WO2006098153A1 - Papier de cigarette possedant des proprietes de faible propagation du feu - Google Patents

Papier de cigarette possedant des proprietes de faible propagation du feu Download PDF

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Publication number
WO2006098153A1
WO2006098153A1 PCT/JP2006/303861 JP2006303861W WO2006098153A1 WO 2006098153 A1 WO2006098153 A1 WO 2006098153A1 JP 2006303861 W JP2006303861 W JP 2006303861W WO 2006098153 A1 WO2006098153 A1 WO 2006098153A1
Authority
WO
WIPO (PCT)
Prior art keywords
wrapping paper
combustion
cigarette
tobacco rod
amount
Prior art date
Application number
PCT/JP2006/303861
Other languages
English (en)
Japanese (ja)
Inventor
Takaaki Matsufuji
Takashi Kominami
Ken Uyama
Original Assignee
Japan Tobacco Inc.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Japan Tobacco Inc. filed Critical Japan Tobacco Inc.
Priority to CA2599753A priority Critical patent/CA2599753C/fr
Priority to JP2007508061A priority patent/JP4335944B2/ja
Priority to ES06714979.9T priority patent/ES2542848T3/es
Priority to CN2006800067255A priority patent/CN101133214B/zh
Priority to EP06714979.9A priority patent/EP1867782B1/fr
Publication of WO2006098153A1 publication Critical patent/WO2006098153A1/fr
Priority to US11/896,849 priority patent/US20080011312A1/en
Priority to HK08103654.3A priority patent/HK1113502A1/xx

Links

Classifications

    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/63—Inorganic compounds
    • D21H17/67—Water-insoluble compounds, e.g. fillers, pigments
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D1/00—Cigars; Cigarettes
    • A24D1/02—Cigars; Cigarettes with special covers
    • A24D1/025—Cigars; Cigarettes with special covers the covers having material applied to defined areas, e.g. bands for reducing the ignition propensity
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/04—Tobacco smoke filters characterised by their shape or structure
    • A24D3/048—Tobacco smoke filters characterised by their shape or structure containing additives
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H19/00—Coated paper; Coating material
    • D21H19/10—Coatings without pigments

