电动电动三通阀一、电动三通阀三、电动三通阀四、电动三通阀二顺序接通命令，启动微型抽气泵，将待测气体压入固定池体至移动窗片保护罩接触池内后端限位传感器停止，固定池体内注入待测气体，打开出气口电动旋塞阀，微型抽气泵连续抽取待测气体，连续扫描待测气体光谱，用于待测气体分析。
本发明的有益效果是：煤矿极性气体红外检测装置中光源与检测器之间设置固定在装置上带移动窗片的气体池组件，提供了气体池的手动或自动真空洗气结构，结合煤矿极性气体红外检测装置的检测方法，实现了气体池的手动或自动真空洗气功能，节省了洗气N2气体，消除了洗气气体成本，简化了洗气程序，节约了人工费用，消除了人工误差，确保了待测气体光谱的真实性，保证了待测气体分析准确性，为煤矿火灾早期预警和抢险救灾危险识别提供科学依据。还可应用于化工等其它领域。
附图说明
下面结合附图和实施例对本发明进一步说明。
图1本发明结构原理图；
图2本发明第一实施例结构原理图；
图3本发明第二实施例结构原理图；
图4本发明第三实施例结构原理图；
图5本发明第四实施例结构原理图；
图6本发明第五实施例结构原理图；
图7本发明图4或图5局部结构原理图；
图8本发明图4或图5局部结构原理图的A-A剖面图。
具体实施方式
附图编号
图中2.电源，3.中央处理器，4.光源，5.带移动窗片的气体池组件，6.检测器，7.数据采集存储模块，8.输入输出模块，9.报警器及指示灯，10.计算机通信接口，11.电源开关， 12.电源接口，20.固定池体，21.固定窗片，22.固定窗片保护罩，23.进气口，24.出气口，25.进气口电动旋塞阀，26.微型抽气泵，27.移动窗片，28.移动池体，29.手动推拉把手，30.限位挡片，31.驱动电机，32.驱动齿轮，33.驱动螺纹，34.池内限位传感器，35.电动三通阀四，36.齿条控位槽，38.圆形支架，134.前端限位传感器，211.限位后盖，212.移动窗片保护罩，250.进气口阀，251.出气口电动旋塞阀，300.泄气槽，341.池外限位传感器，342.限位挡，351.电动三通阀一，352.电动三通阀二，353.电动三通阀三，400.限位后盖内凸起锁扣，401.固定池体外凸起锁扣，1341.后端限位传感器，2501.出气口阀。
实施例一
参见图1、图2，一种煤矿极性气体红外检测装置，包括外壳内中央处理器3分别电连接电源2、光源4、检测器6、报警器及指示灯9、输入输出模块8、数据采集储存模块7，电源2还电连接电源开关11、电源接口12，输入输出模块8还连接计算机通信接口10，数据采集储存模块7还电连接检测器6，特点在于：光源4与检测器6之间设置固定在装置上带移动窗片的气体池组件5。
所述的带移动窗片的气体池组件包括固定池体20上带有进气口阀250的进气口23，前端用固定窗片保护罩22固定固定窗片21，后端用限位后盖211固定在固定池体20上，固定池体20内插入移动池体28前端用移动窗片保护罩212固定移动窗片27，后端带有手动推拉把手29。
其中：移动窗片保护罩212带有泄气槽300。
实施例二
参见图1、图3，一种煤矿极性气体红外检测装置，包括外壳内中央处理器3分别电连接电源2、光源4、检测器6、报警器及指示灯9、输入输出模块8、数据采集储存模块7，电源2还电连接电源开关11、电源接口12，输入输出模块8还连接计算机通信接口10，数据采集储存模块7还电连接检测器6，特点在于：光源4与检测器6之间设置固定在装置上带移动窗片的气体池组件5。
所述的带移动窗片的气体池组件包括固定池体20上带有进气口阀250的进气口23，前端用固定窗片保护罩22固定固定窗片21，后端用限位后盖211固定在固定池体20上，固定池体20内插入移动池体28前端用移动窗片保护罩212固定移动窗片27，后端带有手动推拉把手29。
其中：固定池体20后端设带有出气口阀2501管连接微型抽气泵26的出气口24，用于待测气体连续检测。
其中：移动窗片保护罩212带有泄气槽300。
实施例三
