WO2005098419A1 - Messvorrichtung zur messung des zustands von ölen oder fetten - Google Patents
Messvorrichtung zur messung des zustands von ölen oder fetten Download PDFInfo
- Publication number
- WO2005098419A1 WO2005098419A1 PCT/EP2005/003322 EP2005003322W WO2005098419A1 WO 2005098419 A1 WO2005098419 A1 WO 2005098419A1 EP 2005003322 W EP2005003322 W EP 2005003322W WO 2005098419 A1 WO2005098419 A1 WO 2005098419A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- measuring device
- water content
- sensor
- minimizing
- measuring
- Prior art date
Links
- 239000003921 oil Substances 0.000 title claims description 34
- 239000003925 fat Substances 0.000 title claims description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000000463 material Substances 0.000 claims description 13
- 238000005259 measurement Methods 0.000 claims description 13
- 229920000642 polymer Polymers 0.000 claims description 3
- 238000001914 filtration Methods 0.000 claims description 2
- 230000003287 optical effect Effects 0.000 claims description 2
- 238000000926 separation method Methods 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 5
- 239000000047 product Substances 0.000 abstract 2
- 239000012263 liquid product Substances 0.000 abstract 1
- 238000011156 evaluation Methods 0.000 description 11
- 235000013305 food Nutrition 0.000 description 4
- 239000000853 adhesive Substances 0.000 description 3
- 230000001070 adhesive effect Effects 0.000 description 3
- 239000004519 grease Substances 0.000 description 3
- 230000032683 aging Effects 0.000 description 2
- 239000003990 capacitor Substances 0.000 description 2
- 239000000919 ceramic Substances 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 230000018109 developmental process Effects 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- 230000001681 protective effect Effects 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 229910010293 ceramic material Inorganic materials 0.000 description 1
- 238000005253 cladding Methods 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000010411 cooking Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000010292 electrical insulation Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 239000011888 foil Substances 0.000 description 1
- 235000021588 free fatty acids Nutrition 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000012945 sealing adhesive Substances 0.000 description 1
- 239000013464 silicone adhesive Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N27/00—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
- G01N27/02—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating impedance
- G01N27/22—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating impedance by investigating capacitance
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N27/00—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
- G01N27/02—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating impedance
- G01N27/22—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating impedance by investigating capacitance
- G01N27/223—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating impedance by investigating capacitance for determining moisture content, e.g. humidity
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/02—Food
- G01N33/03—Edible oils or edible fats
Definitions
- Measuring device for measuring the condition of oils or fats
- the invention relates to a measuring device for measuring the state of oils or fats according to the preamble of claim 1.
- Hot oils or fats are often used in the preparation of food, which are not only used once, but are also used in deep fryers for successive cooking of different foods.
- the oil or fat is destroyed at hot operating temperatures between approx. 120 ° and 180 ° C due to oxidation, and undesirable chemical products such as e.g. free fatty acids or polymers that not only cause a deterioration in taste, but can also be harmful to health.
- measuring devices are used to measure the condition of the oils or fats, with which these are examined for their electrical properties.
- the measurement of the dielectric constant which represents a reliable measure of the degree of destruction of the fat or oil, is particularly suitable.
- a measuring device for measuring the condition of an oil or grease which consists of a housing which comprises the electronic evaluation units and a data display, furthermore a tubular connecting element and a sensor arranged at the tip thereof, which can be immersed directly in the hot oil or fat and is suitable for determining the dielectric constants.
- the electrical connection between the sensor and the evaluation electronics takes place via cables freely laid inside the connecting element.
- DE 101 63 760 AI describes a further development of the above-mentioned measuring device.
- the electrical lines between the sensor and the evaluation electronics are formed by metal lines printed on a ceramic carrier.
- the tubular connecting element is shaped in such a way that it surrounds the majority of the carrier and narrows downwards in such a way that only the area of the carrier on which the sensor is arranged is accessible from the outside.
- An insulating sealing adhesive is introduced and cured between the carrier and the connecting element, so that there is no electrical connection between the connecting element and the electrical lines.
- a temperature-stable seal is achieved, which prevents oil from penetrating into the interior of the connecting element.
