WO2005124294A1 - Procede permettant de mesurer le niveau de liquide cryogenique au moyen d'une sonde de niveau - Google Patents

Procede permettant de mesurer le niveau de liquide cryogenique au moyen d'une sonde de niveau Download PDF

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Publication number
WO2005124294A1
WO2005124294A1 PCT/EP2005/006487 EP2005006487W WO2005124294A1 WO 2005124294 A1 WO2005124294 A1 WO 2005124294A1 EP 2005006487 W EP2005006487 W EP 2005006487W WO 2005124294 A1 WO2005124294 A1 WO 2005124294A1
Authority
WO
WIPO (PCT)
Prior art keywords
current
voltage
level
liquid cryogen
superconductive material
Prior art date
Application number
PCT/EP2005/006487
Other languages
English (en)
Inventor
Kevin Jonathan Hickman
Anthony John Salloway
Original Assignee
Siemens Magnet Technology Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from GBGB0413837.6A external-priority patent/GB0413837D0/en
Application filed by Siemens Magnet Technology Ltd filed Critical Siemens Magnet Technology Ltd
Priority to DE112005001261T priority Critical patent/DE112005001261T5/de
Priority to US11/628,722 priority patent/US7966878B2/en
Publication of WO2005124294A1 publication Critical patent/WO2005124294A1/fr

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Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01F—MEASURING VOLUME, VOLUME FLOW, MASS FLOW OR LIQUID LEVEL; METERING BY VOLUME
    • G01F23/00—Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm
    • G01F23/22—Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm by measuring physical variables, other than linear dimensions, pressure or weight, dependent on the level to be measured, e.g. by difference of heat transfer of steam or water
    • G01F23/24—Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm by measuring physical variables, other than linear dimensions, pressure or weight, dependent on the level to be measured, e.g. by difference of heat transfer of steam or water by measuring variations of resistance of resistors due to contact with conductor fluid
    • G01F23/246—Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm by measuring physical variables, other than linear dimensions, pressure or weight, dependent on the level to be measured, e.g. by difference of heat transfer of steam or water by measuring variations of resistance of resistors due to contact with conductor fluid thermal devices