参见图1、图4、图7、图8，一种煤矿极性气体红外检测装置，包括外壳内中央处理器3分别电连接电源2、光源4、检测器6、报警器及指示灯9、输入输出模块8、数据采集储存模块7，电源2还电连接电源开关11、电源接口12，输入输出模块8还连接计算机通信接口10，数据采集储存模块7还电连接检测器6，特点在于：光源4与检测器6之间设置固定在装置上带移动窗片的气体池组件5。
所述的带移动窗片的气体池组件包括固定池体20上带有进气口电动旋塞阀25的进气口23，前端用固定窗片保护罩22固定固定窗片21，固定池体20内设有限位挡片30，后端用限位后盏211固定在固定池体20上，固定池体20内插入移动池体28前端用移动窗片保护罩212固定移动窗片27，后端固定有限位挡342，限位后盖211两侧固定有池内限位传感器34、池外限位传感器341，移动池体28下端固定有带驱动螺纹33的齿条，限位后盖211下部设有齿条控位槽36，池体下端设有驱动电机31带动的驱动齿轮32，中央处理器3电连接带移动窗片的气体池组件5的池内限位传感器34、池外限位传感器341，中央处理器3还分别电连接进气口电动旋塞阀25、驱动电机31开关。
其中：限位后盖211固定在固定池体20上由限位后盖内凸起锁扣400与固定池体外凸起锁扣401扣接实现。
其中：移动窗片保护罩212带有泄气槽300。
实施例四
参见图1、图5、图7、图8，一种煤矿极性气体红外检测装置，包括外壳内中央处理器3分别电连接电源2、光源4、检测器6、报警器及指示灯9、输入输出模块8、数据采集储存模块7，电源2还电连接电源开关11、电源接口12，输入输出模块8还连接计算机通信接口10，数据采集储存模块7还电连接检测器6，特点在于：光源4与检测器6之间设置固定在装置上带移动窗片的气体池组件5。
所述的带移动窗片的气体池组件包括固定池体20上带有进气口电动旋塞阀25的进气口23，前端用固定窗片保护罩22固定固定窗片21，固定池体20内设有限位挡片30，后端用限位后盖211固定在固定池体20上，固定池体20内插入移动池体28前端用移动窗片保护罩212固定移动窗片27，后端固定有限位挡342，限位后盖211两侧固定有池内限位传感器34、池外限位传感器341，移动池体28下端固定有带驱动螺纹33的齿条，限位后盖211下部设有齿条控位槽36，池体下端设有驱动电机31带动的驱动齿轮32，中央处理器3电连接带移动窗片的气体池组件5的池内限位传感器34、池外限位传感器341，中央处理器3还分别电连接 进气口电动旋塞阀25、驱动电机31开关。
其中：固定池体20后端设带有出气口电动旋塞阀251管连接微型抽气泵26的出气口24，用于待测气体连续检测，中央处理器3电连接出气口电动旋塞阀251。
其中：限位后盖211固定在固定池体20上由限位后盖内凸起锁扣400与固定池体外凸起锁扣401扣接实现。
其中：移动窗片保护罩212带有泄气槽300。
实施例五
参见图1、图5、图7、图8，一种煤矿极性气体红外检测装置，包括外壳内中央处理器3分别电连接电源2、光源4、检测器6、报警器及指示灯9、输入输出模块8、数据采集储存模块7，电源2还电连接电源开关11、电源接口12，输入输出模块8还连接计算机通信接口10，数据采集储存模块7还电连接检测器6，特点在于：光源4与检测器6之间设置固定在装置上带移动窗片的气体池组件5。
所述的带移动窗片的气体池组件包括固定池体20上带有进气口电动旋塞阀25的进气口23和出气口电动旋塞阀251的出气口24，进气口电动旋塞阀25与进气口23之间管连接电动三通阀二352、电动三通阀一351，出气口电动旋塞阀251与出气口24之间管连接电动三通阀三353、微型抽气泵26、电动三通阀四35，电动三通阀四35管连接电动三通阀二352，电动三通阀一351管连接电动三通阀三353，前端用固定窗片保护罩22固定固定窗片21，固定池体20内设有限位挡片30、前端限位传感器134、后端限位传感器1341，后端用限位后盖211固定在固定池体20上，固定池体20内放置移动窗片保护罩212固定移动窗片27及圆形支架38。
