WO2014119798A1 - Method for manufacturing beverage containing processed edible-plant powder having improved dispersion stability or redispersability - Google Patents

Method for manufacturing beverage containing processed edible-plant powder having improved dispersion stability or redispersability Download PDF

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Publication number
WO2014119798A1
WO2014119798A1 PCT/JP2014/052583 JP2014052583W WO2014119798A1 WO 2014119798 A1 WO2014119798 A1 WO 2014119798A1 JP 2014052583 W JP2014052583 W JP 2014052583W WO 2014119798 A1 WO2014119798 A1 WO 2014119798A1
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Prior art keywords
beverage
edible plant
powdered
powdered edible
product
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PCT/JP2014/052583
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French (fr)
Japanese (ja)
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今澤 武司
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株式会社明治
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Application filed by 株式会社明治 filed Critical 株式会社明治
Priority to CN201480007044.5A priority Critical patent/CN104968220A/en
Priority to JP2014559805A priority patent/JP6441083B2/en
Priority to SG11201504556XA priority patent/SG11201504556XA/en
Publication of WO2014119798A1 publication Critical patent/WO2014119798A1/en
Priority to HK15110756.6A priority patent/HK1209982A1/en

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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/38Other non-alcoholic beverages
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C9/00Milk preparations; Milk powder or milk powder preparations
    • A23C9/152Milk preparations; Milk powder or milk powder preparations containing additives
    • A23C9/156Flavoured milk preparations ; Addition of fruits, vegetables, sugars, sugar alcohols or sweeteners

Definitions

  • the present invention relates to a beverage containing a powdered edible plant processed product, and improves the dispersion stability of the insoluble solid (powdered edible plant processed product) in the beverage to suppress precipitation.
  • the present invention relates to a beverage whose redispersibility is improved so that the original dispersion state can be easily restored simply by shaking lightly, and a method for producing the same.
  • the present invention also relates to a method for improving the dispersion stability of an insoluble solid (powdered edible plant processed product) in the beverage, including a powdered edible plant processed product,
  • the present invention relates to a method for improving the redispersibility so that the original dispersion state can be easily restored simply by shaking lightly.
  • Matcha is used as a beverage or beverage ingredient or as an additive to various foods and drinks because of its deep natural flavor. Moreover, with the recent health consciousness, dry powders of green and yellow vegetables such as kale and barley (young leaves) are used as beverages or beverage ingredients, or as additives for various foods and drinks.
  • these dry powders are all solids that are insoluble in water (insoluble solids), so when they are blended into beverages, especially in the case of packaged beverages that are filled into containers and distributed to the market.
  • the powder precipitates (settling) during distribution or storage, or it agglomerates and solidifies at the bottom of the container.
  • the vivid color of the dry powder of green and yellow vegetables fades or discolors due to the sterilization treatment performed in the manufacturing process, and the appearance and flavor (texture) of the beverage are impaired along with the above-mentioned precipitation problem. It can also be a cause.
  • a method of suppressing precipitation of insoluble solids by using a stabilizer such as cellulose or thickening polysaccharide is usually employed.
  • a method for improving green color retention and dispersion in an aqueous medium and solubility by incorporating a calcium agent derived from maltose and oyster shells into matcha (Patent Document 1),
  • a stabilizer and water or hot water are added to an insoluble solid such as matcha tea, homogenized at a pressure of 100 to 250 kg / cm 2 , and the stabilizer is dispersed in a colloidal form in the solution.
  • a method of stabilizing an object by holding it has also been proposed.
  • the texture and flavor of the beverage may become unnatural.
  • the use of stabilizers increases the cost of beverages.
  • powdered green tea powder having an average particle size of 7 to 20 ⁇ m is dispersed in water and homogenized at a pressure of 5 MPa or more at 20 to 90 ° C.
  • a method for suppressing precipitation aggregation (Patent Document 3) has been proposed.
  • this method can be applied to powdered green tea powder having an average particle size in the range of 7 to 20 ⁇ m, and it is complicated and practical considering that the average particle size of the powder needs to be adjusted in advance. There is a problem of lacking.
  • the present invention aims to solve the above-mentioned conventional problems. Specifically, the present invention relates to a beverage containing a powdered edible plant processed product, preferably without using a stabilizer, and stable dispersion of insoluble solids (powdered edible plant processed product) in the beverage. To provide a beverage whose redispersibility is improved so that the original dispersion state can be easily restored by simply shaking lightly even if it is precipitated, and a method for producing the same With the goal.
  • the present invention provides a dispersion containing a powdered edible plant processed product, preferably without using a stabilizer, to improve the dispersion stability of the insoluble solid (powdered edible plant processed product) in the beverage. It is an object of the present invention to provide a method for improving redispersibility so that the original dispersion state can be easily restored by simply shaking lightly even when precipitated.
  • the inventors of the present invention have made extensive studies in order to solve the above problems, and in producing a beverage containing a powdered processed edible plant, the powdered edible plant is used in water used for preparing the beverage.
  • a beverage prepared by the above method by blending a powdered edible plant processed product previously mixed with fats and oils (hereinafter used for beverage preparation)
  • Dispersion stability of powdered edible processed plant products in beverages is significantly improved compared to beverages prepared by mixing powdered edible processed plant products with water as they are (control beverages). It was found that precipitation that occurs over time is suppressed, and that the redispersibility of the resulting precipitate is significantly improved, and that the original dispersion state can be restored by simply shaking.
  • the present invention has been completed based on such knowledge and has the following embodiments.
  • the powdered edible plant processed product is a dry powder of at least one plant selected from the group consisting of tea, vegetables, fruits, cereals and beans, (I-1) to (I -4) The production method described in any one of the above.
  • the dispersion obtained in the step (a) does not contain water other than water derived from oils and fats used as raw materials and processed edible plants (I-1) to (I -5) The manufacturing method described in any one of.
  • (II) Beverage containing powdered edible plant processed product (II-1) Processed at least powdered edible plant obtained by the production method described in any one of (I-1) to (I-6) A beverage containing foods, fats and oils, and at least in a beverage compared to a beverage prepared without going through the step of mixing and dispersing the powdered edible plant processed product of (a) with fats and oils A beverage characterized in that the dispersion stability of the powdered edible plant product is improved, or the redispersibility of the powdered edible plant product in the beverage is improved.
  • (II-2) The beverage according to (II-1), wherein fading or discoloration of the powdered edible plant processed product in the beverage is further suppressed.
  • (III-2) In a process for producing a beverage containing a powdered edible plant processed product, (a) a step of dispersing the powdered edible plant processed product in oil and fat, and (b) a powdered edible plant processed A method for improving dispersion stability or redispersibility of a powdered edible plant processed product in a beverage, comprising a step of mixing a dispersion of the product and fat with water and homogenizing the mixture. (III-3) The method according to (III-2), further comprising a homogenization step between the steps (a) and (b). (III-4) The method according to any one of (III-1) to (III-3), wherein the water contains milk or a milk component.
  • (III-5) The method according to any one of (III-1) to (III-4), wherein a stabilizer and / or an emulsifier is not blended.
  • the powdered edible plant processed product is a dry powder of at least one plant selected from the group consisting of tea, vegetables, fruits, cereals and beans, (III-1) to (III -5) The method described in any one of the above.
  • (III-7) Dispersion obtained by dispersing powdered edible plant processed product in oil and fat does not contain water other than water derived from oil and fat used as raw material and processed edible plant product The method according to any one of (III-1) to (III-6).
  • III-8 A method of improving the dispersion stability or redispersibility of a powdered edible plant processed product in a beverage and suppressing discoloration of the powdered edible plant processed product in a beverage.
  • a powder containing powdered edible plant products such as matcha tea is preferably used without using a stabilizer or an emulsifier.
  • the dispersion stability of the insoluble solid (powdered edible plant product) in the beverage is improved.
  • the redispersibility can be improved so that it can be easily returned to the original dispersed state by simply shaking lightly.
  • the powdered edible processed plant is mixed with fats and oils and dispersed. Compared with a beverage prepared without undergoing a step of causing it to fade, discoloration and discoloration caused by heat sterilization and storage can also be suppressed.
  • the present invention is a beverage containing a powdered edible plant processed product, and at least a powdered edible plant processed in the beverage It is a method for producing a beverage characterized in that the dispersion stability of the product is improved, or the redispersibility of the processed powdered edible plant in the beverage is improved.
  • the production method can be carried out by at least the following steps (a) and (b): (A) a step of mixing and dispersing a powdered edible plant processed product in oil and fat; and (b) a step of mixing a dispersion of the powdered edible plant processed product and fat with water and homogenizing.
  • the “powdered edible plant product” used in the step (a) is a water-insoluble edible plant product prepared in a powder form. Specifically, it is prepared by crushing edible parts of plants such as fruits, vegetables (root vegetables, stem vegetables, leaf vegetables, flower vegetables, fruit vegetables) or tea leaves, preferably these dried It is a powder.
  • the “powdered edible plant product” of the present invention is a mixture prepared by arbitrarily combining two or more edible plants, even if it is prepared from one type of edible plant. There may be.
  • the “powder” of the present invention is not limited to the powder itself, but may be a powder processed into granules or solids (tablets, etc.).
  • the vegetables are not particularly limited, and include root vegetables (eg, carrots, burdock, radish, etc.), stem vegetables (eg, asparagus, onions, purple onions, etc.), leaf vegetables (eg, spinach, kale, Barley (young leaves), cabbage, Chinese cabbage, parsley, basil, mugwort, watercress, tomorrow leaves, morohaya, perilla, sesame etc., flower vegetables (eg cauliflower, broccoli etc.), and fruit vegetables (eg peppers, paprika, tomatoes) , pumpkins, etc.) are all applicable, but green-yellow vegetables are preferred.
  • root vegetables eg, carrots, burdock, radish, etc.
  • stem vegetables eg, asparagus, onions, purple onions, etc.
  • leaf vegetables eg, spinach, kale, Barley (young leaves)
  • cabbage Chinese cabbage, parsley, basil, mugwort, watercress, tomorrow leaves, morohaya, perilla, sesame etc.
  • flower vegetables eg cauliflower, broccoli etc.
  • spinach, kale, barley (young leaves), parsley, basil, mugwort, watercress, tomorrow, komatsuna, broccoli, pepper, morroheia, perilla and sesame are more preferred Kale and barley (young leaves), commonly used in green juice beverages.
  • matcha tea which is a powder of tencha
  • Matcha tea is usually steamed from the tea leaves covered with light-shielding treatment, cooled, dried without twisting, and the dried leaves obtained are chopped into small pieces, and the stem, petiole and veins are removed. It is prepared by removing and then drying and producing tea that has been ground to a powder.
  • the “powdered edible plant product” targeted by the present invention is preferably a dry powder of leafy vegetables selected from the group consisting of kale, barley (young leaves), komatsuna, spinach, and matcha tea, and more Preferred are kale, barley (young leaves), and matcha, and more preferred is matcha.
  • the particle size of the “powdered edible plant processed product” (insoluble solid material) used in the present invention is not particularly limited, but for example, the median diameter (grain number median diameter) of the dried product is 5 ⁇ m or more, The range is preferably 10 to 150 ⁇ m, more preferably 10 to 100 ⁇ m, still more preferably 10 to 80 ⁇ m, and still more preferably 20 to 50 ⁇ m.
  • the particle number median diameter can be measured by a device such as a laser diffraction particle size distribution analyzer SALD-2200 (manufactured by Shimadzu Corporation) based on a laser diffraction / scattering method.
  • the “oil and fat” used in the step (a) is not particularly limited, but can include oils and fats usually used in foods. Specifically, vegetable oils (coconut oil, soybean oil, rapeseed oil, cottonseed oil, corn oil, sunflower oil, safflower oil, etc.) and animal oils (beef fat, pork fat, milk fat), preferably It is an oil having a melting point below normal temperature (15-25 ° C.). In other words, oils and fats that are liquid at normal temperature can be preferably cited.
  • Preferred are vegetable oils, more preferred are coconut oil, soybean oil, rapeseed oil, cottonseed oil, corn oil, sunflower oil, safflower oil, and more preferred is coconut oil (rising melting point: 25 ° C.). .
  • Palm oil (refined) is often used from the viewpoint of the flavor and price of fats and oils, and is liquefied by slight heating, so that it is relatively easy to handle at the production site.
  • the fats and oils (refined coconut oil etc.) refine
  • the ratio of the powdered edible plant product to be mixed and dispersed in the fat can be selected from the range of 1 to 200 parts by weight with respect to 100 parts by weight of the fat.
  • the amount is preferably 10 to 150 parts by weight, and more preferably 50 to 100 parts by weight.
  • the ratio (dry weight conversion) of the powdery edible plant processed material contained in the drink of the final product actually manufactured is 0 with respect to 100 weight% of the said drink from a viewpoint of the effect of this invention. It can be selected from the range of 1 to 20% by weight, preferably 0.3 to 10% by weight, more preferably 0.5 to 5% by weight.
  • the ratio of fats and oils can be selected from the range of 0.1 to 50% by weight, preferably 0.5 to 10% by weight, more preferably 1 to 5% by weight. Therefore, in the above-mentioned “ratio of blending of powdered edible plant processed products with respect to fats and oils”, the blending ratio of powdered edible plant processed products and fats and oils in the final product beverage is in the above range. It is preferable to adjust appropriately.
  • the method for dispersing the powdered edible plant processed product in the fat is not particularly limited, for example, the powdered edible plant processed product in the fat, preferably, the dry powder of the edible plant processed product is added as it is, It can be carried out by stirring and mixing according to a conventional method.
  • This dispersion step is preferably in a state in which the oil and fat used as the raw material and water other than water contained in the powdered processed edible plant do not coexist. That is, it is preferable that water is not separately added (externally added) in the dispersion step. Thus, it is possible to efficiently dissolve and disperse components derived from edible plants such as green-yellow natural pigments in fats and oils.
  • distribution process is a process which disperse
  • the stabilizer is a food additive used for improving dispersion in the food and drink with respect to particles, insoluble solids, and the like contained in the food and drink.
  • seaweed polysaccharides carrageenan, sodium alginate, propylene glycol alginate, etc.
  • seed polysaccharides guar gum, tamarind seed gum, etc.
  • resin polysaccharides arabic gum, tragacanth gum, karaya gum, etc.
  • pericarp Sugars pectin, etc.
