WO2015098743A1 - Method for producing tobacco material, and tobacco material produced by said production method - Google Patents
Method for producing tobacco material, and tobacco material produced by said production method Download PDFInfo
- Publication number
- WO2015098743A1 WO2015098743A1 PCT/JP2014/083689 JP2014083689W WO2015098743A1 WO 2015098743 A1 WO2015098743 A1 WO 2015098743A1 JP 2014083689 W JP2014083689 W JP 2014083689W WO 2015098743 A1 WO2015098743 A1 WO 2015098743A1
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- WIPO (PCT)
- Prior art keywords
- tobacco
- heating
- tobacco leaf
- tobacco material
- production method
- Prior art date
Links
- 241000208125 Nicotiana Species 0.000 title claims abstract description 137
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 137
- 239000000463 material Substances 0.000 title claims abstract description 84
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 44
- 238000010438 heat treatment Methods 0.000 claims abstract description 51
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 24
- 238000001035 drying Methods 0.000 claims description 21
- 235000019504 cigarettes Nutrition 0.000 claims description 19
- 235000019505 tobacco product Nutrition 0.000 claims description 11
- 210000000988 bone and bone Anatomy 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 5
- 239000002994 raw material Substances 0.000 abstract description 17
- 239000000796 flavoring agent Substances 0.000 abstract description 11
- 235000019634 flavors Nutrition 0.000 abstract description 11
- 238000000034 method Methods 0.000 description 31
- 238000005259 measurement Methods 0.000 description 3
- 235000010724 Wisteria floribunda Nutrition 0.000 description 2
- 238000003763 carbonization Methods 0.000 description 2
- 239000007799 cork Substances 0.000 description 2
- 238000011049 filling Methods 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 239000004745 nonwoven fabric Substances 0.000 description 2
- 239000005022 packaging material Substances 0.000 description 2
- 238000007789 sealing Methods 0.000 description 2
- 230000002522 swelling effect Effects 0.000 description 2
- 206010015535 Euphoric mood Diseases 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 230000001055 chewing effect Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 238000000691 measurement method Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000013021 overheating Methods 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 230000000391 smoking effect Effects 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 210000003462 vein Anatomy 0.000 description 1
Images
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/18—Other treatment of leaves, e.g. puffing, crimpling, cleaning
- A24B3/182—Puffing
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
- A24D1/02—Cigars; Cigarettes with special covers
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/04—Humidifying or drying tobacco bunches or cut tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
Definitions
- the present invention relates to a method for producing a tobacco material and a tobacco material produced by the production method.
- Patent Document 1 a method of performing pressure drying on a tobacco leaf of Burley type as a tobacco leaf is known (Patent Document 1).
- Patent Document 1 describes that the pressurization condition is 25 kPa to 700 kPa, and that the moisture content of the tobacco leaf is maintained to exceed 10%.
- a mixture of tobacco leaves adjusted to have a moisture content of at least 15% is heat treated (at least 250 ° F.) under conditions sufficient to generate scents and fragrance components (substantially under atmospheric pressure).
- Patent Document 2 describes that the heat treatment time is 10 minutes and the temperature is 121 to 177 ° C. (Example).
- Patent Document 3 a method is known in which a cigarette strip is stacked on a belt conveyor and transported so as to pass through a dryer to perform a drying process.
- tobacco leaves having a moisture content of about 30% are dried to finally reduce the moisture content to about 5%, and the temperature range during drying is also described. 93 to 118 ° C. is described.
- Patent Document 4 a rotary dryer for drying tobacco leaves, tobacco strips, and cut tobacco leaves. Patent Document 4 does not describe specific conditions for drying tobacco leaves. Moreover, there is no description regarding the water content of tobacco leaves.
- Patent Documents 1 to 3 described above all describe a process of heating while keeping the moisture of tobacco leaves above a certain level.
- the water content of the tobacco leaf during heating is maintained above 10%, and the water content of the tobacco leaf after drying is also maintained at 10% or more, so that the filling power of the tobacco leaf pieces is maintained.
- Patent Document 2 describes that a tobacco leaf before drying needs to have a moisture content of at least 15% in order to generate a sufficient amount of aroma components.
- Patent Literature 3 describes that the chemical composition and flavor of tobacco after treatment are affected unless the moisture content of the tobacco leaf is set above a certain level.
- the present invention provides a production method for obtaining a tobacco material that can enhance the bulkiness of tobacco leaves and has a changed flavor.
- the method for treating tobacco leaves includes a step of heating a tobacco leaf material having a water content of 2.5% by weight or less under the condition of a product temperature of 100 to 200 ° C.
- the present invention is as follows.
- a method for producing a tobacco material comprising a step of heating a tobacco leaf material having a water content of 2.5% by weight or less under a condition where the product temperature is 100 to 200 ° C.
- Production method [2] The production method according to [1], including a drying step of reducing the water content of the tobacco leaf material to 2.5% by weight or less before the heating step.
- the method for producing a tobacco material of the present invention includes a step of heating a tobacco leaf material having a water content of 2.5% by weight or less at a product temperature of 100 to 200 ° C.
- the tobacco leaf material having a water content of 2.5% by weight or less can be obtained, for example, by the following two methods.
