WO2014101533A1 - 一种应用于电子烟具及传统水烟的果肉制备方法 - Google Patents

一种应用于电子烟具及传统水烟的果肉制备方法 Download PDF

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Publication number
WO2014101533A1
WO2014101533A1 PCT/CN2013/085387 CN2013085387W WO2014101533A1 WO 2014101533 A1 WO2014101533 A1 WO 2014101533A1 CN 2013085387 W CN2013085387 W CN 2013085387W WO 2014101533 A1 WO2014101533 A1 WO 2014101533A1
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Prior art keywords
pulp
electronic cigarette
liquid
cigarette liquid
hookah
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PCT/CN2013/085387
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English (en)
French (fr)
Inventor
郑志炫
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昌宁德康生物科技有限公司
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Priority to US14/232,909 priority Critical patent/US9565873B2/en
Priority to EP13866479.2A priority patent/EP2786664B1/en
Publication of WO2014101533A1 publication Critical patent/WO2014101533A1/zh

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Classifications

    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
    • A24B15/26—Use of organic solvents for extraction
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10—Chemical features of tobacco products or tobacco substitutes
    • A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10—Chemical features of tobacco products or tobacco substitutes
    • A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F1/00—Tobacco pipes
    • A24F1/30—Hookahs
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00—Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/10—Devices using liquid inhalable precursors

Definitions

  • the present invention relates to a method for preparing a pulp for use in an electronic smoking article and a conventional water-smoke, and belongs to the technical field of chemical preparation.
  • Hookah (hookah) is a tobacco product that is filtered by water (or other liquid) using a special tool "hookah", which is mainly popular in the Middle East. Hookah differs from other tobacco products in that it uses the waste heat from the burning of coal to raise the smoke. When smoking, the user needs to put a burning charcoal fire on the tobacco to help the tobacco burn. The bottom of the box for shisha is filled with water and contains tobacco. The smoke emitted by the burning of tobacco is filtered through water and then passed through a straw to suck the hookah.
  • Electronic cigarette liquid (or electronic cigarette liquid) is currently a popular cigarette replacement product. More and more smokers are beginning to accept the use of electronic cigarettes instead of cigarettes. Therefore, the shisha pulp processed by e-cigarette can meet the consumption needs of traditional shisha and reduce the harm of traditional tobacco to the body.
  • the hookah pulp can be applied to modern electronic smoking articles, which can be absorbed by electronic heating atomization, and can also be baked by the high temperature of charcoal fire using the traditional water-smoke method.
  • the product itself retains the original shape, color, aroma and other characteristics of the fruit, and is a new product of innovative technology.
  • the object of the present invention is to improve and innovate conventional water-smoke raw materials and to apply them to modern electronic smoking articles.
  • the electronic cigarette liquid in the patent adopts a special patent preparation method to extract the aroma substances in the plant materials such as natural tobacco and fruits; in addition, the extracted tobacco liquid is added into the natural pulp, and the fruit is fully immersed by heating and pressing. The smoke liquid is absorbed, and the aroma is fused to each other to achieve a state that can be absorbed by the electronic smoking device and the traditional water pipe.
  • An electronic cigarette liquid which is implemented according to the following technical scheme, and the tobacco leaves with an amount of 5-20% w/V of the electronic cigarette liquid are weighed into an extraction tank, and the prepared solvent is added to the extraction tank to soak the tobacco leaves for 30-10 minutes and then heated. Extract to 40-60 °C for 2-8 hours, filter the extract, add 1 to 10% w / V of cocoa bean extract to the filtrate, stir and mix for 20-40 minutes, then propylene glycol Or glycerin to make up 100% of the volume of the electronic cigarette liquid that is planned to be prepared, and mix and mix to obtain the product.
  • the cocoa bean extract is obtained by pulverizing cocoa beans to 20-60 mesh, into an extraction tank with a sandwich, adding 3-10 times of distilled water of cocoa powder, and soaking the cocoa powder 30- After 90 minutes, heat up to 80-9 (TC, heat extraction for 2-4 hours, release and filter the extract, and concentrate the filtrate under reduced pressure to a specific gravity of 1. 1-1. 4 to obtain cocoa bean extract.
  • the propylene glycol or glycerin solvent and the Tween 80 are all of a medicinal or edible grade, and the propylene glycol and the glycerin are used alone or in combination.
  • the pulp is added to the electronic cigarette liquid, and the electronic cigarette liquid is adsorbed by the pulp after being heated and pressurized, and the water smoke is absorbed by the tobacco liquid, and the excess is filtered.
  • the invention has the beneficial effects that: the electronic cigarette liquid using the plant extract is added into the pulp, and the tobacco liquid is adsorbed by the pulp after warming and pressing soaking, and finally the finished product is obtained by filtration, and the invention is an innovation of the traditional hookah smoke paste. And applied to modern electronic smoking appliances.
  • the innovation of the preparation method is firstly to use natural pulp to give the consumer a more pleasant psychology.
  • a special process is used to prepare the electronic cigarette liquid, and then the soaking is performed by heating and pressing, so that the pulp completely adsorbs the liquid.
  • Example 1 A 500 liter portion of an electronic cigarette liquid was prepared. Weigh 50 kg of tobacco leaves and put them into the extraction tank with interlayer; measure 350 liters of propylene glycol and 1 liter of Tween 80 respectively, pour Tween 80 into propylene glycol and mix for 30 minutes, add the mixture to the extraction tank.
  • the tobacco leaves were soaked for 50 minutes, then heated to 50 ° C by steaming into the interlayer, and after immersion for 4 hours, the extract was discharged and the filtrate was filtered, and 18 kg of cocoa bean extract was added to the filtrate, and the mixture was stirred for 30 minutes. Then add propylene glycol to the filtrate to make up 500 liters of the preparation, and then stir and mix for 35 minutes to obtain the electronic cigarette liquid. After the smoke liquid is obtained, the tobacco liquid and the pulp are put into a stainless steel soaking tank, and heated and soaked. 2-8 hours, filter the liquid smoke, and finally get the hookah pulp product. Description Example 2 It is planned to prepare 500 liters of electronic cigarette liquid.

