WO2006108973A1 - Dispositif, installation et procede d'alignement et/ou d'assemblage d'elements de filtration - Google Patents
Dispositif, installation et procede d'alignement et/ou d'assemblage d'elements de filtration Download PDFInfo
- Publication number
- WO2006108973A1 WO2006108973A1 PCT/FR2006/050195 FR2006050195W WO2006108973A1 WO 2006108973 A1 WO2006108973 A1 WO 2006108973A1 FR 2006050195 W FR2006050195 W FR 2006050195W WO 2006108973 A1 WO2006108973 A1 WO 2006108973A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- elements
- walls
- filter
- cement
- folding
- Prior art date
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D46/00—Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
- B01D46/0001—Making filtering elements
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D46/00—Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
- B01D46/10—Particle separators, e.g. dust precipitators, using filter plates, sheets or pads having plane surfaces
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D46/00—Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
- B01D46/56—Filters or filtering processes specially modified for separating dispersed particles from gases or vapours with multiple filtering elements, characterised by their mutual disposition
- B01D46/58—Filters or filtering processes specially modified for separating dispersed particles from gases or vapours with multiple filtering elements, characterised by their mutual disposition connected in parallel
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B28—WORKING CEMENT, CLAY, OR STONE
- B28B—SHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
- B28B1/00—Producing shaped prefabricated articles from the material
- B28B1/002—Producing shaped prefabricated articles from the material assembled from preformed elements
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B28—WORKING CEMENT, CLAY, OR STONE
- B28B—SHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
- B28B7/00—Moulds; Cores; Mandrels
- B28B7/0029—Moulds or moulding surfaces not covered by B28B7/0058 - B28B7/36 and B28B7/40 - B28B7/465, e.g. moulds assembled from several parts
- B28B7/0035—Moulds characterised by the way in which the sidewalls of the mould and the moulded article move with respect to each other during demoulding
- B28B7/0044—Moulds characterised by the way in which the sidewalls of the mould and the moulded article move with respect to each other during demoulding the sidewalls of the mould being only tilted away from the sidewalls of the moulded article, e.g. moulds with hingedly mounted sidewalls
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T156/00—Adhesive bonding and miscellaneous chemical manufacture
- Y10T156/10—Methods of surface bonding and/or assembly therefor
- Y10T156/1002—Methods of surface bonding and/or assembly therefor with permanent bending or reshaping or surface deformation of self sustaining lamina
- Y10T156/1003—Methods of surface bonding and/or assembly therefor with permanent bending or reshaping or surface deformation of self sustaining lamina by separating laminae between spaced secured areas [e.g., honeycomb expanding]
Definitions
- the invention relates to a method, a device or an installation for assembling and / or manufacturing particulate filters comprising a plurality of monolithic elements, particularly suitable for application in an exhaust line of a diesel engine.
- Particle filters used in the exhaust lines of internal combustion engines most often have a honeycomb structure.
- Such structures comprise a set of adjacent ducts or channels with axes parallel to each other separated by porous filtration walls, which ducts are closed at one or the other of their ends to delimit opening chambers opening following the admission face and exit chambers opening on the evacuation face.
- the materials used are in particular ceramic in nature, for example cordierite, silicon carbide, etc.
- filtration structures have been proposed that combine several blocks or monolithic elements into one another.
- Honeycomb The elements are most often assembled together by gluing by means of an adhesive or cement of a ceramic nature, forming a seal between each element, called joint cement or jointing in the following description. Examples of manufacture of such filtering structures are described, for example, in patent EP 1 479 882 A1.
- the parallelepipedal elements also called monolithic blocks, are glued, one after the other, in a horizontal position in the direction of their length, on a V-shaped guide and formed of two flat supports, usually perpendicular.
- the assembled elements are then dried and machined to form the final structure, the peripheral portion of which is most often surrounded by a coating cement to ensure a good seal in service.
- This assembly process is however tedious because the elements are manipulated one after the other. This makes the process expensive and unproductive.
- the drying time, or even hardening, of the seal cement deposited on the first element is necessarily longer than that of the last assembled element, which can generate an uncontrolled structure inhomogeneity which is detrimental to the lifetime of the filter, or for its simple manipulation.
- the object of the present invention is to provide a method of alignment and / or assembly of such monolithic elements, in particular allowing the manufacture in large numbers of such filters with good productivity and lower cost.
- Another object of the invention is to obtain assembled filters in which the joint cement is distributed between the elements in a controlled and homogeneous manner.
- the present invention relates in a first aspect to a device for aligning and / or assembling filter elements, in particular a particle filter, said device comprising a bottom plate on which said elements, said bottom plate being for example fixed on a base plate, and walls laterally foldable upwards by means of folding, so that said elements are held together tightly when said walls are in the up position.