Definitions

  • the present invention relates to a low-fire-spreading cigarette paper, and more particularly, to a cigarette-wrapping paper having both low fire-spreading properties and a low CZT ratio.
  • the cigarette roll is provided with a band coated with a flame retardant material on the base wrapping paper so that it does not spread easily on the floor.
  • a flame retardant material on the base wrapping paper so that it does not spread easily on the floor.
  • This technology provides high flammability, low flammability, and low flammability areas on tobacco paper, and is capable of smoking in areas where flammability is high. Low flammability! This is based on the knowledge that cigarettes can self-extinguish when there is a substance to be fired.
  • the carbon monoxide Z tar ratio (CZT ratio) per cigarette is not sufficiently low.
  • an object of the present invention is to provide a cigarette wrapping paper that exhibits low fire spread and a low CZT ratio.
  • a basis weight in the one surface of the base wrapping paper is 16 ⁇ 22g / m 2
  • burn suppressing agent is applied
  • a low fire spread cigarette wrapping paper is provided in which combustion suppression regions are provided separately, and the total amount of the combustion inhibitor applied is 0.2 to 1.8 g per area lm 2 of the applied portion.
  • FIG. 1 is a partially broken schematic perspective view showing an example of a cigarette mounted with a cigarette wrapping paper according to one embodiment of the present invention.
  • the cigarette wrapping paper of the present invention is obtained by discretely providing a combustion suppression region in which a combustion inhibitor is applied to a base wrapping paper.
  • the base wrapping paper contains a force filler that is based on pulp such as ordinary flax pulp that is normally used as cigarette wrapping paper for cigarettes at a rate of 2 to 6 g / m 2. , the basis weight is 16 ⁇ 22gZm 2.
  • the filler may be a commonly used material such as a carbonate such as calcium carbonate or potassium carbonate, or a hydroxide such as calcium hydroxide or calcium hydroxide. wear.
  • a combustion modifier such as citrate or a salt thereof (sodium salt, potassium salt) may be added.
  • the combustion modifier is used in a proportion of up to 2% by weight in the base paper when blended.
  • combustion suppression regions formed by application of a combustion inhibitor are discretely provided.
  • the combustion suppression region can be provided in the form of a plurality of stripes extending in the longitudinal direction of the tobacco rod and spaced apart from each other in the circumferential direction of the tobacco rod. It can be provided in the form of a plurality of rings extending in the circumferential direction of the rod and spaced apart from each other in the longitudinal direction of the tobacco rod.
  • the total coating amount (dry basis) of the combustion inhibitor is 0.2 to 1.8 g per area lm 2 of the coated part.
  • Combustion inhibitors include, for example, proteins such as gelatin, casein, albumin, dartene; starch, xanthan gum (echo gum), locust bean gum, guagam (guavac), tragacanth gum, tara gum, tamarind seed polysaccharide (glyroid) ) Polysaccharides with thickening action such as cara gum, arabic gum, pullulan, dextrin, cyclodextrin (oligoseven), gutty; carrageenan, curdlan, agar, gelatin, farcellulan, pectin, dielan gum, kelcogel, etc.
  • proteins such as gelatin, casein, albumin, dartene; starch, xanthan gum (echo gum), locust bean gum, guagam (guavac), tragacanth gum, tara gum, tamarind seed polysaccharide (glyroid)
  • Polysaccharides with thickening action such as cara gum, arabic gum
  • Fine cellulose, microcrystalline cellulose, flax pulp and wood pulp also have the same effect.
  • combustion inhibitors can be used alone or as a mixture of two or more.
  • Sodium alginate is commercially available in various polymerization degree ranges. In the present invention, sodium alginate having a polymerization degree of 500 to 900 is preferred! /. Thus, the sodium salt of alginic acid having a high degree of polymerization exhibits a high combustion suppressing action even in a small amount.
  • the low-flammability wrapping paper of the present invention is equipped with a tobacco rod that also has the strength of cigarette chopping, and usually the surface coated with a combustion inhibitor is in contact with the tobacco rod.
  • FIG. 1 shows a cigarette fitted with a cigarette wrapping paper to which a combustion modifier is applied in the form of a ring.
  • a cigarette 10 has a tobacco rod 11 made of a tapaco filler 13 mounted in a column shape with a base wrapping paper 12.
  • the base wrapping 12 can have a natural air permeability of 10 to 100 cholesterol units.
  • the tobacco rod 11 typically has a circumferential length of 17 mm to 26 mm and a length of 49 mm to 90 mm.
  • a normal filter 18 can be attached to the base end of the tobacco rod 11 (that is, the downstream end in the suction direction) l ib using a tip paper 17 by a conventional method.
  • annular region 14 to which a combustion inhibitor is applied is formed to define a combustion suppression region.
  • annular combustion suppression regions 14 are provided as shown in FIG. 1, they are formed apart from each other in the longitudinal direction of the tobacco rod.
