WO2015035585A1 - Composition de shampooing contenant un agent complexant pour prévenir efficacement la chute de cheveux - Google Patents

Composition de shampooing contenant un agent complexant pour prévenir efficacement la chute de cheveux Download PDF

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Publication number
WO2015035585A1
WO2015035585A1 PCT/CN2013/083393 CN2013083393W WO2015035585A1 WO 2015035585 A1 WO2015035585 A1 WO 2015035585A1 CN 2013083393 W CN2013083393 W CN 2013083393W WO 2015035585 A1 WO2015035585 A1 WO 2015035585A1
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WIPO (PCT)
Prior art keywords
weight
composition
composite active
vitamin
shampoo
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Application number
PCT/CN2013/083393
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English (en)
Chinese (zh)
Inventor
胡卫华
庄严
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拉芳家化股份有限公司
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Priority to CN201380006887.9A priority Critical patent/CN104168883B/zh
Priority to PCT/CN2013/083393 priority patent/WO2015035585A1/fr
Publication of WO2015035585A1 publication Critical patent/WO2015035585A1/fr

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Classifications

    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q7/00—Preparations for affecting hair growth
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36—Carboxylic acids; Salts or anhydrides thereof
    • A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60—Sugars; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60—Sugars; Derivatives thereof
    • A61K8/602—Glycosides, e.g. rutin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67—Vitamins
    • A61K8/673—Vitamin B group
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9789—Magnoliopsida [dicotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00—Preparations for care of the hair
    • A61Q5/02—Preparations for cleaning the hair

