WO2009007079A3 - Vorrichtung mit einer verbindung zweier kapillaren - Google Patents

Vorrichtung mit einer verbindung zweier kapillaren Download PDF

Info

Publication number
WO2009007079A3
WO2009007079A3 PCT/EP2008/005519 EP2008005519W WO2009007079A3 WO 2009007079 A3 WO2009007079 A3 WO 2009007079A3 EP 2008005519 W EP2008005519 W EP 2008005519W WO 2009007079 A3 WO2009007079 A3 WO 2009007079A3
Authority
WO
WIPO (PCT)
Prior art keywords
capillaries
furnace
connection
analyte
soldering
Prior art date
Application number
PCT/EP2008/005519
Other languages
English (en)
French (fr)
Other versions
WO2009007079A2 (de
Inventor
Michael Krummen
Hans-Juergen Schlueter
Original Assignee
Thermo Fisher Scient Bremen
Michael Krummen
Hans-Juergen Schlueter
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Thermo Fisher Scient Bremen, Michael Krummen, Hans-Juergen Schlueter filed Critical Thermo Fisher Scient Bremen
Priority to US12/668,006 priority Critical patent/US20100209302A1/en
Priority to DE112008001721T priority patent/DE112008001721A5/de
Priority to GB1000957A priority patent/GB2463435B/en
Publication of WO2009007079A2 publication Critical patent/WO2009007079A2/de
Publication of WO2009007079A3 publication Critical patent/WO2009007079A3/de

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00—Sampling; Preparing specimens for investigation
    • G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/40—Concentrating samples
    • G01N1/4022—Concentrating samples by thermal techniques; Phase changes
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F16—ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
    • F16L—PIPES; JOINTS OR FITTINGS FOR PIPES; SUPPORTS FOR PIPES, CABLES OR PROTECTIVE TUBING; MEANS FOR THERMAL INSULATION IN GENERAL
    • F16L13/00—Non-disconnectible pipe-joints, e.g. soldered, adhesive or caulked joints
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01L—CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
    • B01L3/00—Containers or dishes for laboratory use, e.g. laboratory glassware; Droppers
    • B01L3/56—Labware specially adapted for transferring fluids
    • B01L3/565—Seals
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F16—ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
    • F16L—PIPES; JOINTS OR FITTINGS FOR PIPES; SUPPORTS FOR PIPES, CABLES OR PROTECTIVE TUBING; MEANS FOR THERMAL INSULATION IN GENERAL
    • F16L13/00—Non-disconnectible pipe-joints, e.g. soldered, adhesive or caulked joints
    • F16L13/007—Non-disconnectible pipe-joints, e.g. soldered, adhesive or caulked joints specially adapted for joining pipes of dissimilar materials
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/62—Detectors specially adapted therefor
    • G01N30/72—Mass spectrometers
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/84—Preparation of the fraction to be distributed
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01L—CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
    • B01L2200/00—Solutions for specific problems relating to chemical or physical laboratory apparatus
    • B01L2200/02—Adapting objects or devices to another
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01L—CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
    • B01L2300/00—Additional constructional details
    • B01L2300/08—Geometry, shape and general structure
    • B01L2300/0832—Geometry, shape and general structure cylindrical, tube shaped
    • B01L2300/0838—Capillaries
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01L—CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
    • B01L7/00—Heating or cooling apparatus; Heat insulating devices
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/84—Preparation of the fraction to be distributed
    • G01N2030/8405—Preparation of the fraction to be distributed using pyrolysis
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/62—Detectors specially adapted therefor
    • G01N30/72—Mass spectrometers
    • G01N30/7206—Mass spectrometers interfaced to gas chromatograph

Landscapes

  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Immunology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Physics & Mathematics (AREA)
  • Pathology (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • Mechanical Engineering (AREA)
  • Clinical Laboratory Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Furnace Details (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

Die Erfindung betrifft eine Vorrichtung mit einem Ofen zur thermischen Behandlung von Gasen, einem dem Ofen vorgeordneten und/oder nachgeordneten Gaschromatographen oder einer anderen Einrichtung zum Trennen gasförmiger Bestandteile, und mit einer Verbindung zweier Kapillaren, welche zur Weiterleitung eines Analyten in der Gasphase vorgesehen sind, wobei eine der beiden Kapillaren ein im Ofen angeordnetes Reaktorrohr ist. Erfindungsgemäß sind die beiden Kapillaren durch Klebung, Adhäsion, Löten oder Pressen dauerhaft gasdicht miteinander verbunden.
PCT/EP2008/005519 2007-07-06 2008-07-07 Vorrichtung mit einer verbindung zweier kapillaren WO2009007079A2 (de)

Priority Applications (3)