- a temperature sensor can be provided, the measurement result of which can also be processed by the evaluation electronics.
- a disadvantage of this measuring device is that the measured values are often above the actual value despite the use of reliable sensors and suitable evaluation electronics.
- the present invention is therefore based on the object of providing a measuring device which delivers more precise and reliable measurement results.
- the invention is based on the finding that, when frying, large quantities of water vapor are expelled from the fried food, a certain part of which remains temporarily in the deep-frying oil. Since the dielectric constant of water is about 20 times greater than that of Frittierol, Even small amounts of water get too high readings. Depending on the age and temperature of the oil, it can take between 5 minutes (fresh oil and high temperature) and 30 minutes (old oil and low temperature) until the water influence has dropped to a tolerable level and the measured value matches the actual value of the oil ,
- the measuring device has means which are suitable for minimizing the falsifying influence of the water content in the material to be measured on the measurement result, as a result of which the measurement result is considerably more precise.
- the means preferably comprise a moisture sensor which is arranged in the area of the measuring device to be immersed. This will safely determine if even small amounts of water are present in the oil.
- the means comprise an electronic circuit for determining the complex impedance and the phase angle of the dielectric constant, as a result of which information is obtained which essentially correlates with the water content of the oil. It is thus possible to distinguish interference effects caused by water from the measurement effects caused by aging of the oil with a single sensor.
- the means have a device for filtering the measured material, which surrounds the carrier of the sensor for determining the dielectric constant. Such a device ensures that only oil reaches the sensor, from which the residual moisture has been extracted by the drying filter device.
- the measuring device also has a temperature sensor, which provides additional information that specifies the determination of the state of the material to be measured.
- Fig. 1 shows a measuring device according to the invention in front view
- FIG. 2 shows an enlarged front view of the lower area of the measuring device from FIG. 1 ;
- FIG. 3 shows an enlarged rear view of the lower area to be immersed in the measuring device from FIG. 1;
- FIG. 4 shows an enlarged rear view of a variant of the lower area to be immersed in the measuring device from FIG. 1;
- FIG. 5 shows an enlarged front view of the lower area to be immersed in a variant of the measuring device
- the 1 shows a measuring device 1 according to the invention for measuring the state of oils or fats, which has a housing 3 in its upper region.
- the housing has a display 5 for the display of measured values.
- the display is preferably designed as an LCD display and can be switched between a graphical representation, for example the color classification of the measured values, and a numerical representation.
- a keyboard 7 is provided for entering control commands, via which commands can be issued to the central control unit (not shown).
- the keyboard 7 is preferably designed as a foil keyboard.
- the housing can preferably also have an interface 9, which can be used for communication with external computers.
- the measuring device 1 is preferably adapted to perform a self-comparison. During the use of the measuring device 1, the housing 3 also serves as a handle for the operator.
- a hollow connecting element 10 which is sufficiently long and is made of a material with poor thermal conductivity, protrudes downward from the housing 3, so that the sensitive evaluation electronics (not shown) of the measuring device 1, which are located in the region of the housing 3 and / or in the area of the connecting element 10 facing the housing 3 is adequately protected from the heat of the oil or fat to be measured. These measures also ensure that the operator can carry out the measurements safely.
- the connecting element 10 is preferably made of stainless steel, which in addition to its low thermal conductivity is also suitable due to its unrestricted use in the food sector.
- the connecting element 10 is designed, for example, as a tubular component and is suitable for receiving electrical lines 12, which are in the
- the electrical lines 12 are arranged on at least one flat carrier 14, which is characterized by electrical insulation properties, for example a carrier 14 made of ceramic material.
- a sensor 16 for measuring electrical properties of the oil or grease there is a sensor 16 for measuring electrical properties of the oil or grease and preferably a temperature sensor 18, the measured values of which via the electrical lines 12 on the carrier
- a protective means 20 can be attached around the lower area of the carrier 14, which protects the sensors 16, 18 against external influences, in particular against contact with the bottom or the walls of the measuring vessel.
- the protective means 20 is designed as a border of the flat carrier 14 connected to the connecting element 10.