  • fermented polysaccharides xanthan gum, gellan gum, curdlan, pullulan, etc.
  • cellulose and its derivatives sodium carboxymethylcellulose, methylcellulose, etc.
  • starch derivatives sodium starch glycolate, etc.
  • shell extract chitosan
  • the emulsifier is a food additive used for improving emulsification in the food and drink with respect to oil droplets (oil phase) and water droplets (water phase) contained in the food and drink.
  • fatty acid esters such as glycerin fatty acid ester, sorbitan fatty acid ester, sucrose fatty acid ester, and propylene glycol fatty acid ester can be mentioned.
  • the temperature condition of this dispersion step is not particularly limited, but is usually 5 to 60 ° C., preferably 10 to 40 ° C., and more preferably 20 to 30 ° C.
  • the dispersion is performed for 0.5 to 15 minutes, preferably about 0.5 to 10 minutes under the above temperature conditions, and the mixture of the oil and fat and the powdered edible plant product is stirred using a stirrer, stirring blade, or spatula. Can be implemented.
  • the homogenization treatment can be performed using ordinary homogenization equipment or equipment, for example, a homogenizer, an ultrasonic emulsifier, a colloid mill, a line mill, a homomixer, an azimuth homomixer, a U mixer, or a milder. It is preferable to use a high-speed homomixer, more preferably a high-pressure homogenizer (for example, Manton Gorin, Microfull Diizer, Nanomizer (all are trade names)).
  • the pressure condition in the case of using a high-pressure homogenizer is not limited, but can usually be in the range of 1 to 50 MPa.
  • the pressure is preferably 5 to 40 MPa, more preferably 10 to 40 MPa.
  • the number of rotations when using a high-speed homomixer is not limited.
  • K. A homomixer (manufactured by PRIMIX Co., Ltd .: a device that promotes emulsification and dispersion by shearing when passing between a high-speed rotating turbine blade having a diameter of 30 mm and a stator), and can usually be in the range of 2000 to 10000 rpm. It is preferably 3000 to 9000 rpm, more preferably 5000 to 7000 rpm.
  • the temperature condition can usually be set in the range of 10 to 80 ° C., preferably 30 to 70 ° C., more preferably 40 to 60 ° C.
  • the homogenization treatment time is not limited, but can be exemplified by 1 to 30 minutes.
  • step (B) Process (homogenization process)
  • the dispersion (oil dispersion) of the powdered edible plant processed product and fat prepared in the step (a) is then water for preparing a beverage (hereinafter referred to as “beverage preparation water”). And the mixture is subjected to a step of homogenizing the mixture (step (b)).
  • the mixing treatment of the fat dispersion and the beverage preparation water in addition to the beverage preparation water, other edible components to be blended in the beverage (except for stabilizers and emulsifiers) may be blended and mixed. it can.
  • blended with a drink contains water, it can replace with the said water for drink preparation, and can mix
  • “Other edible ingredients” are not particularly limited unless they are stabilizers or emulsifiers (food additives).
  • milk raw milk, milk, special milk, raw goat milk, pasteurized goat milk, partially skimmed milk, Non-fat milk, processed milk, etc.
  • dairy products cream, butter, butter oil, whey, concentrated whey, concentrated milk, non-fat concentrated milk, sugar-free skim milk, sugar-free skim milk, sweetened milk, sweetened skim milk, Whole milk powder, skim milk powder, cream powder, whey powder, buttermilk powder, sweetened powdered milk, prepared powdered milk, fermented milk, lactic acid bacteria drink, and milk drink, etc.
  • Eggs or processed products alcohols: sugars, synthetic sweeteners, etc.
  • Sweetener pH adjuster: Starch: Seasoning such as salt and acidulant: Colorant: Extract: Micronutrient: Flavor And it can mix
  • milk beverages (beverages with raw milk, milk, dairy products as the main ingredient and milk solids (nonfat milk solids and milk fats) of 3.0% or more), etc.
  • milk solids nonfat milk solids and milk fats
  • the aforementioned milk or dairy product can be blended.
  • beverage preparation water or in place of the beverage preparation water
  • alcoholic beverages depending on the type of alcoholic beverage, in addition to (or replace with) beverage preparation water, sake, beer, shochu, wine, whiskey, brandy, vodka, gin , Plum wine, etc. can be blended.
  • the proportion of blended water for beverage preparation and other edible components contained in the beverage of the final product actually produced is as described above, with respect to 100% by weight of the beverage,
  • the powdered edible plant product is adjusted to 0.1 to 20% by weight, preferably 0.3 to 10% by weight, more preferably 0.5 to 5% by weight in terms of dry weight.
  • the fat and oil may be adjusted to 0.1 to 50% by weight, preferably 0.5 to 10% by weight, more preferably 1 to 5% by weight.
  • the setting may be adjusted as appropriate according to the characteristics.
  • the homogenization treatment of the mixture produced by the above-mentioned method is carried out by using ordinary homogenization equipment and equipment such as a homogenizer, an ultrasonic emulsifier, a colloid mill, a line mill, a homomixer, an azimuth mixer, a U mixer and a milder.
  • a homogenizer for example, Manton Gorin, Microfull Diizer, Nanomizer (all are trade names)
  • a high-pressure homogenizer for example, Manton Gorin, Microfull Diizer, Nanomizer (all are trade names).
  • the pressure condition when using a high-pressure homogenizer is not limited, but can usually be in the range of 1 to 50 MPa.
  • the pressure is preferably 5 to 40 MPa, more preferably 10 to 40 MPa.
  • the number of rotations when using a high-speed homomixer is not limited.
  • K. A homomixer (manufactured by PRIMIX Co., Ltd .: a device that promotes emulsification and dispersion by shearing when passing between a high-speed rotating turbine blade having a diameter of 30 mm and a stator), and can usually be in the range of 2000 to 10000 rpm. It is preferably 3000 to 9000 rpm, more preferably 5000 to 7000 rpm.
  • the temperature condition can usually be set in the range of 10 to 80 ° C., preferably 30 to 70 ° C., more preferably 40 to 60 ° C.
  • the homogenization treatment time is not limited, but can be exemplified by 5 to 30 minutes.
  • the beverage of the present invention can be produced and obtained.
  • the beverage prepared (manufactured) by the above method can be It is preferable to fill and seal containers such as bottles, paper packs, retort pouches, etc., and then subject to sterilization treatment.
  • a container-packed beverage can be produced and obtained.
  • the sterilization treatment of the mixture or beverage produced by the above method is not particularly limited, but depending on the type of beverage actually produced, normal sterilization treatment (plate type ultra high temperature heat sterilization (UHT), tube type High temperature short time heat sterilization (HTST), retort sterilization, autoclave sterilization, etc.) can be employed.
  • normal sterilization treatment plate type ultra high temperature heat sterilization (UHT), tube type High temperature short time heat sterilization (HTST), retort sterilization, autoclave sterilization, etc.
  • the beverage produced by the above method has an insoluble solid such as a powdered edible plant processed product, but its dispersion stability is improved, and the powdered edible plant processed product itself is dispersed in fats and oils. Compared with a beverage manufactured without passing through the step (control beverage), the phenomenon of sedimentation that occurs over time is significantly suppressed.
  • dispersion stability refers to the beverage (main beverage) produced by the method of the present invention described above and a control beverage, if necessary, after sterilization treatment, and then the beverage is cooled to room temperature condition. It can be evaluated by observing with time the precipitation of insoluble solids produced by this standing (generation of sediment). Specifically, it can be determined that the dispersion stability of the present beverage is improved when the amount of the precipitate produced is small or the production rate is slow compared to the control beverage.
  • the beverage produced by the above method has significantly improved redispersibility even when insoluble solids such as powdered edible processed plant products settle and deposit on the bottom of the container.
  • the powdered edible plant product can be easily returned to its original dispersed state by simply shaking it.
  • “redispersibility” means that the beverage (main beverage) produced by the above-described method of the present invention and a control beverage are sterilized as necessary, and then the beverage is cooled to room temperature. It can be evaluated by comparing the ease of dispersion of the sediment of the insoluble solid produced by this standing. For example, when these two beverages are shaken under the same conditions, the degree to which the insoluble solids settled on the bottom surface of the container is redispersed in the whole beverage is better or redispersed than the control beverage. When the speed is high, it can be determined that redispersion is improved in the beverage.
  • Beverages containing powdered edible plant products Beverages targeted by the present invention are beverages containing at least powdered edible plant products, oils and water, and are powdery edible. Compared to beverages (control beverages) prepared without mixing and dispersing processed plant oils and fats, (i) improved dispersion stability of powdered edible plant processed products contained in beverages Or (ii) the redispersibility of the powdered edible plant processed product in the beverage is improved.
  • the beverage of the present invention having such characteristics can be produced by the production method described in (I), specifically, the production method including at least the steps (a) and (b). Moreover, you may have the homogenization process process between the (a) process and the (b) process.
  • the description of the homogenization process between the steps is as described above in (I), and these descriptions can be used here as well.
  • the beverage of the present invention is a beverage containing at least a powdered edible plant product, fats and oils, and has the above-described feature (i) or (ii). As long as this is the case, the above manufacturing method is not restrictive.
  • a preferable beverage of the present invention is a beverage containing at least a powdered edible plant product, fats and oils, and in addition to the above-described feature (i) or (ii), the feature (iii) Compared with a control drink, the discoloration or discoloration of the powdery edible plant processed material in a drink is suppressed.
  • fading or discoloration is suppressed means that the beverage (main beverage) produced by the above-described method of the present invention and the control beverage are sterilized and / or cooled to cold or heated. It can be evaluated by observing changes in the color tone of these beverages over time using the color tone immediately after the preparation of these beverages as a reference, while standing under warm conditions. For example, it can be determined that fading or discoloration is suppressed in the beverage when the change in color tone is small compared to the control beverage.
  • (III) A method for improving the dispersion stability or redispersibility of a powdered edible plant processed product in a beverage.
  • the present invention also relates to the dispersion stability or redispersion of a powdered edible plant processed product in a beverage. It is a method of improving the property.
  • the method is carried out by mixing a powdered edible plant processed product in advance in oil and fat with water and homogenizing it in a manufacturing process of a beverage containing the powdered edible plant processed product. can do.
  • the method of the present invention uses a powdered edible plant processed product pre-dispersed in oil and fat as a raw material in the production of a beverage containing a powdered edible plant processed product, and this is mixed with water. It is also possible to carry out by homogenizing, or to disperse the powdered edible plant processed product in fats and oils [(a) step], and to mix this with water and homogenize It can also be carried out by carrying out the step [(b) step]. Steps used in this method (step of dispersing powdered edible plant processed product in oil and fat [(a) step], and step of mixing this with water and homogenizing [step (b)]]] The description is also as described above in (I), and these descriptions can be used here as well.
  • Such a method can improve the dispersion stability or redispersibility of a powdered edible plant processed product in a beverage. More specifically, the method of the present invention does not go through the step of mixing and dispersing the powdered edible plant processed product with the fat in the beverage containing at least the powdered edible processed plant product, the fat and the water. Compared with the beverage (control beverage) prepared in (i), the dispersion stability of the powdered edible plant processed product contained in the beverage can be improved, or (ii) the powder form in the beverage The redispersibility of the processed edible plant can be improved.
  • the method of the present invention is the method described in (i) or (ii) above, and (iii) suppresses fading or discoloration of the powdered edible plant processed product in the beverage as compared with the control beverage. can do.
  • Oil dispersion 1-1 (a) skim milk powder, (b) refined coconut oil, and (d) ion-exchanged water are mixed, then (c) powdered green tea powder is blended in this, using a medicine sag well Dispersion was carried out to prepare oil dispersion 1-1 (performed at 25 ° C.).
  • Oil Dispersion 1-2 (c) Matcha tea powder is mixed and dispersed in (b) refined coconut oil using medicinal solution, and then (a) skim milk powder and (d) ion-exchanged water are mixed therewith Thus, an oil dispersion 1-2 was prepared.
  • Oil dispersion 1-3 (c) Matcha powder was mixed and dispersed in (b) refined coconut oil using a medicine sag, and further homogenizer (manufactured by Niro Soavi) under conditions of 50 ° C. and 35 MPa. Then, (a) skim milk powder and (d) ion-exchanged water were mixed with this to prepare an oil dispersion 1-3.
  • Experimental example 2 The matcha powder of Experimental Example 1 is used, except that “Moriko Matcha” (manufactured by Yuriichi Honten) is used as the matcha powder, except that “Kamisu no Shiro” (manufactured by Aiya, number median diameter: 12.23 ⁇ m) is used.
  • Matched milk drinks 2-1 and 2-2 were prepared in the same manner as milk drinks 1-1 and 1-2, respectively.
  • matcha-containing milk drinks 2-1 and 2-2 according to the same method and standard as described in (II) of Experimental Example 1, dispersion stability (presence of sediment), deterioration of color tone ( Fading) and redispersibility were evaluated.
  • a powdered milk powder containing matcha tea can be obtained by using an oil and fat dispersion in which powdered green tea powder is previously mixed with oil and fat (refined palm oil) and dispersed.
  • the dispersion stability of matcha powder is improved compared to milk powder containing matcha 2-1 produced without preparing the oil dispersion, and the settling of matcha powder that occurs during storage after heat sterilization is reduced. It was confirmed that it was significantly suppressed.
  • Oil dispersion 3-1 Refined coconut oil, emulsifier P-1670 (Mitsubishi Chemical Foods, Inc .: sugar ester), emulsifier 681SPV (Taiyo Kagaku), and ion-exchanged water are mixed, and then powdered green tea powder is added thereto Then, using oil squeeze, well dispersed, oil and fat dispersion 3-1 was prepared.
  • Oil dispersion 3-2 Matcha powder is mixed and dispersed in refined coconut oil using a medicine sag, and then emulsifiers P-1670 and 681SPV and ion-exchanged water are mixed with the oil dispersion 3- 2 was prepared.
  • kale powder or barley (young leaf) powder is previously mixed with fat (refined palm oil) and dispersed.
  • the kale powder and barley (young leaves) were compared to beverages 4-1 and 5-1, which were produced without preparing the oil dispersion.
  • the kale powder and barley (young leaves) were compared to beverages 4-1 and 5-1, which were produced without preparing the oil dispersion.
  • was improved in dispersion stability and it was confirmed that sedimentation of insoluble solids generated during storage after heat sterilization was significantly suppressed.