Definitions

  • the present invention relates to a level probe useful for measuring the level of a liquid cryogen.
  • a level probe comprising a length of superconducting material, and an improved method of its use.
  • the present invention relates to the control of a heater for propagating a normal resistive front along the superconducting material of a cryogen level probe, enabling a measurement of liquid cryogen level to be made.
  • Fig. 1 shows a cryostat such as may be employed for holding magnet coils for an MRI (magnetic resonance imaging) system.
  • a cryogenic vessel 1 holds a liquid cryogen 2.
  • the space 3 in the cryogenic vessel above the level of the liquid cryogen may be filled with evaporated cryogen.
  • the cryogenic vessel is contained in a vacuum jacket 4 which serves to reduce the amount of heat flowing to the cryogen 2 from ambient temperature, by reducing the possibility of conduction or convection heating of the cryogen vessel 1.
  • One or more heat shields 5 may be provided in the vacuum space between the cryogenic vessel 1 and the vacuum jacket 4. These shields serve to reduce the amount of radiated heat reaching the cryogenic vessel 1 from the exterior.
  • An access neck 6 is provided, allowing access to the cryogenic vessel from the exterior. This is used to fill the cryogenic vessel, to provide access for current leads and other connections to superconductive coils housed within the cryogenic vessel, and to allow an escape path for boiled-off gaseous cryogen.
  • a guide tube 10 is provided inside the cryogenic chamber for housing a cryogen level probe.
  • the guide tube 10 runs from the access neck 6 to approximately the lower extremity of the cryogenic vessel.
  • the guide tube is not sealed at its end, but fills with liquid cryogen to the level of the liquid cryogen in the cryogenic chamber.
  • the guide tube 10 may house a cryogen level probe for measuring the depth of the liquid cryogen 2 in the cryogenic vessel 1.
  • Fig. 2 shows a cryogen level probe according to the prior art.
  • a protective flexible carrier 20 for example a sleeve or an open-ended, perforated or porous tube of stainless steel, nylon, glass fibre composite, polytetrafluoroethylene or other appropriate material, carries a strip or wire of superconducting material 22.
  • the superconductive strip or wire 22 runs in one direction only down the length of the probe.
  • a return current path conductor 23 is connected to the distal end 24 of the strip or wire of superconducting material 22.
  • This is a normal, resistive material such as copper.
  • Other probe variants include cryogen level probes that have a strip or wire of superconducting material 22 which is bent back on itself, in a U-shape.
  • a small resistance heater 26 is connected to one end of the superconductive strip or wire 22, in close thermal contact with it.
  • the heater may have a resistance of the order of 4 ⁇ , and must be made of a material which is resistive at the temperatures of interest. For example, Ni-chrome or Constantan wire maintains a high electrical resistance, even at temperatures of about 4K.
  • a current source 28 is provided, and in use supplies a current / through the series combination of the heater 26, superconductive strip or wire 22 and the return current path conductor 23.
  • a differential amplifier 30 or other appropriate detector is connected by voltage sensing leads 25, 27, respectively to the superconductive strip or wire 22 just below the heater 26, and to the distal end of the superconductive strip or wire 22.
  • the differential amplifier 30 or other appropriate detector detects the presence of any voltage across the part of the superconductive strip or wire 22 which lies between the respective connection points of the voltage sensing leads.
  • the voltage detector is connected to different points on the strip or wire of superconducting material 22.
  • the voltage sensing leads can be connected to the ends of the strip or wire of superconducting material 22.
  • the upper voltage sensing lead 25 may be connected some distance below the heater, to provide a cryogen level probe which will give a full level (100%) when the cryostat is filled with less helium.
  • the cryogen level probe is dipped into the liquid cryogen to be measured, for example by sliding it into the guide tube 10 illustrated in Fig. 1.
  • the heater 26 heats adjacent part(s) of the superconductive strip or wire 22 above the critical temperature, and such part(s) become(s) resistive.
  • both ends of the strip or wire of superconducting material 22 may be heated, and become resistive.
  • the heater and any further heat supplied by the resistive part(s) of the superconductive strip or wire 22 causes a normal resistive front to propagate down the superconductive strip or wire 22 until the front reaches the level of the cryogen. Below this point, the cryogen maintains the superconductive strip or wire 22 below its critical temperature.
  • the length of the resistive part and hence the level of the cryogen may be determined by supplying a current i through the strip or wire of superconducting material 22 and measuring the resultant voltage across it.