  • a normal combustion region 15 to which no combustion regulator is applied is defined. Since this region 15 is constituted by the base wrapping 12 portion, it can be burned in a normal smoking state as the base wrapping 12 itself. Therefore Region 15 acts as a normal combustion region.
  • the annular combustion suppression region 14 may have a width in the longitudinal direction of 4 mm to 7 mm and a thickness of typically 0.1 to 5 / zm. When multiple combustion suppression areas are provided, the interval between adjacent combustion suppression areas 14 is 18mn! It is preferably ⁇ 25mm.
  • a combustion inhibitor is applied to the region 16 where the tip force is also separated by a distance d.
  • the portion also constitutes a normal combustion region 16 and can correspond to a region where combustion is performed with one or two puffs of a normal cigarette.
  • the distance d can be set to 10 mm to 25 mm from the tobacco rod tip 11a. It is not particularly necessary to form the combustion suppression region 14 on the inner surface of the wrapping paper corresponding to the portion of the paper 12 covered with the chip paper 17.
  • the cigarette 10 when the cigarette 10 is ignited at the tip 11a of the cigarette rod 11, sucked, and the cigarette is burned, in the normal combustion region 15, it can be burned in the same manner as a normal cigarette, and the taste can be enjoyed.
  • a combustible material such as carpet, tatami mat, wooden product, cloth, clothes, etc. in an ignited state, it is contained in the combustion suppression region 14 existing in the combustion direction, the heat absorption by the combustible material and the tobacco filler The cigarette 10 is extinguished in combination with the blown tobacco cigarette, and the spread of combustible materials is suppressed.
  • the cigarette equipped with the cigarette paper of the present invention has a low CZT ratio in the mainstream smoke.
  • Base wrapping paper (27mm wide, 1.500m long) with specifications shown in Table 1 and sodium alginate aqueous solution of various concentrations (0.5-20% by weight) with a constant width of 7mm in the longitudinal direction and a constant value of 20mm
  • a total of 56 areas for applying the combustion inhibitor were provided by applying (printing) in a striped pattern with a direct gravure method.
  • the total application amount of sodium alginate was measured by the following method. The results are also shown in Table 1.
  • Examples 1-13 The application amount of the combustion inhibitor was 0.2 to 1.8 g per lm 2 of the area where the combustion inhibitor (sodium alginate) was applied.
  • the sodium alginate used was I-S manufactured by KIMIKA (registered trademark) (polymerization degree 650 to 670; viscosity at 25 ° O of 3% by weight aqueous solution 29976.9 cP) In other examples, it was IL 2 manufactured by KIMIKA (registered trademark) (polymerization degree: 30 to 180; viscosity at 25 ° C. of 3 wt% aqueous solution: 907.2 cP).
  • a tobacco rod made of American blend chopping (tar amount in the case without a filter: 19-20 mg) is equipped, and the first 5 mm wide from the cigarette burning tip It cut
  • the cigarette length per piece was 59 mm, and there were two areas where the flame retardant was applied.
  • the obtained cigarette was subjected to a fire spread test according to ASTM E-2187-04, and a PFLB (percent fol Hength burn) value was measured.
  • PFLB percent fol Hength burn
  • Sodium alginate standard solution (1 wt% aqueous sodium bicarbonate solution containing sodium alginate at a concentration of 0 to 0.2 mgZmL) -Add 2 mL of hydrochloric acid solution (8.5 M hydrochloric acid containing 0.05 wt% copper sulfate) and 1 mL of naphtholesol cinol solution (0.4 wt% 1,3-dihydroxynaphthalene aqueous solution) and heat in a boiling water bath for 65 minutes Then, cool in ice water, add 4 mL of butyl acetate, shake, and centrifuge.
  • hydrochloric acid solution 8.5 M hydrochloric acid containing 0.05 wt% copper sulfate
  • naphtholesol cinol solution 0.4 wt% 1,3-dihydroxynaphthalene aqueous solution
  • cigarette smoke was collected using an 8-split linear smoker (SM342) manufactured by FILTRONA.
  • Cigarettes were burned in accordance with ISO standards by sucking 35 mLZ for 2 seconds at intervals of 60 seconds, and collecting the smoke that passed through the glass fiber filter in a gas bag.
  • the cigarette sample reached the standard combustion length (5 lmm from the ignition end of the cigarette (the boundary force between the paper roll and tip paper was also 8 mm)
  • suction was stopped. The number of puffs so far was recorded.
  • three empty puffs were performed. In this way, the gas of the cigarette sample was collected in the gas bag, and the total flow material (TPM) was collected in the glass fiber filter.
  • TPM total flow material
  • the amount of CO per cigarette sample was measured with a CO measuring device manufactured by FILTRONA.
  • the total amount of combustion inhibitor applied is 0.2 to 6% on the surface of the base wrapping paper containing 2 to 6 gZm 2 of filler and having a basis weight of 16 to 22 gZm ′. 1. It can be seen that the ones in which the combustion inhibitor was applied in a discrete manner so as to be 8 gZm 2 (Examples 1 to 13) showed low combustibility and low CZT ratio.
  • a cigarette wrapping paper that exhibits low fire spreadability and a low CZT ratio.