- a tobacco leaf material having a water content of, for example, 10 to 40% by weight is placed in the same heating apparatus used in the subsequent heating step (main heating). Examples include a step of heating (preheating or drying) in a temperature range (product temperature) from room temperature to 100 to 200 ° C.
- the second method as shown in FIG.
- the tobacco leaf material having a water content of, for example, 10 to 40% by weight is the same as the heating device used in the subsequent heating step (main heating). Or the method of performing a drying process separately using a different apparatus can be mentioned.
- the heating temperature and heating device at this time are not particularly limited as long as the moisture content of the tobacco leaf material can be reduced to 2.5% by weight or less.
- the tobacco leaf material having a water content of 2.5% by weight or less is heated so that the product temperature of the tobacco leaf material is 100 to 200 ° C.
- a specific heating method a method in which high-temperature steam (200 ° C. or higher) or high-temperature air is brought into contact, or a method in which a heating container heated to 200 ° C. or higher is brought into contact.
- the method of contacting the high temperature steam and the method of contacting the heated container may be performed independently or in combination.
- a means for generating high-temperature steam a known one, for example, a heating steam generator (for example, model: IHSS-20B, manufactured by Fuji Electric Thermo Systems Co., Ltd.) can be used.
- An example of the heated heating container is a drum-type can wall heating dryer.
- Examples of the set temperature of the heating container include an embodiment in which the temperature is set to 200 ° C. to 330 ° C., and preferably about 300 ° C.
- the bulkiness of the tobacco leaf is increased and the change in flavor is increased.
- the carbonization of the tobacco leaf can be prevented by heating the tobacco leaf raw material having a moisture content of 2.5% by weight or less under the condition that the product temperature is 200 ° C. or less. More preferable product temperature conditions are 120 ° C. or more and 200 ° C. or less.
- the time required for the heating step varies depending on the amount of tobacco leaf raw material to be heated and the size of the apparatus, but the time required for the product temperature of the tobacco leaf raw material to be 100 to 200 ° C.
- the heating time is preferably 30 seconds or more, particularly preferably 120 seconds or more as the time when the temperature of the tobacco leaf raw material becomes 100 to 200 ° C., from the viewpoint of increasing the bulkiness of the tobacco leaf raw material. . It is important to avoid inconveniences such as crushing and carbonization of the tobacco leaf material by overheating the tobacco leaf material with the product temperature exceeding 200 ° C., and the product temperature is 200 ° C. or less. If it is a state which can hold
- the time of the heating step (main heating) means the time when the moisture content of the tobacco leaf material is 2.5% by weight or less and the product temperature is 100 to 200 ° C.
- the production method of the present invention includes the preheating described above (in a state where the moisture content exceeds 2.5% by weight and the product temperature is from room temperature to 100 ° C or higher) Includes heating when the temperature of the product is less than 100 ° C. with the water content of the tobacco leaf material being 2.5 weight or less (for example, heating due to residual heat after heating) In a stage, heating may be performed in a state where the product temperature exceeds 200 ° C. for a short time.
- the flavor of tobacco as used in the present invention refers to the strength of a roasted feeling, and the tobacco material obtained using the production method of the present invention increases the roasted feeling. Furthermore, when a tobacco leaf raw material contains a middle bone, a middle bone odor can be reduced.
- the product temperature of the tobacco leaf raw material in the present invention is a temperature measured by the following method.
- the tobacco leaf material heated by the heating means is poured into a dewar into which a thermocouple is inserted within 2 seconds, which is brought into sufficient contact with the thermocouple, and left to stand at the maximum temperature displayed with a cork stopper.
- the product temperature is a temperature measured by the following method.
- the tobacco leaf material heated by the heating means is poured into a dewar into which a thermocouple is inserted within 2 seconds, which is brought into sufficient contact with the thermocouple, and left to stand at the maximum temperature displayed with a cork stopper.
- the product temperature is a temperature measured by the following method.
- the tobacco leaf raw material may be either a tobacco leaf divided into a mesophyll portion (lamina) or a vein portion (central bone), or may include a tobacco stem portion that is not a tobacco leaf portion.
- tobacco leaf materials include those cut to a step width of 0.1 to 2.0 mm. The step size can be appropriately determined according to the use of the tobacco material, for example, the type of cigarette or oral tobacco.
- main varieties such as yellow varieties, Burley varieties, native varieties, oriental varieties, and fermented leaves using them can be used.
- the step width referred to in the present invention is a value set when cutting a raw leaf tobacco with a tobacco cutting machine.
- Tobacco leaf cutting is an operation that cuts raw leaf tobacco into long and narrow fibers with a certain width.
- a device that performs cutting is called a cutting machine, and a rotary type cutting machine or a cutting type cutting machine is a common device, but when cutting tobacco with these devices, the width to cut the raw leaf tobacco
- the value to be set is called step size.
- the manufacturing method of the tobacco material of the present invention can include a known process in addition to the above heating process. For example, a step for cooling the tobacco material after the heating step and various steps necessary for smoking various tobacco products, such as cigarettes and smokeless tobacco, may be included as appropriate.
- a process for producing various tobacco products include a process of adding an additive such as a fragrance to the obtained tobacco material.