- the walls are hinged to the base plate by means of hinges arranged on the periphery of the base plate.
- said side walls are foldably arranged by means of a closing frame movable in height.
- Each wall may be provided with at least one closure cam which is in interaction with a bearing disposed opposite on the closure frame.
- the walls can be locked with locking bolts on the closure frame by locking elements which are arranged on at least two opposite walls, in which the base plate is arranged by fixing on a pallet and wherein the closure frame is operable by means of lifting elements of an electronically controlled lifting device.
- the bearing is a roller bearing.
- the lifting elements of the lifting device can be hydraulic or pneumatic cylinders or linear units, consisting of a rotor and a casing of a linear motor.
- an adapter plate is disposed on each of the inner faces of the walls, said adapter plates being preferably made of a flexible or plastic material or connected to the removable walls by a system of springs or flexible material.
- the invention furthermore relates to an installation for assembling a filter from filter elements, comprising a device as previously described and means of injection or depositing an adhesive or a cement between the elements present within said device.
- Said installation may further comprise means for spacing and tilting said elements on the walls.
- the means for folding the walls are coordinated or slaved to the injection or removal means.
- the invention relates to a method for aligning and / or assembling monolithic filtering elements, in particular for producing a particle filter, said method comprising the following steps: a step of positioning said elements in a device according to one of the preceding claims,
- the outer walls of the elements brought into contact with each other by the movement of the folding walls are previously coated with an adhesive or a cement.
- a step of injecting or removing an adhesive or a cementing cement between said elements is provided.
- the various elements are positioned on the support, according to their respective position in the final assembly, -
- the elements are fixed in a position and with a spacing allowing the injection of cement or glue,
- the glue or the grouting cement is injected and the elements are brought into subjection under the action of the folding walls, the said foldable walls are maintained in the raised position, so as to to keep the elements pressed against each other, until the hardening or setting of the glue or the cement,
- the assembled filter is demolded by reducing the pressure exerted by the withdrawal of the folding walls.
- the method may further comprise a heat treatment step of the filter before the demolding step.
- FIG. 1 gives a three-dimensional representation of the device according to the invention, in a closed position when it contains the filtration elements;
- FIG. 2 represents in three dimensions the device in the open position, before the introduction of said elements,
- - Figure 3 illustrates a particular embodiment of the device and implementation of such a device in a filter assembly plant, wherein a grouting cement is further injected between the elements.
- FIG. 1 represents a device for aligning and / or assembling filter elements 1 of a particulate filter, in particular a particulate diesel filter.
- the filtration elements 1 are placed on a bottom plate 2 in the form of a package.
- the bottom plate 2 is fixed on a base plate 3.
- Upwardly folding walls 4 are hinged to the base plate 3 by means of hinges 5, the walls 4 being foldable by means of a movable closure frame 6 up and down. Moved up, the walls 4 surround the filter elements 1 collected in a package and hold them securely together. If according to the representation in Figure 1, a slot has been formed between the filter elements 1 and the walls 4, an adapter plate 12 closing said slot and, when the walls 4 are folded up, now guaranteed the filter elements 1 against each other, is respectively fixed on the inner faces of the walls 4. To obtain a homogeneous and guided movement during the closing and opening of the walls 4, the latter are provided with at least a closure cam 7.
- closure cams 7 interact with a bearing 8, for example a roller bearing on the closure frame 6.
- a bearing 8 for example a roller bearing on the closure frame 6.
- the closure frame 6 has stop bolts 10 which engage in corresponding locking elements 9 on the walls 4.
- the base plate 3 which carries the bottom plate 2 is fixed on a pallet 11.
- the pallet 11 may be the transport pallet of a transport system for bringing the filtration elements 1 to a drying process, in which the particle filter is created as a fixed package consisting of the filter elements 1.
- the closure 6 is actuated by means of an electronically controlled lifting device, which is not shown in the drawing.
- the lifting elements of the lifting device are adaptively connected to the closure frame 6.
- the lifting elements of the lifting device may be hydraulic cylinders or pneumatic cylinders. Furthermore, they can be designed as a linear unit consisting of a rotor and a housing of a linear motor.
- FIG. 2 shows the open device, without the adapter plates 12.
- the closure frame 6 is moved in the lower position by the lifting element of the lifting device, the laterally folded walls 4 applying to the frame of FIG. closure 6 with the closing cams 7 on the bearings 8.
- the bottom plate 2 is equipped with the filter elements 1 in a mobile package or the particulate filter formed from the package is removed by a process of drying.
