WO2008035673A1 - Process for producing hollow fiber membrane module and apparatus therefor - Google Patents

Process for producing hollow fiber membrane module and apparatus therefor Download PDF

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Publication number
WO2008035673A1
WO2008035673A1 PCT/JP2007/068084 JP2007068084W WO2008035673A1 WO 2008035673 A1 WO2008035673 A1 WO 2008035673A1 JP 2007068084 W JP2007068084 W JP 2007068084W WO 2008035673 A1 WO2008035673 A1 WO 2008035673A1
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WO
WIPO (PCT)
Prior art keywords
hollow fiber
fiber membrane
bundle
cylindrical case
slippery sheet
Prior art date
Application number
PCT/JP2007/068084
Other languages
French (fr)
Japanese (ja)
Inventor
Masatsugu Uehara
Yasutaka Tanaka
Yoshihiko Oosawa
Original Assignee
Toray Industries, Inc.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Toray Industries, Inc. filed Critical Toray Industries, Inc.
Publication of WO2008035673A1 publication Critical patent/WO2008035673A1/en

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D63/00Apparatus in general for separation processes using semi-permeable membranes
    • B01D63/02Hollow fibre modules
    • B01D63/021Manufacturing thereof
    • B01D63/0233Manufacturing thereof forming the bundle
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D63/00Apparatus in general for separation processes using semi-permeable membranes
    • B01D63/02Hollow fibre modules
    • B01D63/025Bobbin units
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D63/00Apparatus in general for separation processes using semi-permeable membranes
    • B01D63/02Hollow fibre modules
    • B01D63/021Manufacturing thereof
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D63/00Apparatus in general for separation processes using semi-permeable membranes
    • B01D63/02Hollow fibre modules
    • B01D63/024Hollow fibre modules with a single potted end
    • B01D63/0241Hollow fibre modules with a single potted end being U-shaped
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D69/00Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
    • B01D69/08Hollow fibre membranes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2313/00Details relating to membrane modules or apparatus
    • B01D2313/23Specific membrane protectors, e.g. sleeves or screens
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2323/00Details relating to membrane preparation
    • B01D2323/42Details of membrane preparation apparatus

Definitions

  • the present invention relates to a method and apparatus for manufacturing a hollow fiber membrane module that enables automatic manufacture of a hollow fiber membrane module in which a hollow fiber membrane bundle is folded in a U shape and stored in a cylindrical case.
  • a water purifier attached to a faucet or the like of a water supply uses a hollow fiber membrane module in which a hollow fiber membrane is bent in a U shape and stored in a cylindrical case.
  • the filling rate of the hollow fiber bundle of the module can be increased, and as a result, it is configured to achieve a small size and high filtration performance.
  • the hollow fiber bundle filling rate represents the ratio of the cross-sectional area of the hollow fiber bundle to the cross-sectional area of the cylindrical case.
  • Patent Documents 1 and 2 disclose a method and an apparatus for automating the process of bending the hollow fiber membrane bundle described above into a U-shape and incorporating it into a cylindrical case. These documents disclose a configuration in which the work is completed by pushing into the cylindrical case as it is deformed into a U-shape by pushing near the center of the hollow fiber membrane bundle aligned in one direction.
  • any of the methods described in any of the documents has a problem that the pushing force acts on the bent portion of the hollow fiber membrane bundle. That is, when the hollow fiber bundle is bent into a U shape, a pressing force that resists the frictional force between the hollow fibers is required. When assembling, it is necessary to stake and push the frictional force generated between the hollow fiber membrane bundle and the inner wall of the cylindrical case. Such force is applied to the hollow fiber membrane bundle by the pushing member. Therefore, the pushing force acts on the bent portion of the hollow fiber membrane bundle. For this reason, there is a risk of damaging the hollow fiber membrane at the bent portion, causing defects such as thread breakage and thread crushing.
  • Patent Document 2 discloses that the use of a slippery sheet can be expected to reduce the frictional force when the hollow fiber membrane bundle is assembled in the cylindrical case. However, the hollow fiber bundle filling rate is disclosed. If it is high, it may not be effective enough!
  • Patent Document 3 discloses a method for housing a hollow fiber membrane bundle in a cylindrical case by vacuum suction as a method for housing a hollow fiber membrane bundle by the same inventors as Patent Document 1. In this method, not only the pushing force but also the bow I penetration force by suction is applied to the hollow fiber membrane bundle, but this method causes partial dropout of the hollow fiber by the same inventors in Patent Document 1. It has been clarified that there is a problem that the storage form becomes uneven.
  • Patent Document 1 Japanese Patent No. 3623856
  • Patent Document 2 Japanese Patent Laid-Open No. 2003-062435
  • Patent Document 3 Japanese Patent Laid-Open No. 2-241521
  • An object of the present invention is to produce a hollow fiber membrane module that reduces the degradation of the quality of the hollow fiber membrane and improves the productivity in the process of folding the hollow fiber membrane bundle into a U-shape and incorporating it in a cylindrical case. It is to provide a method and a manufacturing apparatus.
  • the present invention is characterized by the following configurations.
  • a method for producing a hollow fiber membrane module comprising housing the hollow fiber membrane bundle in the cylindrical case.
  • a device for manufacturing a hollow fiber membrane module in which a hollow fiber membrane bundle is bent and stored in a cylindrical case, and the hollow fiber membrane bundle is U-shaped toward the cylindrical case together with a slippery sheet. Pushing the hollow fiber membrane bundle and a part of the slippery sheet into the cylindrical case while bending it, and gripping part of the slippery sheet and pulling it into the tubular case Thread bundle pulling means for pulling the hollow fiber membrane bundle into the cylindrical case, and the pushing means pulls the slippery sheet of the yarn bundle pulling means.
  • the apparatus for manufacturing a hollow fiber membrane module is configured to move in the pull-in direction of the slippery sheet in synchronism with each other.
  • the push-in means has two flat plates, and one of the two flat plates moves in the pull-in direction in synchronization with the slipping-in sheet of the yarn bundle pull-in means.
  • the quality of the hollow fiber membrane is suppressed and the quality is excellent.
  • a hollow fiber membrane module can be obtained. As a result, productivity is also increased.
  • FIG. 1 shows an embodiment of a manufacturing apparatus of a hollow fiber membrane module of the present invention
  • is a schematic view seen from the front
  • (b) is seen from the direction A in FIG. It is a schematic diagram.
  • FIG. 2 is a perspective view showing the arrangement of a hollow fiber membrane bundle and a slippery sheet.
  • FIG. 3 is a schematic view showing a state in which the hollow fiber membrane bundle is bent into a U shape by the yarn bundle U-shaped means.
  • FIG. 4 is a schematic view showing a place where the yarn bundle drawing means grips the slippery sheet.
  • FIG. 5 is a schematic view showing a state in which a hollow fiber membrane bundle bent in a U shape is housed in a cylindrical case.
  • Fig. 6 is a schematic view showing an operation of extracting the slippery sheet remaining in the cylindrical case.
  • FIG. 1 is a schematic diagram showing an embodiment of a hollow fiber membrane module manufacturing apparatus, in which (a) is a schematic front view and (b) is a schematic side view.
  • the hollow fiber membrane module in the present embodiment is a so-called U-shaped hollow fiber membrane module, and the hollow fiber membrane bundle is folded in half in a U shape and filled into a cylindrical case. After that, both ends of the hollow fiber membrane bundle are configured by potting the resin into the opening of the cylindrical case.
  • the hollow fiber membrane bundle in the present embodiment is composed of a microporous membrane having filtration performance or the like, and is composed of, for example, a polysulfone resin.
  • the hollow fiber membrane bundle may be dry or wet.
  • a wet hollow fiber membrane bundle is preferable from the viewpoint of ease of handling, but it is necessary to perform a drying process in order to prevent poor adhesion in potting in a later step.
  • the drying process is not necessary, but the friction resistance between the hollow fibers and the yarn bundle and the cylindrical shape are compared to the wet state, where the hollow fibers are repelled by the static electricity and are difficult to handle.
  • the case has a high frictional resistance and tends to be difficult to fill.
  • the apparatus shown in FIG. 1 has a pair of freely rotating drum rollers (cylindrical rollers in which the outer diameters at both ends in the rotational axis direction are larger than the outer diameters at the central part) arranged at intervals.
  • 6 Yarn bundle with interior Yarn bundle forming means 3 having pushing means for reciprocating between the guide unit 8 and the pair of drum rollers 6 and the yarn bundle drawing arranged between the pair of drum rollers 6 and below.
  • the cylindrical case 2 is arranged between the yarn bundle drawing-in means 5 and the pair of drum-type rollers 6 during operation.
  • the yarn bundle guide unit 8 has a concave groove to the extent that the hollow fiber membrane bundle 1 can be laid down.
  • the use of the drum roller 6 can also suppress damage to the hollow fiber membrane when the hollow fiber membrane bundle described later is stored in the cylindrical case.
  • a hole through which the bent hollow fiber membrane bundle 1 can be passed to the cylindrical case 2 is provided at the center of the concave groove of the yarn bundle guide unit.
  • the yarn bundle U-shaped means 3 has a pushing member composed of two flat plates 3a and 3b, and the pushing member is disposed between the pair of drum-shaped rollers 6, that is, in a cylindrical shape arranged as described later. Case 2 is arranged to reciprocate in the longitudinal direction.
  • the pushing member can be reciprocated by a necessary amount by a driving means such as a Norse motor.
  • the push-in member may be a single plate-like member, but is preferably composed of two flat plates 3a and 3b as in this embodiment.
  • the flat plate 3a used only when the hollow fiber membrane bundle 1 is bent into a U-shape is bifurcated from the viewpoint of ease of guiding to the cylindrical case 2, and is a portion in contact with the hollow fiber. Is chamfered to the extent that it does not damage the hollow fiber.
  • the tip of the push-in member 3b that is also used when stored in the cylindrical case 2 may have a bifurcated shape like the push-in member 3a, but it is no longer restricted in the case in a direction perpendicular to the push-in direction. However, it is preferable that the corners of the bifurcated portions are flat because they are obstructive.
  • the yarn bundle drawing means 5 is arranged on the opposite side of the cylindrical case 2 from the yarn bundle U-shaped means 3, and a part of the slippery sheet 4 is placed inside the cylindrical case 2.