- the tobacco material obtained by using the production method of the present invention include the following embodiments used for various tobacco products.
- a well-known manufacturing method can be used without a special restriction
- the cigarette may be either with or without a filter.
- a high feeling of smoke is obtained.
- the cigarette material of the present invention contained in the cigarette cigarette material may be 5 to 100% by weight.
- smokeless tobacco is snus.
- a well-known method can be used also about manufacture of snus.
- the tobacco material produced by the above-described production method can be obtained by filling a packaging material using a raw material such as a nonwoven fabric using a known method.
- the amount of tobacco material is adjusted and filled, and snus is obtained by sealing by means such as heat sealing.
- the packaging material can be used without any particular limitation, but a cellulose-based nonwoven fabric is preferably used.
- the smokeless tobacco product is, for example, a gum, it is obtained by mixing the tobacco material obtained using the production method of the present invention with a known gum base and a known method.
- a chewing tobacco, a hooked tobacco, and a compressed tobacco can also be obtained using a known method except that the tobacco material obtained using the production method of the present invention is used.
- a mode in which the ratio of the tobacco material obtained by the production method of the present invention contained in the smokeless tobacco material is 5 to 100% by weight can be mentioned.
- Examples of cigarette products other than cigarettes and smokeless cigarettes include, for example, hand-rolled cigarettes, water cigarettes, cigarettes, and cuticles that users create by wrapping them with wrapping paper. Other than using the tobacco material used in the production method of the present invention, these can be produced using a known method for producing hand-rolled tobacco or water tobacco.
- Tobacco leaf material having a water content of 12% by weight was put into a cylinder-type heat dryer and heated from room temperature (25 ° C.). Heating was performed by contacting can wall heating using a cylinder-type heating dryer heated to 300 ° C. and 320 ° C. heating steam.
- the heat dryer used in this example is of the type illustrated in FIG.
- the cylinder 1 has a cylindrical shape with an inner diameter of 400 mm and a longitudinal length of 1900 mm, rotates at 4 rpm, and is inclined so that the raw material inlet position is higher than the raw material outlet position. The tilt angle is 3 ° with respect to the horizontal direction.
- Tobacco leaf raw material was introduced from the raw material inlet 2 through the rotary valve 3 into the exhaust duct 4 and the cylinder 1 having the blade blade 10 inside.
- the cylinder 1 was heated by superheated steam produced using a heater 6 and a superheated steam generator 7.
- the tobacco leaf material was conveyed by rotation and inclination of the cylinder 1 and taken out from the material outlet 9.
- Fuji Electric Thermo Systems Co., Ltd. (model: IHSS-20B) was used.
- the relationship between the heating time and the product temperature of the tobacco leaf material is as shown in Table 1.
- the processing time described in Table 1 indicates a continuous time from the start of heating.
- the heating time when the product temperature is 100 ° C. or higher is also shown.
- the method for measuring the bulkiness of a tobacco material obtained using the method for producing a tobacco material of the present invention is as follows.
- the method for measuring the product temperature of the tobacco leaf material in the examples is as follows. ⁇ Method for measuring tobacco product temperature> 1. At the cylinder outlet, the tobacco leaf material is collected with a stainless steel scoop. 2. The sample is poured into a Dewar bottle (Thermos, Thermo Cut D-500) into which a thermocouple (Rinden Electric Co., Ltd.) is inserted within 2 seconds. Push the sample with a stick and make good contact with the thermocouple. 3. Put the cork stopper and let it stand, and let the maximum temperature displayed be the tobacco product temperature.
- FIGS. 3 The results shown in Table 1 above are summarized as FIGS. As can be seen from FIG. 2, when heating under the condition that the temperature of the tobacco leaf material is 100 ° C. or higher is included, the bulkiness of the tobacco leaf material obtained increases. Further, when heating in a state where the moisture in the tobacco leaf material is low (product temperature of 100 ° C. or higher) is included, the bulkiness is increased (FIG. 3).
- the tobacco material obtained by using the method for producing a tobacco material according to the present invention was remarkably enhanced in bulkiness.
- the flavor of the tobacco material obtained using the production method of the present invention was greatly changed. Specifically, when used as a cigarette, the roasted feeling was enhanced. Moreover, the inside odor was reduced.
- the tobacco material produced by using the production method of the present invention has a significantly improved bulkiness and a great change in flavor.
- Such a tobacco material can be preferably used as a material for various tobacco products.
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Abstract
Description
また、水分含量が少なくとも15%になるように調整されたたばこ葉の混合物を、香りや芳香成分が発生するのに十分な条件下(実質的に大気圧下)で熱処理(少なくとも250°F)が行われる技術も知られている(特許文献2)。特許文献2には、熱処理の時間は10分、温度は121~177℃であることが記載されている(実施例)。
また、ベルトコンベア上にたばこストリップを積載し、これを乾燥機を通過するように搬送させて、乾燥処理を行う方法が知られている(特許文献3)。この方法では、約30%の水分含有量を有するたばこ葉を乾燥させることで、最終的にその水分含有量を約5%に減少させることが記載されており、また、乾燥の際の温度範囲として93~118℃が記載されている。
また、たばこ葉、たばこストリップ、裁断されたたばこ葉を乾燥させるための回転乾燥機が知られている(特許文献4)。特許文献4には、たばこ葉を乾燥させるための具体的な条件についての記載はない。また、たばこ葉の水分含有量に関する記載もない。 Conventionally, methods for treating tobacco leaves to change the flavor of tobacco leaves have been studied. For example, a method of performing pressure drying on a tobacco leaf of Burley type as a tobacco leaf is known (Patent Document 1).