- This device has the particular advantage that the closing forces and closing speeds of the closing frame 6 are controllable by means of the electronically controlled lifting device.
- the installation comprises the device previously described, in combination for example with spacing means (not shown in Figure 3) and means (14) for injecting a cement between the monolithic elements 1 to be assembled.
- the method of implementing the installation comprises the following steps:
- the elements are placed in the device held in the open position (see Figure 2).
- the elements are placed, still approximate, depending on their respective position in the final assembly.
- the device is initially closed, by moving the closure frame 6 and the walls 4 in their upper position (see Figure 1), to obtain the best positioning of the elements relative to each other.
- the device is then partially open, the walls 4 typically forming an angle between 20 and 50 ° with the vertical.
- a metal frame 14 comprising vertical and horizontal hollow tubes for the passage of the grouting cement is positioned above the elements, as shown in Figure 3.
- the frame is adapted to the configuration and arrangement of the elements in the device.
- the horizontal hollow tubes are equipped in their lower part with grouting cement injection nozzles.
- the elements are spread by tilting towards the walls (4) for example by means of a pneumatic handling system of a known type (not shown in FIG. 3), comprising, for example, gripping fingers in a cylindrical form, with preferably a tip for example based on silicone rubber or any other equivalent means to reduce finger abrasion and avoid deterioration of the elements.
- a pneumatic handling system of a known type (not shown in FIG. 3), comprising, for example, gripping fingers in a cylindrical form, with preferably a tip for example based on silicone rubber or any other equivalent means to reduce finger abrasion and avoid deterioration of the elements.
- the distance 13 thus obtained between the upper edges of the elements 1 then allows the descent of the frame 14 between the elements, as shown in Figure 3.
- the spacing between the side walls 4 has been exaggerated on When the frame is in its lowest position, the grouting cement is injected gradually by the nozzles, so as to fill the space between the elements from bottom to top.
- the injection of the cement is coordinated with a progressive upward movement of the frame 14 and closure of the partitions 4.
- the closure of the assembly device is regulated by and subject to the position of the frame injection.
- Such an arrangement finally allows to obtain an assembled filter having a uniform and homogeneous joint thickness throughout the volume of the filter.
- the use of the present device in a method of assembling a filter as described above also has the advantage of limiting the frequency of cleaning of the necessary equipment, the cement burrs being mainly concentrated between and on the upper faces of the elements. According to the invention, if burrs form during closure of the box due to increased fluidity of the cement, these remain advantageously concentrated on the support plate or pallet 11.
- the handling system, the mechanical elements of the device or the installation are adapted to ceramic elements when they are abrasive like SiC for example.
- the adapter plates 12 visible in FIG. 1 are surface-treated or based on a material of the Teflon or silicone or steel type. treaties.
- the adaptation plates 12 are chosen to be flexible or plastic to dampen the fall of the ceramic elements and prevent their fracture.
- the plates 12 are connected to the removable walls 4 by a system of springs or of flexible material to further improve the flexibility of the process, in particular with respect to the possible dimensional fluctuations of the elements in the same batch of production or production. 'a lot to another.
- the dimensional tolerances of the elements are adapted to the quality of the required joint: dimensions of the section, perpendicularity of the support face with respect to a lateral face or side faces between them, concavity or convexity of the lateral faces.
- the mechanical strength of the element before assembly is selected and adapted firstly to the pressure exerted by the approximation device and secondly to the counter pressure exerted by the grouting cement.
- Such a choice may in particular be a function of the wall thickness of the element, its geometry and its porosity.
- the particle size and the rheology of the grouting cement for assembly are adapted according to the techniques of the art to the chosen mode of implementation and the dimensional characteristics of the required joint.
- the cement or glue has a plasticity adapted to allow it to undergo compression during shaping.
- the cement must have rheological properties allowing its injection without excessive difficulties, a drying time and / or hardening adapted to avoid a catch too fast or clogging of the injection nozzles for example, and preferably a behavior of preferably shear thinning so as not to plug the injection nozzles.
- the device according to the invention has in its closed position an inner shape and volume close to the shape and volume of the assembled filter finally obtained, taking into account the size of the joints between the elements.
- a device is for example consisting of an outer frame that rises and whose speed can be adjusted in combination with closing cams so as to obtain a homogeneous and guided movement of the walls.
- the closure frame has for example stop adjustment bolts to control the pressure exerted on the elements so as not to break them.
- the device is closed at a level that does not correspond to the maximum height of the closure frame but to a fraction thereof, typically about 90%, so that the elements can still slide between them and reposition themselves at the same height on the bottom plate.