  • a sheet gripping mechanism 5a for gripping and a moving mechanism 5b for reciprocating in the longitudinal direction of the cylindrical case 2 are provided. After the hollow fiber membrane bundle 1 is bent by the pushing member, it is between the hollow fiber membrane bundle 1 and the cylindrical case 2 A part of the slippery sheet 4 is gripped in the cylindrical case 2, and the hollow fiber membrane bundle 1 is pulled into the tubular case 2 through the slippery sheet 4.
  • the yarn bundle pull-in means 5 easily and easily sucks air in advance from the viewpoint of reliably gripping a part of the slippery sheet 4 in the cylindrical case 2 and preventing operation stop trouble due to gripping failure. It is also preferable to provide means for cueing a part of the sliding sheet 4. Further, at the time of work, from the viewpoint of suppressing damage to the hollow fiber membrane bundle 1, it is also preferable to dispose a funnel-shaped guide guide 7 in the opening portion on the side of the yarn bundle U-shaped means 3 of the cylindrical case 2. It is possible to prevent a part of the hollow fiber membrane bundle 1 from pulling the end of the opening of the cylindrical case 2 and damaging the hollow fiber membrane.
  • the hollow fiber membranes loaded in the cylindrical case are easily arranged in a state where a plurality of hollow fiber membranes are aligned in one direction and cut to a predetermined length, that is, as a hollow fiber membrane bundle 1. It is arranged in the concave groove of the yarn bundle guide unit 8 together with the sliding sheet 4.
  • the slippery sheet 4 is not particularly limited as long as it has good slipperiness and has a certain tensile strength, but a resin film, a fabric, and the like are preferable.
  • a resin film such as polyethylene, polypropylene, or polyester preferably has a thickness in the range of 5-30111.
  • the supply method of the slippery sheet 4 is such that the slippery sheet 4 is finally disposed between the hollow fiber membrane bundle 1 and the cylindrical case 2, that is, the yarn bundle.
  • a predetermined length may be automatically cut out from a roll-like slippery sheet and placed on the yarn bundle guide unit 8 as long as it can be supplied between the guide unit 8 and the hollow fiber membrane bundle 1. It is preferable from the viewpoint of being able to supply the slippery sheet 4 continuously and efficiently! /.
  • the hollow fiber membrane bundle 1 can be supplied manually, there is no problem, but industrially, a conveyor, a robot or the like is automatically supplied onto the slippery sheet 4, and the yarn bundle guide is supplied. It is a preferred embodiment to set in the concave groove of the unit 8.
  • the central portion of the hollow fiber membrane bundle 1 is pushed in the direction of the cylindrical case 2 by the flat plates 3a and 3b which are pushing members of the yarn bundle U-shaped means 3, and the hollow The membrane bundle 1 is bent into a U shape with a slippery sheet 4.
  • a flat plate as a pushing member 3a and 3b are such that the hollow fiber membrane bundle 1 and the slippery sheet 4 are bent in a U-shape and part of the hollow fiber membrane bundle 1 and the slippery sheet 4 are pushed over the cylindrical case.
  • the sheet gripping mechanism 5a of the yarn bundle drawing means 5 is formed in a cylindrical shape from the opening on the opposite side to the side where the hollow fiber membrane bundle 1 is inserted in the cylindrical case 2. Grip a part of the slippery sheet 4 in the case and pull it into the cylindrical case 2. When a part of the slippery sheet is gripped and pulled into the cylindrical case, at the same time, one flat plate 3b of the pushing member is moved in the pulling direction of the slippery sheet.
  • tension is applied to the film held by the sheet holding mechanism 5a of the yarn bundle drawing means 5.
  • the sheet gripping mechanism 5a starts a pulling operation before the movement of the flat plate 3b starts (that is, after the slipping of the slippery sheet into the cylindrical case by the sheet gripping mechanism 5a starts, It is preferable to start the movement in the sliding sheet retracting direction). Also, from the same viewpoint, the speed at which the yarn bundle drawing means 5 draws the slippery sheet should be equal to or higher than the moving speed of the flat plate 3b (that is, higher than the moving speed of the flat plate 3b in the pulling direction of the slippery sheet). Is also preferable. If the push-in member is not composed of the two flat plates 3a and 3b but is composed of a single plate-like member, the pull-in operation of the sheet gripping mechanism 5a must be started before the movement of the plate-like member.
  • the speed at which the yarn bundle drawing means 5 pulls in the slippery sheet is equal to or higher than the moving speed of the plate-like member.
  • the other flat plate 3a of the pushing member is retracted from the cylindrical case 2 when the sheet gripping mechanism 5a of the yarn bundle drawing means 5 grips a part of the slippery sheet 4. In this way, the hollow fiber membrane bundle 1 bent in a U shape is stored in the cylindrical case 2 in a state of being wrapped in the slippery sheet 4.
  • the hollow fiber membrane bundle 1 and the slippery sheet 4 are pushed toward the cylindrical case 2 with a pressing member. 3 ⁇ 4 After pushing part of the hollow fiber membrane bundle 1 and the slippery sheet 4 into the cylindrical case 2 Then, grip a part of the slippery sheet 4 and pull it into the cylindrical case 2. In this way, the hollow fiber membrane bundle 1 is drawn into the cylindrical case 2. At this time, in order to assist the movement of the hollow fiber membrane bundle, the pushing member is moved in the drawing direction of the slippery sheet simultaneously with the pulling of the slippery sheet 4.
  • the force required to store the hollow fiber membrane bundle 1 in the cylindrical case 2 is generated by the pulling action that basically acts on the yarn bundle via the sheet, and at the same time, the push-in operation is performed. It is set as the structure which assists by the movement by a member.
  • the bending portion of the hollow fiber membrane bundle is not damaged, but if the sheet slips between the hollow fiber membrane bundle or the sheet falls out of the gripping mechanism 5a, the desired position is obtained. The hollow fiber membrane bundle can no longer be drawn.
  • the hollow fiber membrane bundle can be moved to the desired position, but the hollow fiber membrane bundle is moved only by the pushing force applied to the bent portion of the hollow fiber membrane bundle.
  • the force required to store the hollow fiber membrane bundle 1 in the cylindrical case 2 is generated by a pulling action that basically acts on the yarn bundle via the sheet, and at the same time, the pushing portion It is configured to assist by movement with materials.
  • the hollow fiber membrane bundle can be reliably moved to a desired position, and the pushing force applied by the pushing member 3b of the yarn bundle U-shaped means 3 to the bent portion of the hollow fiber membrane bundle 1 can be reduced. Therefore, it is possible to prevent damage such as thread crushing.
  • the thread bundle retracting means 5 retracts the slippery sheet. It is also preferable to set the speed to be higher than the moving speed of the flat plate 3b (that is, higher than the moving speed of the flat plate 3b in the slipping direction of the slippery sheet)!
  • the pushing member may be a single plate-like member as described above, but the significance of the two flat plates 3a and 3b will be described as follows.
  • the contact of the hollow fiber membrane bundle 1 is not limited to chamfering the end face of the pushing member in order to prevent damage such as yarn crushing at the bent portion. It is preferable to reduce the pressure acting on the surface. Therefore, it is preferable to secure a certain pushing area of the pushing member.
  • the hollow fiber membrane bundle is stored in the case, when the pushing member enters the cylindrical case 2, the volume occupied by the hollow fiber membrane bundle 1 in the cylindrical case 2 is reduced by the volume of the pushing member. For this reason, the hollow fiber membrane bundle 1 is pushed to the inner wall of the cylindrical case, and damage such as deformation and thread crushing is likely to occur.
  • the slippery sheet 4 can be expected to have a slippery effect. S For products with a high filling rate, the risk of damage is particularly high. Yes.
  • the thickness of the pushing member is thicker. In order to satisfy the latter requirement, it is preferable that the thickness is thinner. Therefore, the push-in member of the yarn bundle U-shaped means 3 is composed of two flat plates 3a and 3b, and when they are bent into a U shape, the two members act simultaneously to ensure a contact area with the hollow fiber membrane bundle 1. However, when the hollow fiber membrane bundle is accommodated in the cylindrical case, it is preferable that only one sheet acts.
  • the hollow fiber membrane a polysulfone-based hollow fiber membrane having an outer diameter of 0.45 mm was used, and a hollow fiber membrane bundle 1 was obtained by bundling 700 pieces and cutting them to a length of 200 mm.
  • the slippery sheet 4 was configured such that a length of 120 mm was cut out from a polyethylene sheet wound into a roll having a width of 120 mm and a thickness of 0.01 mm and supplied onto the yarn bundle guide unit 8.
  • the hollow fiber membrane bundle 1 is supplied from the previous process by the conveyor, and is inserted into the concave groove of the yarn bundle guide unit 8 by the robot node. It was configured to be transferred.
  • the cylindrical case 2 is made of acrylic styrene having an inner diameter of 26 mm and a length of 70 mm.
  • the cylindrical case 2 is supplied from the case supply conveyor almost simultaneously with the supply of the hollow fiber membrane bundle 1. It was configured to be set below.
  • the flat plates 3a and 3b of the yarn bundle U-shaped means 3 were coated with a fluororesin coating in consideration of the detachability from the hollow fiber membrane, and both thicknesses were 2 mm.
  • a uniaxial actuator manufactured by Nippon Bearing Co., Ltd. was used for the vertical movement of the flat plates 3a and 3b. Set to operate at a low speed (100mm / sec) to prevent damage when the flat plate operates while contacting the yarn bundle, and at a high speed (500mm / sec) to reduce the processing tact in other cases did.
  • the sheet gripping mechanism 5a is configured such that a slip for gripping the slippery sheet 4 is mounted on an air chuck manufactured by SMC Co., Ltd., and the moving mechanism 5b is A 1-axis actuator manufactured by Ning Co., Ltd. was used. Pulling the slippery sheet 4 into the cylindrical case 2 During operation, it was set to operate at a low speed to prevent damage to the hollow fiber, and at other times it was set to operate at a high speed to shorten the processing tart. . In other words, it was set to operate at a speed of 100 mm / second during sheet pull-in operation, and at a speed of 500 mm / second during other operations. Furthermore, the flat plate 3b was set to start moving 0.1 second after the start of the sheet drawing operation of the yarn bundle drawing means 5.
  • Example 1 is the same as Example 1 except that the yarn bundle drawing means 5 is not used.
  • the hollow fiber membrane bundle 1 was accommodated in the cylindrical case 2 to obtain a hollow fiber membrane module.
  • a visual appearance inspection was performed on the hollow fiber membrane module obtained in this comparative example, the hollow fiber was broken inside the bent part of the hollow fiber membrane bundle, and the hollow fiber was broken. Many broken defects were seen.