In addition, a mixture of tobacco leaves adjusted to have a moisture content of at least 15% is heat treated (at least 250 ° F.) under conditions sufficient to generate scents and fragrance components (substantially under atmospheric pressure). There is also known a technique for performing (Patent Document 2).
In addition, a method is known in which a cigarette strip is stacked on a belt conveyor and transported so as to pass through a dryer to perform a drying process (Patent Document 3). In this method, it is described that tobacco leaves having a moisture content of about 30% are dried to finally reduce the moisture content to about 5%, and the temperature range during drying is also described. 93 to 118 ° C. is described.
Also known is a rotary dryer for drying tobacco leaves, tobacco strips, and cut tobacco leaves (Patent Document 4). Patent Document 4 does not describe specific conditions for drying tobacco leaves. Moreover, there is no description regarding the water content of tobacco leaves.
特許文献1には、加熱中のたばこ葉の水分含量を10%を超えて維持し、乾燥後のたばこ葉の水分含量も10%以上に維持することで、たばこ葉片の充填力(filling power)が向上すると記載されている。また、特許文献2には、十分な量の芳香成分を発生させるために、乾燥前のたばこ葉は、少なくとも15%の水分含有量を有している必要が記載されている。
一方、特許文献3には、たばこ葉の水分含有量を一定以上にしないと、処理後のたばこの化学組成や風味に影響を与える旨が記載されている。
In
On the other hand,
上記のいずれの特許文献にも、たばこ葉の水分含有量が非常に少ない条件下で乾燥処理を行うことについては記載がない。また、たばこ葉の水分含有量が非常に少ない条件下で乾燥処理を行った場合のたばこ葉の膨嵩性や香味の変化との関係については記載されていない。 As described above, in the techniques described in each patent document, although tobacco leaves are subjected to drying treatment for various purposes, all of them can be dried after adjusting the moisture content of the tobacco leaves before drying. Are listed. In particular,
None of the above-mentioned patent documents describes that the drying treatment is performed under conditions where the moisture content of the tobacco leaf is very low. In addition, there is no description regarding the relationship between the change in the bulkiness and flavor of tobacco leaves when the drying treatment is performed under conditions where the moisture content of the tobacco leaves is very low.
[1]たばこ材料の製造方法であって、水の含有量が2.5重量%以下のたばこ葉原料を、品温が100~200℃となる条件下で加熱する工程を含む、たばこ材料の製造方法。
[2]前記加熱工程の前に、たばこ葉原料の水の含有量を2.5重量%以下にまで減少させる乾燥工程を含む、[1]に記載の製造方法。
[3]前記乾燥工程に供されるたばこ葉原料の水の含有量が、10~40重量%である、[1]または[2]に記載の製造方法。
[4]前記たばこ葉原料が、刻み幅0.1~2.0mmのラミナ、中骨またはこれらの混合物を含む、[1]~[3]のいずれかに記載の製造方法。
[5][1]~[4]のいずれかに記載の製造方法で作製されたたばこ材料。
[6][5]に記載のたばこ材料を用いたたばこ製品。
[7][5]に記載のたばこ材料を用いたシガレット。
[8][5]に記載のたばこ材料を用いた無煙たばこ製品。 That is, the present invention is as follows.
[1] A method for producing a tobacco material, comprising a step of heating a tobacco leaf material having a water content of 2.5% by weight or less under a condition where the product temperature is 100 to 200 ° C. Production method.
[2] The production method according to [1], including a drying step of reducing the water content of the tobacco leaf material to 2.5% by weight or less before the heating step.
[3] The production method according to [1] or [2], wherein the content of water of the tobacco leaf material used in the drying step is 10 to 40% by weight.
[4] The production method according to any one of [1] to [3], wherein the tobacco leaf material includes lamina having a step width of 0.1 to 2.0 mm, a middle bone, or a mixture thereof.
[5] A tobacco material produced by the production method according to any one of [1] to [4].
[6] A tobacco product using the tobacco material according to [5].
[7] A cigarette using the tobacco material according to [5].
[8] A smokeless tobacco product using the tobacco material according to [5].
水の含有量が2.5重量%以下のたばこ葉原料は、例えば以下の二通りの方法で得ることができる。
第一の方法としては、図1(a)で示すように、水の含有量が例えば10~40重量%であるたばこ葉原料を、後の加熱工程(本加熱)で用いる同じ加熱装置に入れ、常温から100~200℃の温度範囲(品温)で加熱する(予備加熱あるいは乾燥)工程を含ませる態様を挙げることができる。
第二の方法としては、図1(b)で示すように、水の含有量が例えば10~40重量%であるたばこ葉原料を、後の加熱工程(本加熱)で用いる加熱装置とは同じあるいは異なる装置を用いて乾燥処理を別途行う方法を挙げることができる。この際の加熱温度や加熱装置としては特に制限されず、たばこ葉原料の水分含有量を2.5重量%以下まで減少させることができればよい。 The method for producing a tobacco material of the present invention includes a step of heating a tobacco leaf material having a water content of 2.5% by weight or less at a product temperature of 100 to 200 ° C.