- the repositioning in height of the elements thus makes it possible to obtain a good improved flatness of the assembled filter.
- a plate, weight and shape adjusted, is disposed and comes to rest on all the elements after removal of the injection frame. This variant further improves the control of the flatness of the input and output faces of the filter.
- the setting or curing of the adhesive or cement before demolding the assembled filter can be made cold by adding one or more setting accelerators in the cement or by adding IR or UV radiation, microwave, or by any other known means for providing heat.
- the channels opening at each end of the elements are previously alternately plugged before assembly, on the model described for example in applications EP 1508416 or EP 1516658 but optionally, they may also not be plugged.
- the elements may include, but not necessarily, a spacer to control the joint thickness.
- the elements may have been prepared to have different areas of adhesion, as described for example in the applications FR 2853256 or EP 1591431.
- the elements can take all possible forms for the assembly. They may for example have a square or rectangular, triangular, hexagonal, etc. or a mixture of these forms.
- a self-rolling cement is used as a grouting cement.
- the necessary amount of cement is not injected but is simply deposited by appropriate means by simple gravity, that is to say only under the effect of its own weight, between the elements.
- self-rolling cement is understood to mean refractory mortars of the self-flow type, termed "self-flow" in English according to the terminology defined by the ASTM C71 standard "Standard terminology relating to refractories". Typically, they are wet mixtures that can be implemented without vibration or external energy input, without causing segregation. List of landmarks
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Ceramic Engineering (AREA)
- Mechanical Engineering (AREA)
- Filtering Materials (AREA)
- Filtering Of Dispersed Particles In Gases (AREA)
- Producing Shaped Articles From Materials (AREA)
- Control Of Motors That Do Not Use Commutators (AREA)
- Cooling Or The Like Of Electrical Apparatus (AREA)
- Filtration Of Liquid (AREA)
Abstract
Description
Claims
Priority Applications (8)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP06726219A EP1877157B1 (fr) | 2005-04-11 | 2006-03-06 | Dispositif, installation et procede d'alignement et/ou d'assemblage d'elements de filtration |
BRPI0609415-5A BRPI0609415A2 (pt) | 2005-04-11 | 2006-03-06 | dispositivo e processo de alinhamento e/ou de montagem de elementos de filtração e instalação para a montagem de um filtro a partir de elementos de filtração |
DE602006002128T DE602006002128D1 (de) | 2005-04-11 | 2006-03-06 | Vorrichtung, anlage und verfahren zum ausrichten und/oder montieren von filterelementen |
AU2006234562A AU2006234562A1 (en) | 2005-04-11 | 2006-03-06 | Device, installation and method for aligning and/or assembling filtering elements |
CA002604712A CA2604712A1 (fr) | 2005-04-11 | 2006-03-06 | Dispositif, installation et procede d'alignement et/ou d'assemblage d'elements de filtration |
JP2008505931A JP2008536052A (ja) | 2005-04-11 | 2006-03-06 | フィルタ要素を整列及び/又は組み立てるための装置、設備、及び方法 |
US11/911,210 US20090126863A1 (en) | 2005-04-11 | 2006-03-06 | Device, installation and method for aligning and/or assembling filtering elements |
PL06726219T PL1877157T3 (pl) | 2005-04-11 | 2006-03-06 | Urządzenie, instalacja i sposób wyrównania i/lub montażu elementów filtrujących |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE200520005782 DE202005005782U1 (de) | 2005-04-11 | 2005-04-11 | Vorrichtung zum Aneinanderreihen von Filterelementen eines Partikelfilters |
DE202005005782.7 | 2005-04-11 |
Publications (1)
Publication Number | Publication Date |
---|---|
WO2006108973A1 true WO2006108973A1 (fr) | 2006-10-19 |
Family
ID=34833390
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/FR2006/050195 WO2006108973A1 (fr) | 2005-04-11 | 2006-03-06 | Dispositif, installation et procede d'alignement et/ou d'assemblage d'elements de filtration |
