WO2010003571A3 - Method for modifying expanded graphite and use of the modified expanded graphite - Google Patents

Method for modifying expanded graphite and use of the modified expanded graphite Download PDF

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Publication number
WO2010003571A3
WO2010003571A3 PCT/EP2009/004708 EP2009004708W WO2010003571A3 WO 2010003571 A3 WO2010003571 A3 WO 2010003571A3 EP 2009004708 W EP2009004708 W EP 2009004708W WO 2010003571 A3 WO2010003571 A3 WO 2010003571A3
Authority
WO
WIPO (PCT)
Prior art keywords
expanded graphite
modifying
graphite
modified
chemical
Prior art date
Application number
PCT/EP2009/004708
Other languages
German (de)
French (fr)
Other versions
WO2010003571A2 (en
Inventor
Reinhard Mach
Heinz-Eberhard Maneck
Asmus Meyer-Plath
Franz Oleszak
Martin Christ
Original Assignee
BAM Bundesanstalt für Materialforschung und -prüfung
Sgl Carbon Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BAM Bundesanstalt für Materialforschung und -prüfung, Sgl Carbon Ag filed Critical BAM Bundesanstalt für Materialforschung und -prüfung
Priority to EP09776887A priority Critical patent/EP2300365A2/en
Publication of WO2010003571A2 publication Critical patent/WO2010003571A2/en
Publication of WO2010003571A3 publication Critical patent/WO2010003571A3/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09CTREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/44Carbon
    • C09C1/46Graphite
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/20Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising free carbon; comprising carbon obtained by carbonising processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • B01J20/32Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3231Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the coating or impregnating layer
    • B01J20/3242Layers with a functional group, e.g. an affinity material, a ligand, a reactant or a complexing group
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/18Carbon
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/20Graphite
    • C01B32/21After-treatment
    • C01B32/22Intercalation
    • C01B32/225Expansion; Exfoliation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2253/00Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10Inorganic adsorbents
    • B01D2253/102Carbon
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2255/00Catalysts
    • B01D2255/70Non-metallic catalysts, additives or dopants
    • B01D2255/702Carbon
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/34Irradiation by, or application of, electric, magnetic or wave energy, e.g. ultrasonic waves ; Ionic sputtering; Flame or plasma spraying; Particle radiation
    • B01J37/349Irradiation by, or application of, electric, magnetic or wave energy, e.g. ultrasonic waves ; Ionic sputtering; Flame or plasma spraying; Particle radiation making use of flames, plasmas or lasers

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Carbon And Carbon Compounds (AREA)

Abstract

The invention relates to a method for modifying expanded graphite, wherein the surface thereof is brought into contact with a plasma-activated process gas in such a way that the gas forms with the carbon atoms of the graphite stable reaction products in the form of chemical groups covalently bound to the graphite so that the chemical and physisorptive properties of the expanded graphite are modified.
PCT/EP2009/004708 2008-07-11 2009-06-25 Method for modifying expanded graphite and use of the modified expanded graphite WO2010003571A2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
EP09776887A EP2300365A2 (en) 2008-07-11 2009-06-25 Method for modifying expanded graphite and use of the modified expanded graphite

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102008033280A DE102008033280A1 (en) 2008-07-11 2008-07-11 Process for modifying expanded graphite and using the modified expanded graphite
DE102008033280.1 2008-07-11

Publications (2)

Publication Number Publication Date
WO2010003571A2 WO2010003571A2 (en) 2010-01-14
WO2010003571A3 true WO2010003571A3 (en) 2010-07-22

Family

ID=41202301

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2009/004708 WO2010003571A2 (en) 2008-07-11 2009-06-25 Method for modifying expanded graphite and use of the modified expanded graphite

Country Status (3)

Country Link
EP (1) EP2300365A2 (en)
DE (1) DE102008033280A1 (en)
WO (1) WO2010003571A2 (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AT510311B1 (en) * 2010-08-27 2013-02-15 Sunpor Kunststoff Gmbh FLAME-PROTECTED, HEAT-DAMPING POLYMERISATES AND METHOD FOR THE PRODUCTION THEREOF
CN106397094B (en) * 2016-10-27 2020-01-24 新疆兵团现代绿色氯碱化工工程研究中心(有限公司) Method for modifying catalyst carrier by low-temperature plasma
CN108031233A (en) * 2017-12-13 2018-05-15 滁州兄弟科技有限公司 A kind of preparation method of nitrogen oxides waste gas disposal composite adsorbing material