The tobacco leaf material having a water content of 2.5% by weight or less can be obtained, for example, by the following two methods.
As a first method, as shown in FIG. 1 (a), a tobacco leaf material having a water content of, for example, 10 to 40% by weight is placed in the same heating apparatus used in the subsequent heating step (main heating). Examples include a step of heating (preheating or drying) in a temperature range (product temperature) from room temperature to 100 to 200 ° C.
As the second method, as shown in FIG. 1 (b), the tobacco leaf material having a water content of, for example, 10 to 40% by weight is the same as the heating device used in the subsequent heating step (main heating). Or the method of performing a drying process separately using a different apparatus can be mentioned. The heating temperature and heating device at this time are not particularly limited as long as the moisture content of the tobacco leaf material can be reduced to 2.5% by weight or less.
水分測定方法
1.ガラス製の試料容器に、たばこ葉原料を1~2g量り取る。試料容器全体の重量を測定する。
2.試料容器を、ロータリー式乾燥機(松山工業社製、M-104AT)に入れ、回転させながら乾燥させる。その際、ロータリー式乾燥機は100℃に予熱しておく。
3.100℃で1時間乾燥させた後、試料容器を取り出し、デシケーター内で放冷させる。
4.放冷後、試料容器の重量を測定する。
5.水分を下記の式で計算する。
水分=(W1-W2) / (W1-W0) * 100
W0:試料容器の空重量
W1:乾燥前試料と試料容器重量
W2:乾燥後試料と試料容器重量 In addition, content of the water in a tobacco leaf raw material can be measured with the following measuring methods.
Moisture
2. The sample container is placed in a rotary dryer (M-104AT, manufactured by Matsuyama Kogyo Co., Ltd.) and dried while rotating. At that time, the rotary dryer is preheated to 100 ° C.
3. After drying at 100 ° C. for 1 hour, the sample container is taken out and allowed to cool in a desiccator.
4). After standing to cool, the weight of the sample container is measured.
5. The moisture is calculated by the following formula.
Moisture = (W1-W2) / (W1-W0) * 100
W0: Empty weight of sample container W1: Weight of sample and sample container before drying W2: Weight of sample and sample container after drying
高温蒸気を接触させる方法と、加熱された加熱容器に接触させる方法は、それぞれ単独で行ってもよく、それらを併用して行ってもよい。
高温蒸気を発生させる手段としては公知のもの、例えば加熱蒸気発生装置(例えば、富士電機サーモシステムズ株式会社製、型式:IHSS-20B)を用いることができる。
加熱された加熱容器としては、ドラム型の缶壁加熱型乾燥機を挙げることができる。加熱容器の設定温度(缶壁温度の設定)としては、200℃~330℃に設定する態様を挙げることができ、300℃程度に設定することが好ましい。 The tobacco leaf material having a water content of 2.5% by weight or less is heated so that the product temperature of the tobacco leaf material is 100 to 200 ° C. As a specific heating method, a method in which high-temperature steam (200 ° C. or higher) or high-temperature air is brought into contact, or a method in which a heating container heated to 200 ° C. or higher is brought into contact.
The method of contacting the high temperature steam and the method of contacting the heated container may be performed independently or in combination.
As a means for generating high-temperature steam, a known one, for example, a heating steam generator (for example, model: IHSS-20B, manufactured by Fuji Electric Thermo Systems Co., Ltd.) can be used.
An example of the heated heating container is a drum-type can wall heating dryer. Examples of the set temperature of the heating container (setting of the can wall temperature) include an embodiment in which the temperature is set to 200 ° C. to 330 ° C., and preferably about 300 ° C.
また、前記の加熱工程にかかる時間は、加熱されるたばこ葉原料の量や、装置の大きさなどにより条件が異なってくるが、たばこ葉原料の品温が100~200℃となる時間として2秒以上加熱することで、膨嵩性を十分に高めることができ、香味も大きく変化させることができるので好ましい。この加熱時間は、たばこ葉原料の品温が100~200℃となる時間として30秒以上、特に好ましくは120秒以上加熱するようにすることが、たばこ葉原料の膨嵩性を高める観点から好ましい。品温が200℃を超えた状態でたばこ葉原料を加熱しすぎることによりたばこ葉原料の破砕や炭化などの不都合が生じることを回避することが重要であり、品温が200℃以下になる状態を保持できる状態であれば加熱時間の上限は適宜設定可能である。
上記の加熱工程(本加熱)の時間は、たばこ葉原料の水分含有量が2.5重量%以下になっており、かつ品温が100~200℃になっているときの時間を意味する。 By heating under the condition that the product temperature of the tobacco leaf material having a water content of 2.5% by weight or less is 100 ° C. or more, the bulkiness of the tobacco leaf is increased and the change in flavor is increased. The carbonization of the tobacco leaf can be prevented by heating the tobacco leaf raw material having a moisture content of 2.5% by weight or less under the condition that the product temperature is 200 ° C. or less. More preferable product temperature conditions are 120 ° C. or more and 200 ° C. or less.
