WO2009152999A3 - Verfahren zur herstellung von anorganischen fullerenartigen nanostrukturen aus metalldisulfiden, danach hergestellte nanostrukturen und ihre verwendung - Google Patents

Verfahren zur herstellung von anorganischen fullerenartigen nanostrukturen aus metalldisulfiden, danach hergestellte nanostrukturen und ihre verwendung Download PDF

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Publication number
WO2009152999A3
WO2009152999A3 PCT/EP2009/004247 EP2009004247W WO2009152999A3 WO 2009152999 A3 WO2009152999 A3 WO 2009152999A3 EP 2009004247 W EP2009004247 W EP 2009004247W WO 2009152999 A3 WO2009152999 A3 WO 2009152999A3
Authority
WO
WIPO (PCT)
Prior art keywords
nanostructures
producing inorganic
type
produced
inorganic fullerene
Prior art date
Application number
PCT/EP2009/004247
Other languages
English (en)
French (fr)
Other versions
WO2009152999A2 (de
Inventor
Wolfgang Tremel
Helen Annal-Therese
Original Assignee
Johannes Gutenberg-Universität Mainz
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Johannes Gutenberg-Universität Mainz filed Critical Johannes Gutenberg-Universität Mainz
Publication of WO2009152999A2 publication Critical patent/WO2009152999A2/de
Publication of WO2009152999A3 publication Critical patent/WO2009152999A3/de

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G33/00—Compounds of niobium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G35/00—Compounds of tantalum
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/01—Crystal-structural characteristics depicted by a TEM-image
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/78—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by stacking-plane distances or stacking sequences
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/04—Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/30—Particle morphology extending in three dimensions
    • C01P2004/32—Spheres
    • C01P2004/34—Spheres hollow
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer

Abstract

Alkoholate wie Nb(OC2H5)5 oder Ta(OC2H5)5 werden durch Pyrolyse unter Sauerstoffausschluss chemisch gespalten. Das Spaltungs- bzw. Zwischenprodukt sind Nb2O5- bzw. Ta2O5-Nano-partikel. Diese werden mittels Schwefelwasserstoff oder Schwefelkohlenstoff sulfidiert und die erhaltenen IF-NbS2- bzw. TaS2-Fulleren-Partikel getempert.
PCT/EP2009/004247 2008-06-19 2009-06-12 Verfahren zur herstellung von anorganischen fullerenartigen nanostrukturen aus metalldisulfiden, danach hergestellte nanostrukturen und ihre verwendung WO2009152999A2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102008029248.6 2008-06-19
DE200810029248 DE102008029248B4 (de) 2008-06-19 2008-06-19 Verfahren zur Herstellung von anorganischen fullerenartigen Nanostrukturen aus Metalldisulfiden, danach hergestellte Nanostrukturen und ihre Verwendung

Publications (2)

Publication Number Publication Date
WO2009152999A2 WO2009152999A2 (de) 2009-12-23
WO2009152999A3 true WO2009152999A3 (de) 2010-03-25

Family

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PCT/EP2009/004247 WO2009152999A2 (de) 2008-06-19 2009-06-12 Verfahren zur herstellung von anorganischen fullerenartigen nanostrukturen aus metalldisulfiden, danach hergestellte nanostrukturen und ihre verwendung

Country Status (2)

Country Link
DE (1) DE102008029248B4 (de)
WO (1) WO2009152999A2 (de)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IT1402163B1 (it) 2010-10-01 2013-08-28 Univ Degli Studi Salerno Sintesi "one-pot" di nano cristalli 1d, 2d, e 0d di calcogenuri di tungsteno e molibdeno (ws2, mos2) funzionalizzati con ammine e/o acidi grassi a lunga catena e/o tioli
CN103274468B (zh) * 2013-05-29 2014-09-03 复旦大学 一种球形五氧化二钽的制备方法及应用