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  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)
  • Paper (AREA)

Abstract

L’invention concerne un papier de cigarette possédant des propriétés de faible propagation du feu, comprenant une base de papier pour filtres d’un grammage de 16 à 22 g/m2, contenant des charges en quantité allant de 2 à 6 g/m2, et, discrètement disposées sur une de ses surfaces principales, des régions de combustion retardée enduites d’un retardateur de combustion, la quantité totale de retardateur de combustion enduit par m2 de zone enduite étant compris entre 0,2 et 1,8 g.
PCT/JP2006/303861 2005-03-15 2006-03-01 Papier de cigarette possedant des proprietes de faible propagation du feu WO2006098153A1 (fr)

Priority Applications (7)

Application Number Priority Date Filing Date Title
CA2599753A CA2599753C (fr) 2005-03-15 2006-03-01 Papier a cigarettes a faible pouvoir propagateur de flamme
JP2007508061A JP4335944B2 (ja) 2005-03-15 2006-03-01 低延焼性のシガレット用巻紙
ES06714979.9T ES2542848T3 (es) 2005-03-15 2006-03-01 Papel de cigarrillo con baja propagación de la llama
CN2006800067255A CN101133214B (zh) 2005-03-15 2006-03-01 低火焰蔓延性的卷烟用卷纸
EP06714979.9A EP1867782B1 (fr) 2005-03-15 2006-03-01 Papier de cigarette a faible propagation du feu
US11/896,849 US20080011312A1 (en) 2005-03-15 2007-09-06 Low flame-spreading cigarette paper
HK08103654.3A HK1113502A1 (en) 2005-03-15 2008-04-02 Cigarette paper of low fire-spreading property

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2005-073055 2005-03-15
JP2005073055 2005-03-15

Related Child Applications (1)

Application Number Title Priority Date Filing Date
US11/896,849 Continuation US20080011312A1 (en) 2005-03-15 2007-09-06 Low flame-spreading cigarette paper

Publications (1)

Publication Number Publication Date
WO2006098153A1 true WO2006098153A1 (fr) 2006-09-21

Family

ID=36991505

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2006/303861 WO2006098153A1 (fr) 2005-03-15 2006-03-01 Papier de cigarette possedant des proprietes de faible propagation du feu

Country Status (12)

Country Link
US (1) US20080011312A1 (fr)
EP (1) EP1867782B1 (fr)
JP (1) JP4335944B2 (fr)
KR (1) KR100956462B1 (fr)
CN (1) CN101133214B (fr)
CA (1) CA2599753C (fr)
ES (1) ES2542848T3 (fr)
HK (1) HK1113502A1 (fr)
RU (1) RU2357622C1 (fr)
TW (1) TWI302090B (fr)
UA (1) UA90299C2 (fr)
WO (1) WO2006098153A1 (fr)

Cited By (5)

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Publication number Priority date Publication date Assignee Title
WO2009022545A1 (fr) * 2007-08-10 2009-02-19 Japan Tobacco Inc. Papier à rouler les cigarettes à extension de combustion lente
WO2009139228A1 (fr) * 2008-05-16 2009-11-19 日本たばこ産業株式会社 Processus de fabrication de papier pour filtres à cigarette à faible inflammabilité
WO2010055806A1 (fr) * 2008-11-12 2010-05-20 日本たばこ産業株式会社 Papier à rouler pour cigarette à faible propension à l'allumage
JP2010537066A (ja) * 2007-08-23 2010-12-02 フィリップ・モーリス・プロダクツ・ソシエテ・アノニム 見当合わせした帯付きシガレット紙、シガレット、及び製造方法
US11547140B2 (en) 2006-03-31 2023-01-10 Philip Morris Usa Inc. Banded papers, smoking articles and methods