  • This voltage indicated by the output of the differential amplifier 30 or another suitable sensor, will be proportional to the (total) length of the resistive part(s) of the superconductive strip or wire 22, so indicating the amount of superconductive strip or wire 22 which is above the level of the liquid cryogen and so indicating the level of the liquid cryogen.
  • Such apparatus is described, for example, in United States patents 3,496,773 and 3,943,767.
  • a small read current is applied to the heater and the superconductive strip or wire 22.
  • the heater may or may not heat sufficiently to quench the adjacent part of the superconductive strip or wire 22, depending on its temperature at the start of the measurement process. If the read current is too low, the quench process will not begin, and no normal resistive (quench) front will propagate. If the read current is too high, the heat generated by the superconductive strip or wire 22 may form a gas blanket around the superconductive strip or wire 22 under the surface of the liquid cryogen, and a lower-than-actual level of liquid cryogen will be indicated. In an extreme case, an empty level may be indicated if the read current is sufficient to generate a gas blanket around the superconductive strip or wire 22 right to its lower extremity.
  • Fig. 3 shows a current pulse applied by current source 28 to the series combination of the heater 26 and the superconductive strip or wire 22.
  • the current i rises sharply to a brief peak value before dropping to a steady value for a relatively long period of time.
  • the relatively lengthy steady phase may represent a current of 250mA for a time period of about 10 seconds, while the brief peak may represent a current of 400mA which lasts for about 20ms.
  • the intended operation of the level probe is as follows. The brief peak of high value current was intended to heat an adjacent part of the superconductive strip or wire 22 above its critical temperature. This part then becomes resistive.
  • the heat produced by resistor 26 and the additional heat produced by the measurement current flowing through the resistive part of the superconductive strip or wire 22 will propagate the normal resistive (quench) front to the surface of the liquid cryogen, where propagation will stop, since the remainder of the superconductive strip or wire 22 is held below its critical temperature by the liquid cryogen.
  • the voltage across the superconductive strip or wire 22, as detected by differential amplifier 30 or another suitable detector is recorded. The depth of cryogen in the cryogen vessel is calculated from this detected voltage.
  • United States patent 3,943,767 describes a method of operation of a liquid cryogen level sensor such as that shown in Fig. 2. According to that document, a constant read current is applied to the superconductive strip or wire 22, and the rate of increase of the detected voltage is monitored. When the rate of increase of the voltage falls to near zero, it is assumed that the normal resistive (quench) front has reached the upper surface of the liquid cryogen, the voltage is used to determine the level of the liquid, and the read current is stopped.
  • cryogen level indicating method and apparatus described above is conventional. In this conventional apparatus and method, the following problems are encountered.
  • This method of operation illustrated in Fig. 3 is not very reliable.
  • the short initial peak may not be sufficient to reliably induce quench in the superconductive strip or wire 22. If the magnitude or duration of the short initial peak were increased, then there is a risk of over heating the superconductive wire, so that the normal (quench) front propagates below the surface of the liquid cryogen, giving a falsely low reading of cryogen depth.
  • the cryogen level probe In the presence of boiled-off cryogen in the space 3, the cryogen level probe is cooled by the boiled off cryogen, meaning that it is difficult to propagate a resistive quench front all the way to the surface of the liquid cryogen.
  • This difficulty has been overcome in the past by increasing the current supplied to the heater, to increase the heat supplied to the superconductive strip or wire 22, and improve the resistive quench propagation. This in turn raises further problems.
  • the heat provided by the heater 26 and the resistive parts of the superconductive strip or wire 22 may heat the superconductive strip or wire 22 to such an extent that the quench front is propagated below the surface of the liquid cryogen.
  • the present invention provides an improved method for operating a liquid cryogen level probe such as that illustrated in Fig. 2, in a manner so as to address at least some of the problems of the known methods of operation.
  • Fig. 1 shows a cryostat which may benefit from application of the present invention
  • Fig. 2 shows a liquid cryogen level probe which may be operated according to the present invention
  • Fig. 3 shows a current pulse which rises sharply to a brief peak before dipping to a steady value for a relatively long period
  • Fig. 4 illustrates an arrangement according to an embodiment of the present invention.
  • Fig. 5 shows a current pulse according to an aspect of an embodiment of the present invention.