The time required for the heating step varies depending on the amount of tobacco leaf raw material to be heated and the size of the apparatus, but the time required for the product temperature of the tobacco leaf raw material to be 100 to 200 ° C. is 2 Heating for 2 seconds or more is preferable because the bulkiness can be sufficiently increased and the flavor can be greatly changed. The heating time is preferably 30 seconds or more, particularly preferably 120 seconds or more as the time when the temperature of the tobacco leaf raw material becomes 100 to 200 ° C., from the viewpoint of increasing the bulkiness of the tobacco leaf raw material. . It is important to avoid inconveniences such as crushing and carbonization of the tobacco leaf material by overheating the tobacco leaf material with the product temperature exceeding 200 ° C., and the product temperature is 200 ° C. or less. If it is a state which can hold | maintain, the upper limit of heating time can be set suitably.
The time of the heating step (main heating) means the time when the moisture content of the tobacco leaf material is 2.5% by weight or less and the product temperature is 100 to 200 ° C.
加熱手段により加熱されたたばこ葉原料を、熱電対を差し込んだデュアー瓶に2秒以内に流し込み、これを熱電対に十分に接触させ、コルク栓をして静置して表示される最高温度を品温とする。 In addition, the product temperature of the tobacco leaf raw material in the present invention is a temperature measured by the following method.
The tobacco leaf material heated by the heating means is poured into a dewar into which a thermocouple is inserted within 2 seconds, which is brought into sufficient contact with the thermocouple, and left to stand at the maximum temperature displayed with a cork stopper. The product temperature.
本発明でいう刻み幅とは、たばこ裁刻機で原料葉たばこを裁刻する際に設定される値である。たばこ葉の裁刻とは原料葉たばこを一定の幅の細長い繊維状に刻む操作であり、刻まれたものをたばこ刻という。裁刻を行う装置を裁刻機と呼び、回転型裁刻機や栽落型裁刻機が一般的な装置であるが、これらの装置でたばこを裁刻する際に原料葉たばこを刻む幅として設定する値を刻み幅と呼ぶ。 As the form of the tobacco leaf material used in the method for producing a tobacco material of the present invention, a tobacco leaf material that has been cut or a tobacco leaf material that has not been cut can be used. In addition, the tobacco leaf raw material may be either a tobacco leaf divided into a mesophyll portion (lamina) or a vein portion (central bone), or may include a tobacco stem portion that is not a tobacco leaf portion. Examples of tobacco leaf materials include those cut to a step width of 0.1 to 2.0 mm. The step size can be appropriately determined according to the use of the tobacco material, for example, the type of cigarette or oral tobacco. As tobacco leaf varieties, main varieties such as yellow varieties, Burley varieties, native varieties, oriental varieties, and fermented leaves using them can be used.
The step width referred to in the present invention is a value set when cutting a raw leaf tobacco with a tobacco cutting machine. Tobacco leaf cutting is an operation that cuts raw leaf tobacco into long and narrow fibers with a certain width. A device that performs cutting is called a cutting machine, and a rotary type cutting machine or a cutting type cutting machine is a common device, but when cutting tobacco with these devices, the width to cut the raw leaf tobacco The value to be set is called step size.
種々のたばこ製品を作製するための工程としては、得られたたばこ材料に香料のような添加剤を添加する工程を挙げることができる。また、必要に応じて調湿工程を含ませてもよい。
本発明の製造方法を用いて得られるたばこ材料は、以下のような種々のたばこ製品の用途に用いる態様を挙げることができる。 The manufacturing method of the tobacco material of the present invention can include a known process in addition to the above heating process. For example, a step for cooling the tobacco material after the heating step and various steps necessary for smoking various tobacco products, such as cigarettes and smokeless tobacco, may be included as appropriate.
Examples of a process for producing various tobacco products include a process of adding an additive such as a fragrance to the obtained tobacco material. Moreover, you may include a humidity control process as needed.
Examples of the tobacco material obtained by using the production method of the present invention include the following embodiments used for various tobacco products.
本発明の製造方法を用いて得られたたばこ材料をシガレットに用いた場合には、高い煙量感が得られる。
シガレットのたばこ材料に含まれる本発明で得られるたばこ材料の割合は5~100重量%である態様を挙げることができる。 As a manufacturing method of a cigarette, a well-known manufacturing method can be used without a special restriction | limiting except using what was obtained using the manufacturing method of said invention as a tobacco material. The cigarette may be either with or without a filter.
When the cigarette material obtained using the production method of the present invention is used for a cigarette, a high feeling of smoke is obtained.
The cigarette material of the present invention contained in the cigarette cigarette material may be 5 to 100% by weight.