其中：移动窗片保护罩212带有泄气槽300。
实施例六
参见图1、图2、图3，一种利用所述煤矿极性气体红外检测装置检测煤矿极性气体的方法，包括人工采气检测时，手动打开进气口阀250，推动手动推拉把手29至移动窗片保护罩212接触固定窗片21，进气口23接入待测气体采气袋后，拉出手动推拉把手29至移动窗片保护罩212接触限位后盖211后，固定池体20内注入待测气体，关闭进气口阀250，扫描待测气体光谱，用于待测气体分析。
其中：连续采样时，用微型抽气泵抽放管路中的气体至管路中气体充满待测气体，关闭管路上的阀门，手动打开进气口阀250，推动手动推拉把手29至移动窗片保护罩212接触固定窗片21，进气口23接入待测气体管路后，打开管路上的阀门，拉出手动推拉把手29至移动窗片保护罩212接触限位后盖211后，固定池体20内注入待测气体，打开出气口阀2501， 微型抽气泵26连续抽取待测气体，连续扫描待测气体光谱，用于待测气体分析。
实施例七
参见图1、图4、图5，一种利用所述煤矿极性气体红外检测装置检测煤矿极性气体的方法，包括人工采气检测时，计算机接入计算机通信接口10发出进气口电动旋塞阀25、驱动电机31开关打开指令，驱动电机31工作推动移动池体28至后端固定有限位挡342接触池外限位传感器341停止，进气口23接入待测气体采气袋后，发出驱动电机31反向运行指令，驱动电机31工作拉动移动池体28至移动窗片保护罩212接触池内限位传感器34停止，固定池体20内注入待测气体，关闭进气口电动旋塞阀25，扫描待测气体光谱，用于待测气体分析。
其中：连续采样时，用微型抽气泵抽放管路中的气体至管路中气体充满待测气体，关闭管路上的阀门，计算机接入计算机通信接口10发出进气口电动旋塞阀25、驱动电机31开关打开指令，驱动电机31工作推动移动池体28至后端固定有限位挡342接触池外限位传感器341停止，进气口23接入待测气体管路后，打开管路上的阀门，驱动电机31工作拉动移动池体28至移动窗片保护罩212接触池内限位传感器34停止，固定池体20内注入待测气体，打开出气口电动旋塞阀251，微型抽气泵26连续抽取待测气体，连续扫描待测气体光谱，用于待测气体分析。
实施例八
参见图1、图6，一种利用所述煤矿极性气体红外检测装置检测煤矿极性气体的方法，包括人工采气检测时，计算机接入计算机通信接口10发出进气口电动旋塞阀25打开，管路上电动三通阀二352、电动三通阀一351、电动三通阀三353、电动三通阀四35顺序接通命令，启动微型抽气泵26，抽取固定池体20内气体至移动窗片保护罩212接触池内前端限位传感器134停止，进气口23接入待测气体采气袋后，计算机通过计算机通信接口10发出管路上电动三通阀一351、电动三通阀三353、电动三通阀四35、电动三通阀二352顺序接通命令，启动微型抽气泵26，将待测气体压入固定池体20至移动窗片保护罩212接触池内后端限位传感器1341停止，固定池体20内注入待测气体，关闭进气口电动旋塞阀25，扫描待测气体光谱，用于待测气体分析。
其中：连续采样时，用微型抽气泵抽放管路中的气体至管路中气体充满待测气体，关闭管路上的阀门，计算机接入计算机通信接口10发出进气口电动旋塞阀25打开，管路上电动三通阀二352、电动三通阀一351、电动三通阀三353、电动三通阀四35顺序接通命令，启动微型抽气泵26，抽取固定池体20内气体至移动窗片保护罩212接触池内前端限位传感器 134停止，进气口23接入待测气体管路后，打开管路上的阀门，计算机通过计算机通信接口10发出管路上电动电动三通阀一351、电动三通阀三353、电动三通阀四35、电动三通阀二352顺序接通命令，启动微型抽气泵26，将待测气体压入固定池体20至移动窗片保护罩212接触池内后端限位传感器1341停止，固定池体20内注入待测气体，打开出气口电动旋塞阀251，微型抽气泵26连续抽取待测气体，连续扫描待测气体光谱，用于待测气体分析。