  • leak tests were performed on 100 hollow fiber membrane modules created in this comparative example, 6 leak-outs occurred.
  • the hollow fiber membrane module leaked out was disassembled and inspected, it was found that the thread was broken or cracked at the site that was a defect in the appearance inspection.
  • the present invention can also be suitably used in the production of a medical hollow fiber membrane module that is used only for water purification.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)

Abstract

A process for producing a hollow fiber membrane module through inflecting of hollow fiber membrane bundle and placing of the same in a tubular case, characterized in that while by a pusher member, while inflecting the hollow fiber membrane bundle and an easily slidable sheet disposed in advance between the tubular case and the hollow fiber membrane bundle in U-form toward the tubular case, portions of the easily slidable sheet and the hollow fiber membrane bundle are pressed in the tubular case, and that thereafter the portion of the easily slidable sheet is grasped and drawn into the tubular case and simultaneously the pusher member is shifted toward the in-draw direction of the easily slidable sheet to thereby accomplish placing of the hollow fiber membrane bundle in the tubular case.

Description

明 細 書  Specification
中空糸膜モジュールの製造方法および製造装置  Method and apparatus for manufacturing hollow fiber membrane module
技術分野  Technical field
[0001] 本発明は、中空糸膜束を U字状に折り曲げた状態で筒状ケースに収納した中空糸 膜モジュールの自動製作を可能にする中空糸膜モジュールの製造方法および製造 装置に関する。  TECHNICAL FIELD [0001] The present invention relates to a method and apparatus for manufacturing a hollow fiber membrane module that enables automatic manufacture of a hollow fiber membrane module in which a hollow fiber membrane bundle is folded in a U shape and stored in a cylindrical case.
背景技術  Background art
[0002] 水道の蛇口等に取り付けられる浄水器には、中空糸膜を U字状に折り曲げて筒状 ケースに収納した中空糸膜モジュールが使用されている。中空糸を U字状に折り曲 げることにより、モジュールの中空糸束充填率を高めることができ、結果として小型か つ高濾過性能を実現できるように構成されている。ここで、中空糸束充填率とは、筒 状ケース断面積に占める中空糸束断面積の割合のことを表す。  A water purifier attached to a faucet or the like of a water supply uses a hollow fiber membrane module in which a hollow fiber membrane is bent in a U shape and stored in a cylindrical case. By bending the hollow fiber into a U shape, the filling rate of the hollow fiber bundle of the module can be increased, and as a result, it is configured to achieve a small size and high filtration performance. Here, the hollow fiber bundle filling rate represents the ratio of the cross-sectional area of the hollow fiber bundle to the cross-sectional area of the cylindrical case.
[0003] 従来、上記のような中空糸膜束を U字状に折り曲げて筒状ケースに組み込む工程 は、手作業で行われていた。熟練した作業者は作業効率、製品完成度も一定レベル をクリアできたが、習熟度の浅い作業者等は損傷しやすい中空糸を极うため、歩留ま りがなかなか上がらないという状況であった。また、 U字状に折り曲げる作業とケース に組み込む工程が別々となっていたり、一旦、 U字状に折り曲げた状態を保持する ために不織布等を巻き付けておき、ケース組込後に抜き取るといった煩雑な作業が 必要であり、生産性向上を困難としていた。  [0003] Conventionally, the process of bending a hollow fiber membrane bundle as described above into a U-shape and incorporating it into a cylindrical case has been performed manually. Skilled workers could achieve a certain level of work efficiency and product perfection, but workers with a low level of proficiency could not easily increase the yield because they had hollow fibers that were easily damaged. It was. In addition, the work of folding into a U-shape and the process of incorporating it into the case are separate, or a complicated work such as wrapping a non-woven fabric etc. once to fold the U-shape and pulling it out after assembling the case Therefore, it was difficult to improve productivity.
[0004] 上述の中空糸膜束を U字状に折り曲げて筒状ケースに組み込む工程を自動化す る方法および装置が特許文献 1および 2に開示されている。これらの文献には、一方 向に引き揃えた中空糸膜束の中央部付近を押し込むことで U字状に変形させると共 に、そのまま筒状ケースに押し込む動作により作業が完了する構成が開示されてい  [0004] Patent Documents 1 and 2 disclose a method and an apparatus for automating the process of bending the hollow fiber membrane bundle described above into a U-shape and incorporating it into a cylindrical case. These documents disclose a configuration in which the work is completed by pushing into the cylindrical case as it is deformed into a U-shape by pushing near the center of the hollow fiber membrane bundle aligned in one direction. Have
[0005] しかしながら、いずれの文献に記載の方法も、押し込み力が中空糸膜束の屈曲部 分に集中して作用するという問題がある。すなわち、中空糸束を U字状に折り曲げる 際には、中空糸どうしの摩擦力に抗する押し込み力が必要であり、筒状ケースへの 組込の際には、中空糸膜束と筒状ケース内壁との間に生ずる摩擦力に杭して押し込 む必要があるが、そのような力を押し込み部材で中空糸膜束に付与するため、押し 込み力が中空糸膜束の屈曲部分に集中して作用する。そのため、屈曲部分の中空 糸膜を損傷する恐れがあり、糸切れや糸潰れ等の欠陥が発生する原因となる問題が ある。特許文献 2には、易滑性シートを用いることで、中空糸膜束を筒状ケースに組 み込む際の摩擦力を低減させる効果が期待できることが開示されているが、中空糸 束充填率が高レ、場合には十分な効果を奏さな!/、恐れがある。 [0005] However, any of the methods described in any of the documents has a problem that the pushing force acts on the bent portion of the hollow fiber membrane bundle. That is, when the hollow fiber bundle is bent into a U shape, a pressing force that resists the frictional force between the hollow fibers is required. When assembling, it is necessary to stake and push the frictional force generated between the hollow fiber membrane bundle and the inner wall of the cylindrical case. Such force is applied to the hollow fiber membrane bundle by the pushing member. Therefore, the pushing force acts on the bent portion of the hollow fiber membrane bundle. For this reason, there is a risk of damaging the hollow fiber membrane at the bent portion, causing defects such as thread breakage and thread crushing. Patent Document 2 discloses that the use of a slippery sheet can be expected to reduce the frictional force when the hollow fiber membrane bundle is assembled in the cylindrical case. However, the hollow fiber bundle filling rate is disclosed. If it is high, it may not be effective enough!
[0006] また、特許文献 3には、特許文献 1と同一発明者らにより中空糸膜束のケース収納 方法として、真空吸引によって筒状ケースへ収納させる方法が開示されている。中空 糸膜束に押し込み力だけでなく、吸引による弓 Iき込み力を作用させる方法であるが、 この方法については、特許文献 1で同一発明者等により、中空糸の部分的な脱落が 生じたり、収納形態が不揃いになったりする問題があることが明らかにされている。 特許文献 1:特許第 3623856号公報 [0006] Further, Patent Document 3 discloses a method for housing a hollow fiber membrane bundle in a cylindrical case by vacuum suction as a method for housing a hollow fiber membrane bundle by the same inventors as Patent Document 1. In this method, not only the pushing force but also the bow I penetration force by suction is applied to the hollow fiber membrane bundle, but this method causes partial dropout of the hollow fiber by the same inventors in Patent Document 1. It has been clarified that there is a problem that the storage form becomes uneven. Patent Document 1: Japanese Patent No. 3623856
特許文献 2:特開 2003— 062435号公報  Patent Document 2: Japanese Patent Laid-Open No. 2003-062435
特許文献 3:特開平 2— 241521号公報  Patent Document 3: Japanese Patent Laid-Open No. 2-241521
発明の開示  Disclosure of the invention
発明が解決しょうとする課題  Problems to be solved by the invention
[0007] 本発明の目的は、中空糸膜束を U字状に折り曲げて筒状ケースに組み込む工程 における中空糸膜の品位低下を低減し、かつ生産性を向上させる中空糸膜モジユー ルの製造方法および製造装置を提供することにある。 [0007] An object of the present invention is to produce a hollow fiber membrane module that reduces the degradation of the quality of the hollow fiber membrane and improves the productivity in the process of folding the hollow fiber membrane bundle into a U-shape and incorporating it in a cylindrical case. It is to provide a method and a manufacturing apparatus.
課題を解決するための手段  Means for solving the problem
[0008] 上記目的を達成するための本発明は以下の構成を特徴とするものである。 In order to achieve the above object, the present invention is characterized by the following configurations.
(1)中空糸膜束を屈曲させて筒状ケースに収納する中空糸膜モジュールの製造方 法であって、前記中空糸膜束ならびに前記筒状ケースと前記中空糸膜束との間に予 め配置された易滑性シートを押し込み部材で前記筒状ケースに向けて U字状に屈曲 させながら前記中空糸膜束および前記易滑性シートの一部を前記筒状ケースに押し 込み、その後、前記易滑性シートの一部を把持して前記筒状ケース内へ引き込むと 同時に前記押し込み部材を前記易滑性シートの引き込み方向に移動させ、前記中 空糸膜束を前記筒状ケース内へ収納することを特徴とする中空糸膜モジュールの製 造方法。 (1) A method of manufacturing a hollow fiber membrane module in which a hollow fiber membrane bundle is bent and stored in a cylindrical case, wherein the hollow fiber membrane bundle and the tubular case and the hollow fiber membrane bundle are The hollow fiber membrane bundle and a part of the slippery sheet are pushed into the tubular case while the slippery sheet disposed in the direction is bent in a U shape toward the tubular case by a pushing member, and then And gripping a part of the slippery sheet and pulling it into the cylindrical case, and simultaneously moving the pushing member in the pulling direction of the slippery sheet, A method of manufacturing a hollow fiber membrane module, comprising storing a hollow fiber membrane bundle in the cylindrical case.
