WO2008117844A1 - アリールヒドロキシルアミンの製造法 - Google Patents

アリールヒドロキシルアミンの製造法 Download PDF

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Publication number
WO2008117844A1
WO2008117844A1 PCT/JP2008/055850 JP2008055850W WO2008117844A1 WO 2008117844 A1 WO2008117844 A1 WO 2008117844A1 JP 2008055850 W JP2008055850 W JP 2008055850W WO 2008117844 A1 WO2008117844 A1 WO 2008117844A1
Authority
WO
WIPO (PCT)
Prior art keywords
arylhydroxylamine
producing
compound
disclosed
coexistence
Prior art date
Application number
PCT/JP2008/055850
Other languages
English (en)
French (fr)
Inventor
Yasumasa Takenaka
Jun-Chul Choi
Toshiyasu Sakakura
Hiroyuki Yasuda
Takahiro Kiyosu
Original Assignee
Wako Pure Chemical Industries, Ltd.
National Institute Of Advanced Industrial Science And Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Wako Pure Chemical Industries, Ltd., National Institute Of Advanced Industrial Science And Technology filed Critical Wako Pure Chemical Industries, Ltd.
Priority to CN200880009961.1A priority Critical patent/CN101663265B/zh
Priority to US12/532,945 priority patent/US8455690B2/en
Priority to EP08739000A priority patent/EP2154125A4/en
Priority to JP2009506371A priority patent/JP5425619B2/ja
Publication of WO2008117844A1 publication Critical patent/WO2008117844A1/ja

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/1616—Coordination complexes, e.g. organometallic complexes, immobilised on an inorganic support, e.g. ship-in-a-bottle type catalysts
    • B01J31/1625—Coordination complexes, e.g. organometallic complexes, immobilised on an inorganic support, e.g. ship-in-a-bottle type catalysts immobilised by covalent linkages, i.e. pendant complexes with optional linking groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/1608—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes the ligands containing silicon
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C239/00—Compounds containing nitrogen-to-halogen bonds; Hydroxylamino compounds or ethers or esters thereof
    • C07C239/08—Hydroxylamino compounds or their ethers or esters
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C239/00—Compounds containing nitrogen-to-halogen bonds; Hydroxylamino compounds or ethers or esters thereof
    • C07C239/08—Hydroxylamino compounds or their ethers or esters
    • C07C239/10—Hydroxylamino compounds or their ethers or esters having nitrogen atoms of hydroxylamino groups further bound to carbon atoms of unsubstituted hydrocarbon radicals or of hydrocarbon radicals substituted by halogen atoms or by nitro or nitroso groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C239/00—Compounds containing nitrogen-to-halogen bonds; Hydroxylamino compounds or ethers or esters thereof
    • C07C239/08—Hydroxylamino compounds or their ethers or esters
    • C07C239/12—Hydroxylamino compounds or their ethers or esters having nitrogen atoms of hydroxylamino groups further bound to carbon atoms of hydrocarbon radicals substituted by singly-bound oxygen atoms
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2231/00—Catalytic reactions performed with catalysts classified in B01J31/00
    • B01J2231/60—Reduction reactions, e.g. hydrogenation
    • B01J2231/64—Reductions in general of organic substrates, e.g. hydride reductions or hydrogenations
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/80—Complexes comprising metals of Group VIII as the central metal
    • B01J2531/82—Metals of the platinum group
    • B01J2531/828—Platinum

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

課題 　穏和な条件下で、効率的且つ安全にアリールヒドロキシルアミン化合物を製造する方法を提供すること 解決手段 　本発明は、アミノ基配位シリカ担持白金触媒及び被毒剤の共存下、ニトロアリール化合物と水素源とを接触させることを特徴とする、アリールヒドロキシルアミン化合物の製造法、の発明である。
PCT/JP2008/055850 2007-03-27 2008-03-27 アリールヒドロキシルアミンの製造法 WO2008117844A1 (ja)

Priority Applications (4)

Application Number Priority Date Filing Date Title
CN200880009961.1A CN101663265B (zh) 2007-03-27 2008-03-27 芳基羟基胺的制造方法
US12/532,945 US8455690B2 (en) 2007-03-27 2008-03-27 Method for producing arylhydroxylamine
EP08739000A EP2154125A4 (en) 2007-03-27 2008-03-27 PROCESS FOR PRODUCTION OF ARYLHYDROXYLAMINE
JP2009506371A JP5425619B2 (ja) 2007-03-27 2008-03-27 アリールヒドロキシルアミンの製造法

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
JP2007-081040 2007-03-27
JP2007081040 2007-03-27
JP2007240585 2007-09-18
JP2007-240585 2007-09-18

Publications (1)

Publication Number Publication Date
WO2008117844A1 true WO2008117844A1 (ja) 2008-10-02

Family

ID=39788577

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2008/055850 WO2008117844A1 (ja) 2007-03-27 2008-03-27 アリールヒドロキシルアミンの製造法

Country Status (5)