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH01122911A (en) * 1987-11-07 1989-05-16 Nippon Steel Corp Production of graphite material having hardened surface
DE4432865A1 (en) * 1994-09-15 1996-03-21 Plasmachem Produktions Und Han Highly oriented pyro:graphite
US5607889A (en) * 1994-01-19 1997-03-04 Elf Aquitaine Process for producing an active composite and active composite produced by this process
EP1247856A1 (en) * 2001-04-02 2002-10-09 Viktor Ivanovich Petrik Method for removing oil, petroleum products and/or chemical pollutants from liquid and/or gas and/or surface
US20060154147A1 (en) * 2003-06-30 2006-07-13 Tdk Corporation Carbon material for electrode and method for producing same, battery electrode and method for producing same, and battery and method for producing same
US20080009640A1 (en) * 2005-10-24 2008-01-10 Wei Li Supported amorphous ni-b alloy catalyst, its preparation and use

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE66804C (en) Dr. phil. W. luzi in Leipzig, Hospitalstr. 18 Process for processing graphite
SU1657473A1 (en) * 1988-07-11 1991-06-23 Институт элементоорганических соединений им.А.Н.Несмеянова Method of producing thermally expanded graphite
US5282975A (en) 1989-12-25 1994-02-01 Technion Research And Development Foundation Ltd. Removal of oil from water
CA2286212A1 (en) * 1998-02-06 1999-08-12 Nisshinbo Industries Inc. Fuel cell separator and process for producing the same
WO2008013899A2 (en) 2006-07-27 2008-01-31 Aurora Advance Beauty Labs Rhamnolipid-based formulations
DE102007023315B3 (en) * 2007-05-16 2008-10-16 BAM Bundesanstalt für Materialforschung und -prüfung Process for producing a latent heat storage material

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH01122911A (en) * 1987-11-07 1989-05-16 Nippon Steel Corp Production of graphite material having hardened surface
US5607889A (en) * 1994-01-19 1997-03-04 Elf Aquitaine Process for producing an active composite and active composite produced by this process
DE4432865A1 (en) * 1994-09-15 1996-03-21 Plasmachem Produktions Und Han Highly oriented pyro:graphite
EP1247856A1 (en) * 2001-04-02 2002-10-09 Viktor Ivanovich Petrik Method for removing oil, petroleum products and/or chemical pollutants from liquid and/or gas and/or surface
US20060154147A1 (en) * 2003-06-30 2006-07-13 Tdk Corporation Carbon material for electrode and method for producing same, battery electrode and method for producing same, and battery and method for producing same
US20080009640A1 (en) * 2005-10-24 2008-01-10 Wei Li Supported amorphous ni-b alloy catalyst, its preparation and use

Non-Patent Citations (6)

* Cited by examiner, † Cited by third party
Title
DATABASE WPI Week 198925, Derwent World Patents Index; AN 1989-183479, XP002577997 *
MOMOSE Y: "ELECTRICAL PROPERTIES OF O2 PLASMA TREATED SOLID SURFACES", APPLIED POLYMER SYMPOSIA, JOHN WILEY AND SONS,INC. NEW YORK, US LNKD- DOI:10.1002/APP.1990.070460009, vol. 46, 1 April 1990 (1990-04-01), pages 153 - 172, XP000218661, ISSN: 0570-4898 *
See also references of EP2300365A2 *
W.-P. WANG, C.-Y. PAN: "Synthesis and characterizations of poly(ethylene oxide) methyl ether grafted on the expanded graphite with isocyanate groups", EUROPEAN POLYMER JOURNAL, vol. 40, 2004, pages 543 - 548, XP002577998 *
Y. MOMOSE, T. OAKU, H. CHUMA, S. OKAZAKI, T. SARUTA, M. MASUI, M. TAKEUCHI: "Electrical properties of O2 plasma treated solid surfaces", POLYMERIC MATERIALS SCIENCE AND ENGINEERING, vol. 62, 1990, pages 353 - 357, XP008121441 *
Y. MOMOSE, T. OHAKU, S. OKAZAKI: "Thermally stimulated exoelectron emission from graphite surfaces exposed to oxygen, tetrafluoromethane, and argon plasmas", JOURNAL OF VACUUM SCIENCE AND TECHNOLOGY A, vol. 10, 1992, pages 353 - 361, XP002577996 *

Also Published As

Publication number Publication date
DE102008033280A1 (en) 2010-01-14
WO2010003571A2 (en) 2010-01-14
EP2300365A2 (en) 2011-03-30

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