(2)中空糸膜束を屈曲させて筒状ケースに収納する中空糸膜モジュールの製造方 法であって、前記中空糸膜束ならびに前記筒状ケースと前記中空糸膜束との間に予 め配置された易滑性シートを 2枚の平板を有する押し込み部材で前記筒状ケースに 向けて U字状に屈曲させながら前記中空糸膜束および前記易滑性シートの一部を 前記筒状ケースに押し込み、その後、前記易滑性シートの一部を把持して前記筒状 ケース内へ引き込むと同時に前記 2枚の平板のうちの 1枚を前記易滑性シートの引き 込み方向に移動させ、前記中空糸膜束を前記筒状ケース内へ収納することを特徴と する中空糸膜モジュールの製造方法。  (2) A method of manufacturing a hollow fiber membrane module in which a hollow fiber membrane bundle is bent and stored in a cylindrical case, wherein the hollow fiber membrane bundle and the tubular case and the hollow fiber membrane bundle are The hollow fiber membrane bundle and a part of the slippery sheet are placed in the tubular shape while bending the slippery sheet arranged in a U shape toward the tubular case with a pushing member having two flat plates. After pushing into the case, a part of the slippery sheet is gripped and pulled into the cylindrical case, and at the same time, one of the two flat plates is moved in the pulling direction of the slippery sheet. A method for producing a hollow fiber membrane module, comprising housing the hollow fiber membrane bundle in the cylindrical case.
(3)前記易滑性シートの一部を把持して前記筒状ケース内へ引き込むと同時に前記 押し込み部材または前記 2枚の平板のうちの前記 1枚を前記易滑性シートの前記弓 I き込み方向に移動させるに際しては、前記易滑性シートの前記筒状ケース内への引 き込み開始以後に、前記押し込み部材または前記 2枚の平板のうちの前記 1枚の、 前記易滑性シートの前記引き込み方向への移動を開始する、前記(1)または(2)記 載の中空糸膜モジュールの製造方法。  (3) A part of the slippery sheet is gripped and pulled into the cylindrical case, and at the same time, the pushing member or the one of the two flat plates is attached to the bow I of the slippery sheet. When the slippery sheet is moved, the slippery sheet or the one of the two flat plates, after the start of pulling of the slippery sheet into the cylindrical case, The manufacturing method of the hollow fiber membrane module according to (1) or (2), wherein the movement in the pull-in direction is started.
(4)前記易滑性シートの一部を把持して前記筒状ケース内へ引き込むと同時に前記 押し込み部材または前記 2枚の平板のうちの前記 1枚を前記易滑性シートの引き込 み方向に移動させるに際しては、前記易滑性シートの引き込みスピードを、前記押し 込み部材または前記 2枚の平板のうちの 1枚の前記易滑性シートの前記引き込み方 向への移動スピード以上にする、前記(1)〜(3)の!/、ずれか記載の中空糸膜モジュ ールの製造方法。  (4) A part of the slippery sheet is gripped and pulled into the cylindrical case, and at the same time, the pushing member or the one of the two flat plates is pulled in the slipping direction of the slippery sheet. When moving the slippery sheet, the pulling speed of the slippery sheet is set to be equal to or higher than the moving speed of the one slippery sheet of the push-in member or the two flat plates in the pulling direction. The method for producing a hollow fiber membrane module according to any one of! /, (1) to (3).
(5)中空糸膜束を屈曲させて筒状ケースに収納する中空糸膜モジュールの製造装 置であって、前記中空糸膜束を易滑性シートと共に前記筒状ケースに向けて U字状 に屈曲させながら前記中空糸膜束および前記易滑性シートの一部を前記筒状ケー スに押し込む押し込み手段と、前記易滑性シートの一部を把持して前記筒状ケース 内へ引き込むことで前記中空糸膜束を前記筒状ケース内へ引き込む糸束引き込み 手段とを備え、前記押し込み手段が、前記糸束引き込み手段の易滑性シート引き込 み時に同期して前記易滑性シートの引き込み方向に移動するように構成されている ことを特徴とする中空糸膜モジュールの製造装置。 (5) A device for manufacturing a hollow fiber membrane module in which a hollow fiber membrane bundle is bent and stored in a cylindrical case, and the hollow fiber membrane bundle is U-shaped toward the cylindrical case together with a slippery sheet. Pushing the hollow fiber membrane bundle and a part of the slippery sheet into the cylindrical case while bending it, and gripping part of the slippery sheet and pulling it into the tubular case Thread bundle pulling means for pulling the hollow fiber membrane bundle into the cylindrical case, and the pushing means pulls the slippery sheet of the yarn bundle pulling means. The apparatus for manufacturing a hollow fiber membrane module is configured to move in the pull-in direction of the slippery sheet in synchronism with each other.
(6)前記押し込み手段は 2枚の平板を有し、該 2枚の平板のうちの 1枚が、前記糸束 引き込み手段の易滑性シート引き込み時に同期して前記引き込み方向に移動する、 前記(5)記載の中空糸膜モジュールの製造装置。  (6) The push-in means has two flat plates, and one of the two flat plates moves in the pull-in direction in synchronization with the slipping-in sheet of the yarn bundle pull-in means. (5) The apparatus for producing a hollow fiber membrane module according to (5).
(7)前記 2枚の平板のうち 1枚の平板のみが先端部に二股部を有し、二股部を備え ていない平板が、易滑性シート引き込み時に同期して前記引き込み方向に移動する 、前記(6)記載の中空糸膜モジュールの製造装置。  (7) Of the two flat plates, only one flat plate has a bifurcated portion at the tip, and the flat plate not having the bifurcated portion moves in the retracting direction in synchronization with the slipping of the slippery sheet. The apparatus for producing a hollow fiber membrane module according to (6) above.
発明の効果  The invention's effect
[0009] 本発明によれば、以下に説明するとおり、中空糸膜束を U字状に折り曲げて筒状ケ ースに組み込む工程において、中空糸膜の品位低下を抑制し、品位に優れた中空 糸膜モジュールを得ることができる。また、その結果、生産性も高まる。  [0009] According to the present invention, as described below, in the process of folding a hollow fiber membrane bundle into a U-shape and incorporating it into a cylindrical case, the quality of the hollow fiber membrane is suppressed and the quality is excellent. A hollow fiber membrane module can be obtained. As a result, productivity is also increased.
図面の簡単な説明  Brief Description of Drawings
[0010] [図 1]本発明の中空糸膜モジュールの製造装置の一実施形態を示し、 ωは正面か ら見た模式図であり、 (b)は(a)図における A方向から見た模式図である。  FIG. 1 shows an embodiment of a manufacturing apparatus of a hollow fiber membrane module of the present invention, ω is a schematic view seen from the front, and (b) is seen from the direction A in FIG. It is a schematic diagram.
[図 2]中空糸膜束と易滑性シートの配置を示す斜視図である。  FIG. 2 is a perspective view showing the arrangement of a hollow fiber membrane bundle and a slippery sheet.
[図 3]糸束 U字化手段により中空糸膜束が U字状に屈曲した状態を示す概略図であ  FIG. 3 is a schematic view showing a state in which the hollow fiber membrane bundle is bent into a U shape by the yarn bundle U-shaped means.
[図 4]糸束引き込み手段が易滑性シートを把持するところを示す概略図である。 FIG. 4 is a schematic view showing a place where the yarn bundle drawing means grips the slippery sheet.
[図 5]U字状に屈曲した中空糸膜束が筒状ケースに収納された状態を示す概略図で ある。  FIG. 5 is a schematic view showing a state in which a hollow fiber membrane bundle bent in a U shape is housed in a cylindrical case.
[図 6]筒状ケース内に残る易滑性シートを抜き取る動作を示す概略図である。  [Fig. 6] Fig. 6 is a schematic view showing an operation of extracting the slippery sheet remaining in the cylindrical case.
符号の説明  Explanation of symbols
[0011] 1 中空糸膜束 [0011] 1 Hollow fiber membrane bundle
2 筒状ケース  2 Tubular case
3 糸束 U字化手段  3 Thread bundle U-shaped means
3a 平板(二股部あり)  3a Flat plate (with bifurcated part)
3b 平板(二股部なし) 4 易滑性シート 3b Flat plate (without bifurcated part) 4 Slippery sheet
5 糸束引き込み手段  5 Thread bundle pull-in means
5a シート把持機構  5a Sheet gripping mechanism
5b 移動機構  5b Movement mechanism
6 鼓型ローラ  6 drum roller
7 案内ガイド  7 Guide
8 糸束ガイドユニット  8 Yarn bundle guide unit
9 糸束固定用エアチャック  9 Thread bundle fixing air chuck
10 シート抜き取り用エアチャック  10 Air chuck for sheet removal
11 シート抜き取り用エアシリンダー  11 Air cylinder for sheet removal
発明を実施するための最良の形態  BEST MODE FOR CARRYING OUT THE INVENTION
[0012] 以下、本発明の最良の実施形態の例を、図面を参照しながら説明する。図 1は、中 空糸膜モジュール製造装置の一実施形態を示す模式図であり、 (a)が正面模式図 で、(b)が側面模式図である。 Hereinafter, an example of the best embodiment of the present invention will be described with reference to the drawings. FIG. 1 is a schematic diagram showing an embodiment of a hollow fiber membrane module manufacturing apparatus, in which (a) is a schematic front view and (b) is a schematic side view.
[0013] なお、本実施形態における中空糸膜モジュールは、いわゆる U字型中空糸膜モジ ユールと言われるもので、中空糸膜束を U字状に二つ折りにして筒状ケースに充填し た後、中空糸膜束の両端部を筒状ケースの開口部に樹脂等によりポッティング処理 することで構成される。 [0013] The hollow fiber membrane module in the present embodiment is a so-called U-shaped hollow fiber membrane module, and the hollow fiber membrane bundle is folded in half in a U shape and filled into a cylindrical case. After that, both ends of the hollow fiber membrane bundle are configured by potting the resin into the opening of the cylindrical case.
[0014] また、本実施形態における中空糸膜束は、濾過性能を有する微多孔膜などから構 成されており、例えばポリスルホン系樹脂などから構成されている。中空糸膜束は乾 燥状態であっても湿潤状態であってもよレ、。筒状ケースに充填されるためには湿潤 状態の中空糸膜束が取り扱いやすさの点で好ましいが、後工程のポッティングにお ける接着不良を防止するために乾燥処理を施す必要がある。乾燥状態の場合は、乾 燥処理が不要であるが、静電気を帯びて中空糸どうしが反発してまとまらず扱いにく ぐ湿潤状態に比べて、中空糸どうしの摩擦抵抗や糸束と筒状ケースの摩擦抵抗が 大きく充填しにくい傾向がある。  [0014] Further, the hollow fiber membrane bundle in the present embodiment is composed of a microporous membrane having filtration performance or the like, and is composed of, for example, a polysulfone resin. The hollow fiber membrane bundle may be dry or wet. In order to fill a cylindrical case, a wet hollow fiber membrane bundle is preferable from the viewpoint of ease of handling, but it is necessary to perform a drying process in order to prevent poor adhesion in potting in a later step. In the dry state, the drying process is not necessary, but the friction resistance between the hollow fibers and the yarn bundle and the cylindrical shape are compared to the wet state, where the hollow fibers are repelled by the static electricity and are difficult to handle. The case has a high frictional resistance and tends to be difficult to fill.