Country Status (12)
Country | Link |
---|---|
US (1) | US20090126863A1 (fr) |
EP (1) | EP1877157B1 (fr) |
JP (1) | JP2008536052A (fr) |
CN (1) | CN101193689A (fr) |
AT (1) | ATE403484T1 (fr) |
AU (1) | AU2006234562A1 (fr) |
BR (1) | BRPI0609415A2 (fr) |
CA (1) | CA2604712A1 (fr) |
DE (2) | DE202005005782U1 (fr) |
PL (1) | PL1877157T3 (fr) |
RU (1) | RU2007141643A (fr) |
WO (1) | WO2006108973A1 (fr) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2010222156A (ja) * | 2009-03-20 | 2010-10-07 | Tokyo Yogyo Co Ltd | 吸水性セラミックス構造体の充填部形成方法及びその充填部形成方法により充填部が形成された吸水性セラミックス構造体 |
EP3224010A2 (fr) * | 2014-11-25 | 2017-10-04 | Corning Incorporated | Appareil et procédé de fabrication de corps en nid d'abeilles en céramique |
CN107596816B (zh) * | 2017-05-19 | 2019-10-25 | 朱飞龙 | 一种可一键拆卸的空气净化装置 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3582301A (en) * | 1968-10-07 | 1971-06-01 | Corning Glass Works | Method for forming glass-ceramic honeycomb structures |
DE3132666A1 (de) * | 1981-08-18 | 1983-03-17 | Krauss-Maffei AG, 8000 München | Vorrichtung zum verbinden mehrerer baustoffsteine mittels eines kunststoffes |
WO2004031101A1 (fr) * | 2002-10-07 | 2004-04-15 | Ibiden Co., Ltd. | Corps structural en nid d'abeilles |
WO2004063122A1 (fr) * | 2003-01-14 | 2004-07-29 | Ngk Insulators, Ltd. | Procede d'assemblage d'un corps de structure en nid d'abeilles en ceramique |
EP1468801A1 (fr) * | 2002-01-24 | 2004-10-20 | Ngk Insulators, Ltd. | Dispositif et procede destines a joindre des corps structuraux de ceramique |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2708862A (en) * | 1951-01-11 | 1955-05-24 | Perilli Louis | Box blank setting up machine |
-
2005
- 2005-04-11 DE DE200520005782 patent/DE202005005782U1/de not_active Expired - Lifetime
-
2006
- 2006-03-06 US US11/911,210 patent/US20090126863A1/en not_active Abandoned
- 2006-03-06 RU RU2007141643/15A patent/RU2007141643A/ru unknown
- 2006-03-06 WO PCT/FR2006/050195 patent/WO2006108973A1/fr active IP Right Grant
- 2006-03-06 CN CNA2006800202628A patent/CN101193689A/zh active Pending
- 2006-03-06 DE DE602006002128T patent/DE602006002128D1/de active Active
- 2006-03-06 AT AT06726219T patent/ATE403484T1/de not_active IP Right Cessation
- 2006-03-06 PL PL06726219T patent/PL1877157T3/pl unknown
- 2006-03-06 JP JP2008505931A patent/JP2008536052A/ja active Pending
- 2006-03-06 CA CA002604712A patent/CA2604712A1/fr not_active Abandoned
- 2006-03-06 AU AU2006234562A patent/AU2006234562A1/en not_active Abandoned
- 2006-03-06 EP EP06726219A patent/EP1877157B1/fr not_active Not-in-force
- 2006-03-06 BR BRPI0609415-5A patent/BRPI0609415A2/pt not_active Application Discontinuation
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3582301A (en) * | 1968-10-07 | 1971-06-01 | Corning Glass Works | Method for forming glass-ceramic honeycomb structures |
DE3132666A1 (de) * | 1981-08-18 | 1983-03-17 | Krauss-Maffei AG, 8000 München | Vorrichtung zum verbinden mehrerer baustoffsteine mittels eines kunststoffes |
EP1468801A1 (fr) * | 2002-01-24 | 2004-10-20 | Ngk Insulators, Ltd. | Dispositif et procede destines a joindre des corps structuraux de ceramique |
WO2004031101A1 (fr) * | 2002-10-07 | 2004-04-15 | Ibiden Co., Ltd. | Corps structural en nid d'abeilles |
WO2004063122A1 (fr) * | 2003-01-14 | 2004-07-29 | Ngk Insulators, Ltd. | Procede d'assemblage d'un corps de structure en nid d'abeilles en ceramique |
Also Published As
Publication number | Publication date |
---|---|
CN101193689A (zh) | 2008-06-04 |
EP1877157B1 (fr) | 2008-08-06 |
CA2604712A1 (fr) | 2006-10-19 |
PL1877157T3 (pl) | 2009-02-27 |
DE602006002128D1 (de) | 2008-09-18 |
DE202005005782U1 (de) | 2005-08-04 |
ATE403484T1 (de) | 2008-08-15 |
JP2008536052A (ja) | 2008-09-04 |
RU2007141643A (ru) | 2009-05-20 |
BRPI0609415A2 (pt) | 2011-10-11 |
AU2006234562A1 (en) | 2006-10-19 |
EP1877157A1 (fr) | 2008-01-16 |
US20090126863A1 (en) | 2009-05-21 |
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