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UA92852C2 (uk) * 2006-12-11 2010-12-10 Джапан Тобакко Инк. Сигарета з низькою запалювальною здатністю, обгортковий папір для неї і спосіб виготовлення обгорткового паперу
CN101372820B (zh) * 2007-08-21 2010-11-17 马铁良 一种香烟自熄液及其制备方法
ATE488147T1 (de) * 2007-12-20 2010-12-15 Reemtsma H F & Ph Rauchware mit verbesserten auslöscheigenschaften
BRPI0907699A2 (pt) * 2008-02-08 2015-07-21 Japan Tobacco Inc Método de produção para produzir um envoltório para cigarros
KR101050100B1 (ko) * 2008-06-26 2011-07-19 주식회사 케이티앤지 궐련연소 강하제를 처리한 궐련지와 이를 포함하는화재안전 담배
TWI402397B (zh) * 2009-07-13 2013-07-21 Univ Da Yeh The flame retardant is internally filled or coated on the surface of a pulp molded product
CN102666988B (zh) * 2009-11-25 2014-11-19 日本烟草产业株式会社 低延烧性卷纸、其制造方法以及制造机器
ES2554661T3 (es) * 2010-02-26 2015-12-22 Japan Tobacco, Inc. Método de producción y dispositivo de producción para papel recubierto
CN102906334B (zh) * 2010-03-25 2016-08-10 日本烟草产业株式会社 低延烧性卷筒纸的制造机器及其制造方法以及用于香烟的低延烧性卷纸的制造方法
US11707082B2 (en) 2010-12-13 2023-07-25 Altria Client Services Llc Process of preparing printing solution and making patterned cigarette wrapper
US10375988B2 (en) 2010-12-13 2019-08-13 Altria Client Services Llc Cigarette wrapper with novel pattern
KR20140018213A (ko) 2010-12-13 2014-02-12 알트리아 클라이언트 서비시스 인코포레이티드 프린팅 용액의 준비 및 패턴화된 궐련 권지 제조 프로세스
GB201100218D0 (en) * 2011-01-07 2011-02-23 British American Tobacco Co Smoking article
CN102199902B (zh) * 2011-05-13 2014-02-12 民丰特种纸股份有限公司 一种低引燃倾向性卷烟纸及制备方法
CA2833971A1 (fr) 2011-05-16 2012-11-22 Altria Client Services Inc. Motifs alternes dans un papier de cigarette, article a fumer et procede
KR101382650B1 (ko) * 2011-10-25 2014-04-08 주식회사 케이티앤지 저발화성 궐련지의 코팅 조성물 및 이를 이용하는 담배
US11064729B2 (en) 2012-05-16 2021-07-20 Altria Client Services Llc Cigarette wrapper with novel pattern
JP6193363B2 (ja) 2012-05-16 2017-09-06 アルトリア クライアント サービシーズ エルエルシー 開口領域のあるバンドを有するバンド付シガレットラッパー
CN103205913A (zh) * 2013-04-09 2013-07-17 广东中烟工业有限责任公司 烟草纤维在接装原纸上的应用
BR112015032030B1 (pt) * 2013-07-18 2022-01-18 Philip Morris Products S.A. Artigo para fumar e invólucro de artigo para fumar
CN104805730B (zh) * 2015-04-07 2017-04-26 牡丹江恒丰纸业股份有限公司 卷烟纸降低一氧化碳的燃烧抑制组合物及施加、制造方法
CN106690408B (zh) * 2017-01-23 2018-09-11 安徽天翔高新特种包装材料集团有限公司 过滤接装纸的制备方法
US11346051B2 (en) 2017-03-02 2022-05-31 Iiw Entourage Delivery Systems Ltd. Aromatized and flavored paper products
PL3446573T3 (pl) * 2017-08-24 2021-05-04 Jt International S.A. Papier owijający do wyrobu do palenia
GB201803328D0 (en) * 2018-03-01 2018-04-18 British American Tobacco Investments Ltd A gel composition and tobacco industry products including the same
WO2020044343A1 (fr) * 2018-08-31 2020-03-05 Iiw Entourage Delivery Systems Ltd. Produits en papier aromatisés et parfumés comprenant des terpènes et des cannabinoïdes
CN112030605A (zh) * 2020-09-02 2020-12-04 云南中烟工业有限责任公司 一种用于卷烟纸的微生物多糖阻燃涂料及其制备方法和应用
WO2023223266A1 (fr) * 2022-05-20 2023-11-23 Buzzelet Development And Technologies Ltd. Cigarettes contenant du cannabis