  • beverages 4-2 and 5-2 have improved redispersibility compared to beverages 4-1 and 5-1, and once the kale powder and barley young leaf powder that has been precipitated are shaken, It was confirmed that it could be easily dispersed.
  • the samples (1) and (2) prepared above were allowed to stand at room temperature (25 ° C.) for 20 minutes, their properties were visually confirmed, and then centrifuged (1000 rpm, 5 minutes, 25 ° C.).
  • FIG. 1 (A) The state of the samples (1) and (2) allowed to stand at room temperature (25 ° C.) for 20 minutes is shown in FIG. 1 (A), and they are placed in a centrifuge tube and further centrifuged. The later state is shown in FIG. In each figure, the left side shows the state of the sample (1) and the right side shows the state of the sample (2). In this case, the samples (1) and (2) were observed as an emulsion having a large particle size.

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Abstract

Provided is a beverage containing a processed edible-plant powder wherein either the dispersion stability of insoluble solid matter in said beverage is improved, reducing settling, or redispersability is improved, such that if settling does occur, the beverage can be easily returned to the original dispersion state thereof by gentle shaking. Also provided is a method for manufacturing the aforementioned beverage. Said method includes the following steps: (a) a step in which a processed edible-plant powder is mixed with and dispersed in an oil or fat; and (b) a step in which the dispersion consisting of the processed edible-plant powder and the oil or fat is mixed with water and homogenized.

Description

分散安定性または再分散性が向上した粉末状の可食性植物加工物を含む飲料の製造方法Method for producing a beverage comprising a powdered edible plant product with improved dispersion stability or redispersibility
 本発明は、粉末状の可食性植物加工物を含む飲料に関して、当該飲料中の不溶性固形物(粉末状の可食性植物加工物)の分散安定性を向上して沈殿を抑制し、また、沈殿した場合でも、軽く振るだけで容易に元の分散状態が復元できるように再分散性が向上されてなる飲料、およびその製造方法に関する。 The present invention relates to a beverage containing a powdered edible plant processed product, and improves the dispersion stability of the insoluble solid (powdered edible plant processed product) in the beverage to suppress precipitation. In this case, the present invention relates to a beverage whose redispersibility is improved so that the original dispersion state can be easily restored simply by shaking lightly, and a method for producing the same.
 また、本発明は、粉末状の可食性植物加工物を含む飲料について、当該飲料中の不溶性固形物(粉末状の可食性植物加工物)の分散安定性を向上する方法、また、沈殿した場合でも、軽く振るだけで容易に元の分散状態が復元できるように再分散性を向上するための方法に関する。 The present invention also relates to a method for improving the dispersion stability of an insoluble solid (powdered edible plant processed product) in the beverage, including a powdered edible plant processed product, However, the present invention relates to a method for improving the redispersibility so that the original dispersion state can be easily restored simply by shaking lightly.
 抹茶は、その深みのある自然な風味から、飲料若しくは飲料用成分として、または各種の飲食品への添加材料として用いられている。また、近年の健康志向に伴い、ケールや大麦(若葉)等の緑黄色野菜の乾燥粉末が、飲料若しくは飲料用成分として、または各種の飲食品への添加材料として用いられるようになっている。 Matcha is used as a beverage or beverage ingredient or as an additive to various foods and drinks because of its deep natural flavor. Moreover, with the recent health consciousness, dry powders of green and yellow vegetables such as kale and barley (young leaves) are used as beverages or beverage ingredients, or as additives for various foods and drinks.
 しかし、これらの乾燥粉末は、いずれも水に不溶の固形物(不溶性固形物)であることから、それらを飲料に配合する場合、特に容器に充填して、市場に流通させる容器詰飲料の場合、流通中または保存中に粉末が沈殿(沈降)する、または、それが容器の底で凝集固結するという問題がある。また、容器詰飲料の場合、製造工程で行う殺菌処理により、緑黄色野菜の乾燥粉末の鮮やかな色が退色または変色してしまい、上記沈殿の問題とともに、飲料の外観および風味(食感)を損なう原因ともなる。 However, these dry powders are all solids that are insoluble in water (insoluble solids), so when they are blended into beverages, especially in the case of packaged beverages that are filled into containers and distributed to the market. There is a problem that the powder precipitates (settling) during distribution or storage, or it agglomerates and solidifies at the bottom of the container. Moreover, in the case of a container-packed beverage, the vivid color of the dry powder of green and yellow vegetables fades or discolors due to the sterilization treatment performed in the manufacturing process, and the appearance and flavor (texture) of the beverage are impaired along with the above-mentioned precipitation problem. It can also be a cause.
 かかる問題を解消する方法として、通常、セルロースや増粘多糖類などの安定剤を用いることで、不溶性固形物の沈殿を抑制する方法が採用されている。また、他の方法として、抹茶にマルトースおよび牡蠣殻等に由来するカルシウム剤を混合して含有させることにより、緑色の保持や水系媒体への分散および溶解性を改善する方法(特許文献1)、ならびに、抹茶等の不溶性固形物に、安定剤と水もしくは湯を加え、100~250kg/cm2の圧力でホモゲナイズ処理を行い、溶液中に安定剤をコロイド状に分散させ、当該コロイドに不溶性固形物を保持させて安定化する方法(特許文献2)なども提案されている。しかし、安定剤などを用いることで、飲料の食感や風味が不自然になることもある。また、安定剤などを用いることで飲料原価がコストアップする。 As a method of solving such a problem, a method of suppressing precipitation of insoluble solids by using a stabilizer such as cellulose or thickening polysaccharide is usually employed. In addition, as another method, a method for improving green color retention and dispersion in an aqueous medium and solubility by incorporating a calcium agent derived from maltose and oyster shells into matcha (Patent Document 1), In addition, a stabilizer and water or hot water are added to an insoluble solid such as matcha tea, homogenized at a pressure of 100 to 250 kg / cm 2 , and the stabilizer is dispersed in a colloidal form in the solution. A method of stabilizing an object by holding it (Patent Document 2) has also been proposed. However, by using a stabilizer or the like, the texture and flavor of the beverage may become unnatural. In addition, the use of stabilizers increases the cost of beverages.
 一方、安定剤を用いない方法として、平均粒子径が7~20μmの抹茶粉末を水に分散させて、20~90℃にて5MPa以上の圧力で均質化処理し、飲料中の不溶性固形物の沈殿凝集を抑制する方法(特許文献3)が提案されている。しかし、この方法が適用できるのは、平均粒子径が7~20μmの範囲にある抹茶粉末であり、粉末の平均粒径を予め調整する必要があることなどを考慮すると、煩雑であり、実用性に欠けるという問題がある。 On the other hand, as a method not using a stabilizer, powdered green tea powder having an average particle size of 7 to 20 μm is dispersed in water and homogenized at a pressure of 5 MPa or more at 20 to 90 ° C. A method for suppressing precipitation aggregation (Patent Document 3) has been proposed. However, this method can be applied to powdered green tea powder having an average particle size in the range of 7 to 20 μm, and it is complicated and practical considering that the average particle size of the powder needs to be adjusted in advance. There is a problem of lacking.
特開2003-259805号公報JP 2003-259805 A 特開2001-29053号公報JP 2001-29053 A 特開2007-53913号公報JP 2007-53913 A
 本発明は、前述する従来の問題を解決することを目的とする。具体的には、本発明は、粉末状の可食性植物加工物を含む飲料に関して、好ましくは安定剤を用いることなく、当該飲料中の不溶性固形物(粉末状可食性植物加工物)の分散安定性を向上して沈殿を抑制し、また、沈殿した場合でも、軽く振るだけで元の分散状態が簡単に復元できるように再分散性が向上されてなる飲料、およびその製造方法を提供することを目的とする。 The present invention aims to solve the above-mentioned conventional problems. Specifically, the present invention relates to a beverage containing a powdered edible plant processed product, preferably without using a stabilizer, and stable dispersion of insoluble solids (powdered edible plant processed product) in the beverage. To provide a beverage whose redispersibility is improved so that the original dispersion state can be easily restored by simply shaking lightly even if it is precipitated, and a method for producing the same With the goal.
 また、本発明は、粉末状の可食性植物加工物を含む飲料について、好ましくは安定剤を用いることなく、当該飲料中の不溶性固形物(粉末状の可食性植物加工物)の分散安定性を向上する方法、また、沈殿した場合でも、軽く振るだけで元の分散状態が簡単に復元できるように再分散性を向上するための方法を提供することを目的とする。 In addition, the present invention provides a dispersion containing a powdered edible plant processed product, preferably without using a stabilizer, to improve the dispersion stability of the insoluble solid (powdered edible plant processed product) in the beverage. It is an object of the present invention to provide a method for improving redispersibility so that the original dispersion state can be easily restored by simply shaking lightly even when precipitated.
 本発明者らは、上記課題を解決すべく鋭意検討を重ねていたところ、粉末状の可食性植物加工物を含む飲料を製造するに際して、飲料の調製に用いる水に、粉末状の可食性植物加工物をそのまま配合するのではなく、粉末状の可食性植物加工物を予め油脂と混合して分散させたものを配合することで、上記方法で調製される飲料(以下、飲料の調製に用いる水に粉末状可食性植物加工物をそのまま配合して調製される飲料を「コントロール飲料」という)に比べて、飲料中の粉末状の可食性植物加工物の分散安定性が有意に向上されて、経時的に生じる沈殿が抑制されること、また、生じた沈降物の再分散性が有意に向上されて、軽く振るだけで元の分散状態が復元できることを見出した。 The inventors of the present invention have made extensive studies in order to solve the above problems, and in producing a beverage containing a powdered processed edible plant, the powdered edible plant is used in water used for preparing the beverage. Instead of blending the processed product as it is, a beverage prepared by the above method by blending a powdered edible plant processed product previously mixed with fats and oils (hereinafter used for beverage preparation) Dispersion stability of powdered edible processed plant products in beverages is significantly improved compared to beverages prepared by mixing powdered edible processed plant products with water as they are (control beverages). It was found that precipitation that occurs over time is suppressed, and that the redispersibility of the resulting precipitate is significantly improved, and that the original dispersion state can be restored by simply shaking.
 本発明は、かかる知見に基づいて完成したものであり、下記の実施形態を有するものである。 The present invention has been completed based on such knowledge and has the following embodiments.
 (I)粉末状の可食性植物加工物を含有する飲料の製造方法
(I-1)(a)粉末状の可食性植物加工物を油脂に混合して分散させる工程、および
(b)粉末状の可食性植物加工物と油脂との分散物を水と混合して均質化処理する工程
を含む、粉末状の可食性植物加工物を含有する飲料の製造方法。
(I-2)(a)工程と(b)工程の間に、さらに均質化処理する工程を有する、(I-1)に記載する製造方法。
(I-3)上記(b)工程で用いる水が乳または乳成分を含むものである、(I-1)または(I-2)に記載する製造方法。
(I-4)安定剤および/または乳化剤を配合しないことを特徴とする、(I-1)乃至(I-3)のいずれかに記載する製造方法。
(I-5)粉末状の可食性植物加工物が、茶、野菜、果実、穀物および豆類からなる群から選択される少なくとも1種の植物の乾燥粉末である、(I-1)乃至(I-4)のいずれかに記載する製造方法。
(I-6)(a)工程で得られる分散物が、原料として使用する油脂および可食性植物加工物に由来する水以外の水を含まないことを特徴とする(I-1)乃至(I-5)のいずれかに記載する製造方法。
(I) Manufacturing method of beverage containing powdered edible plant processed product (I-1) (a) Step of mixing powdered edible plant processed product with oil and fat, and (b) Powdered A method for producing a beverage containing a powdered edible processed plant product, comprising a step of mixing a dispersion of the processed edible plant product and fats and oils with water and homogenizing the mixture.
(I-2) The production method according to (I-1), further comprising a homogenization step between the steps (a) and (b).
(I-3) The production method according to (I-1) or (I-2), wherein the water used in the step (b) contains milk or a milk component.
(I-4) The production method according to any one of (I-1) to (I-3), wherein a stabilizer and / or an emulsifier is not blended.
(I-5) The powdered edible plant processed product is a dry powder of at least one plant selected from the group consisting of tea, vegetables, fruits, cereals and beans, (I-1) to (I -4) The production method described in any one of the above.
(I-6) The dispersion obtained in the step (a) does not contain water other than water derived from oils and fats used as raw materials and processed edible plants (I-1) to (I -5) The manufacturing method described in any one of.
 (II)粉末状の可食性植物加工物を含有する飲料
(II-1)(I-1)乃至(I-6)のいずれかに記載する製造方法で得られる少なくとも粉末状の可食性植物加工物、油脂および水を含有する飲料であって、(a)の粉末状の可食性植物加工物を油脂と混合して分散させる工程を経ないで調製される飲料と比べて、少なくとも、飲料中の粉末状の可食性植物加工物の分散安定性が向上しているか、または飲料中の粉末状の可食性植物加工物の再分散性が向上してなることを特徴とする、飲料。
(II-2)さらに飲料中の粉末状の可食性植物加工物の退色または変色が抑制されてなる、(II-1)に記載する飲料。
(II) Beverage containing powdered edible plant processed product (II-1) Processed at least powdered edible plant obtained by the production method described in any one of (I-1) to (I-6) A beverage containing foods, fats and oils, and at least in a beverage compared to a beverage prepared without going through the step of mixing and dispersing the powdered edible plant processed product of (a) with fats and oils A beverage characterized in that the dispersion stability of the powdered edible plant product is improved, or the redispersibility of the powdered edible plant product in the beverage is improved.
(II-2) The beverage according to (II-1), wherein fading or discoloration of the powdered edible plant processed product in the beverage is further suppressed.