[0015] 図 1に示す装置は、間隔をおいて配置された自由回転する一対の鼓型ローラ(回 転軸方向両端部の外径が中央部の外径よりも大きい筒状のローラ) 6を内装した糸束 ガイドユニット 8と、その一対の鼓型ローラ 6の間を往復動する押し込み手段を備えた 糸束 U字化手段 3と、一対の鼓型ローラ 6の間でかつ下方に配置された糸束引き込 み手段 5とを備えており、作業時には、糸束引き込み手段 5と一対の鼓型ローラ 6との 間に筒状ケース 2が配置される。 The apparatus shown in FIG. 1 has a pair of freely rotating drum rollers (cylindrical rollers in which the outer diameters at both ends in the rotational axis direction are larger than the outer diameters at the central part) arranged at intervals. 6 Yarn bundle with interior Yarn bundle forming means 3 having pushing means for reciprocating between the guide unit 8 and the pair of drum rollers 6 and the yarn bundle drawing arranged between the pair of drum rollers 6 and below. The cylindrical case 2 is arranged between the yarn bundle drawing-in means 5 and the pair of drum-type rollers 6 during operation.
[0016] 糸束ガイドユニット 8は、中空糸膜束 1を横たえることができる程度の凹状溝を有し ている。鼓型ローラ 6の使用は、後述する中空糸膜束の筒型ケース収納時における 中空糸膜損傷をも抑制することができる。該糸束ガイドユニットの凹状溝の中央部に は屈曲させた中空糸膜束 1を筒状ケース 2へと通過させることができる穴が設けられ ている。 [0016] The yarn bundle guide unit 8 has a concave groove to the extent that the hollow fiber membrane bundle 1 can be laid down. The use of the drum roller 6 can also suppress damage to the hollow fiber membrane when the hollow fiber membrane bundle described later is stored in the cylindrical case. A hole through which the bent hollow fiber membrane bundle 1 can be passed to the cylindrical case 2 is provided at the center of the concave groove of the yarn bundle guide unit.
[0017] 糸束 U字化手段 3は 2枚の平板 3a、 3bからなる押し込み部材を有し、押し込み部材 がー対の鼓型ローラ 6の間、すなわち、後述するように配置される筒状ケース 2の長 手方向に往復動するように配設されている。押し込み部材は、ノ ルスモータ等の駆 動手段によって必要量だけ往復動できる構成となっている。  [0017] The yarn bundle U-shaped means 3 has a pushing member composed of two flat plates 3a and 3b, and the pushing member is disposed between the pair of drum-shaped rollers 6, that is, in a cylindrical shape arranged as described later. Case 2 is arranged to reciprocate in the longitudinal direction. The pushing member can be reciprocated by a necessary amount by a driving means such as a Norse motor.
[0018] 押し込み部材は一枚の板状の部材としてもよいが、本実施形態のように 2枚の平板 3a、 3bから構成することが好ましい。その結果、中空糸膜束 1を U字状に屈曲させる 時には二枚の押し込み部材を用い、中空糸膜を実際に筒状ケース 2へ引き込む時 には二枚のうちの一枚をガイドとして糸束引き込み手段 5に同期させて移動させるこ と力 Sできる。  [0018] The push-in member may be a single plate-like member, but is preferably composed of two flat plates 3a and 3b as in this embodiment. As a result, when pushing the hollow fiber membrane bundle 1 into a U shape, two pushing members are used, and when the hollow fiber membrane is actually pulled into the cylindrical case 2, one of the two pieces is used as a guide. The force S can be moved in synchronization with the bundle pull-in means 5.
[0019] そして、中空糸膜束 1を U字状に屈曲させる時にのみ用いる平板 3aは、筒状ケース 2への案内しやすさの点から二股形状になっており、中空糸に接触する部分は中空 糸を損傷しない程度に面取りされている。また、筒状ケース 2へ収納する時にも用い る押し込み部材 3bの先端部は、押し込み部材 3aのように二股形状になっていても良 いが、ケース内ではもはや押し込み方向と直交する方向へ規制する必要はなぐむし ろ二股部の角部は邪魔になるので、平坦になっていることが好ましい。  [0019] The flat plate 3a used only when the hollow fiber membrane bundle 1 is bent into a U-shape is bifurcated from the viewpoint of ease of guiding to the cylindrical case 2, and is a portion in contact with the hollow fiber. Is chamfered to the extent that it does not damage the hollow fiber. The tip of the push-in member 3b that is also used when stored in the cylindrical case 2 may have a bifurcated shape like the push-in member 3a, but it is no longer restricted in the case in a direction perpendicular to the push-in direction. However, it is preferable that the corners of the bifurcated portions are flat because they are obstructive.
[0020] 糸束引き込み手段 5は、筒状ケース 2に対して糸束 U字化手段 3と反対側に配設さ れており、筒状ケース 2内で易滑性シート 4の一部を把持するシート把持機構 5aと、 筒状ケース 2の長手方向に往復動する移動機構 5bなどを備えている。中空糸膜束 1 が前記押し込み部材により屈曲された後、中空糸膜束 1と筒状ケース 2との間にある 易滑性シート 4の一部を筒状ケース 2内で把持し、易滑性シート 4を介して中空糸膜 束 1を筒状ケース 2内へ引き込む動作をする。そして、糸束引き込み手段 5は、易滑 性シート 4の一部を筒状ケース 2内で確実に把持し、把持失敗による動作停止トラブ ルを防止するという観点から、事前にエア吸引して易滑性シート 4の一部を頭出しす る手段を備えておくことも好ましい。また、作業時には、中空糸膜束 1の損傷を抑制す るという観点から、筒状ケース 2の糸束 U字化手段 3側開口部に漏斗型の案内ガイド 7を配置することも好ましい。中空糸膜束 1の一部が筒状ケース 2の開口部の端部に 引つ力、かり中空糸膜を損傷することを防ぐことができる。 [0020] The yarn bundle drawing means 5 is arranged on the opposite side of the cylindrical case 2 from the yarn bundle U-shaped means 3, and a part of the slippery sheet 4 is placed inside the cylindrical case 2. A sheet gripping mechanism 5a for gripping and a moving mechanism 5b for reciprocating in the longitudinal direction of the cylindrical case 2 are provided. After the hollow fiber membrane bundle 1 is bent by the pushing member, it is between the hollow fiber membrane bundle 1 and the cylindrical case 2 A part of the slippery sheet 4 is gripped in the cylindrical case 2, and the hollow fiber membrane bundle 1 is pulled into the tubular case 2 through the slippery sheet 4. The yarn bundle pull-in means 5 easily and easily sucks air in advance from the viewpoint of reliably gripping a part of the slippery sheet 4 in the cylindrical case 2 and preventing operation stop trouble due to gripping failure. It is also preferable to provide means for cueing a part of the sliding sheet 4. Further, at the time of work, from the viewpoint of suppressing damage to the hollow fiber membrane bundle 1, it is also preferable to dispose a funnel-shaped guide guide 7 in the opening portion on the side of the yarn bundle U-shaped means 3 of the cylindrical case 2. It is possible to prevent a part of the hollow fiber membrane bundle 1 from pulling the end of the opening of the cylindrical case 2 and damaging the hollow fiber membrane.
[0021] 上記のような装置において中空糸膜束 1を筒状ケース 2に組み込む手順を、図 2〜 5を用いて以下に説明する。  [0021] A procedure for incorporating the hollow fiber membrane bundle 1 into the cylindrical case 2 in the apparatus as described above will be described below with reference to Figs.
[0022] まず、筒状ケースに装填される中空糸膜は、図 2に示すように、複数本が一方向に 引き揃えられ所定長にカットされた状態、すなわち中空糸膜束 1として、易滑性シート 4と共に糸束ガイドユニット 8の凹状溝に配置される。  [0022] First, as shown in FIG. 2, the hollow fiber membranes loaded in the cylindrical case are easily arranged in a state where a plurality of hollow fiber membranes are aligned in one direction and cut to a predetermined length, that is, as a hollow fiber membrane bundle 1. It is arranged in the concave groove of the yarn bundle guide unit 8 together with the sliding sheet 4.
[0023] 易滑性シート 4は、滑り性が良好で、かつ、一定の引張り強度があることがあれば特 に限定されないが、好ましくは、樹脂フィルム、布帛などが好ましい。特にポリェチレ ン、ポリプロピレン、ポリエステル等の樹脂フィルムが好ましぐ厚みは 5〜30 111の 範囲のものがよい。  [0023] The slippery sheet 4 is not particularly limited as long as it has good slipperiness and has a certain tensile strength, but a resin film, a fabric, and the like are preferable. In particular, a resin film such as polyethylene, polypropylene, or polyester preferably has a thickness in the range of 5-30111.
[0024] 易滑性シート 4の供給方法は、易滑性シート 4を、最終的に中空糸膜束 1と筒状ケ ース 2との間に配置されるような位置、すなわち、糸束ガイドユニット 8と中空糸膜束 1 との間に供給できればよいが、例えば、ロール状の易滑性シートから所定の長さを自 動で切り出して糸束ガイドユニット 8の上に配置することが連続的に効率よく易滑性シ ート 4を供給できると!/、う観点から好まし!/、態様である。  [0024] The supply method of the slippery sheet 4 is such that the slippery sheet 4 is finally disposed between the hollow fiber membrane bundle 1 and the cylindrical case 2, that is, the yarn bundle. For example, a predetermined length may be automatically cut out from a roll-like slippery sheet and placed on the yarn bundle guide unit 8 as long as it can be supplied between the guide unit 8 and the hollow fiber membrane bundle 1. It is preferable from the viewpoint of being able to supply the slippery sheet 4 continuously and efficiently! /.
[0025] また、中空糸膜束 1の供給は、人手により供給しても問題はないが、工業的にはコ ンベアやロボットなど自動で易滑性シート 4の上に供給し、糸束ガイドユニット 8の凹 状溝にセットすることが好ましい態様である。  [0025] Although the hollow fiber membrane bundle 1 can be supplied manually, there is no problem, but industrially, a conveyor, a robot or the like is automatically supplied onto the slippery sheet 4, and the yarn bundle guide is supplied. It is a preferred embodiment to set in the concave groove of the unit 8.