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See also references of EP1867782A4 *

Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11547140B2 (en) 2006-03-31 2023-01-10 Philip Morris Usa Inc. Banded papers, smoking articles and methods
KR101201155B1 (ko) * 2007-08-10 2012-11-13 니뽄 다바코 산교 가부시키가이샤 저연소성의 궐련용 권지
JP5037617B2 (ja) * 2007-08-10 2012-10-03 日本たばこ産業株式会社 低延焼性のシガレット用巻紙
EP2177663A4 (fr) * 2007-08-10 2012-10-10 Japan Tobacco Inc Papier à rouler les cigarettes à extension de combustion lente
US8302612B2 (en) 2007-08-10 2012-11-06 Japan Tobacco Inc. Low ignition propensity cigarette paper
WO2009022545A1 (fr) * 2007-08-10 2009-02-19 Japan Tobacco Inc. Papier à rouler les cigarettes à extension de combustion lente
JP2010537066A (ja) * 2007-08-23 2010-12-02 フィリップ・モーリス・プロダクツ・ソシエテ・アノニム 見当合わせした帯付きシガレット紙、シガレット、及び製造方法
JP5000758B2 (ja) * 2008-05-16 2012-08-15 日本たばこ産業株式会社 着火傾向の低いシガレット用巻紙の製造方法
CN101983270B (zh) * 2008-05-16 2012-11-21 日本烟草产业株式会社 低着火倾向的卷烟用卷纸的制造方法
WO2009139228A1 (fr) * 2008-05-16 2009-11-19 日本たばこ産業株式会社 Processus de fabrication de papier pour filtres à cigarette à faible inflammabilité
WO2010055806A1 (fr) * 2008-11-12 2010-05-20 日本たばこ産業株式会社 Papier à rouler pour cigarette à faible propension à l'allumage
CN102216526A (zh) * 2008-11-12 2011-10-12 日本烟草产业株式会社 低延烧性香烟用卷纸
JP5228061B2 (ja) * 2008-11-12 2013-07-03 日本たばこ産業株式会社 低延焼性のシガレット用巻紙
US9903071B2 (en) 2008-11-12 2018-02-27 Japan Tobacco Inc. Low flame-spreading cigarette paper

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EP1867782A4 (fr) 2011-02-23
CN101133214B (zh) 2011-02-09
ES2542848T3 (es) 2015-08-12
UA90299C2 (uk) 2010-04-26
EP1867782A1 (fr) 2007-12-19
KR20070104598A (ko) 2007-10-26
TW200638885A (en) 2006-11-16
US20080011312A1 (en) 2008-01-17
CA2599753A1 (fr) 2006-09-21
JP4335944B2 (ja) 2009-09-30
HK1113502A1 (en) 2008-10-03
CA2599753C (fr) 2011-02-01
CN101133214A (zh) 2008-02-27
EP1867782B1 (fr) 2015-07-15
TWI302090B (en) 2008-10-21
KR100956462B1 (ko) 2010-05-07
JPWO2006098153A1 (ja) 2008-08-21
RU2357622C1 (ru) 2009-06-10

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