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5958358A (en) * 1992-07-08 1999-09-28 Yeda Research And Development Co., Ltd. Oriented polycrystalline thin films of transition metal chalcogenides
WO2006106517A2 (en) * 2005-04-07 2006-10-12 Yeda Research And Development Company Ltd. Process and apparatus for producing inorganic fullerene-like nanoparticles
WO2007107283A1 (de) * 2006-03-21 2007-09-27 Johannes Gutenberg-Universität Mainz Verfahren zur herstellung von anorganischen fullerenartigen nanostrukturen, danach hergestellte nanostrukturen und ihre verwendung

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5958358A (en) * 1992-07-08 1999-09-28 Yeda Research And Development Co., Ltd. Oriented polycrystalline thin films of transition metal chalcogenides
WO2006106517A2 (en) * 2005-04-07 2006-10-12 Yeda Research And Development Company Ltd. Process and apparatus for producing inorganic fullerene-like nanoparticles
WO2007107283A1 (de) * 2006-03-21 2007-09-27 Johannes Gutenberg-Universität Mainz Verfahren zur herstellung von anorganischen fullerenartigen nanostrukturen, danach hergestellte nanostrukturen und ihre verwendung

Non-Patent Citations (7)

* Cited by examiner, † Cited by third party
Title
C. FELDMANN: "Darstellung und Charakterisierung der nanoskaligen Vb-Metalloxide M2O5 (M = V, Nb, Ta)", ZEITSCHRIFT FÜR ANORGANISCHE UND ALLGEMEINE CHEMIE, vol. 630, no. 13-14, 2004, pages 2473 - 2477, XP002564083 *
C. SCHUFFENHAUER,B. PARKINSON, N. JIN-PHILLIPP,L. JOLY-POTTUZ, J-M. MARTIN, R. POPOVITZ-BIRO, R. TENNE: "Synthesis of Fullerene-Like Tantalum Disulfide Nanoparticles by a Gas-Phase Reaction and Laser Ablation", SMALL, vol. 1, no. 11, 2005, pages 1100 - 1109, XP002564080, DOI: 10.1002/smll.200500133 *
FRANCIS LEONARD DEEPAK, RESHEF TENNE ET AL.: "Fullerene-Like (IF) NbxMo1-xS2 Nanoparticles", J. AM. CHEM. SOC., vol. 129, no. 41, 2007, pages 12549 - 12562, XP002564084 *
MANDYAM A. SRIRAM AND PRASHANT N. KUMTA: "The thio-sol-gel synthesis of titanium disulfide and niobium disulfide. Part 1.-Materials chemistry", J. MATER. CHEM., vol. 8, no. 11, 1998, pages 2441 - 2451, XP002564082 *
SCHUFFENHAUER C ET AL: "Synthesis of NbS2 nanoparticles with (nested) fullerene-like structure (IF)", JOURNAL OF MATERIALS CHEMISTRY, THE ROYAL SOCIETY OF CHEMISTRY, CAMBRIDGE, GB, vol. 12, 1 January 2002 (2002-01-01), pages 1587 - 1591, XP003007412, ISSN: 0959-9428 *
WEIBING HU ET AL: "NbS2/Nb2O5 nanocables", NANOTECHNOLOGY, IOP, BRISTOL, GB, vol. 18, no. 9, 7 March 2007 (2007-03-07), pages 95605, XP020119909, ISSN: 0957-4484 *
YAN QIU ZHU, RESHEF TENNE ET AL.: "Shock-Absorbing and Failure Mechanisms of WS2 and MoS2 Nanoparticles with Fullerene-like Structures under Shock Wave Pressure", J. AM. CHEM. SOC., vol. 27, no. 46, 2005, pages 16263 - 16272, XP002564081 *

Also Published As

Publication number Publication date
DE102008029248A1 (de) 2009-12-24
WO2009152999A2 (de) 2009-12-23
DE102008029248B4 (de) 2011-02-17

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