Country Link
US (1) US8455690B2 (ja)
EP (1) EP2154125A4 (ja)
JP (1) JP5425619B2 (ja)
CN (1) CN101663265B (ja)
WO (1) WO2008117844A1 (ja)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010241691A (ja) * 2009-03-31 2010-10-28 National Institute Of Advanced Industrial Science & Technology 金属ナノ粒子担持ｍｃｍ−４１触媒を用いるニトロ化合物の水素還元方法
WO2022224741A1 (ja) * 2021-04-21 2022-10-27 千代田化工建設株式会社 水素化触媒ならびにこれを用いたフロー式有機合成システム及び水素化有機化合物の製造方法

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107759520A (zh) * 2016-08-17 2018-03-06 浙江中山化工集团股份有限公司 一种n‑羟基‑n‑2‑[（n‑对氯苯基）‑3‑吡唑氧基甲基]苯基羟胺的合成工艺
CN109503398B (zh) * 2018-12-19 2021-07-02 江苏智远科创科技有限公司 一种n-甲基-4-甲氧基苯胺的制备方法

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3694509A (en) 1970-04-16 1972-09-26 Engelhard Min & Chem Selective hydrogenation of nitroaromatics to the corresponding n-arylhydroxylamine
JPS5424837A (en) * 1977-07-28 1979-02-24 Showa Denko Kk Selective hyerogenation of aromatic nitro compound
JPS60139649A (ja) * 1983-12-06 1985-07-24 アクゾ・ナームローゼ・フエンノートシャツプ ヒドロキシルアミンの製造方法
WO1999028289A1 (de) 1997-12-02 1999-06-10 Consortium für elektrochemische Industrie GmbH Verfahren zur herstellung organischer hydroxylamine
WO2004072019A1 (ja) 2003-02-14 2004-08-26 Wako Pure Chemical Industries, Ltd. イオン交換樹脂固定化白金触媒を用いたヒドロキシルアミン化合物の製造方法

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4571437A (en) * 1982-01-29 1986-02-18 Mallinckrodt, Inc. Process for preparing p-aminophenol and alkyl substituted p-aminophenol
US5166435A (en) 1983-12-06 1992-11-24 Akzo N.V. Process for the preparation of a hydroxylamine
US4723030A (en) * 1985-08-05 1988-02-02 General Electric Company Moderated reduction reactions for producing arylhydroxylamines
FR2688001B1 (fr) * 1992-02-28 1994-05-20 Rhone Poulenc Chimie Procede de preparation de p-aminophenols.
DE19502700A1 (de) * 1995-01-28 1996-08-01 Basf Ag Verfahren zur Herstellung von N-Aryl- und N-Hetarylhydroxylaminen
DE19610571A1 (de) * 1996-03-18 1997-09-25 Basf Ag Verfahren und Zwischenprodukte zur Herstellung von Pyridyl-4-Fluoranilinen
US6028227A (en) * 1999-02-12 2000-02-22 Council Of Scientific & Industrial Research Single step process for the preparation of p-aminophenol

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3694509A (en) 1970-04-16 1972-09-26 Engelhard Min & Chem Selective hydrogenation of nitroaromatics to the corresponding n-arylhydroxylamine
JPS5424837A (en) * 1977-07-28 1979-02-24 Showa Denko Kk Selective hyerogenation of aromatic nitro compound
JPS60139649A (ja) * 1983-12-06 1985-07-24 アクゾ・ナームローゼ・フエンノートシャツプ ヒドロキシルアミンの製造方法
WO1999028289A1 (de) 1997-12-02 1999-06-10 Consortium für elektrochemische Industrie GmbH Verfahren zur herstellung organischer hydroxylamine
WO2004072019A1 (ja) 2003-02-14 2004-08-26 Wako Pure Chemical Industries, Ltd. イオン交換樹脂固定化白金触媒を用いたヒドロキシルアミン化合物の製造方法

Non-Patent Citations (8)

* Cited by examiner, † Cited by third party
Title
"Science", SCIENCE, vol. 279, 1998, pages 548 - 552
C. T. KRESGE, NATURE, vol. 359, 1992, pages 710
D. ZHAO, SCIENCE, vol. 279, 1998, pages 548
J. AM. CHEM. SOC., vol. 120, 1998, pages 6024 - 6036
JOURNAL OF ORGANOMETALLIC CHEMISTRY, vol. 689, 2004, pages 309 - 316
S. INAGAKI, J CHEM. SOC. CHEM. COMMUN., 1993, pages 680
SCIENCE, vol. 279, 1998, pages 548 - 552
See also references of EP2154125A4 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010241691A (ja) * 2009-03-31 2010-10-28 National Institute Of Advanced Industrial Science & Technology 金属ナノ粒子担持ｍｃｍ−４１触媒を用いるニトロ化合物の水素還元方法
WO2022224741A1 (ja) * 2021-04-21 2022-10-27 千代田化工建設株式会社 水素化触媒ならびにこれを用いたフロー式有機合成システム及び水素化有機化合物の製造方法

Also Published As

Publication number Publication date
CN101663265B (zh) 2016-06-08
EP2154125A4 (en) 2012-02-22
JPWO2008117844A1 (ja) 2010-07-15
US20100113830A1 (en) 2010-05-06
EP2154125A1 (en) 2010-02-17
CN101663265A (zh) 2010-03-03
JP5425619B2 (ja) 2014-02-26
US8455690B2 (en) 2013-06-04

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