Claims (13)

  1. 一种煤矿极性气体红外检测装置，包括外壳内中央处理器分别电连接电源、光源、检测器、报警器及指示灯、输入输出模块、数据采集储存模块，电源还电连接电源开关、电源接口，输入输出模块还连接计算机通信接口，数据采集储存模块还电连接检测器，光源与检测器之间设置固定在装置上带移动窗片的气体池组件，特征在于：所述的带移动窗片的气体池组件包括固定池体上带有进气口阀的进气口，前端用固定窗片保护罩固定固定窗片，后端用限位后盖固定在固定池体上，固定池体内插入移动池体前端用移动窗片保护罩固定移动窗片，后端带有手动推拉把手。
  2. 根据权利要求1所述的一种煤矿极性气体红外检测装置，特征在于：固定池体后端设带有出气口阀管连接微型抽气泵的出气口。
  3. 一种煤矿极性气体红外检测装置，包括外壳内中央处理器分别电连接电源、光源、检测器、报警器及指示灯、输入输出模块、数据采集储存模块，电源还电连接电源开关、电源接口，输入输出模块还连接计算机通信接口，数据采集储存模块还电连接检测器，光源与检测器之间设置固定在装置上带移动窗片的气体池组件，特征在于：所述的带移动窗片的气体池组件包括固定池体上带有进气口电动旋塞阀的进气口，前端用固定窗片保护罩固定固定窗片，固定池体内设有限位挡片，后端用限位后盖固定在固定池体上，固定池体内插入移动池体前端用移动窗片保护罩固定移动窗片，后端固定有限位挡，限位后盖两侧固定有池内限位传感器、池外限位传感器，移动池体下端固定有带驱动螺纹的齿条，限位后盖下部设有齿条控位槽，池体下端设有驱动电机带动的驱动齿轮，中央处理器电连接带移动窗片的气体池组件的池内限位传感器、池外限位传感器，中央处理器还分别电连接进气口电动旋塞阀、驱动电机开关。
  4. 根据权利要求3所述的一种煤矿极性气体红外检测装置，特征在于：固定池体后端设带有出气口电动旋塞阀管连接微型抽气泵的出气口，用于待测气体连续检测，中央处理器电连接出气口电动旋塞阀。
  5. 根据权利要求4所述的一种煤矿极性气体红外检测装置，特征在于：限位后盖固定在固定池体上由限位后盖内凸起锁扣与固定池体外凸起锁扣扣接实现。
  6. 一种煤矿极性气体红外检测装置，包括外壳内中央处理器分别电连接电源、光源、检测器、报警器及指示灯、输入输出模块、数据采集储存模块，电源还电连接电源开关、电源接口，输入输出模块还连接计算机通信接口，数据采集储存模块还电连接检测器，光源与检测器之间设置固定在装置上带移动窗片的气体池组件，特征在于：所述的带移动窗片的气体池组件包括固定池体上带有进气口电动旋塞阀的进气口和出气口电动旋塞阀的出气口，进气口电动旋塞阀与进气口之间管连接电动三通阀二、电动三通阀一，出气口电动旋塞阀与出气口之间管连接电动三通阀三、微型抽气泵、电动三通阀四，电动三通阀四管连接电动三通阀二，电动三通阀一管连接电动三通阀三，前端用固定窗片保护罩固定固定窗片，固定池体内设有限位挡片、前端限位传感器、后端限位传感器，后端用限位后盖固定在固定池体上，固定池体内放置移动窗片保护罩固定移动窗片及圆形支架。
  7. 根据权利要求1或2或3或4或5或6所述的一种煤矿极性气体红外检测装置，特征在于：移动窗片保护罩带有泄气槽。
  8. 一种利用权利要求1所述煤矿极性气体红外检测装置检测煤矿极性气体的方法，特征在于：包括人工采气检测时，手动打开进气口阀，推动手动推拉把手至移动窗片保护罩接触固定窗片，进气口接入待测气体采气袋后，拉出手动推拉把手至移动窗片保护罩接触限位后盖后，固定池体内注入待测气体，关闭进气口阀，扫描待测气体光谱，用于待测气体分析。