Definitions

  • Fragrance compound containing high-efficiency anti-debinding agent Fragrance compound containing high-efficiency anti-debinding agent
  • the invention belongs to the field of daily chemicals, and particularly relates to a shampoo composition containing a high-efficiency anti-debonding agent.
  • Hair is the first element of human beauty, and hair loss is a major social problem facing many people. Hair loss is the biggest damage to the appearance. It will affect the shape of the person, reduce the attractiveness and charm, and it will be a great blow to self-confidence. It will also affect career choice, marriage, and even future.
  • the hair's growth cycle can be divided into raw to maintain normal 50-75 hairs per day. Abnormal hair loss or excessive shedding causes pathological hair loss.
  • the main causes of hair loss include internal factors such as mental factors, congenital genetic factors and hormones, and nutritional factors such as protein, amino acids, and vitamins, as well as seborrheic alopecia.
  • It is an object of the present invention to provide a shampoo composition comprising a synergistic anti-hair loss complex derived from plant and biochemical synthesis, which can promote hair growth, improve the ratio of long-term and rest periods of the head, and promote healthy formation.
  • the scalp and hair help the hair loss to return to normal hair loss.
  • the shampoo contains: the shampoo contains: (A) an anionic surfactant in an amount of from 0.5% to 40% by weight of the composition;
  • an anti-de-complexing active comprising from 0.1% to 10% by weight of the composition, said anti-de-complexing active comprising, in addition to water,
  • Hydrolyzed soy protein comprising 1-5% by weight of the composite active
  • amino acid mixture is arginine: acetyl tyrosine: citrulline: ornithine hydrochloride is mixed in a weight ratio of 1: 1: 1: 1:
  • vitamin B group mixture is vitamin B3: vitamin B5: vitamin H is mixed in a weight ratio of 1: 1: 1:
  • Zinc gluconate 1-5% by weight of the composite active
  • PEG-12 disiloxane based on 5% by weight of the composite active
  • the shampoo composition of the present invention wherein the anti-de-complexing active is hydrolyzed soy protein, an amino acid mixture containing arginine, acetyl tyrosine, citrulline, ornithine hydrochloride, glucosamine hydrochloride, A mixture of a vitamin B group containing vitamin B3, vitamin B5, vitamin H, zinc gluconate, ginseng essence, May burdock root essence and a combination of PEG-12 dimercaptosilicone oil and polyquaternium-11.
  • the shampoo composition of the present invention wherein the anionic surfactant is selected from the group consisting of: alkyl sulfate salts, alkyl polyoxyethylene ether sulfate salts, fatty acid monoglyceride sulfates, alkyl sulfonates, N-acyl groups At least one of a salt, an N-glutamate, and a thiophosphate salt.
  • the shampoo composition of the present invention wherein the ratio of the sodium cocoamphoacetate to the alkyl glucoside is
  • the shampoo composition of the present invention wherein the cationic polymer is selected from the group consisting of at least one of a cationic cellulose polymer and a cationic guar polymer.
  • the present invention has the following advantages:
  • the shampoo composition of the present invention is a synergistic anti-hair loss complex derived from plant and biochemical synthesis, which can promote hair growth, improve the ratio of long-term and rest periods of the head, and promote the formation of healthy scalp and hair, and help The hair loss patient returns to normal hair loss rate.
  • the shampoo composition of the present invention contains from 0.1% to 10% by weight of the composition, preferably from 5% to 10%, of the anti-de-complexing active, which is a clear pale yellow liquid with ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ . ⁇ .
  • Hydrolyzed soy protein hydrolyzed soybean sulfurized peptide, MW "15000Da” can provide cell nutrition and growth regulation, and promote protein biosynthesis; amino acids including tyrosine, sulphuric acid , ornithine, citrulline is a precursor of protein and melanin; alcohol-based glucose strengthens the dermal papilla and its surrounding matrix; vitamin B group regulates cell nutrition; zinc salt regulates oil secretion; ginseng essence and May burdock root extract The substance can improve microcirculation; silicone and polyquaternium provide conditioning of the hair.
  • Hydrolyzed soy protein hydrolyzed soybean sulfurized peptide, MW "15000Da
  • amino acids including tyrosine, sulphuric acid , ornithine, citrulline is a precursor of protein and melanin
  • alcohol-based glucose strengthens the dermal papilla and its surrounding matrix
  • vitamin B group regulates cell nutrition
  • zinc salt regulates oil secretion
  • the shampoo composition of the present invention comprises a composition of 5.0% to 40% by weight of the composition of ammonium lauryl sulfate and lauryl ammonium polyoxyethylene sulfate, the ammonium lauryl sulfate and lauryl polyoxyethylene acid.
  • the ratio of ammonium sulfate is 1: 2 - 2: 1.
  • the ammonium lauryl citrate is abbreviated as K 12 A or SLSA, and its structural formula is:
  • ROS0 3 NH 4 + , R C 12 _C 16 fluorenyl group, having an active content of 70%, and its appearance is a white or pale yellow paste.
  • the ammonium lauryl sulfate has a mild action, can leave a good conditioning on the hair, has good bubble performance and cleaning performance, and can provide better compatibility for the appearance and viscosity rheological properties of the product.
  • the fatty alcohol polyoxyethylene ether LS LS is referred to as AESA, and its structural formula is
  • the commercial product of the ammonium laureth sulfate ammonium sulfate product has an active content of 70%, and its appearance is a white or pale yellow paste.
  • the lauryl polyoxyethylene ether ammonium sulfate also has the characteristics of a nonionic surfactant, and still has a good detergency in hard water.
  • the combination of ammonium lauryl sulfate and lauryl polyoxyethylene ⁇ 4 ammonium sulfate can produce good synergistic effects, such as: good washing ability, excellent mildness and excellent thickening performance.
  • the composition of the shampoo composition of the present invention comprises from 1.0% to 1.0% by weight of the composition of sodium cocoamphoacetate and alkyl glucoside, the ratio of sodium cocoamphoacetate to alkyl glucoside. For 3: ⁇ : 3.
  • the sodium cocoamphoacetate is a colorless to slightly yellow transparent viscous liquid, and the commercial product has an active content of 30%, a viscosity of 5000-10000 at 25 ° C, and a sodium chloride content of less than 9 0%, 1% aqueous solution has a pH of 6. 0 ⁇ 8. 0, and its structural formula is RN (CH2C00Na) 2 , the coconut oil-based amphoteric sodium acetate has low irritation, is particularly mild to the skin and eyes, and an anionic surface.