 (III)飲料中の粉末状の可食性植物加工物の分散安定性または再分散性を向上させる方法
(III-1)粉末状の可食性植物加工物を含む飲料の製造工程において、粉末状の可食性植物加工物を予め油脂に分散させたものを水と混合して均質化処理する工程を有することを特徴とする、飲料中の粉末状の可食性植物加工物の分散安定性または再分散性を向上させる方法。
(III-2)粉末状の可食性植物加工物を含む飲料の製造工程において、(a)粉末状の可食性植物加工物を油脂に分散させる工程、および(b)粉末状の可食性植物加工物と油脂との分散物を水と混合して均質化処理する工程を有することを特徴とする、飲料中の粉末状の可食性植物加工物の分散安定性または再分散性を向上させる方法。
(III-3)(a)工程と(b)工程の間に、さらに均質化処理する工程を有する、(III-2)に記載する方法。
(III-4)上記水が乳または乳成分を含むものである、(III-1)乃至(III-3)のいずれかに記載する方法。
(III-5)安定剤および/または乳化剤を配合しないことを特徴とする、(III-1)乃至(III-4)のいずれかに記載する方法。
(III-6)粉末状の可食性植物加工物が、茶、野菜、果実、穀物および豆類からなる群から選択される少なくとも1種の植物の乾燥粉末である、(III-1)乃至(III-5)のいずれかに記載する方法。
(III-7)粉末状の可食性植物加工物を油脂に分散させることで得られる分散物が、原料として使用する油脂および可食性植物加工物に由来する水以外の水を含まないことを特徴とする(III-1)乃至(III-6)のいずれかに記載する方法。
(III-8)飲料中の粉末状の可食性植物加工物の分散安定性または再分散性を向上させるとともに、飲料中の粉末状の可食性植物加工物の退色を抑制する方法である、(III-1)乃至(III-7)のいずれかに記載する方法。
(III) Method for improving dispersion stability or redispersibility of powdered edible plant processed product in beverage (III-1) In the production process of beverage containing powdered edible plant processed product, Dispersion stability or redispersion of powdered edible plant products in beverages, characterized by having a step of mixing edible plant products in advance in oil and fat with water and homogenizing the mixture. To improve performance.
(III-2) In a process for producing a beverage containing a powdered edible plant processed product, (a) a step of dispersing the powdered edible plant processed product in oil and fat, and (b) a powdered edible plant processed A method for improving dispersion stability or redispersibility of a powdered edible plant processed product in a beverage, comprising a step of mixing a dispersion of the product and fat with water and homogenizing the mixture.
(III-3) The method according to (III-2), further comprising a homogenization step between the steps (a) and (b).
(III-4) The method according to any one of (III-1) to (III-3), wherein the water contains milk or a milk component.
(III-5) The method according to any one of (III-1) to (III-4), wherein a stabilizer and / or an emulsifier is not blended.
(III-6) The powdered edible plant processed product is a dry powder of at least one plant selected from the group consisting of tea, vegetables, fruits, cereals and beans, (III-1) to (III -5) The method described in any one of the above.
(III-7) Dispersion obtained by dispersing powdered edible plant processed product in oil and fat does not contain water other than water derived from oil and fat used as raw material and processed edible plant product The method according to any one of (III-1) to (III-6).
(III-8) A method of improving the dispersion stability or redispersibility of a powdered edible plant processed product in a beverage and suppressing discoloration of the powdered edible plant processed product in a beverage. The method according to any one of III-1) to (III-7).
 本発明の製造方法、ならびに分散安定性または再分散性を向上させる方法によれば、抹茶等の粉末状の可食性植物加工物を含む飲料について、好ましくは安定剤や乳化剤を用いることなく、粉末状の可食性植物加工物を油脂と混合して分散させる工程を経ないで調製される飲料と比べて、当該飲料中の不溶性固形物(粉末状の可食性植物加工物)の分散安定性を向上させることができ、また、沈殿した場合でも、軽く振るだけで元の分散状態に簡単に戻るように再分散性を向上させることができる。また、可食性植物加工物として、緑黄色野菜、特に緑色色素であるクロロフィルを含む野菜を使用した場合、本発明の製造方法によれば、粉末状の可食性植物加工物を油脂と混合して分散させる工程を経ないで調製される飲料と比べて、加熱殺菌や保存によって生じる退色や変色を抑制することもできる。 According to the production method of the present invention and the method for improving dispersion stability or redispersibility, a powder containing powdered edible plant products such as matcha tea is preferably used without using a stabilizer or an emulsifier. Compared to a beverage prepared without passing through a step of mixing and dispersing the edible edible plant product with fats and oils, the dispersion stability of the insoluble solid (powdered edible plant product) in the beverage is improved. In addition, even when it is precipitated, the redispersibility can be improved so that it can be easily returned to the original dispersed state by simply shaking lightly. Moreover, when using green edible vegetables, especially vegetables containing chlorophyll, which is a green pigment, as the processed edible plant, according to the production method of the present invention, the powdered edible processed plant is mixed with fats and oils and dispersed. Compared with a beverage prepared without undergoing a step of causing it to fade, discoloration and discoloration caused by heat sterilization and storage can also be suppressed.
実験例5の実験結果を示す。(A)試料を作成した後に20分間、静置した際の試料の状態を示すカラー画像に代わる図面、および(B)試料作成後、20分間静置した後に、遠心分離に供した後の試料の状態を示すカラー画像に代わる図面である。(A)および(B)各図において、向かって左側は、抹茶を油脂に分散することなく水に分散した試料(1)(比較例)の画像であり、向かって右側は、抹茶を油脂に分散させた試料(2)(実施例)の画像である。The experimental result of Experimental example 5 is shown. (A) Drawing instead of a color image showing the state of the sample when it is allowed to stand for 20 minutes after the sample was prepared, and (B) Sample after being left for 20 minutes after the sample was prepared and then subjected to centrifugation It is drawing which replaces the color image which shows the state. (A) and (B) In each figure, the left side is an image of sample (1) (comparative example) in which green tea is dispersed in water without being dispersed in oil and fat, and the right side is green tea in oil and fat. It is an image of the dispersed sample (2) (Example).
(I)粉末状の可食性植物加工物を含有する飲料の製造方法
 本発明は、粉末状の可食性植物加工物を含有する飲料であって、少なくとも、飲料中の粉末状の可食性植物加工物の分散安定性が向上しているか、または飲料中の粉末状の可食性植物加工物の再分散性が向上してなることを特徴とする飲料の製造方法である。
(I) Method for producing a beverage containing a powdered edible plant processed product The present invention is a beverage containing a powdered edible plant processed product, and at least a powdered edible plant processed in the beverage It is a method for producing a beverage characterized in that the dispersion stability of the product is improved, or the redispersibility of the processed powdered edible plant in the beverage is improved.
 当該製造方法は、少なくとも下記(a)および(b)の工程により実施することができる:
(a)粉末状の可食性植物加工物を油脂に混合し分散させる工程、および
(b)粉末状の可食性植物加工物と油脂との分散物を水と混合して均質化処理する工程。
The production method can be carried out by at least the following steps (a) and (b):
(A) a step of mixing and dispersing a powdered edible plant processed product in oil and fat; and (b) a step of mixing a dispersion of the powdered edible plant processed product and fat with water and homogenizing.
 以下、各工程について説明する。
(a)工程(分散処理工程)
 (a)工程で用いる「粉末状の可食性植物加工物」とは、粉末状に調製された水不溶性の可食性植物加工物である。具体的には、果実、野菜(根菜類、茎菜類、葉菜類、花菜類、果菜類)または茶葉等の植物の可食性部位を粉砕して調製されたものであり、好ましくは、これらの乾燥粉末である。なお、本発明の「粉末状の可食性植物加工物」は、1種類の可食性植物から調製されるものであっても、また、2種類以上の可食性植物を任意に組み合わせてなる混合物であってもよい。そして、本発明の「粉末状」は、粉末状そのものの形状を有するものだけでなく、粉末を顆粒状や固形状(タブレット状等)に加工したものであってもよい。
Hereinafter, each step will be described.
(A) Process (dispersion process)
The “powdered edible plant product” used in the step (a) is a water-insoluble edible plant product prepared in a powder form. Specifically, it is prepared by crushing edible parts of plants such as fruits, vegetables (root vegetables, stem vegetables, leaf vegetables, flower vegetables, fruit vegetables) or tea leaves, preferably these dried It is a powder. The “powdered edible plant product” of the present invention is a mixture prepared by arbitrarily combining two or more edible plants, even if it is prepared from one type of edible plant. There may be. The “powder” of the present invention is not limited to the powder itself, but may be a powder processed into granules or solids (tablets, etc.).
 ここで、野菜は、特に制限されることなく、根菜類(例えば、人参、ゴボウ、大根等)、茎菜類(例えば、アスパラガス、玉葱、紫玉葱等)、葉菜類(例えば、ホウレン草、ケール、大麦(若葉)、キャベツ、白菜、パセリ、バジル、ヨモギ、クレソン、明日葉、モロヘイヤ、シソ、エゴマ等)、花菜類(例えば、カリフラワー、ブロッコリー等)、および果菜類(例えば、ピーマン、パプリカ、トマト、カボチャ等)のいずれも該当するが、好ましくは、緑黄色野菜である。緑黄色野菜でも、好ましくは、緑色系野菜であるホウレン草、ケール、大麦(若葉)、パセリ、バジル、ヨモギ、クレソン、明日葉、小松菜、ブロッコリー、ピーマン、モロヘイヤ、シソ、およびゴマであり、より好ましくは、一般的に青汁飲料に用いられるケール、大麦(若葉)である。 Here, the vegetables are not particularly limited, and include root vegetables (eg, carrots, burdock, radish, etc.), stem vegetables (eg, asparagus, onions, purple onions, etc.), leaf vegetables (eg, spinach, kale, Barley (young leaves), cabbage, Chinese cabbage, parsley, basil, mugwort, watercress, tomorrow leaves, morohaya, perilla, sesame etc., flower vegetables (eg cauliflower, broccoli etc.), and fruit vegetables (eg peppers, paprika, tomatoes) , Pumpkins, etc.) are all applicable, but green-yellow vegetables are preferred. Among green and yellow vegetables, spinach, kale, barley (young leaves), parsley, basil, mugwort, watercress, tomorrow, komatsuna, broccoli, pepper, morroheia, perilla and sesame are more preferred Kale and barley (young leaves), commonly used in green juice beverages.
 茶葉の粉末として、好ましくは、碾茶(てんちゃ)の粉末である抹茶を挙げることができる。抹茶は、通常、遮光処理を施した茶葉の覆下茶を蒸した後に冷却し、その茶葉を揉捻せずに乾燥し、この得られた乾燥葉を刻んで小片にし、茎、葉柄および葉脈を取り除き、更に乾燥して製造した碾茶を臼で挽いて粉(粉末)にすることで調製される。 As the tea leaf powder, preferably, matcha tea, which is a powder of tencha, can be mentioned. Matcha tea is usually steamed from the tea leaves covered with light-shielding treatment, cooled, dried without twisting, and the dried leaves obtained are chopped into small pieces, and the stem, petiole and veins are removed. It is prepared by removing and then drying and producing tea that has been ground to a powder.
 本発明が対象とする「粉末状の可食性植物加工物」は、好ましくは、ケール、大麦(若葉)、小松菜、ホウレン草からなる群から選択される葉菜の乾燥粉末、ならびに抹茶であり、より好ましくは、ケール、大麦(若葉)、ならびに抹茶であり、さらに好ましくは、抹茶である。 The “powdered edible plant product” targeted by the present invention is preferably a dry powder of leafy vegetables selected from the group consisting of kale, barley (young leaves), komatsuna, spinach, and matcha tea, and more Preferred are kale, barley (young leaves), and matcha, and more preferred is matcha.
 なお、本発明で用いる「粉末状の可食性植物加工物」(不溶性固形物)の粒径は、特に制限されないが、例えば、その乾燥物のメディアン直径(粒数メディアン直径)として、5μm以上、好ましくは10~150μmの範囲、より好ましくは10~100μm、さらに好ましくは10~80μmの範囲、よりさらに好ましくは20~50μmの範囲を挙げることができる。ここで粒数メディアン直径は、レーザー回折・散乱法に基づいて、レーザー回折式粒子径分布測定装置SALD-2200(島津製作所製)等の装置によって測定することができる。 The particle size of the “powdered edible plant processed product” (insoluble solid material) used in the present invention is not particularly limited, but for example, the median diameter (grain number median diameter) of the dried product is 5 μm or more, The range is preferably 10 to 150 μm, more preferably 10 to 100 μm, still more preferably 10 to 80 μm, and still more preferably 20 to 50 μm. Here, the particle number median diameter can be measured by a device such as a laser diffraction particle size distribution analyzer SALD-2200 (manufactured by Shimadzu Corporation) based on a laser diffraction / scattering method.
 (a)工程で用いる「油脂」は、特に制限されないが、通常、食品に用いられている油脂を挙げることができる。具体的には、植物性油脂(ヤシ油、大豆油、菜種油、綿実油、コーン油、ひまわり油、サフラワー油等)、および動物性油脂(牛脂、豚脂、乳脂肪)であり、好ましくは、融点が常温(15~25℃)以下の油脂である。つまり、常温で液状である油脂を好適に挙げることができる。好ましくは、植物性油脂であり、より好ましくは、ヤシ油、大豆油、菜種油、綿実油、コーン油、ひまわり油、サフラワー油であり、さらに好ましくは、ヤシ油(上昇融点:25℃)である。油脂の風味や価格等の観点から、ヤシ油(精製)は良く用いられており、若干の加温により、液状化するので、製造現場における取扱が比較的に容易である。なお、その臭いや色が最終の飲料に影響しないように精製された油脂(精製ヤシ油等)を好適に挙げることができる。 The “oil and fat” used in the step (a) is not particularly limited, but can include oils and fats usually used in foods. Specifically, vegetable oils (coconut oil, soybean oil, rapeseed oil, cottonseed oil, corn oil, sunflower oil, safflower oil, etc.) and animal oils (beef fat, pork fat, milk fat), preferably It is an oil having a melting point below normal temperature (15-25 ° C.). In other words, oils and fats that are liquid at normal temperature can be preferably cited. Preferred are vegetable oils, more preferred are coconut oil, soybean oil, rapeseed oil, cottonseed oil, corn oil, sunflower oil, safflower oil, and more preferred is coconut oil (rising melting point: 25 ° C.). . Palm oil (refined) is often used from the viewpoint of the flavor and price of fats and oils, and is liquefied by slight heating, so that it is relatively easy to handle at the production site. In addition, the fats and oils (refined coconut oil etc.) refine | purified so that the smell and color may not influence a final drink can be mentioned suitably.
 (a)工程において、油脂に混合分散させる粉末状の可食性植物加工物の割合(乾燥重量換算)は、油脂の100重量部に対して、1~200重量部の範囲から選択することができ、好ましくは、10~150重量部であり、より好ましくは、50~100重量部である。 In the step (a), the ratio of the powdered edible plant product to be mixed and dispersed in the fat (in terms of dry weight) can be selected from the range of 1 to 200 parts by weight with respect to 100 parts by weight of the fat. The amount is preferably 10 to 150 parts by weight, and more preferably 50 to 100 parts by weight.