  • a control circuit 40 is provided, receiving the output of the differential amplifier 30 or other voltage sensor. According to the received output from the differential amplifier 30 or other voltage sensor, the control circuit produces a control signal over feedback path 42 to the current source 28. 1 ⁇
  • the cryogen level probe is operated as follows.
  • a propagation current of relatively high value is first applied through the heater 26, superconductive strip or wire 22 and current return path 23, as instructed by the control circuit 40 to the current source 28. Since the superconductive strip or wire 22 will at least initially be in a superconducting state, no voltage will be detected by detector 30.
  • Control circuit 40 will maintain the current i at its relatively high propagation level. With the current i at such a high value, the adjacent part of the superconductive strip or wire 22 will be quenched, and enter a resistive state. A corresponding voltage will be developed across the corresponding part of the superconductive strip or wire 22, and this voltage will be detected by the detector 30. The detection of this voltage is provided to the control circuit 40. The detection of this voltage indicates that part of the superconductive strip or wire 22 has been quenched, and is in a normal, resistive, mode of conduction.
  • the control circuit 40 is arranged to halt the propagation current being supplied by current source 28 once a certain voltage level has been detected by detector 30.
  • the control circuit 40 may be arranged to halt the propagation pulse once a voltage of 0.5V is measured.
  • the threshold voltage for propagation current turn-off may be set to the voltage corresponding to a "full" level of liquid cryogen.
  • other values and proportions may be chosen, and may be determined to provide optimum performance based on routine trial and error.
  • the current source 28 provides a measurement current enabling propagation of the normal resistive (quench) front to the liquid cryogen surface and measurement of the liquid cryogen level.
  • the magnitudes of the propagation and measurement currents may be, for example, 400mA and 250mA respectively.
  • the duration of the propagation current will depend on the initial temperature of the superconductive strip or wire 22, and so will adapt to the initial temperature of the probe at each measurement. Furthermore, the method of the present invention is reactive to variations in the characteristics of the probe. For example, different probes may need different levels of heating to initiate a quench, and different heaters may provide different heat output for a same applied current.
  • the voltage sense leads 25, 27 connecting the detector 30 to the superconductive strip or wire 22 also provide a thermal drain on the heater.
  • the guide tube 10 shown in Fig. 1 will have a certain thermal conductivity, and will be in contact with the level probe at certain points. This will accordingly present an unpredictable thermal load, and may prevent quench initiation in known arrangements.
  • the gaseous cryogen within the cryogen vessel 1 may be stratified, meaning that the ambient temperature experienced by the heater is higher than the boiling point of the cryogen. In this case, the amount of heat required to begin a quench will be reduced compared to the amount of heat required to commence a quench from the lower boiling point temperature which may be expected.
  • the present invention by using feedback of measured voltage across the superconductive strip or wire 22, ensures that quench propagation begins, but heating stops as soon as possible, to avoid measurement errors introduced by over-heating of the superconductive strip or wire 22, and reduces to a minimum the level of cryogen boil- off caused by the measurement process.
  • the superconducting material is provided with a cupro- nickel cladding. This provides the wire with a known resistance per unit length when the superconductor element is in the normal state and gives the wire a low temperature coefficient of resistance.
  • the superconducting material itself may be any superconducting material having a transition temperature above the boiling point of the liquid cryogen.
  • a Niobium-Titanium (Nb-Ti) superconducting alloy having a critical temperature of 9K may be suitable for systems using liquid helium as the cryogen.
  • fluctuations may be introduced into the measurement current, for example a ⁇ 10% variation. If the measured voltage indicated by detector 30 also fluctuates by a corresponding ⁇ 10%, one may be sure that the resistive quench front has propagated to the surface of the liquid cryogen. If the normal (quench) front has not propagated to the surface of the liquid cryogen, the measurement current would still likely be aiding propagation of the front. In this case, the ⁇ 10% variation in the measurement current would not produce a corresponding variation in the voltage detected by detector 30. In response to the absence of detection of corresponding fluctuations, the measurement current may be continued to be applied until such corresponding fluctuations are detected.