  9. 一种利用权利要求2所述煤矿极性气体红外检测装置检测煤矿极性气体的方法，特征在于：连续采样时，用微型抽气泵抽放管路中的气体至管路中气体充满待测气体，关闭管路上的阀门，手动打开进气口阀，推动手动推拉把手至移动窗片保护罩接触固定窗片，进气口接入待测气体管路后，打开管路上的阀门，拉出手动推拉把手至移动窗片保护罩接触限位后盖后，固定池体内注入待测气体，打开出气口阀，微型抽气泵连续抽取待测气体，连续扫描特测气体光谱，用于待测气体分析。
  10. 一种利用权利要求3所述煤矿极性气体红外检测装置检测煤矿极性气体的方法，特征在于：包括人工采气检测时，计算机接入计算机通信接口发出进气口电动旋塞阀、驱动电机开关打开指令，驱动电机工作推动移动池体至后端固定有限位挡接触池外限位传感器停止，进气口接入待测气体采气袋后，发出驱动电机反向运行指令，驱动电机工作拉动移动池体至移动窗片保护罩接触池内限位传感器停止，固定池体内注入待测气体，关闭进气口电动旋塞阀，扫描待测气体光谱，用于待测气体分析。
  11. 一种利用权利要求4所述煤矿极性气体红外检测装置检测煤矿极性气体的方法，特征在于：连续采样时，用微型抽气泵抽放管路中的气体至管路中气体充满待测气体，关闭管路上的阀门，计算机接入计算机通信接口发出进气口电动旋塞阀、驱动电机开关打开指令，驱动电机工作推动移动池体至后端固定有限位挡接触池外限位传感器停止，进气口接入待测气体管路后，打开管路上的阀门，驱动电机工作拉动移动池体至移动窗片保护罩接触池内限位传感器停止，固定池体内注入待测气体，打开出气口电动旋塞阀，微型抽气泵连续抽取待测气体，连续扫描待测气体光谱，用于待测气体分析。
  12. 一种利用权利要求6所述煤矿极性气体红外检测装置检测煤矿极性气体的方法，特征在于：包括人工采气检测时，计算机接入计算机通信接口发出进气口电动旋塞阀打开，管路上电动三通阀二、电动三通阀一、电动三通阀三、电动三通阀四顺序接通命令，启动微型抽气泵，抽取固定池体内气体至移动窗片保护罩接触池内前端限位传感器停止，进气口接入待测气体采气袋后，计算机通过计算机通信接口发出管路上电动三通阀一、电动三通阀三、电动三通阀四、电动三通阀二顺序接通命令，启动微型抽气泵，将待测气体压入固定池体至移动窗片保护罩接触池内后端限位传感器停止，固定池体内注入待测气体，关闭进气口电动旋塞阀，扫描待测气体光谱，用于待测气体分析。
  13. 根据权利要求12所述一种利用煤矿极性气体红外检测装置检测煤矿极性气体的方法，特征在于：连续采样时，用微型抽气泵抽放管路中的气体至管路中气体充满待测气体，关闭管路上的阀门，计算机接入计算机通信接口发出进气口电动旋塞阀打开，管路上电动三 通阀二、电动三通阀一、电动三通阀三、电动三通阀四顺序接通命令，启动微型抽气泵，抽取固定池体内气体至移动窗片保护罩接触池内前端限位传感器停止，进气口接入待测气体管路后，打开管路上的阀门，计算机通过计算机通信接口发出管路上电动电动三通阀一、电动三通阀三、电动三通阀四、电动三通阀二顺序接通命令，启动微型抽气泵，将待测气体压入固定池体至移动窗片保护罩接触池内后端限位传感器停止，固定池体内注入待测气体，打开出气口电动旋塞阀，微型抽气泵连续抽取待测气体，连续扫描待测气体光谱，用于待测气体分析。
PCT/CN2015/000516 2014-07-31 2015-07-20 煤矿极性气体红外检测装置及检测方法 WO2016015451A1 (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CN201410371238.5A CN104165858B (zh) 2014-07-31 2014-07-31 煤矿极性气体红外检测装置及检测方法
CN201410371238.5 2014-07-31