 なお、実際に製造される最終製品の飲料に含まれる粉末状の可食性植物加工物の割合(乾燥重量換算)は、本発明の効果の観点から、当該飲料の100重量%に対して、0.1~20重量%の範囲から選択することができ、好ましくは、0.3~10重量%、より好ましくは、0.5~5重量%である。また、油脂の割合は、当該飲料の100重量%に対して、0.1~50重量%の範囲から選択することができ、好ましくは、0.5~10重量%、より好ましくは、1~5重量%である。従って、前述する「油脂に対する粉末状の可食性植物加工物の配合の割合」では、最終製品の飲料中の粉末状の可食性植物加工物および油脂の配合の割合を、前記の範囲になるように、適宜調整することが好ましい。 In addition, the ratio (dry weight conversion) of the powdery edible plant processed material contained in the drink of the final product actually manufactured is 0 with respect to 100 weight% of the said drink from a viewpoint of the effect of this invention. It can be selected from the range of 1 to 20% by weight, preferably 0.3 to 10% by weight, more preferably 0.5 to 5% by weight. The ratio of fats and oils can be selected from the range of 0.1 to 50% by weight, preferably 0.5 to 10% by weight, more preferably 1 to 5% by weight. Therefore, in the above-mentioned “ratio of blending of powdered edible plant processed products with respect to fats and oils”, the blending ratio of powdered edible plant processed products and fats and oils in the final product beverage is in the above range. It is preferable to adjust appropriately.
 油脂に粉末状の可食性植物加工物を分散させる方法は、特に制限されないが、例えば、油脂に粉末状の可食性植物加工物、好ましくは、可食性植物加工物の乾燥粉末をそのまま添加し、定法に従って撹拌混合することによって実施することができる。 The method for dispersing the powdered edible plant processed product in the fat is not particularly limited, for example, the powdered edible plant processed product in the fat, preferably, the dry powder of the edible plant processed product is added as it is, It can be carried out by stirring and mixing according to a conventional method.
 この分散工程は、原料として使用する油脂と粉末状の可食性植物加工物に含まれている水以外の水が共存しない状態であることが好ましい。つまり、当該分散工程において、水は別途添加(外添)されないことが好ましい。斯くして効率的に、油脂中に緑黄色系の天然色素を始めとする可食性植物に由来する成分を溶出させて溶解や分散させることができる。 This dispersion step is preferably in a state in which the oil and fat used as the raw material and water other than water contained in the powdered processed edible plant do not coexist. That is, it is preferable that water is not separately added (externally added) in the dispersion step. Thus, it is possible to efficiently dissolve and disperse components derived from edible plants such as green-yellow natural pigments in fats and oils.
 なお、この分散工程は、基本的に、油脂そのものに粉末状の可食性植物加工物のみを単独で分散する工程であり、この工程において別途、安定剤や乳化剤等の添加剤を配合することは、特に必要とされない。つまり、この分散工程は、安定剤や乳化剤等の添加剤を用いないことが好ましい。 In addition, this dispersion | distribution process is a process which disperse | distributes only powdery edible plant processed material to fats and oils itself independently, In this process, separately adding additives, such as a stabilizer and an emulsifier, Not particularly needed. That is, it is preferable that this dispersion process does not use additives such as stabilizers and emulsifiers.
 なお、ここで、安定剤は、飲食品に含まれる粒子や不溶性固形物等について、その飲食品中の分散を改善するために用いられる食品添加剤である。制限はされないものの、例えば、海藻多糖類(カラギナン、アルギン酸ナトリウム、アルギン酸プロピレングリコールエステル等)、種子多糖類(グアーガム、タマリンドシードガム等)、樹脂多糖類(アラビアガム、トラガントガム、カラヤガム等)、果皮多糖類(ペクチン等)、発酵多糖類(キサンタンガム、ジェランガム、カードラン、プルラン等)、セルロース、およびその誘導体(カルボキシメチルセルロースナトリウム、メチルセルロース等)、澱粉誘導体(デンプングリコール酸ナトリウム等)、甲殻抽出物(キトサン等)を挙げることができる。 Here, the stabilizer is a food additive used for improving dispersion in the food and drink with respect to particles, insoluble solids, and the like contained in the food and drink. Although not limited, for example, seaweed polysaccharides (carrageenan, sodium alginate, propylene glycol alginate, etc.), seed polysaccharides (guar gum, tamarind seed gum, etc.), resin polysaccharides (arabic gum, tragacanth gum, karaya gum, etc.), pericarp Sugars (pectin, etc.), fermented polysaccharides (xanthan gum, gellan gum, curdlan, pullulan, etc.), cellulose and its derivatives (sodium carboxymethylcellulose, methylcellulose, etc.), starch derivatives (sodium starch glycolate, etc.), shell extract (chitosan) Etc.).
 また、乳化剤は、飲食品に含まれる油滴(油相)や水滴(水相)等について、その飲食品中の乳化を改善するために用いられる食品添加剤である。制限はされないものの、例えば、グリセリン脂肪酸エステル、ソルビタン脂肪酸エステル、ショ糖脂肪酸エステル、およびプロピレングリコール脂肪酸エステル等の脂肪酸エステルを挙げることができる。 Further, the emulsifier is a food additive used for improving emulsification in the food and drink with respect to oil droplets (oil phase) and water droplets (water phase) contained in the food and drink. Although not limited, for example, fatty acid esters such as glycerin fatty acid ester, sorbitan fatty acid ester, sucrose fatty acid ester, and propylene glycol fatty acid ester can be mentioned.
 この分散工程の温度条件は、特に制限されないが、通常、5~60℃であり、好ましくは、10~40℃であり、より好ましくは、20~30℃である。分散は、上記の温度条件で0.5~15分間、好ましくは0.5~10分間程度、スターラー、撹拌翼、スパチュラーを用いて、油脂と粉末状可食性植物加工物との混合物を撹拌することで実施することができる。 The temperature condition of this dispersion step is not particularly limited, but is usually 5 to 60 ° C., preferably 10 to 40 ° C., and more preferably 20 to 30 ° C. The dispersion is performed for 0.5 to 15 minutes, preferably about 0.5 to 10 minutes under the above temperature conditions, and the mixture of the oil and fat and the powdered edible plant product is stirred using a stirrer, stirring blade, or spatula. Can be implemented.
 なお、当該分散工程の後に、この得られた油脂分散物に対し、必要に応じて、さらに均質化処理してもよい。均質化処理は、通常の均質化の設備や装置、例えば、ホモジナイザー、超音波式乳化機、コロイドミル、ラインミル、ホモミキサー、アジホモミキサー、Uミキサー、マイルダーを用いて行うことができる。好ましくは、高速ホモミキサー、より好ましくは、高圧ホモジナイザー(例えば、マントンゴーリン、マイクロフルダイザー、ナノマイザー(いずれも商標名))を用いることが好ましい。高圧ホモジナイザーを用いる場合の圧力条件としては、制限されないものの、通常1~50MPaの範囲を挙げることができる。好ましくは5~40MPaであり、より好ましくは10~40MPaである。高速ホモミキサーを用いる場合の回転数としては、制限されないものの、例えばラボスケールでの条件では、T.K.ホモミキサー(プライミクス社製:直径30mmの高速回転タービン羽根とステーターとの間を通過する際の剪断により乳化、分散を促進する装置)で、通常2000~10000rpmの範囲を挙げることができる。好ましくは3000~9000rpmであり、より好ましくは5000~7000rpmである。温度条件は、通常、10~80℃、好ましくは30~70℃、より好ましくは40~60℃の範囲に設定することができる。均質化処理時間は、制限されないものの、1~30分間を例示することができる。 In addition, you may further homogenize the obtained fat dispersion after the said dispersion | distribution process as needed. The homogenization treatment can be performed using ordinary homogenization equipment or equipment, for example, a homogenizer, an ultrasonic emulsifier, a colloid mill, a line mill, a homomixer, an azimuth homomixer, a U mixer, or a milder. It is preferable to use a high-speed homomixer, more preferably a high-pressure homogenizer (for example, Manton Gorin, Microfull Diizer, Nanomizer (all are trade names)). The pressure condition in the case of using a high-pressure homogenizer is not limited, but can usually be in the range of 1 to 50 MPa. The pressure is preferably 5 to 40 MPa, more preferably 10 to 40 MPa. The number of rotations when using a high-speed homomixer is not limited. K. A homomixer (manufactured by PRIMIX Co., Ltd .: a device that promotes emulsification and dispersion by shearing when passing between a high-speed rotating turbine blade having a diameter of 30 mm and a stator), and can usually be in the range of 2000 to 10000 rpm. It is preferably 3000 to 9000 rpm, more preferably 5000 to 7000 rpm. The temperature condition can usually be set in the range of 10 to 80 ° C., preferably 30 to 70 ° C., more preferably 40 to 60 ° C. The homogenization treatment time is not limited, but can be exemplified by 1 to 30 minutes.
 (b)工程(均質化処理工程)
 上記(a)工程により調製された粉末状の可食性植物加工物と油脂との分散物(油脂分散物)は、その後に、飲料を調製するための水(以下、「飲料調製用水」という)と混合し、当該混合物を均質化処理する工程((b)工程)に供される。
(B) Process (homogenization process)
The dispersion (oil dispersion) of the powdered edible plant processed product and fat prepared in the step (a) is then water for preparing a beverage (hereinafter referred to as “beverage preparation water”). And the mixture is subjected to a step of homogenizing the mixture (step (b)).
 ここで、油脂分散物と飲料調製用水との混合処理に際して、飲料調製用水とは別に、飲料に配合する他の可食性成分(但し、安定剤や乳化剤を除く)を配合して混合することもできる。また、飲料に配合する可食性成分が水を含むものである場合、上記飲料調製用水に代えて、当該水を含む可食性成分を配合して混合することもできる。 Here, in the mixing treatment of the fat dispersion and the beverage preparation water, in addition to the beverage preparation water, other edible components to be blended in the beverage (except for stabilizers and emulsifiers) may be blended and mixed. it can. Moreover, when the edible component mix | blended with a drink contains water, it can replace with the said water for drink preparation, and can mix | blend and mix the edible component containing the said water.
 「他の可食性成分」は、安定剤や乳化剤(食品添加剤)でなければ、特に制限されないが、例えば、乳(生乳、牛乳、特別牛乳、生山羊乳、殺菌山羊乳、部分脱脂乳、脱脂乳、加工乳等)または乳製品(クリーム、バター、バターオイル、ホエイ、濃縮ホエイ、濃縮乳、脱脂濃縮乳、無糖れん乳、無糖脱脂れん乳、加糖れん乳、加糖脱脂れん乳、全粉乳、脱脂粉乳、クリームパウダー、ホエイパウダー、バターミルクパウダー、加糖粉乳、調整粉乳、発酵乳、乳酸菌飲料、および乳飲料等):卵またはその加工品:アルコール類:糖類や合成甘味料等の甘味料:pH調整剤:澱粉:塩類や酸味料等の調味料:着色料:エキス:微量栄養素:香料等を挙げることができる。そして、実際に製造する飲料の種類に応じて、適宜配合することができる。 “Other edible ingredients” are not particularly limited unless they are stabilizers or emulsifiers (food additives). For example, milk (raw milk, milk, special milk, raw goat milk, pasteurized goat milk, partially skimmed milk, Non-fat milk, processed milk, etc.) or dairy products (cream, butter, butter oil, whey, concentrated whey, concentrated milk, non-fat concentrated milk, sugar-free skim milk, sugar-free skim milk, sweetened milk, sweetened skim milk, Whole milk powder, skim milk powder, cream powder, whey powder, buttermilk powder, sweetened powdered milk, prepared powdered milk, fermented milk, lactic acid bacteria drink, and milk drink, etc.): Eggs or processed products: alcohols: sugars, synthetic sweeteners, etc. Sweetener: pH adjuster: Starch: Seasoning such as salt and acidulant: Colorant: Extract: Micronutrient: Flavor And it can mix | blend suitably according to the kind of drink actually manufactured.
 例えば、乳飲料(生乳や牛乳、乳製品を主原料とした飲料で、乳固形分(無脂乳固形分、および乳脂肪分)が3.0%以上である飲料)等を製造する場合には、乳飲料等の種類に応じて、飲料調製用水に加えて(または飲料調製用水に替えて)、前述する乳または乳製品を配合することができる。また、アルコール飲料を製造する場合には、アルコール飲料の種類に応じて、飲料調製用水に加えて(または飲料調製用水に替えて)、日本酒、ビール、焼酎、ワイン、ウイスキー、ブランデー、ウォッカ、ジン、梅酒等を配合することができる。 For example, when producing milk beverages (beverages with raw milk, milk, dairy products as the main ingredient and milk solids (nonfat milk solids and milk fats) of 3.0% or more), etc. Depending on the type of milk beverage or the like, in addition to the beverage preparation water (or in place of the beverage preparation water), the aforementioned milk or dairy product can be blended. In addition, when producing alcoholic beverages, depending on the type of alcoholic beverage, in addition to (or replace with) beverage preparation water, sake, beer, shochu, wine, whiskey, brandy, vodka, gin , Plum wine, etc. can be blended.
 実際に製造される最終製品の飲料に含まれる飲料調製用水やその他の可食性成分の配合の割合は、本発明の効果の観点から、前述するように、当該飲料の100重量%に対して、粉末状の可食性植物加工物が乾燥重量に換算して0.1~20重量%、好ましくは、0.3~10重量%、より好ましくは、0.5~5重量%となるように調整し:また、油脂が0.1~50重量%、好ましくは、0.5~10重量%、より好ましくは、1~5重量%となるように調整すればよく、その範囲において、飲料の嗜好性に応じて、適宜設定調整すればよい。 From the viewpoint of the effect of the present invention, the proportion of blended water for beverage preparation and other edible components contained in the beverage of the final product actually produced is as described above, with respect to 100% by weight of the beverage, The powdered edible plant product is adjusted to 0.1 to 20% by weight, preferably 0.3 to 10% by weight, more preferably 0.5 to 5% by weight in terms of dry weight. In addition, the fat and oil may be adjusted to 0.1 to 50% by weight, preferably 0.5 to 10% by weight, more preferably 1 to 5% by weight. The setting may be adjusted as appropriate according to the characteristics.