Abstract

一种电子烟液及应用于该电子烟液中的果肉制备方法，步骤如下：使用500升容量带加热加压功能的不锈钢浸泡罐，将果肉及用于浸泡的原液按配比进行投料，经过加热加压浸泡，使果肉吸附饱满；打开球阀，仅将浸泡灌中的液体排出、收集；取出粘稠状果肉进行分装，即得水烟果肉产品，固形物应在内容物的90%以上。该制备方法的创新首先是采用天然果肉，从感官上给消费者一种更愉悦的心理，其次采用特有的工艺来制备电子烟液，再通过加热加压浸泡，使果肉完全吸附电子烟液。该产品使用传统水烟或电子烟具来吸取，天然水果香气饱满、烟草香气醇厚，观感及香气表现均明显优于传统水烟烟膏，更能迎合消费者的品味追求。

Description

说 明 书 一种应用于电子烟具及传统水烟的果肉制备方法 技术领域 本发明涉及一种应用于电子烟具及传统水烟的果肉制备方法，属 于化工制备技术领域。 背景技术 水烟 （hookah) 是一种采用专用工具 "水烟袋" ， 用水（或其它 液体）过滤后吸食的一种烟草制品， 主要在中东地区流行。水烟不同 于其他烟草制品， 它使用煤炭烧完后的余热来使烟上升。 吸食时， 使 用者需在烟草上面放上燃烧的炭火帮助烟草燃烧。抽水烟用的盒子底 部装有水， 上面装着烟草。 烟草燃烧放出的烟， 经过水的过滤， 再通 过一个吸管， 来吸食水烟。
传统水烟原料一般采用烟草和各种香精混合而成，该方法沿用了 几个世纪，到目前为止，水烟因烟草燃烧所产生的危害一直争议不断。
电子烟液 (或称电子烟雾化液)是目前流行的香烟替代产品。越来 越多的吸烟者开始接受使用电子烟代替香烟，因此通过电子烟液来加 工的水烟果肉， 从口感上既能满足传统水烟的消费需求， 又能降低传 统烟草对身体的危害。水烟果肉可应用于现代电子烟具， 通过电子加 热雾化来实现吸取，也能使用传统水烟的方法，用炭火的高温来烘烤。 该产品本身保留水果原有的形状、颜色、 香气等特征， 是一种创新工 艺的新产品。
说 明 书 发明内容 本发明的目的是针对传统水烟原料进行改良创新，并应用于现代 电子烟具。
本专利中的电子烟液采用特有的专利制备方法， 提取天然烟草、 水果等植物原料中的致香物质；另外将提取出来的烟液加入天然果肉 中， 通过加温加压浸泡， 使水果充分吸收烟液， 香气互相融合， 达到 可以被电子烟具及传统水烟吸取的状态。
本发明按以下技术方案实施
一种电子烟液， 其按以下技术方案实施， 称取电子烟液量 5 一 20 % w / V的烟叶投入提取罐， 将配制好的溶媒加入到提取罐中 浸泡烟叶 30— 10Q分钟后加热至 40— 60 °C温浸提取 2— 8小时， 过 滤提取液， 向滤液中加入电子烟液量的 1一 10 % w / V的可可豆提 取物， 搅拌混合 20— 40分钟， 再以丙二醇或甘油补足到 100 %计 划制备的电子烟液体积， 搅拌混合均匀即得产品。
作为优选的技术方案， 所述的溶媒的配制是分别量取电子烟 液体积量的 30— 80 %的丙二醇或甘油及 0. 1—0. 5 %的吐温 80， 将二者搅拌混合 20— 40分钟， 得到混合均匀的溶媒。