Application Number Priority Date Filing Date Title
US12/668,006 US20100209302A1 (en) 2007-07-06 2008-07-07 Apparatus With A Connection Between Two Capillaries
DE112008001721T DE112008001721A5 (de) 2007-07-06 2008-07-07 Vorrichtung mit einer Verbindung zweier Kapillaren
GB1000957A GB2463435B (en) 2007-07-06 2008-07-07 Apparatus with a connection between two capillaries

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102007031678A DE102007031678A1 (de) 2007-07-06 2007-07-06 Vorrichtung mit einer Verbindung zweier Kapillaren
DE102007031678.1 2007-07-06

Publications (2)

Publication Number Publication Date
WO2009007079A2 WO2009007079A2 (de) 2009-01-15
WO2009007079A3 true WO2009007079A3 (de) 2009-05-22

Family

ID=40092543

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2008/005519 WO2009007079A2 (de) 2007-07-06 2008-07-07 Vorrichtung mit einer verbindung zweier kapillaren

Country Status (4)

Country Link
US (1) US20100209302A1 (de)
DE (2) DE102007031678A1 (de)
GB (1) GB2463435B (de)
WO (1) WO2009007079A2 (de)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8727231B2 (en) 2011-11-18 2014-05-20 Dh Technologies Development Pte. Ltd. Sealed microfluidic conduit assemblies and methods for fabricating them

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2729359A1 (de) * 1976-07-19 1978-01-26 Perkin Elmer Corp Rohrverbindung fuer eine chromatographische saeule
DE2852495A1 (de) * 1978-12-05 1980-06-19 Karl Heinz Vahlbrauk Verfahren zum verbinden zweier rohrenden aus metall
US4713963A (en) * 1986-06-26 1987-12-22 Daryl Sharp Method and device for vacuum chromatography
WO1989009486A1 (en) * 1988-03-22 1989-10-05 Indiana University Foundation Isotope-ratio-monitoring gas chromatography-mass spectrometry apparatus and method
EP0519223A1 (de) * 1991-06-15 1992-12-23 Krupp VDM GmbH Gasdichte Verbindung zwischen Rohren kleinen Durchmessers sowie Verfahren und Anlage zu deren Herstellung
GB2270977A (en) * 1992-09-26 1994-03-30 Finnigan Mat Gmbh Interface between a gas chromatograph and mass spectrometer
EP0636882A1 (de) * 1993-07-30 1995-02-01 Microsensor Technology, Inc. Kapillarrohrverbindung
US5783741A (en) * 1997-01-31 1998-07-21 Atlantic Richfield Company Capillary furnace for improved peak resolution in gas isotope chromatography
DE19816348C1 (de) * 1998-04-02 1999-08-05 Ufz Leipzighalle Gmbh Pyrolysereaktor zur Pyrolyse organischer und anorganischer Proben, Elementaranalysator enthaltend diesen Pyrolysereaktor und Verfahren zur massenspektrometrischen on-line Bestimmung der Sauerstoffisotopenzusammensetzung organischer und anorganischer Proben

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1667324C3 (de) * 1966-11-24 1975-02-06 Friedrich Uhde Gmbh, 4600 Dortmund Röhrenspaltofen mit am unteren Ende mit Innenisolierung versehenen Reaktionsrohren
DE3045654C2 (de) * 1980-12-04 1985-03-28 Carlo Erba Strumentazione S.p.A., Rodano, Milano Vorrichtung zum Verbinden von pneumatischen und/oder hydraulischen Kreisen in der Trenntechnik
DE10100921A1 (de) * 2001-01-10 2002-07-11 Abb Research Ltd Trennsäule für die Untersuchung von Gasen
AU2002334887A1 (en) * 2001-10-05 2003-04-22 Vanderbilt University Capillary tube printing tips for microarray printing
DE102005027327A1 (de) * 2005-06-13 2007-01-04 Man Nutzfahrzeuge Aktiengesellschaft Verfahren zur Herstellung einer elektrischen Verbindungsstelle, sowie Verbindung zwischen einem elektrischen Leiter und einem metallischen Gehäuse sowie metallisches Gehäuse, bspw. ausgebildet an einem Kabelschuh

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2729359A1 (de) * 1976-07-19 1978-01-26 Perkin Elmer Corp Rohrverbindung fuer eine chromatographische saeule
DE2852495A1 (de) * 1978-12-05 1980-06-19 Karl Heinz Vahlbrauk Verfahren zum verbinden zweier rohrenden aus metall
US4713963A (en) * 1986-06-26 1987-12-22 Daryl Sharp Method and device for vacuum chromatography
WO1989009486A1 (en) * 1988-03-22 1989-10-05 Indiana University Foundation Isotope-ratio-monitoring gas chromatography-mass spectrometry apparatus and method
EP0519223A1 (de) * 1991-06-15 1992-12-23 Krupp VDM GmbH Gasdichte Verbindung zwischen Rohren kleinen Durchmessers sowie Verfahren und Anlage zu deren Herstellung
GB2270977A (en) * 1992-09-26 1994-03-30 Finnigan Mat Gmbh Interface between a gas chromatograph and mass spectrometer
EP0636882A1 (de) * 1993-07-30 1995-02-01 Microsensor Technology, Inc. Kapillarrohrverbindung
US5783741A (en) * 1997-01-31 1998-07-21 Atlantic Richfield Company Capillary furnace for improved peak resolution in gas isotope chromatography
DE19816348C1 (de) * 1998-04-02 1999-08-05 Ufz Leipzighalle Gmbh Pyrolysereaktor zur Pyrolyse organischer und anorganischer Proben, Elementaranalysator enthaltend diesen Pyrolysereaktor und Verfahren zur massenspektrometrischen on-line Bestimmung der Sauerstoffisotopenzusammensetzung organischer und anorganischer Proben