 上記の方法で製造された混合物の均質化処理は、通常の均質化の設備や装置、例えば、ホモジナイザー、超音波式乳化機、コロイドミル、ラインミル、ホモミキサー、アジホモミキサー、Uミキサー、マイルダーを用いてもよいが、好ましくは、高速ホモミキサー、より好ましくは、高圧ホモジナイザー(例えば、マントンゴーリン、マイクロフルダイザー、ナノマイザー(いずれも商標名))を用いることが好ましい。 The homogenization treatment of the mixture produced by the above-mentioned method is carried out by using ordinary homogenization equipment and equipment such as a homogenizer, an ultrasonic emulsifier, a colloid mill, a line mill, a homomixer, an azimuth mixer, a U mixer and a milder. Although it may be used, it is preferable to use a high-speed homomixer, more preferably a high-pressure homogenizer (for example, Manton Gorin, Microfull Diizer, Nanomizer (all are trade names)).
 高圧ホモジナイザーを用いる場合の圧力条件としては、制限されないものの、通常1~50MPaの範囲を挙げることができる。好ましくは5~40MPaであり、より好ましくは10~40MPaである。高速ホモミキサーを用いる場合の回転数としては、制限されないものの、例えばラボスケールでの条件では、T.K.ホモミキサー(プライミクス社製:直径30mmの高速回転タービン羽根とステーターとの間を通過する際の剪断により乳化、分散を促進する装置)で、通常2000~10000rpmの範囲を挙げることができる。好ましくは3000~9000rpmであり、より好ましくは5000~7000rpmである。温度条件は、通常、10~80℃、好ましくは30~70℃、より好ましくは40~60℃の範囲に設定することができる。均質化処理時間は、制限されないものの、5~30分間を例示することができる。 The pressure condition when using a high-pressure homogenizer is not limited, but can usually be in the range of 1 to 50 MPa. The pressure is preferably 5 to 40 MPa, more preferably 10 to 40 MPa. The number of rotations when using a high-speed homomixer is not limited. K. A homomixer (manufactured by PRIMIX Co., Ltd .: a device that promotes emulsification and dispersion by shearing when passing between a high-speed rotating turbine blade having a diameter of 30 mm and a stator), and can usually be in the range of 2000 to 10000 rpm. It is preferably 3000 to 9000 rpm, more preferably 5000 to 7000 rpm. The temperature condition can usually be set in the range of 10 to 80 ° C., preferably 30 to 70 ° C., more preferably 40 to 60 ° C. The homogenization treatment time is not limited, but can be exemplified by 5 to 30 minutes.
 以上の方法に従って、本発明の飲料を製造・取得することができるが、商品として市場に流通させる飲料を製造する場合には、上記の方法で調製(製造)された飲料を、さらに、缶、瓶、紙パック、レトルトパウチ等の容器に充填して密封し、次いで殺菌処理に供することが好ましく、斯くして、容器詰めの飲料(容器詰飲料)を製造・取得することができる。 According to the above method, the beverage of the present invention can be produced and obtained. However, when producing a beverage to be distributed as a product on the market, the beverage prepared (manufactured) by the above method can be It is preferable to fill and seal containers such as bottles, paper packs, retort pouches, etc., and then subject to sterilization treatment. Thus, a container-packed beverage (contained beverage) can be produced and obtained.
 上記の方法で製造された混合物や飲料の殺菌処理は、特に制限されないが、実際に製造する飲料の種類に応じて、通常の殺菌処理(プレート式の超高温加熱殺菌(UHT)、チューブ式の高温短時間加熱殺菌(HTST)、レトルト殺菌、オートクレーブ殺菌等)を採用することができる。 The sterilization treatment of the mixture or beverage produced by the above method is not particularly limited, but depending on the type of beverage actually produced, normal sterilization treatment (plate type ultra high temperature heat sterilization (UHT), tube type High temperature short time heat sterilization (HTST), retort sterilization, autoclave sterilization, etc.) can be employed.
 上記の方法で製造された飲料では、粉末状の可食性植物加工物といった不溶性固形物を含みながらも、その分散安定性が向上されており、粉末状の可食性植物加工物そのものを油脂に分散させる工程を経ずに製造された飲料(コントロール飲料)と比べて、経時的に生じる沈降の現象が有意に抑制されていることを特徴とする。 The beverage produced by the above method has an insoluble solid such as a powdered edible plant processed product, but its dispersion stability is improved, and the powdered edible plant processed product itself is dispersed in fats and oils. Compared with a beverage manufactured without passing through the step (control beverage), the phenomenon of sedimentation that occurs over time is significantly suppressed.
 ここで、「分散安定性」は、前述する本発明の方法で製造された飲料(本飲料)と、コントロール飲料とを、必要に応じて、殺菌処理した後に、これら飲料を冷温~常温条件下で静置し、この静置で生成した不溶性固形物の沈殿(沈降物の生成)を経時的に観察することによって評価することができる。具体的には、コントロール飲料と比べて、この沈降物の生成量が少ないか、または生成速度が遅い場合に、本飲料において分散安定性が向上されていると判断することができる。 Here, “dispersion stability” refers to the beverage (main beverage) produced by the method of the present invention described above and a control beverage, if necessary, after sterilization treatment, and then the beverage is cooled to room temperature condition. It can be evaluated by observing with time the precipitation of insoluble solids produced by this standing (generation of sediment). Specifically, it can be determined that the dispersion stability of the present beverage is improved when the amount of the precipitate produced is small or the production rate is slow compared to the control beverage.
 また、上記の方法で製造された飲料では、粉末状の可食性植物加工物といった不溶性固形物が容器の底面に沈降して堆積した場合でも、その再分散性が有意に向上されており、コントロール飲料と比べて、それを軽く振るだけで、粉末状の可食性植物加工物が簡単に元の分散状態に戻すことができることを特徴とする。 In addition, the beverage produced by the above method has significantly improved redispersibility even when insoluble solids such as powdered edible processed plant products settle and deposit on the bottom of the container. Compared to beverages, the powdered edible plant product can be easily returned to its original dispersed state by simply shaking it.
 ここで、「再分散性」は、前述する本発明の方法で製造された飲料(本飲料)と、コントロール飲料とを、必要に応じて、殺菌処理した後に、これら飲料を冷温~常温条件下で静置し、この静置で生成した不溶性固形物の沈降物の分散しやすさを対比することによって評価することができる。例えば、これら両者の飲料を同じ条件で振とうした際に、コントロール飲料と比べて、容器の底面に沈降した不溶性固形物が飲料の全体に再分散する程度が良好であるか、または再分散する速度が速い場合に、本飲料において再分散が向上されていると判断することができる。 Here, “redispersibility” means that the beverage (main beverage) produced by the above-described method of the present invention and a control beverage are sterilized as necessary, and then the beverage is cooled to room temperature. It can be evaluated by comparing the ease of dispersion of the sediment of the insoluble solid produced by this standing. For example, when these two beverages are shaken under the same conditions, the degree to which the insoluble solids settled on the bottom surface of the container is redispersed in the whole beverage is better or redispersed than the control beverage. When the speed is high, it can be determined that redispersion is improved in the beverage.
 (II)粉末状の可食性植物加工物を含有する飲料
 本発明が対象とする飲料は、少なくとも粉末状の可食性植物加工物、油脂および水を含有する飲料であって、粉末状の可食性植物加工物を油脂と混合して分散させる工程を経ないで調製される飲料(コントロール飲料)と比べて、(i)飲料中に含まれる粉末状の可食性植物加工物の分散安定性が向上しているか、または(ii)飲料中の粉末状の可食性植物加工物の再分散性が向上してなることを特徴とするものである。
(II) Beverages containing powdered edible plant products Beverages targeted by the present invention are beverages containing at least powdered edible plant products, oils and water, and are powdery edible. Compared to beverages (control beverages) prepared without mixing and dispersing processed plant oils and fats, (i) improved dispersion stability of powdered edible plant processed products contained in beverages Or (ii) the redispersibility of the powdered edible plant processed product in the beverage is improved.
 かかる特徴を有する本発明の飲料は、(I)にて説明する製造方法、具体的には、少なくとも(a)工程および(b)工程を含む製造方法により製造することができる。また(a)工程と(b)工程との間に、さらに均質化処理工程を有していてもよい。ここで、本発明の飲料の成分である粉末状の可食性植物加工物および油脂の種類と、その配合の割合、ならびに(a)工程および(b)工程、さらに(a)工程と(b)工程との間の均質化処理の説明は、(I)において前述した通りであり、これらの記述は、ここでも同様に援用することができる。 The beverage of the present invention having such characteristics can be produced by the production method described in (I), specifically, the production method including at least the steps (a) and (b). Moreover, you may have the homogenization process process between the (a) process and the (b) process. Here, the powdery edible plant processed product and fats and oils that are components of the beverage of the present invention, the proportion of the blend, and the (a) step and (b) step, and further the (a) step and (b) The description of the homogenization process between the steps is as described above in (I), and these descriptions can be used here as well.
 ただし、本発明の飲料は、前述するように、少なくとも粉末状の可食性植物加工物、油脂および水を含有する飲料であり、前述する(i)または(ii)の特徴を備えるものであればよく、この限りにおいて、上記の製造方法に拘束されるものではない。 However, as described above, the beverage of the present invention is a beverage containing at least a powdered edible plant product, fats and oils, and has the above-described feature (i) or (ii). As long as this is the case, the above manufacturing method is not restrictive.
 さらに、本発明の好ましい飲料は、少なくとも粉末状の可食性植物加工物、油脂および水を含有する飲料であり、前述する(i)または(ii)の特徴に加えて、(iii)の特徴として、コントロール飲料と比べて、飲料中の粉末状の可食性植物加工物の退色または変色が抑制されてなるものである。 Furthermore, a preferable beverage of the present invention is a beverage containing at least a powdered edible plant product, fats and oils, and in addition to the above-described feature (i) or (ii), the feature (iii) Compared with a control drink, the discoloration or discoloration of the powdery edible plant processed material in a drink is suppressed.
 ここで、「退色または変色が抑制されてなる」とは、前述する本発明の方法で製造された飲料(本飲料)と、コントロール飲料とを、それぞれ殺菌処理するか、および/または冷温~加温条件下で静置し、これら飲料の調製直後の色調を基準として、これら飲料の色調の変化を経時的に観察することによって評価することができる。例えば、コントロール飲料と比べて、その色調の変化が小さい場合に、本飲料において退色または変色が抑制されてなると判断することができる。 Here, “fading or discoloration is suppressed” means that the beverage (main beverage) produced by the above-described method of the present invention and the control beverage are sterilized and / or cooled to cold or heated. It can be evaluated by observing changes in the color tone of these beverages over time using the color tone immediately after the preparation of these beverages as a reference, while standing under warm conditions. For example, it can be determined that fading or discoloration is suppressed in the beverage when the change in color tone is small compared to the control beverage.
 (III)飲料中の粉末状の可食性植物加工物の分散安定性または再分散性を向上させる方法
 また、本発明は、飲料中の粉末状の可食性植物加工物の分散安定性または再分散性を向上させる方法である。
(III) A method for improving the dispersion stability or redispersibility of a powdered edible plant processed product in a beverage. The present invention also relates to the dispersion stability or redispersion of a powdered edible plant processed product in a beverage. It is a method of improving the property.
 当該方法は、粉末状の可食性植物加工物を含む飲料の製造工程において、粉末状の可食性植物加工物を予め油脂に分散させたものを、水と混合して均質化処理することで実施することができる。 The method is carried out by mixing a powdered edible plant processed product in advance in oil and fat with water and homogenizing it in a manufacturing process of a beverage containing the powdered edible plant processed product. can do.
 この方法で使用する粉末状の可食性植物加工物および油脂の種類と、その配合の割合の説明は、(I)において前述した通りであり、これらの記述は、ここでも同様に援用することができる。 The description of the types of powdered edible plant products and oils and fats used in this method, and the proportions of the fats and oils are as described above in (I), and these descriptions can be used here as well. it can.
 なお、本発明の方法は、粉末状の可食性植物加工物を含む飲料の製造に際して、粉末状の可食性植物加工物を予め油脂に分散させたものを原料として用いて、これを水と混合して均質化処理することで実施することもできるし、また、粉末状の可食性植物加工物を油脂に分散させる工程[(a)工程]、およびこれを水と混合して均質化処理する工程[(b)工程]を行うことでも実施できる。この方法で使用する工程(粉末状の可食性植物加工物を予め油脂に分散させる工程[(a)工程]、およびこれを水と混合して均質化処理する工程[(b)工程])の説明も、(I)において前述した通りであり、これらの記述は、ここでも同様に援用することができる。 In addition, the method of the present invention uses a powdered edible plant processed product pre-dispersed in oil and fat as a raw material in the production of a beverage containing a powdered edible plant processed product, and this is mixed with water. It is also possible to carry out by homogenizing, or to disperse the powdered edible plant processed product in fats and oils [(a) step], and to mix this with water and homogenize It can also be carried out by carrying out the step [(b) step]. Steps used in this method (step of dispersing powdered edible plant processed product in oil and fat [(a) step], and step of mixing this with water and homogenizing [step (b)]] The description is also as described above in (I), and these descriptions can be used here as well.
 かかる方法により、飲料中の粉末状の可食性植物加工物の分散安定性または再分散性を向上させることができる。より詳細には、本発明の方法は、少なくとも粉末状の可食性植物加工物、油脂および水を含有する飲料において、粉末状の可食性植物加工物を油脂と混合して分散させる工程を経ないで調製される飲料(コントロール飲料)と比べて、(i)飲料中に含まれる粉末状の可食性植物加工物の分散安定性を向上させることができるか、または(ii)飲料中の粉末状の可食性植物加工物の再分散性を向上させることができる。 Such a method can improve the dispersion stability or redispersibility of a powdered edible plant processed product in a beverage. More specifically, the method of the present invention does not go through the step of mixing and dispersing the powdered edible plant processed product with the fat in the beverage containing at least the powdered edible processed plant product, the fat and the water. Compared with the beverage (control beverage) prepared in (i), the dispersion stability of the powdered edible plant processed product contained in the beverage can be improved, or (ii) the powder form in the beverage The redispersibility of the processed edible plant can be improved.