作为优选的技术方案， 所述的可可豆提取物， 是将可可豆粉 碎至 20— 60目， 投入带夹层的提取罐， 加入可可豆粉重量的 3— 10倍蒸馏水， 浸泡可可豆粉 30— 90分钟， 加热升温至 80— 9(TC， 保温提取 2— 6小时， 放出并过滤提取液， 滤液减压浓缩至比重为 1 . 1-1 . 4的浸膏， 即得可可豆提取物。
作为优选的技术方案， 所述的丙二醇或甘油溶媒及吐温 80， 均为药用或食用级别， 丙二醇和甘油单独用或混合用。
作为优选的技术方案， 在电子烟液中加入果肉， 经过加温加压 浸泡使电子烟液被果肉所吸附， 水烟果肉把烟液吸收后， 过滤多余 说 明 书 的液体， 仅保留果肉固形物。
一种传统水烟的果肉制备方法， 其具体步骤如下：
( 1 ) 称取一定量的新鲜果肉 （水份含量应符合工艺要求）；
( 2 )称取水烟果肉量 (体积）5-20% (w/v) 的电子烟液， 加入浸 泡罐，加热至 40-60 °C， 压力 IMpa, 浸泡 2-8小时。
( 3 ) 打开球阀， 仅将浸泡灌中的液体排出、 收集； 取出粘稠状 果肉进行分装， 即得水烟果肉产品， 固形物应在内容物的 90%以上。
本发明的有益效果是：将采用植物提取物的电子烟液中加入果肉 中， 经过加温加压浸泡使烟液被果肉所吸附， 过滤最后得成品， 本发 明是对传统水烟烟膏的创新， 并应用于现代电子烟具上面。该制备方 法的创新首先是采用天然果肉， 从感官上给消费者一种更愉悦的心 理， 其次采用特有的工艺来制备电子烟液， 再通过加温加压浸泡， 使 果肉完全吸附烟液。该产品使用传统水烟或电子烟具来吸取， 天然水 果香气饱满、烟草香气醇厚， 观感及香气表现均明显优于传统水烟烟 膏， 更能迎合消费者的品味追求。 具体实施方式 实例 1 : 计划制备 500升的电子烟液。 称取 50公斤烟叶， 投入 带夹层的提取罐中； 分别量取 350升丙二醇和 1升吐温 80， 将吐温 80倒入丙二醇中并搅拌混合 30分钟， 将此混合液加入至提取罐中浸 泡烟叶 50分钟， 然后向夹层中通入蒸汽加热升温至 50 °C， 保温浸提 4小时后， 放出提取液并过滤得滤液， 向滤液中加入 18公斤可可豆 提取物， 搅拌混合 30分钟， 再向滤液中加入丙二醇补足至计划制备 的 500升， 再搅拌混合 35分钟， 即得所述电子烟液， 得所述烟液后， 将烟液及果肉投入不锈钢浸泡罐， 经过加热加温浸泡 2-8小时， 过滤 烟液， 最终得到水烟果肉产品。 说 明 书 实例 2计划制备 500升的电子烟液。 称取 50公斤烟叶， 投入带 夹层的提取罐中； 先量按 1 : 1的比例量取丙二醇和甘油 380升混合， 再量取 1 . 5升吐温 80， 将吐温 80倒入丙二醇和甘油混合液中并搅 拌混合 40分钟， 加入至提取罐中浸泡烟叶 60分钟， 然后向夹层中通 入蒸汽加热升温至 60°C， 保温浸提 6小时后， 放出提取液并过滤得 滤液， 向滤液中加入 20公斤可可豆提取物， 搅拌混合 40分钟； 再向 滤液中加入甘油补足至 500升， 搅拌混合 30分钟， 得所述烟液。 后 将烟液及果肉投入不锈钢浸泡罐， 经过加热加温浸泡 2-8小时， 过滤 烟液， 最终得到水烟果肉产品。