[0026] 次に、図 3に示すように、糸束 U字化手段 3の押し込み部材である平板 3aおよび 3b により、中空糸膜束 1の中央部分が筒状ケース 2方向に押し込まれ、中空糸膜束 1は 易滑性シート 4を伴って U字状に屈曲させられる。このとき、押し込み部材である平板 3aおよび 3bは、中空糸膜束 1および易滑性シート 4が U字状に屈曲するとともに当該 中空糸膜束 1および易滑性シート 4の一部が前記筒状ケースにかかるように押し込むNext, as shown in FIG. 3, the central portion of the hollow fiber membrane bundle 1 is pushed in the direction of the cylindrical case 2 by the flat plates 3a and 3b which are pushing members of the yarn bundle U-shaped means 3, and the hollow The membrane bundle 1 is bent into a U shape with a slippery sheet 4. At this time, a flat plate as a pushing member 3a and 3b are such that the hollow fiber membrane bundle 1 and the slippery sheet 4 are bent in a U-shape and part of the hollow fiber membrane bundle 1 and the slippery sheet 4 are pushed over the cylindrical case.
Yes
[0027] そして、図 4、 5に示すように、筒状ケース 2の中空糸膜束 1を揷入する側とは反対 側の開口部から糸束引き込み手段 5のシート把持機構 5aが筒状ケース内で易滑性 シート 4の一部を把持し筒状ケース 2内に引き込む。易滑性シートの一部を把持して 筒状ケース内へ引き込む際には、同時に、押し込み部材の一方の平板 3bを易滑性 シートの引き込み方向に移動させる。ここで、引き込み動作が有効に作用するために は糸束引き込み手段 5のシート把持機構 5aが把持しているフィルムに張力が作用し ていることが好ましい。そのため、シート把持機構 5aは、平板 3bの移動開始以前に 引き込み動作を開始する (すなわち、シート把持機構 5aによる易滑性シートの筒状ケ ース内への引き込み開始以後に、平板 3bの易滑性シート引き込み方向への移動を 開始する)ことが好ましい。また、同様の観点から、糸束引き込み手段 5が易滑性シー トを引き込む速度を平板 3bの移動速度以上 (すなわち平板 3bの易滑性シート引き込 み方向への移動スピード以上)とすることも好ましい。なお、押し込み部材を 2枚の平 板 3aおよび 3bから構成せず、 1枚の板状部材から構成する場合は、当該板状部材 の移動開始以前にシート把持機構 5aの引き込み動作を開始することが好ましぐま た、糸束引き込み手段 5が易滑性シートを引き込む速度を当該板状部材の移動速度 以上とすることが好ましい。押し込み部材の他方の平板 3aは、糸束引き込み手段 5の シート把持機構 5aが易滑性シート 4の一部を把持したら、筒状ケース 2から退避する 。このようにして、 U字状に屈曲された中空糸膜束 1は、易滑性シート 4に包まれた状 態で筒状ケース内 2へ収納される。  [0027] As shown in Figs. 4 and 5, the sheet gripping mechanism 5a of the yarn bundle drawing means 5 is formed in a cylindrical shape from the opening on the opposite side to the side where the hollow fiber membrane bundle 1 is inserted in the cylindrical case 2. Grip a part of the slippery sheet 4 in the case and pull it into the cylindrical case 2. When a part of the slippery sheet is gripped and pulled into the cylindrical case, at the same time, one flat plate 3b of the pushing member is moved in the pulling direction of the slippery sheet. Here, in order for the drawing operation to work effectively, it is preferable that tension is applied to the film held by the sheet holding mechanism 5a of the yarn bundle drawing means 5. Therefore, the sheet gripping mechanism 5a starts a pulling operation before the movement of the flat plate 3b starts (that is, after the slipping of the slippery sheet into the cylindrical case by the sheet gripping mechanism 5a starts, It is preferable to start the movement in the sliding sheet retracting direction). Also, from the same viewpoint, the speed at which the yarn bundle drawing means 5 draws the slippery sheet should be equal to or higher than the moving speed of the flat plate 3b (that is, higher than the moving speed of the flat plate 3b in the pulling direction of the slippery sheet). Is also preferable. If the push-in member is not composed of the two flat plates 3a and 3b but is composed of a single plate-like member, the pull-in operation of the sheet gripping mechanism 5a must be started before the movement of the plate-like member. It is preferable that the speed at which the yarn bundle drawing means 5 pulls in the slippery sheet is equal to or higher than the moving speed of the plate-like member. The other flat plate 3a of the pushing member is retracted from the cylindrical case 2 when the sheet gripping mechanism 5a of the yarn bundle drawing means 5 grips a part of the slippery sheet 4. In this way, the hollow fiber membrane bundle 1 bent in a U shape is stored in the cylindrical case 2 in a state of being wrapped in the slippery sheet 4.
[0028] その後、必要に応じて、易滑性シート 4の除去、中空糸膜束 1の端部封止、切除、 そして、中空糸膜束が湿潤している場合には乾燥などの処理が行われ、中空糸膜モ ジユーノレが完成する。  [0028] Thereafter, if necessary, treatment such as removal of the slippery sheet 4, sealing of the end of the hollow fiber membrane bundle 1, excision, and drying when the hollow fiber membrane bundle is wet is performed. This completes the hollow fiber membrane module.
[0029] ここで、本実施形態においては、上述したように、筒状ケース収納の際、中空糸膜 束 1と易滑性シート 4とを押し込み部材で筒状ケース 2に向けて U字状に屈曲させな 力 ¾当該中空糸膜束 1および易滑性シート 4の一部を筒状ケース 2に押し込んだ後は 、易滑性シート 4の一部を把持して筒状ケース 2内へ引き込む。こうすることで中空糸 膜束 1を筒状ケース 2内へ引き込む。また、このとき中空糸膜束の移動を補助するた めに、易滑性シート 4の引き込みと同時に押し込み部材を易滑性シートの引き込み方 向に移動させる。すなわち、本実施形態においては、中空糸膜束 1を筒状ケース 2へ 収納するために必要な力を、基本的にはシートを介して糸束に作用させる引き込み 動作で発生させると同時に、押し込み部材による移動で補助する構成とする。引き込 み動作のみの場合、中空糸膜束の屈曲部分に損傷は生じないが、シートと中空糸膜 束との間で滑りが生じたり、把持機構 5aからシートが抜け落ちたりすると、所望の位置 まで中空糸膜束を引き込むことができなくなる。一方、押し込み動作のみの場合、所 望の位置まで中空糸膜束を移動させることはできるが、中空糸膜束の屈曲部分に作 用する押し込み力のみで中空糸膜束を移動させることになり、中空糸膜の充填率を 高める場合には中空糸膜束の屈曲部分が損傷する恐れがある。そこで本実施形態 においては、中空糸膜束 1を筒状ケース 2へ収納するために必要な力を、基本的に はシートを介して糸束に作用させる引き込み動作で発生させると同時に、押し込み部 材による移動で補助する構成とする。これにより、所望の位置まで確実に中空糸膜束 を移動させることが可能となると共に、糸束 U字化手段 3の押し込み部材 3bが中空糸 膜束 1の屈曲部分に作用させる押し込み力を小さく抑えることができ、糸潰れ等の損 傷を防止することが可能となる。 [0029] Here, in the present embodiment, as described above, when storing the cylindrical case, the hollow fiber membrane bundle 1 and the slippery sheet 4 are pushed toward the cylindrical case 2 with a pressing member. ¾ After pushing part of the hollow fiber membrane bundle 1 and the slippery sheet 4 into the cylindrical case 2 Then, grip a part of the slippery sheet 4 and pull it into the cylindrical case 2. In this way, the hollow fiber membrane bundle 1 is drawn into the cylindrical case 2. At this time, in order to assist the movement of the hollow fiber membrane bundle, the pushing member is moved in the drawing direction of the slippery sheet simultaneously with the pulling of the slippery sheet 4. That is, in the present embodiment, the force required to store the hollow fiber membrane bundle 1 in the cylindrical case 2 is generated by the pulling action that basically acts on the yarn bundle via the sheet, and at the same time, the push-in operation is performed. It is set as the structure which assists by the movement by a member. In the case of only the pull-in operation, the bending portion of the hollow fiber membrane bundle is not damaged, but if the sheet slips between the hollow fiber membrane bundle or the sheet falls out of the gripping mechanism 5a, the desired position is obtained. The hollow fiber membrane bundle can no longer be drawn. On the other hand, in the case of only the pushing operation, the hollow fiber membrane bundle can be moved to the desired position, but the hollow fiber membrane bundle is moved only by the pushing force applied to the bent portion of the hollow fiber membrane bundle. When the filling rate of the hollow fiber membrane is increased, the bent portion of the hollow fiber membrane bundle may be damaged. Therefore, in the present embodiment, the force required to store the hollow fiber membrane bundle 1 in the cylindrical case 2 is generated by a pulling action that basically acts on the yarn bundle via the sheet, and at the same time, the pushing portion It is configured to assist by movement with materials. Thus, the hollow fiber membrane bundle can be reliably moved to a desired position, and the pushing force applied by the pushing member 3b of the yarn bundle U-shaped means 3 to the bent portion of the hollow fiber membrane bundle 1 can be reduced. Therefore, it is possible to prevent damage such as thread crushing.
そして、各動作の開始タイミングと速度について述べる。引き込み動作が有効に作 用するためには糸束引き込み手段 5のシート把持機構 5aが把持しているシートに張 力が作用していることが必要である。糸束引き込み手段 5が動作する前に平板 3bが 移動を開始すると中空糸膜束と把持機構 5aの距離が短くなり把持している部分のシ ートが弛んでしまい、この状態で糸束引き込み手段を動作しはじめても引き込み力は 発生しないことがある。従って、平板 3bの移動開始以前に糸束引き込み手段の動作 を開始すること(すなわち、シート把持機構 5aによる易滑性シートの筒状ケース内へ の引き込み開始以後に、平板 3bの易滑性シート引き込み方向への移動を開始する こと)が好ましい。また、押し込み動作が引き込み動作よりも速いと同様に把持してい る部分のシートが弛んでしまう。従って、糸束引き込み手段 5が易滑性シートを引き込 む速度を、平板 3bの移動速度以上 (すなわち平板 3bの易滑性シート引き込み方向 への移動スピード以上)とすることも好まし!/、。 Then, the start timing and speed of each operation will be described. In order for the pulling operation to work effectively, it is necessary that a tension is applied to the sheet gripped by the sheet gripping mechanism 5a of the yarn bundle pulling means 5. If the flat plate 3b starts moving before the thread bundle pulling means 5 operates, the distance between the hollow fiber membrane bundle and the gripping mechanism 5a is shortened, and the sheet of the gripping part is loosened. The pulling force may not be generated even if the means starts to operate. Therefore, the operation of the thread bundle pulling means is started before the movement of the flat plate 3b (that is, after the slipping of the slippery sheet into the cylindrical case by the sheet gripping mechanism 5a is started, the slippery sheet of the flat plate 3b is started. It is preferable to start movement in the pull-in direction). In addition, if the push-in operation is faster than the pull-in operation, the gripping portion of the sheet is loosened. Therefore, the thread bundle retracting means 5 retracts the slippery sheet. It is also preferable to set the speed to be higher than the moving speed of the flat plate 3b (that is, higher than the moving speed of the flat plate 3b in the slipping direction of the slippery sheet)!