 さらに、本発明の方法は、上記(i)または(ii)に記載する方法であるとともに、(iii)コントロール飲料と比べて、飲料中の粉末状の可食性植物加工物の退色または変色を抑制することができる。 Furthermore, the method of the present invention is the method described in (i) or (ii) above, and (iii) suppresses fading or discoloration of the powdered edible plant processed product in the beverage as compared with the control beverage. can do.
 ここで、「分散安定性」、「再分散性」、および「退色または変色が抑制されてなる」の意味およびその評価は、前述する(II)において説明した通りであり、当該説明は、ここでも同様に援用することができる。 Here, the meanings and evaluations of “dispersion stability”, “redispersibility”, and “fading or discoloration are suppressed” are as described in (II) above, and the explanation is as follows. But it can be used as well.
 以下、実験例および実施例を挙げて、本発明を説明するが、本発明は、これらの実験例等になんら制限されるものではない。 Hereinafter, the present invention will be described with reference to experimental examples and examples, but the present invention is not limited to these experimental examples.
 実験例1
(I)乳入り飲料の調製
(1)表1に記載する成分を表記載の割合で、下記の方法に従って混合し、油脂分散物1-1~1-3を調製した。このとき、抹茶粉末(乾燥物)として、辻利抹茶(辻利一本店製、粒数メディアン直径:24.69μm)を用いた。
Experimental example 1
(I) Preparation of Beverage with Milk (1) Ingredients listed in Table 1 were mixed in the proportions shown in the table according to the following method to prepare oil dispersions 1-1 to 1-3. At this time, as a matcha powder (dried product), Tori Matcha (manufactured by Toriichi Honten, grain number median diameter: 24.69 μm) was used.
Figure JPOXMLDOC01-appb-T000001
Figure JPOXMLDOC01-appb-T000001
油脂分散物1-1:(a)脱脂粉乳、(b)精製ヤシ油、および(d)イオン交換水を混合した後に、これに(c)抹茶粉末を配合し、薬サジを用いて、よく分散させて、油脂分散物1-1を調製した(25℃にて実施した)。
油脂分散物1-2:薬サジを用いて、(c)抹茶粉末を(b)精製ヤシ油に混合・分散させ、次いで、これに(a)脱脂粉乳、および(d)イオン交換水を混合して、油脂分散物1-2を調製した。
油脂分散物1-3:薬サジを用いて、(c)抹茶粉末を(b)精製ヤシ油に混合・分散させ、さらにホモゲナイザー(Niro Soavi社製)を用いて、50℃、35MPaの条件下で均質化処理し、次いで、これに(a)脱脂粉乳、および(d)イオン交換水を混合して、油脂分散物1-3を調製した。
Oil dispersion 1-1 : (a) skim milk powder, (b) refined coconut oil, and (d) ion-exchanged water are mixed, then (c) powdered green tea powder is blended in this, using a medicine sag well Dispersion was carried out to prepare oil dispersion 1-1 (performed at 25 ° C.).
Oil Dispersion 1-2 : (c) Matcha tea powder is mixed and dispersed in (b) refined coconut oil using medicinal solution, and then (a) skim milk powder and (d) ion-exchanged water are mixed therewith Thus, an oil dispersion 1-2 was prepared.
Oil dispersion 1-3 : (c) Matcha powder was mixed and dispersed in (b) refined coconut oil using a medicine sag, and further homogenizer (manufactured by Niro Soavi) under conditions of 50 ° C. and 35 MPa. Then, (a) skim milk powder and (d) ion-exchanged water were mixed with this to prepare an oil dispersion 1-3.
 (2)上記で得られた各油脂分散物1-1~1-3を、それぞれ60℃まで加温した後に、ホモミキサー(プライミクス社製)を用いて、60℃、7000rpm、60秒間の条件下で均質化処理した。その後、ホモジナイザー(Niro Soavi社製)で50℃、35MPaの均質化処理を行った。 (2) Each of the oil dispersions 1-1 to 1-3 obtained above was heated to 60 ° C., and then subjected to conditions of 60 ° C., 7000 rpm, 60 seconds using a homomixer (manufactured by Primex). Homogenized under. Thereafter, homogenization was performed at 50 ° C. and 35 MPa with a homogenizer (manufactured by Niro Soavi).
 (3)上記で得られた均質化処理物1-1~1-3を、それぞれ耐熱ビン(80ml)に充填して密封した状態において、110℃、5分間の条件下で加熱殺菌し、抹茶入り乳飲料1-1~1-3を調製した。 (3) The homogenized processed products 1-1 to 1-3 obtained above are each heat-sterilized under conditions of 110 ° C. for 5 minutes in a heat-resistant bottle (80 ml) and sealed, and matcha tea Entered milk beverages 1-1 to 1-3 were prepared.
 (II)分散安定性(沈殿抑制性)および再分散性の評価/退色の評価
 上記で調製した抹茶入り乳飲料1-1~1-3を、色調を評価した後に、常温に3日間で静置保存し、次いで、各飲料の色調と、各飲料のビンの底面に沈降した沈降物の有無を目視で評価した。次いで、抹茶入り乳飲料の入った耐熱ビンを一回転倒させて(一回転倒させた後に、元に戻して)、沈降物の再分散性を評価した。なお、これらの評価は、下記に記載する判断基準に従って実施した(以下、実験例2~4においても同じ。)。
(II) Evaluation of dispersion stability (precipitation inhibition) and redispersibility / Evaluation of fading After the color tone of milk drinks 1-1 to 1-3 prepared above were evaluated, they were allowed to stand at room temperature for 3 days. Then, the color tone of each beverage and the presence or absence of sediment that settled on the bottom of each beverage bottle were visually evaluated. Next, the heat-resistant bottle containing the matcha-containing milk beverage was turned down once (turned back once and then returned), and the redispersibility of the sediment was evaluated. These evaluations were performed according to the criteria described below (the same applies to Experimental Examples 2 to 4 below).
 <判断基準>
*1:沈降物の有無
「-」:なし、「±」:ややあり、「+」:あり、「++」:著しくあり
*2:色調
「◎」:褐変なし、「○」:やや褐変、「△」:褐変、「×」:顕著に褐変
*3:再分散性
「A」:良好(ほぼ元の分散状態に戻る)、「B」:やや不良(ビン底面に沈殿物が残留している)、「C」:不良(ほとんど分散しない)。
<Judgment criteria>
* 1: Presence / absence of sediment “-”: None, “±”: Slightly present, “+”: Present, “++”: Remarkably present * 2: Color tone “◎”: No browning, “O”: Slightly browned , “△”: Browning, “×”: Remarkably browning * 3: Redispersibility “A”: Good (almost returns to the original dispersion state), “B”: Slightly poor (precipitate remains on the bottom of the bottle) ”,“ C ”: poor (mostly not dispersed).
 結果を表2に示す。 The results are shown in Table 2.
Figure JPOXMLDOC01-appb-T000002
Figure JPOXMLDOC01-appb-T000002
 上記表2に記載するように、抹茶入り乳飲料の調製に際して、抹茶を予め油脂(精製ヤシ油)と混合して分散させておいた油脂分散物を用いた抹茶入り乳飲料1-2および1-3では、当該油脂分散物を調製せずに製造した抹茶入り乳飲料1-1と比べて、抹茶の分散安定性が向上しており、加熱殺菌後の保存中に生じる抹茶粉末の沈降が有意に抑制されることが確認された。また、抹茶入り乳飲料1-2および1-3では、抹茶入り乳飲料1-1と比べて、抹茶粉末の加熱殺菌による色調の劣化(退色)も有意に抑制されることが確認された。 As described in Table 2 above, in the preparation of a milk tea-containing milk beverage, matcha-containing milk beverages 1-2 and 1 using an oil-and-fat dispersion in which matcha was previously mixed with oil and fat (refined palm oil) and dispersed. -3, the green tea-containing milk beverage 1-1 produced without preparing the oil dispersion has improved the green tea dispersion stability, and the powdered green tea powder settled during storage after heat sterilization. It was confirmed that it was significantly suppressed. In addition, it was confirmed that in the milk drinks with matcha 1-2 and 1-3, the color tone deterioration (fading) due to heat sterilization of the matcha powder was significantly suppressed as compared with the milk drinks with matcha 1-1.
 なお、油脂分散物を均質化処理する場合(抹茶入り乳飲料1-3)と、均質化処理しない場合(抹茶入り乳飲料1-2)とで、分散安定性(沈降物の有無)、色調の劣化(退色)、および再分散性に大きな変化はなかった。 In addition, dispersion stability (presence of sediment), color tone when homogenizing the fat dispersion (milk powder with matcha 1-3) and without homogenization (milk drink 1-2 with green tea) There was no significant change in degradation (fading) and redispersibility.
 実験例2
 抹茶粉末として、「辻利抹茶」(辻利一本店製)に代えて、「神苑の白」(あいや製、粒数メディアン直径:12.23μm)を用いる以外は、実験例1の抹茶入り乳飲料1-1および1-2と同様にして、それぞれ抹茶入り乳飲料2-1および2-2を調製した。また、これらの抹茶入り乳飲料2-1および2-2について、実験例1の(II)に記載する方法と同様の方法および基準に従って、分散安定性(沈降物の有無)、色調の劣化(退色)、および再分散性を評価した。
Experimental example 2
The matcha powder of Experimental Example 1 is used, except that “Moriko Matcha” (manufactured by Yuriichi Honten) is used as the matcha powder, except that “Kamisu no Shiro” (manufactured by Aiya, number median diameter: 12.23 μm) is used. Matched milk drinks 2-1 and 2-2 were prepared in the same manner as milk drinks 1-1 and 1-2, respectively. In addition, for these matcha-containing milk drinks 2-1 and 2-2, according to the same method and standard as described in (II) of Experimental Example 1, dispersion stability (presence of sediment), deterioration of color tone ( Fading) and redispersibility were evaluated.
 結果を表3に示す。 The results are shown in Table 3.
Figure JPOXMLDOC01-appb-T000003
Figure JPOXMLDOC01-appb-T000003
 上記表3に記載するように、抹茶入り乳飲料の調製に際して、抹茶粉末を予め油脂(精製ヤシ油)と混合して分散させておいた油脂分散物を用いることで、抹茶入り乳飲料2-2では、当該油脂分散物を調製せずに製造した抹茶入り乳飲料2-1と比べて、抹茶粉末の分散安定性が向上しており、加熱殺菌後の保存中に生じる抹茶粉末の沈降が有意に抑制されることが確認された。また、抹茶入り乳飲料2-2では、抹茶入り乳飲料2-1と比べて、抹茶粉末の加熱殺菌による色調の劣化(退色)も有意に抑制されることが確認された。 As shown in Table 3 above, when preparing a milk drink containing matcha tea, a powdered milk powder containing matcha tea can be obtained by using an oil and fat dispersion in which powdered green tea powder is previously mixed with oil and fat (refined palm oil) and dispersed. 2, the dispersion stability of matcha powder is improved compared to milk powder containing matcha 2-1 produced without preparing the oil dispersion, and the settling of matcha powder that occurs during storage after heat sterilization is reduced. It was confirmed that it was significantly suppressed. In addition, it was confirmed that in the matcha-containing milk beverage 2-2, color deterioration (fading) due to heat sterilization of the matcha powder was significantly suppressed as compared to the matcha-containing milk beverage 2-1.
 実験例3
(I)抹茶入り飲料の調製
(1)表4に記載する成分を表記載の割合で、下記の方法に従って混合し、油脂分散物3-1~3-2を調製した。このとき、抹茶粉末として、神苑の白(あいや製、粒数メディアン直径:12.23μm)を用いた。
Experimental example 3
(I) Preparation of Matcha-Containing Beverage (1) Ingredients listed in Table 4 were mixed in the proportions shown in the table according to the following method to prepare oil dispersions 3-1 to 3-2. At this time, as a matcha powder, a white shrine (made by Aiya, number of medians of diameter: 12.23 μm) was used.
Figure JPOXMLDOC01-appb-T000004
Figure JPOXMLDOC01-appb-T000004
油脂分散物3-1:精製ヤシ油、乳化剤 P-1670(三菱化学フーズ社製:シュガーエステル)、乳化剤 681SPV(太陽化学社製)、およびイオン交換水を混合した後に、これに抹茶粉末を配合し、薬サジを用いて、よく分散させて、油脂分散物3-1を調製した。
油脂分散物3-2:薬サジを用いて、抹茶粉末を精製ヤシ油に混合・分散させ、次いで、これに乳化剤P-1670および681SPV、並びにイオン交換水を混合して、油脂分散物3-2を調製した。
Oil dispersion 3-1 : Refined coconut oil, emulsifier P-1670 (Mitsubishi Chemical Foods, Inc .: sugar ester), emulsifier 681SPV (Taiyo Kagaku), and ion-exchanged water are mixed, and then powdered green tea powder is added thereto Then, using oil squeeze, well dispersed, oil and fat dispersion 3-1 was prepared.
Oil dispersion 3-2 : Matcha powder is mixed and dispersed in refined coconut oil using a medicine sag, and then emulsifiers P-1670 and 681SPV and ion-exchanged water are mixed with the oil dispersion 3- 2 was prepared.
 (2)上記で得られた各油脂分散物3-1および3-2を、それぞれ60℃まで加温した後に、ホモミキサー(プライミクス社製)を用いて、60℃、7000rpm、60秒間の条件下で均質化処理した。 (2) After each oil dispersion 3-1 and 3-2 obtained above was heated to 60 ° C., using a homomixer (manufactured by Primics), conditions of 60 ° C., 7000 rpm, 60 seconds Homogenized under.
 (3)上記で得られた均質化処理物3-1および3-2を、それぞれ耐熱ビン(80ml)に充填して密封した状態において、110℃、5分間の条件下で加熱殺菌し、抹茶入り乳飲料3-1および3-2を調製した。 (3) The homogenized products 3-1 and 3-2 obtained above were each heat-sterilized under conditions of 110 ° C. for 5 minutes in a heat-resistant bottle (80 ml) and sealed, and matcha tea Milk drinks 3-1 and 3-2 were prepared.