  • the active agent can significantly reduce the irritation, and has good foaming power.
  • the foam is rich and fine, and the skin feel is good, which can significantly improve the foam state of the formulation system.
  • the alkyl glucoside comprises lauryl glucoside, coco glucoside, decyl glucoside, and octyl/decyl glucoside, preferably decyl glucoside, which is a pale yellow turbid viscous liquid, which is commercially available. 5, 25, 25, 5, 25, 5, 25 Under the condition of °C, the viscosity is 1000-6000.
  • the mercaptoglucoside is derived from nature and has excellent mild cleansing ability to improve the foaming properties of shampoo. Increase the amount of foam and foam stability.
  • the combination of sodium cocoamphoacetate and decyl glucoside has good foam and skin compatibility, minimizing irritation.
  • the cationic composition of the present invention comprises from 0.05% to 3.0% by weight of the composition of the cationic polymer, the cationic polymer being selected from the group consisting of: at least one of a cationic cellulose polymer and a cationic guar polymer.
  • a cationic guar gum is preferred.
  • the cationic guar gum is a product obtained by quaternizing guar gum, and the main component thereof is guar gum propyltrimethylammonium chloride, and a series of cationic guar gum can be obtained according to the degree of substitution.
  • the product has a preferred degree of substitution of from 0.1 to 0.2, a nitrogen content of from 1. 3-1.
  • the cationic guar gum used in the present invention at 25 ° C, 1 ° /.
  • the viscosity of the aqueous solution is from 3500 mPa ⁇ s to 4500 mPa ⁇ s;
  • the cationic cellulose polymer is a copolymer of hydroxyethyl cellulose and alkyltrimethyl ammonium chloride, which can be classified according to the degree of cationic substitution: There are three types of high cationic substitution degree JR, medium cationic substitution degree LR and low cationic substitution degree LK, and cationic cellulose having a degree of cationic substitution is preferred.
  • the shampoo compositions of the present invention may also contain other optional ingredients including pearlizing agents, viscosity modifiers, chelating agents, pH adjusting agents, preservatives, colors, flavors and the like.
  • the pearlescent agent comprises from 0. 05% to 3.0% by weight of the composition, and non-limiting examples of the pearlizing agent are: ethylene glycol stearic acid monoester and ethylene glycol stearic acid diester, single hard Fatty acid and propylene glycol palmitate and glycerides, magnesium stearate amide, magnesium stearate, finely divided zinc oxide and titanium dioxide, preferably ethylene glycol stearate.
  • the viscosity adjusting agent comprises 0.1% to 5.0% by weight of the composition
  • non-limiting examples of the viscosity adjusting agent are: sodium chloride, ammonium chloride, monoethanolamine chloride, sodium sulfate, ammonium phosphate , hydroxyethyl cellulose, hydroxypropyl cellulose, acrylic acid and long-chain alkyl methacrylate copolymer, acrylate/stearyl ether-20/mercapto acrylate copolymer, decyl glucoside polyoxyethylene Ether (120) dioleate and the like. 01% ⁇ The chelating agent by weight of the composition of 0.01% to 0.
  • non-limiting examples of the chelating agent are: ethylenediaminetetraacetic acid, disodium edetate, trisodium ethylenediaminetetraacetate, tetrasodium ethylenediaminetetraacetate, etc., preferably ethylene ⁇ 5. 5 ⁇ 6.
  • the selection of the preservatives, flavors and pigments meets the requirements of cosmetic hygiene standards and uses safe raw materials.
  • the shampoo compositions of the present invention are supplemented with water to the required amount in addition to the components described above. Preparation
  • the shampoo compositions of the present invention can be prepared by any of the known or otherwise effective techniques suitable for providing shampoo compositions.
  • the methods of preparing the shampoo compositions of the present invention include conventional formulation and mixing techniques.
  • the shampoo compositions of the present invention are used in a conventional manner for cleansing and conditioning hair, and include the following steps:
  • the effective dose generally ranging from 1 gram to 50 grams, preferably from 2 to 20 grams;
  • shampoo compositions of the present invention are non-limiting examples.
  • the examples are given for illustrative purposes only and are not to be construed as limiting the invention, as Many modifications of the invention are possible on the basis of the scope.
  • all concentrations are by weight unless otherwise stated.
  • the term "minor matter” refers to those substances which are optional, such as preservatives, viscosity modifiers, pH adjusters, perfumes, pigments, etc. These small amounts of materials will be selected
  • PREPARATION EXAMPLE I - X Suitable methods for preparing the shampoo compositions of Examples I-X are as follows: Add an appropriate amount of water to the reaction tank, add guar gum for dispersion under slow agitation, and heat to 60 with slow agitation. From °C to 80 ° C, add an appropriate amount of citric acid to neutralize. Next, add ammonium lauryl sulfate, ammonium laureth sulfate, sodium cocoamphoacetate, decyl glucoside, ethylene glycol stearate, disodium edetate (if these substances are used) After completely dissolving and dissolving these substances, keep them warm for 30 minutes and start to cool down.
  • the preferred embodiment of the invention is: Component content % by weight ammonium lauryl ammonium sulfate (70%) 10. 0 Lauryl alcohol polyoxyethylene ether ammonium sulfate (70%) 12. 0 Cocoamphos sodium acetate 3. 0 Mercaptoglucoside 5.0 guar 0.3 anti-decomplex active 8
  • Test Method Forty volunteers with hair loss who were allergic, no wounds, and no systemic local disease were selected. The ratio of growth period and rest period of the patient's hair was lower than normal. Before the trial, the patient was evaluated for sensory and hair images, and the patient was treated with the best embodiment of the shampoo, for 112 days, and for sensory evaluation and hair image evaluation on days 56 and 112. During the trial, volunteers used the shampoo at the usual frequency of shampooing, requiring the shampoo to stay on the hair for 3-5 minutes and perform a gentle scalp massage before rinsing with warm water. For the sensory evaluation of the hair before and after the use of the shampoo, see Table 1, Table 2 and hair image evaluation are shown in Table 3:
  • Forehead head head total In the first 56 days of the growing season 30% 60% 140% 80% Growth rate 112 days 110% 95% 170% 120%