[0031] また、押し込み部材は、上述したように一枚の板状部材であってもよいが、二枚の 平板 3aおよび 3bで構成される意義について説明すると次のようになる。  [0031] The pushing member may be a single plate-like member as described above, but the significance of the two flat plates 3a and 3b will be described as follows.
[0032] 中空糸膜束 1を U字状に屈曲させる際、屈曲部の糸潰れ等の損傷を防止するため には、押し込み部材の端面に面取りを施すだけではなぐ中空糸膜束 1の接触面に 作用する圧力を小さくするのが好ましい。従って、押し込み部材の押し込み面積を一 定以上確保することが好ましい。一方、中空糸膜束のケース収納時は、押し込み部 材が筒状ケース 2内へ進入すると、筒状ケース 2内において押し込み部材の容積分 だけ中空糸膜束 1が占める容積が小さくなる。このため、中空糸膜束 1は筒状ケース 内壁へ押しやられることとなり、変形、糸潰れ等の損傷が生じ易い。易滑性シート 4に より滑りやすくする効果は期待できる力 S、充填率の高い製品の場合は、特に損傷の 危険性が高くなるため、押し込み部材のケース進入部分の体積は小さいことが好まし い。このように、前者の要求を満たすためには押し込み部材の板厚は厚い方が好ま しぐ後者の要求を満たすためには逆に板厚は薄い方が好ましい。そこで、糸束 U字 化手段 3の押し込み部材を 2枚の平板 3a、 3bから構成し、 U字状に屈曲させるときに は 2枚同時に作用させ、中空糸膜束 1への接触面積を確保し、中空糸膜束の筒状ケ ース収納の際は 1枚のみで作用させることが好ましい。  [0032] When the hollow fiber membrane bundle 1 is bent into a U-shape, the contact of the hollow fiber membrane bundle 1 is not limited to chamfering the end face of the pushing member in order to prevent damage such as yarn crushing at the bent portion. It is preferable to reduce the pressure acting on the surface. Therefore, it is preferable to secure a certain pushing area of the pushing member. On the other hand, when the hollow fiber membrane bundle is stored in the case, when the pushing member enters the cylindrical case 2, the volume occupied by the hollow fiber membrane bundle 1 in the cylindrical case 2 is reduced by the volume of the pushing member. For this reason, the hollow fiber membrane bundle 1 is pushed to the inner wall of the cylindrical case, and damage such as deformation and thread crushing is likely to occur. The slippery sheet 4 can be expected to have a slippery effect. S For products with a high filling rate, the risk of damage is particularly high. Yes. As described above, in order to satisfy the former requirement, it is preferable that the thickness of the pushing member is thicker. In order to satisfy the latter requirement, it is preferable that the thickness is thinner. Therefore, the push-in member of the yarn bundle U-shaped means 3 is composed of two flat plates 3a and 3b, and when they are bent into a U shape, the two members act simultaneously to ensure a contact area with the hollow fiber membrane bundle 1. However, when the hollow fiber membrane bundle is accommodated in the cylindrical case, it is preferable that only one sheet acts.
実施例  Example
[0033] (実施例 1) [Example 1]
以上の中空糸膜モジュールの製造装置を用いて、中空糸膜モジュールを製造した  Using the above hollow fiber membrane module manufacturing apparatus, a hollow fiber membrane module was manufactured.
[0034] 中空糸膜としては外径 0. 45mmのポリスルホン系中空糸膜を用い、これを 700本 束ねて 200mmの長さにカットしたものを中空糸膜束 1とした。易滑性シート 4は、幅 1 20mm,厚さ 0. 01mmのロール状に巻き取られたポリエチレンシートから長さ 120m mを切り出して糸束ガイドユニット 8の上に供給されるよう構成した。 [0034] As the hollow fiber membrane, a polysulfone-based hollow fiber membrane having an outer diameter of 0.45 mm was used, and a hollow fiber membrane bundle 1 was obtained by bundling 700 pieces and cutting them to a length of 200 mm. The slippery sheet 4 was configured such that a length of 120 mm was cut out from a polyethylene sheet wound into a roll having a width of 120 mm and a thickness of 0.01 mm and supplied onto the yarn bundle guide unit 8.
[0035] 易滑性シート 4が糸束ガイドユニット 8上にセットされた後、中空糸膜束 1がコンベア によって前工程から供給され、ロボットノヽンドによって糸束ガイドユニット 8の凹状溝に 移載されるように構成した。 [0035] After the slippery sheet 4 is set on the yarn bundle guide unit 8, the hollow fiber membrane bundle 1 is supplied from the previous process by the conveyor, and is inserted into the concave groove of the yarn bundle guide unit 8 by the robot node. It was configured to be transferred.
[0036] 筒状ケース 2は、内径 φ 26mm,長さ 70mmのアクリルスチレン製とし、中空糸膜束 1の供給とほぼ同時にケース供給用コンベアから供給され、ロボットノ、ンドによって糸 束ガイドユニット 8の下にセットされるよう構成した。  [0036] The cylindrical case 2 is made of acrylic styrene having an inner diameter of 26 mm and a length of 70 mm. The cylindrical case 2 is supplied from the case supply conveyor almost simultaneously with the supply of the hollow fiber membrane bundle 1. It was configured to be set below.
[0037] 糸束 U字化手段 3の平板 3a、 3bは中空糸膜との乖離性を考慮してフッ素樹脂コー ティング仕上げとし、厚みはともに 2mmとした。平板 3a、 3bの上下動には日本べァリ ング (株)製の 1軸ァクチユエータをそれぞれ用いた。平板が糸束に接触しながら動作 するときは損傷防止のため低速(100mm/秒)で動作し、それ以外のときは処理タク ト短縮のために高速(500mm/秒)で動作するように設定した。  [0037] The flat plates 3a and 3b of the yarn bundle U-shaped means 3 were coated with a fluororesin coating in consideration of the detachability from the hollow fiber membrane, and both thicknesses were 2 mm. A uniaxial actuator manufactured by Nippon Bearing Co., Ltd. was used for the vertical movement of the flat plates 3a and 3b. Set to operate at a low speed (100mm / sec) to prevent damage when the flat plate operates while contacting the yarn bundle, and at a high speed (500mm / sec) to reduce the processing tact in other cases did.
[0038] 糸束引き込み手段 5について、シート把持機構 5aは SMC (株)製エアチャックに易 滑性シート 4を把持するためのッメが装着された構成とし、移動機構 5bは日本べァリ ング (株)製の 1軸ァクチユエータを用いた。易滑性シート 4を筒状ケース 2へ引き込む 動作のときは中空糸への損傷防止のために低速で動作し、それ以外のときは処理タ タト短縮のために高速で動作するように設定した。すなわちシート引き込み動作時は 100mm/秒、それ以外の動作時は 500mm/秒の速度で動作するように設定した 。さらに、糸束引き込み手段 5のシート引き込み動作開始 0. 1秒後に平板 3bが移動 開始するよう設定した。  [0038] With respect to the yarn bundle drawing-in means 5, the sheet gripping mechanism 5a is configured such that a slip for gripping the slippery sheet 4 is mounted on an air chuck manufactured by SMC Co., Ltd., and the moving mechanism 5b is A 1-axis actuator manufactured by Ning Co., Ltd. was used. Pulling the slippery sheet 4 into the cylindrical case 2 During operation, it was set to operate at a low speed to prevent damage to the hollow fiber, and at other times it was set to operate at a high speed to shorten the processing tart. . In other words, it was set to operate at a speed of 100 mm / second during sheet pull-in operation, and at a speed of 500 mm / second during other operations. Furthermore, the flat plate 3b was set to start moving 0.1 second after the start of the sheet drawing operation of the yarn bundle drawing means 5.
[0039] 以上の装置構成で中空糸膜束 1を筒状ケース 2内へ収納した後、図 6に示すように 、まず筒状ケース上端部から突出している中空糸膜束 1の端部を糸束固定用エアチ ャック 9で把持して筒状ケースから抜け落ちないよう固定した後、筒状ケース 2内に残 つている易滑性シート 4をシート抜き取り用エアチャック 10で把持し、シート抜き取り 用エアチャック 10に結合したシート抜き取り用エアシリンダー 11にてゆっくりと下方向 へ引っ張って抜き取った。  [0039] After the hollow fiber membrane bundle 1 is stored in the cylindrical case 2 with the above apparatus configuration, as shown in Fig. 6, first, the end of the hollow fiber membrane bundle 1 protruding from the upper end of the cylindrical case is removed. After gripping with the thread bundle fixing air chuck 9 and fixing it so that it does not fall out of the cylindrical case, grip the slippery sheet 4 remaining in the cylindrical case 2 with the sheet pulling air chuck 10 to remove the sheet. The sheet was removed by slowly pulling downward with an air cylinder 11 for removing the sheet connected to the air chuck 10.
[0040] 以上のようにして中空糸膜束 1を筒状ケース 2へ U字状に組み込んだところ、中空 糸膜束 1の屈曲部内側の糸潰れや擦過などの問題となる損傷はほとんど見られず、 また、ポッティング後に実施したリークテストの結果も良好であった。  [0040] When the hollow fiber membrane bundle 1 is assembled into the cylindrical case 2 in a U-shape as described above, damage that causes problems such as thread crushing and rubbing inside the bent portion of the hollow fiber membrane bundle 1 is hardly observed. Moreover, the result of the leak test conducted after potting was also good.