Publications (1)

Publication Number Publication Date
WO2016015451A1 true WO2016015451A1 (zh) 2016-02-04

Family

ID=51909770

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/CN2015/000516 WO2016015451A1 (zh) 2014-07-31 2015-07-20 煤矿极性气体红外检测装置及检测方法

Country Status (3)

Country Link
US (3) US9588040B2 (zh)
CN (1) CN104165858B (zh)
WO (1) WO2016015451A1 (zh)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109342498A (zh) * 2018-10-15 2019-02-15 西安科技大学 一种煤自燃过程阶段判定方法
CN112268833A (zh) * 2020-09-27 2021-01-26 周少玺 一种多功能瓦斯参数测试仪器及其使用方法

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104165858B (zh) * 2014-07-31 2015-11-11 煤科集团沈阳研究院有限公司 煤矿极性气体红外检测装置及检测方法
CN110362946B (zh) * 2019-07-22 2022-11-11 河南理工大学 一种针对煤矿典型事故的应急救援仿真方法及仿真系统
CN110470626A (zh) * 2019-08-28 2019-11-19 贵州大学 一种用于矿井内部瓦斯浓度在线检测装置
CN111006917A (zh) * 2019-11-15 2020-04-14 中国辐射防护研究院 一种用于碘吸附器效率试验的连续取样装置
US20230143377A1 (en) * 2021-11-09 2023-05-11 Ccteg Shenyang Research Institute Gas chromatograph for underground mine
CN115165754B (zh) * 2022-09-07 2022-11-15 江苏三恒科技股份有限公司 一种煤矿用高浓度激光甲烷传感器组件

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH09310125A (ja) * 1996-05-16 1997-12-02 Nakayama Steel Works Ltd 焼結焼成ガスの連続分析方法及びその分析設備
CN1384350A (zh) * 2001-04-30 2002-12-11 众智光电科技股份有限公司 具有卡匣式光路系统的多化合物气体分析仪
CN201763345U (zh) * 2009-03-19 2011-03-16 河南理工大学 煤矿井下采空区气样采集分析装置
CN102138067A (zh) * 2008-08-28 2011-07-27 森谢尔公司 适于对小浓度气体进行光谱分析的设备
CN202562784U (zh) * 2012-04-28 2012-11-28 河南中医学院 香烟烟雾收集装置
CN103900988A (zh) * 2014-04-18 2014-07-02 重庆川仪分析仪器有限公司 红外气体传感器气室及其红外气体传感器
CN104165858A (zh) * 2014-07-31 2014-11-26 煤科集团沈阳研究院有限公司 煤矿极性气体红外检测装置及检测方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1057794A (en) * 1964-04-07 1967-02-08 Ustav Pro Vyzkum A Vyuziti Tuh Improvements in and relating to non-dispersive infra-red analysers
GB8309211D0 (en) * 1983-04-05 1983-05-11 Edinburgh Instr Infra red absorption gas detectors
US5708273A (en) * 1996-05-09 1998-01-13 Foss Nirsystems, Inc. Transflectance probe having adjustable window gap adapted to measure viscous substances for spectrometric analysis and method of use
WO2005093390A1 (en) * 2004-03-29 2005-10-06 Noveltech Solutions Oy Method and system for detecting one or more gases or gas mixtures and/or for measuring the concentration of one or more gases or gas mixtures
US20050264815A1 (en) * 2004-05-07 2005-12-01 Mark Wechsler Sample element with fringing-reduction capabilities
US7956761B2 (en) * 2007-05-29 2011-06-07 The Aerospace Corporation Infrared gas detection and spectral analysis method
CN201707293U (zh) * 2010-03-05 2011-01-12 煤炭科学研究总院沈阳研究院 煤矿井下极性混合气体测定装置
CN102419311B (zh) * 2011-08-31 2013-06-19 赵捷 一种具有自动校准功能的矿用红外气体传感器
CN202939125U (zh) * 2012-12-08 2013-05-15 西安科技大学 一种煤矿瓦斯气体浓度红外检测装置
DE102014000210B3 (de) * 2014-01-14 2015-05-13 Dräger Safety AG & Co. KGaA Modifizierte Messküvette