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
ANONYMOUS: "PROTECOL Unions", SGE PRODUCT DATA, May 2004 (2004-05-01), pages 1 - 2, XP002520306, Retrieved from the Internet <URL:www.sge.com> [retrieved on 20090320] *

Also Published As

Publication number Publication date
GB2463435B (en) 2011-10-26
US20100209302A1 (en) 2010-08-19
WO2009007079A2 (de) 2009-01-15
DE112008001721A5 (de) 2010-11-04
DE102007031678A1 (de) 2009-01-08
GB2463435A (en) 2010-03-17
GB201000957D0 (en) 2010-03-10

Similar Documents

Publication Publication Date Title
WO2006055314A3 (en) Reynolds number correction function for mass flow rate sensor
WO2009010690A3 (fr) Procede de purification d&#39;un gaz contenant du co2
HK1091165A1 (en) A process for joining ceramic components and monoliths produced thereof
NO20082280L (no) Gjennvinningssystem for viderebehandling av en krakkinggasstrom i et etylenanlegg
TW200632288A (en) Thermal mass flow rate sensor having fixed bypass ratio
EA200970976A1 (ru) Адсорбция за счет температурного перепада coиз топочного газа с использованием теплоты сжатия
ZA200802365B (en) Process and apparatus for the purification of methane rich gas streams
MX2008000527A (es) Membrana compuesta para la separacion de dioxido de carbono.
EP2260940B8 (de) Kohlenstoffhaltiger katalysator für die rauchgasentschwefelung, herstellungsverfahren dafür und verwendung davon zur entfernung von quecksilber aus abgas
WO2007094908A3 (en) Integrated gasification combined cycle with preheating of nitrogen / oxygen from air separator
WO2006084563A3 (de) Verfahren zur sauerstoffanreicherung in gasen, dafür geeignete anlagen sowie deren verwendung
PL2002877T3 (pl) Sposób oddzielania wodoru ze strumieni gazu za pomocą procesu adsorpcji pod zmiennym ciśnieniem
GB2467672A (en) Natural gas analyzer on a micro-chip
WO2006119298A3 (en) Method and apparatus for converting oxidized mercury into elemental mercury
EP2067814A4 (de) Fluorharzmembran, fuorharzverbundwerkstoff, poröser fluorharzverbundwerkstoff, herstellungsverfahren dafür und trennmembranelement
WO2009098452A3 (en) Conversion of ammonia into nitrogen and hydrogen
WO2008006787A3 (en) Process to prepare a synthesis gas
GB0916863D0 (en) Device for, and method of, separating condensate from respiratory gas.
MY159969A (en) Gas separation composite membrane, and gas separating module, gas separation apparatus and gas separation method using the same
DK2061113T3 (da) Brændselscellesystem og fremgangsmåde til dettes drift
WO2009007079A3 (de) Vorrichtung mit einer verbindung zweier kapillaren
WO2007036660A3 (fr) Procede de production d’un flux gazeux enrichi en hydrogene a partir de flux gazeux hydrogenes comprenant des hydrocarbures
WO2008134009A3 (en) Non-cryogenic nitrogen generators and methods of use
ZA200809049B (en) FGEPSC (flared, gas exhaust, pneumatic, saturation and condensation) process and system
CN203178242U (zh) 一种气相色谱仪氢火焰检测器喷嘴

Legal Events

Date Code Title Description
ENP Entry into the national phase

Ref document number: 1000957

Country of ref document: GB

Kind code of ref document: A

Free format text: PCT FILING DATE = 20080707

WWE Wipo information: entry into national phase

Ref document number: 1000957.9

Country of ref document: GB

REG Reference to national code

Ref country code: DE

Ref legal event code: 8642

WWE Wipo information: entry into national phase

Ref document number: 12668006

Country of ref document: US

121 Ep: the epo has been informed by wipo that ep was designated in this application

Ref document number: 08773890

Country of ref document: EP

Kind code of ref document: A2

REF Corresponds to

Ref document number: 112008001721

Country of ref document: DE

Date of ref document: 20101104

Kind code of ref document: P