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Abstract

La présente invention concerne une composition de shampooing contenant un agent complexant pour prévenir efficacement la chute de cheveux, le shampooing contenant en plus de l'eau : (A) 5,0 % à 40 % de tensioactif anionique par rapport au poids de la composition; (B) 1,0 % à 10,0 % d'une composition d'acétate de sodium amphotère contenant de l'huile de coco et de glucoside d'alkyle par rapport au poids de la composition; (C) 0,1 % à 10 % d'un principe actif composite antichute de cheveux par rapport au poids de la composition, le principe actif composite antichute de cheveux étant des protéines de soja hydrolysées, des acides aminés, des osamines, des groupes de vitamine B, des sels de zinc, de l'essence de ginseng, de l'essence de racine de bardane et une composition constituée de silicium organique et de sels d'ammonium polyquaternaire; et (D) 0,05 % à 3,0 % de polymère cationique par rapport au poids de la composition.
PCT/CN2013/083393 2013-09-12 2013-09-12 Composition de shampooing contenant un agent complexant pour prévenir efficacement la chute de cheveux WO2015035585A1 (fr)

Priority Applications (2)

Application Number Priority Date Filing Date Title
CN201380006887.9A CN104168883B (zh) 2013-09-12 2013-09-12 一种含高效防脱复合剂的香波组合物
PCT/CN2013/083393 WO2015035585A1 (fr) 2013-09-12 2013-09-12 Composition de shampooing contenant un agent complexant pour prévenir efficacement la chute de cheveux

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/CN2013/083393 WO2015035585A1 (fr) 2013-09-12 2013-09-12 Composition de shampooing contenant un agent complexant pour prévenir efficacement la chute de cheveux

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Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105213251B (zh) * 2015-09-22 2017-11-07 拉芳家化股份有限公司 一种具有热感的防脱香波
CN107454837B (zh) * 2016-09-12 2019-08-20 拉芳家化股份有限公司 一种含头发保湿复合剂的香波组合物
CN106265458A (zh) * 2016-10-08 2017-01-04 拉芳家化股份有限公司 一种含高效抗老化及防脱复合剂的香波组合物
JP6997222B2 (ja) 2017-06-23 2022-01-17 ザ プロクター アンド ギャンブル カンパニー 皮膚の外観を改善するための組成物及び方法
JP2021530447A (ja) 2018-07-03 2021-11-11 ザ プロクター アンド ギャンブル カンパニーThe Procter & Gamble Company 皮膚状態の治療方法
WO2020132930A1 (fr) * 2018-12-26 2020-07-02 拉芳家化股份有限公司 Composition de shampoing antipelliculaire antipelliculaire contenant du zinc à plusieurs composants
JP2023528616A (ja) 2020-06-01 2023-07-05 ザ プロクター アンド ギャンブル カンパニー ビタミンｂ３化合物の皮膚への浸透を改善する方法
US10959933B1 (en) 2020-06-01 2021-03-30 The Procter & Gamble Company Low pH skin care composition and methods of using the same

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JP3834570B2 (ja) * 2003-07-23 2006-10-18 株式会社ピュール 染毛効果を有する養毛・育毛剤
CN101835462A (zh) * 2007-10-25 2010-09-15 荷兰联合利华有限公司 头发护理组合物
WO2010121919A1 (fr) * 2009-04-23 2010-10-28 Unilever Plc Composition de soin capillaire comprenant un complexe trichogénique et un azole
DE102011089357A1 (de) * 2011-12-21 2012-08-23 Henkel Ag & Co. Kgaa Haarbehandlungsmittel mit kationischen Pflegestoffen und alpha-Hydroxysäuren
CN102920619A (zh) * 2012-10-09 2013-02-13 拉芳家化股份有限公司 含少量硫酸盐阴离子表面活性剂的调理香波组合物

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JP3834570B2 (ja) * 2003-07-23 2006-10-18 株式会社ピュール 染毛効果を有する養毛・育毛剤
CN101835462A (zh) * 2007-10-25 2010-09-15 荷兰联合利华有限公司 头发护理组合物
WO2010121919A1 (fr) * 2009-04-23 2010-10-28 Unilever Plc Composition de soin capillaire comprenant un complexe trichogénique et un azole
DE102011089357A1 (de) * 2011-12-21 2012-08-23 Henkel Ag & Co. Kgaa Haarbehandlungsmittel mit kationischen Pflegestoffen und alpha-Hydroxysäuren
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