Claims

权利 要求 书
1 . 一种电子烟液， 其特征在于： 其按以下技术方案实施， 称取电子烟液量 5 20 % w / V的烟叶投入提取罐， 将配制好的溶 媒加入到提取罐中浸泡烟叶 30— 100分钟后加热至 40— 60 °C温浸 提取 2— 8小时， 过滤提取液， 向滤液中加入电子烟液量的 1 10 % w / v的可可豆提取物， 搅拌混合 20— 40分钟， 再以丙二醇或甘 油补足到 100 %计划制备的电子烟液体积， 搅拌混合均匀即得产
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ΡΠ o
2. 根据权利要求 1所述的电子烟液， 其特征在于： 所述的溶 媒的配制是分别量取电子烟液体积量的 30— 80 %的丙二醇或甘 油及 0. 1-0. 5 %的吐温 80， 将二者搅拌混合 20— 40分钟， 得到 混合均匀的溶媒。
3. 根据权利要求 1所述的电子烟液， 其特征在于： 所述的可 可豆提取物，是将可可豆粉碎至 20— 60目，投入带夹层的提取罐， 加入可可豆粉重量的 3— 10倍蒸馏水， 浸泡可可豆粉 30— 90分钟， 加热升温至 80— 9(TC， 保温提取 2— 6小时， 放出并过滤提取液， 滤液减压浓缩至比重为 1 . 1- 1 - 4的浸膏， 即得可可豆提取物。
4. 根据权利要求 1所述的电子烟液， 其特征在于： 所述的丙 二醇或甘油溶媒及吐温 80， 均为药用或食用级别， 丙二醇和甘油 单独用或混合用。
5. 根据权利要求 1所述的电子烟液， 其特征在于： 在电子烟 液中加入果肉， 经过加热加压浸泡使电子烟液被果肉所吸附， 果肉 把原液吸收后成为粘稠状果肉或带有固体果肉的液体， 果肉应保 持其形状、 颜色特征。
6.一种如权利要求 5所述的传统水烟的果肉制备方法，其具体 步骤如下：
( 1 ) 称取一定量的新鲜果肉 （水份含量应符合工艺要求）； 权利 要求 书
(2)称取水烟果肉量 (体积）5-20% (w/v) 的电子烟液， 加入浸 泡罐，加热至 40-60°C， 压力 IMpa, 浸泡 2-8小时。
(3) 打开球阀， 仅将浸泡灌中的液体排出、 收集； 取出粘稠状 果肉进行分装， 即得水烟果肉产品， 固形物应在内容物的 90%以上。
PCT/CN2013/085387 2012-12-28 2013-10-17 一种应用于电子烟具及传统水烟的果肉制备方法 WO2014101533A1 (zh)

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Application Number Priority Date Filing Date Title
US14/232,909 US9565873B2 (en) 2012-12-28 2013-10-17 Method of producing pulp for use in electronic cigarette and traditional hookah
EP13866479.2A EP2786664B1 (en) 2012-12-28 2013-10-17 Pulp preparation method for electronic smoking set and traditional hookah

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CN2012105940211A CN103054170A (zh) 2012-12-28 2012-12-28 一种水烟果肉雾化液的制备方法
CN201210594021.1 2012-12-28

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CN103054170A (zh) 2013-04-24
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