  • Another improvement to the method of the current invention is to detect changes in the voltage detected when the superconducting wire or strip of the probe has a normal front which has propagated to the level of the cryogen and the measurement current is being used to determine the liquid cryogen level.
  • the voltage oscillates due to the liquid level changing as a result of the localised gas movement and hence effective liquid level change. If the superconducting wire or strip of the probe has a normal front which has propagated so the normal resistive front moves down the superconductive strip or wire 22, the voltage detector (30) may give a constant voltage reading indicating a particular cryogen liquid level.
  • the level indicated by the constant voltage output of the probe may be spurious and not representative of the liquid cryogen level, but may rather indicate the location of a thermal load on the probe.
  • the voltage from the detector (30) needs to be examined. As the measurement current flows through the resistive (quenched) part of the superconductive strip or wire 22, heat is generated. This heat will cause boiling of the surface of the liquid cryogen, at least in the vicinity of the superconductive strip or wire 22 where it meets the surface of the liquid cryogen. The boiling effect will cause small variations in the level of the liquid cryogen, and so small variations in the measured voltage.
  • the voltage level can be used to give the correct liquid cryogen fill level. If voltage oscillations cannot be detected, the normal propagation front on the superconductive strip or wire 22 may have "stuck". This will occur if the heat causing the normal front to propagate down the superconductive strip or wire 22 is conducted away from the superconductive strip or wire 22 due to its contact with other materials. In this case, additional heat needs to be generated in the superconductive strip or wire 22 so that the resistive front can propagate further. Under these conditions, the current from the constant current source would be increased to allow the level to be detected which would be verified by the detection of the voltage oscillations at another detected voltage level.
  • the propagation current applied to the heater may not be a constant current, but may be ramped.
  • the propagation current i applied to the heater 26 and the superconductive strip or wire 22 may have the time profile as shown in Fig. 5.
  • the applied propagation current i initially rises very sharply, with the rate of increase gradually slowing as the magnitude of propagation current i increases.
  • the current increases rapidly to values which may be expected to cause the heater to cause propagation of the normal front.
  • the rate of change of the current is reduced at this point to allow the propagation heater current to be turned off as soon as normal resistive wire is detected.
  • the voltage detector 30 will detect a corresponding voltage, being a product of the resistance of the quenched part of the superconductive strip or wire 22 and the magnitude of the current i.
  • the magnitude of this voltage will increase with the increasing magnitude of current i and also with the increasing resistance of the superconductive strip or wire 22 as the normal (quench) front propagates towards the surface of the liquid cryogen.
  • a signal is sent along the feedback path 42 to control the current source 28 so as to reduce current i to its measurement value.
  • a certain delay period is allowed to ensure that the normal resistive (quench) front has propagated to the surface of the liquid cryogen, and the voltage detected by the detector 30 at time t m is recorded, for example by the control circuit 40, and used to determine the level of the liquid cryogen.
  • the method of the present invention may be applied to probes such as those illustrated in Figs 2 and 4, in which the superconductive strip or wire 22 runs in one direction only along the length of the probe.
  • the present invention may also be applied to probes which have a superconductive strip or wire bet into a U-shape.
  • the voltage sense lead 25 at the heater end of the superconductive strip or wire 22 may be in different positions. This connection may be as shown in figure 4, at the top of the superconductive strip or wire 22 between the superconductive strip or wire 22 and the heater or on the other side of the heater.
  • the threshold voltage to turn off the propagation current to the heater would be different. This voltage would be set so that the superconductive strip or wire 22 under the heater changed into the normal state. Both positions can be used with different threshold voltages to achieve the same improvement in the quench initiation before the read current is enabled.
  • the 100% fill level and scaling can then be changed for any probe configuration.
  • the present invention has been described with particular reference to embodiments in which the heater and the superconducting wire or strip are placed in series, with a single current source providing a current i through the series arrangement.
  • currents may be separately applied to the heater and to the superconducting wire or strip, such that the propagating current is applied only to the heater and the measurement current is applied only to the superconducting wire or strip.