(比較例 1)  (Comparative Example 1)
実施例 1において、糸束引き込み手段 5を使わない以外は、実施例 1と同様にして 筒状ケース 2へ中空糸膜束 1を収納し、中空糸膜モジュールを得た。本比較例で得 られた中空糸膜モジュールについて、 目視による外観検査を実施したところ、中空糸 膜束の屈曲部内側に中空糸が潰れてしまっている潰れ欠点や中空糸が折れてしま つている折れ欠点が多数見られた。また、本比較例で作成した中空糸膜モジュール 100個に対してリークテストを実施したところ、 6個のリークアウトが発生してしまった。 リークアウトした中空糸膜モジュールを解体検査したところ、上記外観検査で欠点と なった部位において、糸が破断してしまったり、亀裂が生じていることがわかった。 産業上の利用可能性 Example 1 is the same as Example 1 except that the yarn bundle drawing means 5 is not used. The hollow fiber membrane bundle 1 was accommodated in the cylindrical case 2 to obtain a hollow fiber membrane module. When a visual appearance inspection was performed on the hollow fiber membrane module obtained in this comparative example, the hollow fiber was broken inside the bent part of the hollow fiber membrane bundle, and the hollow fiber was broken. Many broken defects were seen. In addition, when leak tests were performed on 100 hollow fiber membrane modules created in this comparative example, 6 leak-outs occurred. When the hollow fiber membrane module leaked out was disassembled and inspected, it was found that the thread was broken or cracked at the site that was a defect in the appearance inspection. Industrial applicability
本発明は、浄水用だけでなぐ医療用の中空糸膜モジュールの製造にあたっても 好適に用いることができる。  The present invention can also be suitably used in the production of a medical hollow fiber membrane module that is used only for water purification.

Claims

請求の範囲 The scope of the claims
[1] 中空糸膜束を屈曲させて筒状ケースに収納する中空糸膜モジュールの製造方法 であって、前記中空糸膜束ならびに前記筒状ケースと前記中空糸膜束との間に予め 配置された易滑性シートを押し込み部材で前記筒状ケースに向けて U字状に屈曲さ せながら前記中空糸膜束および前記易滑性シートの一部を前記筒状ケースに押し 込み、その後、前記易滑性シートの一部を把持して前記筒状ケース内へ引き込むと 同時に前記押し込み部材を前記易滑性シートの引き込み方向に移動させ、前記中 空糸膜束を前記筒状ケース内へ収納することを特徴とする中空糸膜モジュールの製 造方法。  [1] A method for manufacturing a hollow fiber membrane module in which a hollow fiber membrane bundle is bent and accommodated in a cylindrical case, the hollow fiber membrane bundle being arranged in advance between the hollow fiber membrane bundle and the cylindrical case and the hollow fiber membrane bundle The hollow fiber membrane bundle and a part of the slippery sheet are pushed into the cylindrical case while bending the formed slippery sheet toward the tubular case with a pushing member and then bent into a U shape. When a part of the slippery sheet is gripped and pulled into the cylindrical case, the pushing member is moved in the pulling direction of the slippery sheet and the hollow fiber membrane bundle is moved into the tubular case. A method for producing a hollow fiber membrane module comprising storing.
[2] 中空糸膜束を屈曲させて筒状ケースに収納する中空糸膜モジュールの製造方法 であって、前記中空糸膜束ならびに前記筒状ケースと前記中空糸膜束との間に予め 配置された易滑性シートを 2枚の平板を有する押し込み部材で前記筒状ケースに向 けて U字状に屈曲させながら前記中空糸膜束および前記易滑性シートの一部を前 記筒状ケースに押し込み、その後、前記易滑性シートの一部を把持して前記筒状ケ ース内へ引き込むと同時に前記 2枚の平板のうちの 1枚を前記易滑性シートの引き込 み方向に移動させ、前記中空糸膜束を前記筒状ケース内へ収納することを特徴とす る中空糸膜モジュールの製造方法。  [2] A method for manufacturing a hollow fiber membrane module in which a hollow fiber membrane bundle is bent and accommodated in a cylindrical case, the hollow fiber membrane bundle being arranged in advance between the hollow fiber membrane bundle and the cylindrical case and the hollow fiber membrane bundle The hollow fiber membrane bundle and a part of the slippery sheet are part of the cylindrical shape while the easy slippery sheet is bent into a U shape toward the tubular case by a pushing member having two flat plates. Push into the case, and then grip a part of the slippery sheet and pull it into the cylindrical case. At the same time, pull in one of the two flat plates in the slipping direction of the slippery sheet And manufacturing the hollow fiber membrane module by storing the bundle of hollow fiber membranes in the cylindrical case.
[3] 前記易滑性シートの一部を把持して前記筒状ケース内へ引き込むと同時に前記押 し込み部材または前記 2枚の平板のうちの前記 1枚を前記易滑性シートの前記弓 Iき 込み方向に移動させるに際しては、前記易滑性シートの前記筒状ケース内への引き 込み開始以後に、前記押し込み部材または前記 2枚の平板のうちの前記 1枚の、前 記易滑性シートの前記引き込み方向への移動を開始する、請求項 1または 2記載の 中空糸膜モジュールの製造方法。  [3] A part of the slippery sheet is gripped and pulled into the cylindrical case, and at the same time, the pushing member or the one of the two flat plates is used as the bow of the slippery sheet. When moving in the I-insertion direction, after the pull-in of the slippery sheet into the cylindrical case, the one of the push-in member or the two flat plates, the slippery sheet as described above, is started. The method for producing a hollow fiber membrane module according to claim 1 or 2, wherein movement of the adhesive sheet in the pull-in direction is started.
[4] 前記易滑性シートの一部を把持して前記筒状ケース内へ引き込むと同時に前記押 し込み部材または前記 2枚の平板のうちの前記 1枚を前記易滑性シートの引き込み 方向に移動させるに際しては、前記易滑性シートの引き込みスピードを、前記押し込 み部材または前記 2枚の平板のうちの 1枚の前記易滑性シートの前記引き込み方向 への移動スピード以上にする、請求項;!〜 3のいずれかに記載の中空糸膜モジユー ルの製造方法。 [4] A part of the slippery sheet is gripped and pulled into the cylindrical case, and at the same time, the pushing member or the one of the two flat plates is pulled in the slippery sheet direction. When moving the slippery sheet, the pulling speed of the slippery sheet is set to be equal to or higher than the moving speed of the one slippery sheet of the push-in member or the two flat plates in the pulling direction. Claims;! ~ 3 hollow fiber membrane module Manufacturing method.
[5] 中空糸膜束を屈曲させて筒状ケースに収納する中空糸膜モジュールの製造装置 であって、前記中空糸膜束を易滑性シートと共に前記筒状ケースに向けて U字状に 屈曲させながら前記中空糸膜束および前記易滑性シートの一部を前記筒状ケース に押し込む押し込み手段と、前記易滑性シートの一部を把持して前記筒状ケース内 へ引き込むことで前記中空糸膜束を前記筒状ケース内へ引き込む糸束引き込み手 段とを備え、前記押し込み手段が、前記糸束引き込み手段の易滑性シート引き込み 時に同期して前記易滑性シートの引き込み方向に移動するように構成されていること を特徴とする中空糸膜モジュールの製造装置。  [5] A device for manufacturing a hollow fiber membrane module that bends a hollow fiber membrane bundle and stores it in a cylindrical case, wherein the hollow fiber membrane bundle is U-shaped toward the cylindrical case together with a slippery sheet. Pushing means for pushing the hollow fiber membrane bundle and a part of the slippery sheet into the cylindrical case while bending, and holding the part of the slippery sheet and pulling it into the tubular case. A thread bundle pulling means for pulling the hollow fiber membrane bundle into the cylindrical case, and the pushing means is synchronized with the pulling of the slippery sheet of the thread bundle pulling means in the pulling direction of the slippery sheet. An apparatus for manufacturing a hollow fiber membrane module, wherein the apparatus is configured to move.
[6] 前記押し込み手段は 2枚の平板を有し、該 2枚の平板のうちの 1枚が、前記糸束引 き込み手段の易滑性シート引き込み時に同期して前記引き込み方向に移動する、請 求項 5記載の中空糸膜モジュールの製造装置。  [6] The push-in means has two flat plates, and one of the two flat plates moves in the pull-in direction in synchronization with the slippery sheet pull-in of the yarn bundle pull-in means. The apparatus for producing a hollow fiber membrane module according to claim 5.
[7] 前記 2枚の平板のうち 1枚の平板のみが先端部に二股部を有し、二股部を備えて いない平板が、易滑性シート引き込み時に同期して前記引き込み方向に移動する、 請求項 6記載の中空糸膜モジュールの製造装置。  [7] Of the two flat plates, only one flat plate has a bifurcated portion at the tip, and the flat plate not having the bifurcated portion moves in the retracting direction in synchronization with the slipping of the slippery sheet. The apparatus for producing a hollow fiber membrane module according to claim 6.
PCT/JP2007/068084 2006-09-20 2007-09-18 Process for producing hollow fiber membrane module and apparatus therefor WO2008035673A1 (en)

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JPH02241521A (en) * 1989-03-14 1990-09-26 Mitsubishi Rayon Co Ltd Apparatus to pack hollow yarn bundle in cylinder
JPH08117564A (en) * 1994-10-19 1996-05-14 Nok Corp Method and apparatus for yarn packing of hollow yarn membrane bundle
JPH105549A (en) * 1996-06-26 1998-01-13 Mitsubishi Rayon Co Ltd Hollow yarn bundle housing device for cylindrical body for membrane module
JP2003062435A (en) * 2001-08-24 2003-03-04 Toray Ind Inc Method and apparatus for manufacturing hollow fiber membrane module
JP3623856B2 (en) * 1996-07-05 2005-02-23 三菱レイヨン株式会社 Hollow fiber bundle storage device in cylindrical body

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Publication number Priority date Publication date Assignee Title
JPH02241521A (en) * 1989-03-14 1990-09-26 Mitsubishi Rayon Co Ltd Apparatus to pack hollow yarn bundle in cylinder
JPH08117564A (en) * 1994-10-19 1996-05-14 Nok Corp Method and apparatus for yarn packing of hollow yarn membrane bundle
JPH105549A (en) * 1996-06-26 1998-01-13 Mitsubishi Rayon Co Ltd Hollow yarn bundle housing device for cylindrical body for membrane module
JP3623856B2 (en) * 1996-07-05 2005-02-23 三菱レイヨン株式会社 Hollow fiber bundle storage device in cylindrical body
JP2003062435A (en) * 2001-08-24 2003-03-04 Toray Ind Inc Method and apparatus for manufacturing hollow fiber membrane module

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