 (II)分散安定性(沈殿抑制性)および再分散性の評価/退色の評価
 上記で調製した抹茶入り飲料3-1および3-2を、常温に3日間で静置保存し、次いで、各飲料のビンの底面に沈降した沈降物の有無を目視で評価した。次いで、抹茶入り飲料の入った耐熱ビンを一回転倒させ(一回転倒させた後に、元に戻して)、沈降物の再分散性を評価した。なお、これらの評価は、実験例1に記載する判断基準に従って実施した。
(II) Evaluation of dispersion stability (precipitation inhibition) and redispersibility / evaluation of fading The green tea-containing beverages 3-1 and 3-2 prepared above were stored at room temperature for 3 days, and then each The presence or absence of sediment that settled on the bottom of the beverage bottle was visually evaluated. Subsequently, the heat-resistant bottle containing the matcha-containing beverage was turned down once (turned back once and then returned), and the redispersibility of the sediment was evaluated. These evaluations were performed according to the criteria described in Experimental Example 1.
 結果を表5に示す。 The results are shown in Table 5.
Figure JPOXMLDOC01-appb-T000005
Figure JPOXMLDOC01-appb-T000005
 上記表5に記載するように、抹茶入り飲料の調製に際して、抹茶粉末を予め油脂(精製ヤシ油)と混合して分散させておいた油脂分散物を用いた抹茶入り飲料3-2では、当該油脂分散物を調製せずに製造した抹茶入り乳飲料3-1と比べて、抹茶粉末の分散安定性が向上しており、加熱殺菌後の保存中に生じる抹茶粉末の沈降が有意に抑制されることが確認された。また、抹茶入り乳飲料3-2では、抹茶入り乳飲料3-1と比べて、再分散性が向上しており、一旦沈殿した抹茶粉末も容器を振とうすることで簡単に分散できることが確認された。 As described in Table 5 above, in the preparation of a matcha-containing beverage, in the matcha-containing beverage 3-2 using an oil-and-fat dispersion in which matcha powder was previously mixed with oil and fat (refined palm oil) and dispersed, Compared with milk powder containing powdered green tea 3-1 produced without preparing an oil dispersion, the powdered green tea powder has improved dispersion stability and significantly reduced the powdered green tea powder during storage after heat sterilization. It was confirmed that In addition, Matcha milk drink 3-2 has improved redispersibility compared to Matcha milk drink 3-1, and it is confirmed that powdered green tea powder can be easily dispersed by shaking the container. It was done.
 実験例4
 抹茶の「辻利抹茶」(辻利一本店製)に代えて、ケールの粉末(こだま食品社製、粒数メディアン直径:124μm)、または大麦(若葉)のマイクロパウダー(こだま食品社製、粒数メディアン直径:40μm)を用いる以外は、実験例1の抹茶入り乳飲料1-1および1-2と同様にして、それぞれケールの粉末入り飲料4-1および4-2、ならびに大麦(若葉)の粉末入り飲料5-1および5-2を調製した。また、これらの抹茶入り飲料4-1、4-2、5-1および5-2について、実験例1の(II)に記載する方法と類似する方法(保存条件を「常温、3日間」を「冷蔵、4日間」に変更)、および実験例1の(II)に記載する基準に従って、分散安定性(沈降物の有無)、色調の劣化(退色)、および再分散性を評価した。
Experimental Example 4
Instead of “Mori Matcha” (Made by Ichiichi Honten), matcha powder (made by Kodama Foods Co., Ltd., grain number median diameter: 124 μm), or barley (wakaba) micropowder (made by Kodama Foods Co., Ltd., grain) Except for the use of several median diameters: 40 μm), in the same manner as the milk tea drinks 1-1 and 1-2 with green tea in Experimental Example 1, kale powder drinks 4-1 and 4-2, and barley (young leaves), respectively. The powdered beverages 5-1 and 5-2 were prepared. In addition, for these matcha tea drinks 4-1, 4-2, 5-1 and 5-2, a method similar to the method described in (II) of Experimental Example 1 (with storage conditions of “normal temperature, 3 days” The dispersion stability (presence of sediment), deterioration of color tone (fading), and redispersibility were evaluated according to the criteria described in (II) of “Refrigerated, 4 days”) and Experimental Example 1 (II).
 結果を表6に示す。 The results are shown in Table 6.
Figure JPOXMLDOC01-appb-T000006
Figure JPOXMLDOC01-appb-T000006
 上記表6に記載するように、ケールの粉末入り飲料および大麦(若葉)の粉末入り飲料の調製に際して、ケールの粉末または大麦(若葉)の粉末を予め油脂(精製ヤシ油)と混合して分散させておいた油脂分散物を用いた飲料4-2および5-2では、当該油脂分散物を調製せずに製造した飲料4-1や5-1と比べて、ケールの粉末や大麦(若葉)の粉末の分散安定性が向上しており、加熱殺菌後の保存中に生じる不溶性固形物の沈降が有意に抑制されることが確認された。また、飲料4-2や5-2では、飲料4-1や5-1と比べて、再分散性が向上しており、一旦沈殿したケール末および大麦若葉粉末も容器を振とうすることで簡単に分散できることが確認された。 As described in Table 6 above, when preparing beverages containing kale powder and barley (young leaves) powder, kale powder or barley (young leaf) powder is previously mixed with fat (refined palm oil) and dispersed. In beverages 4-2 and 5-2 using the oil dispersion, the kale powder and barley (young leaves) were compared to beverages 4-1 and 5-1, which were produced without preparing the oil dispersion. ) Was improved in dispersion stability, and it was confirmed that sedimentation of insoluble solids generated during storage after heat sterilization was significantly suppressed. Also, beverages 4-2 and 5-2 have improved redispersibility compared to beverages 4-1 and 5-1, and once the kale powder and barley young leaf powder that has been precipitated are shaken, It was confirmed that it could be easily dispersed.
 実験例5
 表7に記載する成分を、下記(1)の順番で混合した場合と、(2) の順番で混合した場合とで、それぞれ得られた試料の性状を評価した。抹茶として、「辻利抹茶」(辻利一本店製、粒数メディアン直径:24.69μm)を用いた。
Experimental Example 5
The properties of the obtained samples were evaluated when the components listed in Table 7 were mixed in the following order (1) and when they were mixed in the order (2). As Matcha, “Mori Matcha” (manufactured by Yariichi Honten, grain median diameter: 24.69 μm) was used.
Figure JPOXMLDOC01-appb-T000007
Figure JPOXMLDOC01-appb-T000007
 (1)抹茶粉末をイオン交換水に添加・混合し、次いで、これに精製ヤシ油を添加し、薬サジを用いて、よく混合・分散させて、試料(1)を調製した。 (1) Matcha powder was added to and mixed with ion-exchanged water, and then refined coconut oil was added thereto, and well mixed and dispersed using a medicine sag to prepare sample (1).
 (2)抹茶粉末を精製ヤシ油に添加し、薬サジを用いて、よく掻き混ぜて、均一なペーストにした。次いで、これにイオン交換水を添加して、薬サジを用いて、よく混合し、試料(2)を調製した。 (2) Matcha powder was added to refined coconut oil and stirred well with a medicine sword to make a uniform paste. Next, ion-exchanged water was added thereto, and well mixed using a medicine sword to prepare a sample (2).
 上記で調製した試料(1)および(2)を、室温(25℃)に20分間静置させ、性状を目視で確認した後に、これらを遠心分離処理(1000rpm、5分間、25℃)した。 The samples (1) and (2) prepared above were allowed to stand at room temperature (25 ° C.) for 20 minutes, their properties were visually confirmed, and then centrifuged (1000 rpm, 5 minutes, 25 ° C.).
 室温(25℃)に20分間で静置させた試料(1)および(2)の状態を、図1(A)に、また、それらを遠心分離用のチューブに入れて、さらに遠心分離処理した後の状態を、図1(B)に示す。各図において、向かって左側が試料(1)、右側が試料(2)の状態を示す。なお、この場合において、この試料(1)および(2)は、粒径の大きい乳濁液として観察された。 The state of the samples (1) and (2) allowed to stand at room temperature (25 ° C.) for 20 minutes is shown in FIG. 1 (A), and they are placed in a centrifuge tube and further centrifuged. The later state is shown in FIG. In each figure, the left side shows the state of the sample (1) and the right side shows the state of the sample (2). In this case, the samples (1) and (2) were observed as an emulsion having a large particle size.
 図1に示すように、抹茶粉末をヤシ油と直接混合すると、抹茶粉末に含まれる天然色素成分であるクロロフィル(葉緑素)が油相(上層)に大量に溶け込むのに対して、抹茶粉末を一旦水に溶解した後にヤシ油と混合すると、クロロフィル(葉緑素)は、あまり油相(上層)に溶け込まなかった。このことから、抹茶粉末(粉末状の可食性植物加工物)、油脂および水を混合する順番によって、性状の異なった組成物(混合物)が得られることがわかる。 As shown in FIG. 1, when green tea powder is directly mixed with coconut oil, the natural pigment component chlorophyll (chlorophyll) contained in the green tea powder dissolves in a large amount in the oil phase (upper layer). When dissolved in water and then mixed with coconut oil, chlorophyll (chlorophyll) did not dissolve much in the oil phase (upper layer). From this, it is understood that compositions (mixtures) having different properties can be obtained depending on the order of mixing matcha powder (powdered edible plant processed product), fats and oils, and water.

Claims (14)

  1. (a)粉末状の可食性植物加工物を油脂に混合して分散させる工程、および
    (b)粉末状の可食性植物加工物と油脂との分散物を水と混合して均質化処理する工程
    を含む、粉末状の可食性植物加工物を含有する飲料の製造方法。
    (A) a step of mixing and dispersing a powdered edible plant product in oil and fat; and (b) a step of mixing a dispersion of the powdered edible plant product and fat with water and homogenizing the mixture. A method for producing a beverage containing a processed powdered edible plant product.
  2. (a)工程と(b)工程の間に、さらに均質化処理する工程を有する、請求項1に記載する製造方法。 The manufacturing method according to claim 1, further comprising a homogenization step between the step (a) and the step (b).
  3. 上記(b)工程で用いる水が乳または乳成分を含むものである、請求項1または2に記載する製造方法。 The production method according to claim 1 or 2, wherein the water used in the step (b) contains milk or a milk component.
  4. 安定剤および/または乳化剤を配合しないことを特徴とする、請求項1乃至3のいずれかに記載する製造方法。 The production method according to any one of claims 1 to 3, wherein a stabilizer and / or an emulsifier is not blended.
  5. 粉末状の可食性植物加工物が、茶、野菜、果実、穀物および豆類からなる群から選択される少なくとも1種の植物の乾燥粉末である、請求項1乃至4のいずれかに記載する製造方法。 The manufacturing method according to any one of claims 1 to 4, wherein the powdered edible plant processed product is a dry powder of at least one plant selected from the group consisting of tea, vegetables, fruits, grains and beans. .
  6. (a)工程で得られる分散物が、原料として使用する油脂および可食性植物加工物に由来する水以外の水を含まないことを特徴とする、請求項1乃至5のいずれかに記載する製造方法。 6. The production according to any one of claims 1 to 5, wherein the dispersion obtained in the step (a) does not contain water other than water derived from fats and edible plant products used as raw materials. Method.
  7. 請求項1乃至6のいずれかに記載する製造方法で得られる、少なくとも粉末状の可食性植物加工物、油脂および水を含有する飲料であって、粉末状の可食性植物加工物を油脂と混合して分散させる工程を経ないで調製される飲料と比べて、少なくとも、飲料中の粉末状の可食性植物加工物の分散安定性が向上しているか、または飲料中の粉末状の可食性植物加工物の再分散性が向上してなることを特徴とする、飲料。 A beverage containing at least a powdered edible plant product, fats and oils, and water obtained by the production method according to claim 1, wherein the powdered edible plant products are mixed with fats and oils The dispersion stability of the powdered edible plant processed product in the beverage is improved, or the powdered edible plant in the beverage, compared to the beverage prepared without passing through the step of dispersing the A beverage characterized by improved redispersibility of a processed product.
  8. さらに飲料中の粉末状の可食性植物加工物の退色が抑制されてなる、請求項7に記載する飲料。 Furthermore, the drink of Claim 7 formed by the fading of the powdery edible plant processed material in a drink being suppressed.
  9. 粉末状の可食性植物加工物を含む飲料の製造工程において、粉末状の可食性植物加工物を予め油脂に分散させたものを水と混合して均質化処理する工程を有することを特徴とする、飲料中の粉末状の可食性植物加工物の分散安定性または再分散性を向上させる方法。 In a process for producing a beverage containing a powdered edible plant product, the powdered edible plant product is previously dispersed in an oil and fat and mixed with water for homogenization. A method for improving the dispersion stability or redispersibility of a powdered edible plant product in a beverage.
  10. 上記水が乳または乳成分を含むものである、請求項9に記載する方法。 The method according to claim 9, wherein the water contains milk or a milk component.
  11. 安定剤および/または乳化剤を配合しないことを特徴とする、請求項9または10に記載する方法。 The method according to claim 9 or 10, characterized in that no stabilizer and / or emulsifier is incorporated.
  12. 粉末状の可食性植物加工物が、茶、野菜、果実、穀物および豆類からなる群から選択される少なくとも1種の植物の乾燥粉末である、請求項9乃至11のいずれかに記載する方法。 The method according to any one of claims 9 to 11, wherein the powdered edible plant processed product is a dry powder of at least one plant selected from the group consisting of tea, vegetables, fruits, grains and beans.
  13. 粉末状の可食性植物加工物を油脂に分散させたものが、当該油脂および可食性植物加工物に由来する水以外の水を含まないことを特徴とする、請求項9乃至12のいずれかに記載する方法。 The powdered edible plant processed product dispersed in fats and oils does not contain water other than the water derived from the fats and edible plant processed products. How to describe.
  14. 飲料中の粉末状の可食性植物加工物の分散安定性または再分散性を向上させるとともに、飲料中の粉末状の可食性植物加工物の退色を抑制する方法である、請求項9乃至13のいずれかに記載する方法。 The method according to claim 9, wherein the dispersion stability or redispersibility of the powdered edible plant processed product in the beverage is improved, and the discoloration of the powdered edible plant processed product in the beverage is suppressed. The method described in any one.
PCT/JP2014/052583 2013-02-04 2014-02-04 Method for manufacturing beverage containing processed edible-plant powder having improved dispersion stability or redispersability WO2014119798A1 (en)

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JP2015198586A (en) * 2014-04-07 2015-11-12 日清オイリオグループ株式会社 Green juice food product, and method for producing the same
JP2018027065A (en) * 2016-08-19 2018-02-22 日清オイリオグループ株式会社 Fading inhibitor for green food product
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