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  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Fluid Mechanics (AREA)
  • General Physics & Mathematics (AREA)
  • Measurement Of Levels Of Liquids Or Fluent Solid Materials (AREA)

Abstract

L'invention concerne un procédé permettant de mesurer le niveau de liquide cryogénique, comprenant les étapes consistant à immerger une sonde de niveau dans un liquide cryogénique, à appliquer un courant de propagation au dispositif (26) de chauffage afin d'induire une transition résistive (quench) au moins dans une partie adjacente du matériau supraconducteur (22), à supprimer le courant de propagation dans le dispositif de chauffage, à appliquer un courant de mesure au matériau supraconducteur, et à mesurer (30) la tension dans le matériau supraconducteur afin de déterminer le niveau de liquide cryogénique. Ce procédé comprend en particulier les étapes consistant à mesurer (40) en continu la tension aux bornes du supraconducteur pendant l'application du courant de propagation, et à interrompre l'application du courant de propagation en réponse à la détection d'une tension dépassant un niveau seuil donné aux bornes du matériau supraconducteur.
PCT/EP2005/006487 2004-06-21 2005-06-16 Procede permettant de mesurer le niveau de liquide cryogenique au moyen d'une sonde de niveau WO2005124294A1 (fr)

Priority Applications (2)

Application Number Priority Date Filing Date Title
DE112005001261T DE112005001261T5 (de) 2004-06-21 2005-06-16 Verfahren zur Messung des Füllstandes flüssiger Kryogene mit einer Füllstandssonde
US11/628,722 US7966878B2 (en) 2004-06-21 2005-06-16 Method for measuring liquid cryogen level using a level probe

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
GBGB0413837.6A GB0413837D0 (en) 2004-06-21 2004-06-21 Improvements to helium level probe
GB0413837.6 2004-06-21
GB0428174.7 2004-12-23
GB0428174A GB2415512B (en) 2004-06-21 2004-12-23 Method for measuring liquid cryogen level using a level probe

Publications (1)

Publication Number Publication Date
WO2005124294A1 true WO2005124294A1 (fr) 2005-12-29

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DE (1) DE112005001261T5 (fr)
WO (1) WO2005124294A1 (fr)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2290334A1 (fr) * 2009-09-01 2011-03-02 Siemens Plc Sonde de niveau cryogène
US8225653B2 (en) 2006-03-06 2012-07-24 Magna Steyr Fahrzeugtechnik Ag & Co. Kg Level sensor for cryogenic liquids, and receptacle comprising such a level sensor
FR2985801A1 (fr) * 2012-01-18 2013-07-19 Entrepose Projets Dispositif et procede de detection du sur-remplissage d'un reservoir de gaz liquefie basse temperature
CN103376143A (zh) * 2012-04-13 2013-10-30 上海联影医疗科技有限公司 液氦液面的测量方法

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3496773A (en) * 1966-05-26 1970-02-24 Atomic Energy Authority Uk Liquid level gauges
US3943767A (en) * 1974-07-22 1976-03-16 American Magnetics, Inc. Level detector system for cryogenic liquids

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3496773A (en) * 1966-05-26 1970-02-24 Atomic Energy Authority Uk Liquid level gauges
US3943767A (en) * 1974-07-22 1976-03-16 American Magnetics, Inc. Level detector system for cryogenic liquids

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8225653B2 (en) 2006-03-06 2012-07-24 Magna Steyr Fahrzeugtechnik Ag & Co. Kg Level sensor for cryogenic liquids, and receptacle comprising such a level sensor
EP2290334A1 (fr) * 2009-09-01 2011-03-02 Siemens Plc Sonde de niveau cryogène
FR2985801A1 (fr) * 2012-01-18 2013-07-19 Entrepose Projets Dispositif et procede de detection du sur-remplissage d'un reservoir de gaz liquefie basse temperature
EP2618118A1 (fr) * 2012-01-18 2013-07-24 Entrepose Projets Dispositif et procede de detection du sur-remplissage d'un reservoir de gaz liquefie basse temperature
CN103376143A (zh) * 2012-04-13 2013-10-30 上海联影医疗科技有限公司 液氦液面的测量方法
CN103376143B (zh) * 2012-04-13 2015-05-20 上海联影医疗科技有限公司 液氦液面的测量方法

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