包装材としては特段の限定なく用いることができるが、セルロース系の不織布などが好ましく用いられる。
無煙たばこ製品として、例えばガムとする場合は、本発明の製造方法を用いて得られる上記たばこ材料を公知のガムベースと公知の方法を用いて混合することで得られる。かみたばこやかぎたばこ、圧縮たばこについても、本発明の製造方法を用いて得られる上記たばこ材料を用いること以外は、公知の方法を用いて得ることができる。
また、無煙たばこ材料に含まれる本発明の製造方法で得られるたばこ材料の割合は、5~100重量%である態様を挙げることができる。 An example of smokeless tobacco is snus. A well-known method can be used also about manufacture of snus. In this case, the tobacco material produced by the above-described production method can be obtained by filling a packaging material using a raw material such as a nonwoven fabric using a known method. For example, the amount of tobacco material is adjusted and filled, and snus is obtained by sealing by means such as heat sealing.
The packaging material can be used without any particular limitation, but a cellulose-based nonwoven fabric is preferably used.
When the smokeless tobacco product is, for example, a gum, it is obtained by mixing the tobacco material obtained using the production method of the present invention with a known gum base and a known method. A chewing tobacco, a hooked tobacco, and a compressed tobacco can also be obtained using a known method except that the tobacco material obtained using the production method of the present invention is used.
In addition, a mode in which the ratio of the tobacco material obtained by the production method of the present invention contained in the smokeless tobacco material is 5 to 100% by weight can be mentioned.
本実施例で用いた加熱乾燥器は図4で例示されている型のものである。シリンダー1は内寸が直径400mm、長手方向長さが1900mmの円筒形であり、4rpmで回転し、原料入口位置が原料出口位置と比較して、高い位置となるように傾けている。傾ける角度は、水平方向に対して3°である。
たばこ葉原料は原料入口部2からロータリーバルブ3を介して、排気ダクト4および内部に羽根ブレード10を有するシリンダー1に投入した。
シリンダー1はヒーター6および過熱水蒸気発生装置7を用いて製造した過熱水蒸気によって加熱した。
たばこ葉原料はシリンダー1の回転および傾斜により搬送され、原料出口部9から取り出した。
加熱蒸気発生装置は、富士電機サーモシステムズ株式会社製(型式:IHSS-20B)を用いた。 Tobacco leaf material having a water content of 12% by weight (inner bone cut to have a step width of 0.2 mm) was put into a cylinder-type heat dryer and heated from room temperature (25 ° C.). Heating was performed by contacting can wall heating using a cylinder-type heating dryer heated to 300 ° C. and 320 ° C. heating steam.
The heat dryer used in this example is of the type illustrated in FIG. The
Tobacco leaf raw material was introduced from the
The
The tobacco leaf material was conveyed by rotation and inclination of the
As the heating steam generator, Fuji Electric Thermo Systems Co., Ltd. (model: IHSS-20B) was used.
表1に記載の処理時間は、加熱を開始してからの連続時間を示している。また、品温が100℃以上であるときの加熱時間も示す。 The relationship between the heating time and the product temperature of the tobacco leaf material is as shown in Table 1.
The processing time described in Table 1 indicates a continuous time from the start of heating. The heating time when the product temperature is 100 ° C. or higher is also shown.
1.測定試料を予め温度22℃、湿度60%_R.H.の環境で72時間以上静置しておく。
2.上記試料を十分に混和する。
3.試料を8~10g量り取る。
4.シリンダーに試料を入れ、膨嵩性測定器(ボルグワルド社製、DD-60A)にセットし、測定を開始する。荷重時間は30秒とする。
5.30秒後、表示される値(試料の高さ)を読み取る。
6.膨嵩性を以下の式で計算する。
膨嵩性=(A * h) / W * 0.1
A:シリンダー底面積
h:試料高さ(表示値)
W:測定試料重量 <Method of measuring bulkiness>
1. The measurement sample is allowed to stand for 72 hours or more in an environment of a temperature of 22 ° C. and a humidity of 60% _R.H. In advance.
2. Mix the sample thoroughly.
3. Weigh 8-10 g of sample.
4). Put the sample in the cylinder, set it in the bulge measuring instrument (Borgwald, DD-60A) and start the measurement. The loading time is 30 seconds.
5. After 30 seconds, read the displayed value (sample height).
6). The bulkiness is calculated by the following formula.
Bulkiness = (A * h) / W * 0.1
A: Cylinder bottom area h: Sample height (displayed value)
W: Measurement sample weight
<たばこ品温測定方法>
1.シリンダー出口で、たばこ葉原料をステンレス製のスコップで採取する。
2.熱電対(林電工社製)を差し込んだデュワー瓶(Thermos社製、サーモカットD-500)に、試料を2秒以内に流し込む。棒で試料を押し、熱電対に十分接触させる。
3.コルク栓をして静置し、表示される最高温度を、たばこ品温とする。 The method for measuring the product temperature of the tobacco leaf material in the examples is as follows.
<Method for measuring tobacco product temperature>
1. At the cylinder outlet, the tobacco leaf material is collected with a stainless steel scoop.
2. The sample is poured into a Dewar bottle (Thermos, Thermo Cut D-500) into which a thermocouple (Rinden Electric Co., Ltd.) is inserted within 2 seconds. Push the sample with a stick and make good contact with the thermocouple.