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH09310125A (ja) * 1996-05-16 1997-12-02 Nakayama Steel Works Ltd 焼結焼成ガスの連続分析方法及びその分析設備
CN1384350A (zh) * 2001-04-30 2002-12-11 众智光电科技股份有限公司 具有卡匣式光路系统的多化合物气体分析仪
CN102138067A (zh) * 2008-08-28 2011-07-27 森谢尔公司 适于对小浓度气体进行光谱分析的设备
CN201763345U (zh) * 2009-03-19 2011-03-16 河南理工大学 煤矿井下采空区气样采集分析装置
CN202562784U (zh) * 2012-04-28 2012-11-28 河南中医学院 香烟烟雾收集装置
CN103900988A (zh) * 2014-04-18 2014-07-02 重庆川仪分析仪器有限公司 红外气体传感器气室及其红外气体传感器
CN104165858A (zh) * 2014-07-31 2014-11-26 煤科集团沈阳研究院有限公司 煤矿极性气体红外检测装置及检测方法

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109342498A (zh) * 2018-10-15 2019-02-15 西安科技大学 一种煤自燃过程阶段判定方法
CN112268833A (zh) * 2020-09-27 2021-01-26 周少玺 一种多功能瓦斯参数测试仪器及其使用方法
CN112268833B (zh) * 2020-09-27 2024-05-07 周少玺 一种多功能瓦斯参数测试仪器及其使用方法

Also Published As

Publication number Publication date
CN104165858A (zh) 2014-11-26
CN104165858B (zh) 2015-11-11
US20170108432A1 (en) 2017-04-20
US20170108431A1 (en) 2017-04-20
US9588040B2 (en) 2017-03-07
US20160033396A1 (en) 2016-02-04
US9702814B2 (en) 2017-07-11
US9927353B2 (en) 2018-03-27

Similar Documents

Publication Publication Date Title
WO2016015451A1 (zh) 煤矿极性气体红外检测装置及检测方法
CN104502160B (zh) 一种与机器人配合使用的有害气体采集及检测仪器
CN202083635U (zh) 石油天然气气体分析仪
CN106525999B (zh) 气体气相色谱检测方法
CN201707293U (zh) 煤矿井下极性混合气体测定装置
CN204214860U (zh) 一种土壤呼吸连续测定装置
CN203275127U (zh) 变压器取油装置
CN104990883A (zh) 一种利用光谱仪检测气体浓度的装置
CN109444127A (zh) 一种高锰酸盐指数在线检测方法及系统
CN202033225U (zh) 职业环境气体采样检测仪
CN202837159U (zh) 一种暗箱式四用紫外分析仪
CN205139004U (zh) 一种六氟化硫气体组分取样分析装置
CN202562838U (zh) 一种光学甲烷检测仪
CN213715134U (zh) 一种气体继电器可燃气体自动检测系统
CN205262802U (zh) 气体分析取样装置
CN212180797U (zh) 一种油中溶解气体在线监测系统
CN203443942U (zh) 一种色谱分析仪
CN210376250U (zh) 一种具有监测堵塞情况的气相色谱仪
CN207976330U (zh) 一种便携式大流量低浓度烟尘自动测试仪
CN202256298U (zh) 石油储罐机械清洗罐内气体的检测装置
CN103309374A (zh) 氢氧分析仪
CN207488175U (zh) 超灵敏高时间分辨一氧化氮光谱在线分析装置
CN201340355Y (zh) 防疫用气体采样检测仪
CN203276065U (zh) 氢氧分析仪
CN219369290U (zh) 空气采样装置

Legal Events

Date Code Title Description
121 Ep: the epo has been informed by wipo that ep was designated in this application

Ref document number: 15828241

Country of ref document: EP

Kind code of ref document: A1

NENP Non-entry into the national phase

Ref country code: DE

122 Ep: pct application non-entry in european phase

Ref document number: 15828241

Country of ref document: EP

Kind code of ref document: A1