3. Put the cork stopper and let it stand, and let the maximum temperature displayed be the tobacco product temperature.
2 原料入口部
3 ロータリーバルブ
4 排気ダクト
5 ダンパー
6 ヒーター
7 過熱水蒸気発生装置
8 バルブ
9 原料出口部
10 羽根ブレード DESCRIPTION OF
Claims (8)
- たばこ材料の製造方法であって、含水量が2.5重量%以下のたばこ葉原料を、品温が100~200℃となる条件下で加熱する工程を含む、たばこ材料の製造方法。 A method for producing a tobacco material, comprising a step of heating a tobacco leaf material having a water content of 2.5% by weight or less under a condition where the product temperature is 100 to 200 ° C.
- 前記加熱工程の前に、たばこ葉原料の水の含有量を2.5重量%以下にまで減少させる乾燥工程を含む、請求項1に記載の製造方法。 The production method according to claim 1, further comprising a drying step for reducing the water content of the tobacco leaf material to 2.5 wt% or less before the heating step.
- 前記乾燥工程に供されるたばこ葉原料の水の含有量が、10~40重量%である、請求項1または2に記載の製造方法。 The production method according to claim 1 or 2, wherein the content of water of the tobacco leaf material used in the drying step is 10 to 40% by weight.
- 前記たばこ葉原料が、刻み幅0.1~2.0mmのラミナ、中骨またはこれらの混合物を含む、請求項1~3のいずれか一項に記載の製造方法。 The production method according to any one of claims 1 to 3, wherein the tobacco leaf material contains lamina having a step width of 0.1 to 2.0 mm, a middle bone, or a mixture thereof.
- 請求項1~4のいずれか一項に記載の製造方法で作製されたたばこ材料。 A tobacco material produced by the production method according to any one of claims 1 to 4.
- 請求項5に記載のたばこ材料を用いたたばこ製品。 Tobacco products using the tobacco material according to claim 5.
- 請求項5に記載のたばこ材料を用いたシガレット。 A cigarette using the tobacco material according to claim 5.
- 請求項5に記載のたばこ材料を用いた無煙たばこ製品。 A smokeless tobacco product using the tobacco material according to claim 5.
Priority Applications (6)
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RU2016128821A RU2649926C2 (en) | 2013-12-26 | 2014-12-19 | Method of producing tobacco material and tobacco material produced by said production method |
ES14874689T ES2821431T3 (en) | 2013-12-26 | 2014-12-19 | Method of producing tobacco material and tobacco material produced by said production method |
EP14874689.4A EP3087851B1 (en) | 2013-12-26 | 2014-12-19 | Method for producing tobacco material, and tobacco material produced by said production method |
PL14874689T PL3087851T3 (en) | 2013-12-26 | 2014-12-19 | Method for producing tobacco material, and tobacco material produced by said production method |
JP2015554833A JP6560125B2 (en) | 2013-12-26 | 2014-12-19 | Tobacco material manufacturing method and tobacco material manufactured by the manufacturing method |
KR1020167014771A KR20160082542A (en) | 2013-12-26 | 2014-12-19 | Method for producing tobacco material, and tobacco material produced by said production method |
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EP (1) | EP3087851B1 (en) |
JP (2) | JP6560125B2 (en) |
KR (1) | KR20160082542A (en) |
ES (1) | ES2821431T3 (en) |
MY (2) | MY176773A (en) |
PL (1) | PL3087851T3 (en) |
RU (1) | RU2649926C2 (en) |
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JP2021516549A (en) * | 2018-03-12 | 2021-07-08 | ブリティッシュ アメリカン タバコ (インヴェストメンツ) リミテッドBritish American Tobacco (Investments) Limited | Methods for processing tobacco materials, equipment for processing tobacco materials, processed tobacco materials and their use |
JP2021523732A (en) * | 2018-07-11 | 2021-09-09 | ブリティッシュ アメリカン タバコ (インヴェストメンツ) リミテッドBritish American Tobacco (Investments) Limited | How to treat chopped petiole tobacco |
WO2021220790A1 (en) * | 2020-04-28 | 2021-11-04 | 日本たばこ産業株式会社 | Method for manufacturing processed leaf tobacco, and method for storing leaf tobacco |
CN113995166A (en) * | 2020-07-28 | 2022-02-01 | 贵州中烟工业有限责任公司 | Tobacco shred, preparation method thereof, smoking substrate and heating non-combustible tobacco product |
WO2023112518A1 (en) * | 2021-12-15 | 2023-06-22 | 日本たばこ産業株式会社 | Tobacco material containing tobacco stem raw material |
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Also Published As
Publication number | Publication date |
---|---|
EP3087851A4 (en) | 2017-08-30 |
TW201531240A (en) | 2015-08-16 |
RU2016128821A (en) | 2018-01-31 |
PL3087851T3 (en) | 2020-12-28 |
MY193133A (en) | 2022-09-26 |
KR20160082542A (en) | 2016-07-08 |
ES2821431T3 (en) | 2021-04-26 |
JP2018108087A (en) | 2018-07-12 |
JP6545305B2 (en) | 2019-07-17 |
EP3087851B1 (en) | 2020-08-19 |
MY176773A (en) | 2020-08-21 |
JPWO2015098743A1 (en) | 2017-03-23 |
TWI573533B (en) | 2017-03-11 |
JP6560125B2 (en) | 2019-08-14 |
EP3087851A1 (en) | 2016-11-02 |
RU2649926C2 (en) | 2018-04-05 |
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