- the intermediate region between the carrier 14 and the connecting element 10 is sealed in one place by means of suitable sealing means (not shown).
- a suitable adhesive for example a silicone adhesive, is injected into the intermediate area between the carrier 14 and the connecting element 10, so that they do not touch directly and are therefore insulated from one another.
- the adhesive serves as a seal for the connecting element 10, so that no oil or grease can penetrate into the interior of the connecting element 10.
- the design of the adhesive surface must be secure against water inclusions, since otherwise there is a risk of explosion and, on the other hand, contamination of the measured material cannot be ruled out.
- the carrier 14 can extend as a one-piece element to the evaluation electronics, but there is also the possibility of decoupling, in that several carrier sections are strung together using suitable conductive connecting means. This provides advantages in particular with regard to the thermal load on the evaluation electronics.
- the sensor 16 for measuring the dielectric constant consists of a capacitor which measures the dielectric constant of the oil. It is preferably designed as an interdigital capacitor which consists of fine interlocking metal lines, each of which merges into one of the electrical lines 12, which lead to the evaluation electronics.
- the lines 12 can consist of a fine layer of gold or copper on the carrier 14, the layer being printed directly on the ceramic component.
- a multi-layer construction of the carrier 14 is also conceivable, as a result of which the sensitive lines 12 can be better protected against environmental influences.
- the temperature sensor 18 is designed, for example, as an electrical resistor, which can be formed, for example, from platinum or another suitable material. The temperature sensor 18 can also be arranged on the opposite side of the carrier 14 in the region of the tip of the carrier 14, as a result of which the size of the measuring device can be further reduced and both sensors 16, 18 are nevertheless exposed to the same ambient temperature.
- a moisture sensor 25 is arranged on the back of the carrier 14, which measures the residual moisture in the oil.
- the moisture sensor 25 is also connected via lines 12 to the evaluation electronics, which use the signals supplied by the moisture sensor 25 to correct the measured values of the sensor 16.
- a polymer sensor is preferably used as the moisture sensor 25.
- the entire lower region of the measuring device 1 can be surrounded by a cladding tube (not shown). It is also conceivable to arrange the moisture sensor 25 on the area to be immersed on the outside of the connecting element 10.
- two moisture sensors 25 a, 25 b are attached to the connecting element 10, the lower moisture sensor 25 a being positioned near the surface of the measured material and registering rising moisture therefrom, while the upper moisture sensor 25 b is at a greater distance from Surface to be measured is arranged.
- the ambient humidity measures the ambient humidity, and the difference between the measured values of the two sensors 25 a and 25 b is a measure of the moisture in the material to be measured.
- a filter device 30 can be arranged around the lower area of the measuring device 1 to be immersed, which filters water components out of the material to be measured.
- An oil-permeable water retention filter which is preferably designed as an exchangeable attachment, is suitable for this. It is also possible to determine the complex impedance and the phase angle of the dielectric constant using an electronic circuit known per se. From this, information can be found that essentially correlates with the water content of the oil. This makes it possible to distinguish the effects of interference from water from the effects of aging of the oil.
- the measuring device can also have means for compensating for the measurement error in the measurement signal and / or a display device which provides a corresponding optical and / or acoustic signal when the water content is increased.
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Food Science & Technology (AREA)
- Physics & Mathematics (AREA)
- Analytical Chemistry (AREA)
- Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Medicinal Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Investigating Or Analyzing Materials By The Use Of Electric Means (AREA)
Abstract
Description
Claims
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US11/547,761 US7652490B2 (en) | 2004-04-06 | 2005-03-30 | Measuring device for measuring the state of oils or fats |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102004016957.8 | 2004-04-06 | ||
DE102004016957A DE102004016957B4 (de) | 2004-04-06 | 2004-04-06 | Messvorrichtung zum Messen des Zustands von Ölen oder Fetten |
Publications (1)
Publication Number | Publication Date |
---|---|
WO2005098419A1 true WO2005098419A1 (de) | 2005-10-20 |
Family
ID=34963441
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/EP2005/003322 WO2005098419A1 (de) | 2004-04-06 | 2005-03-30 | Messvorrichtung zur messung des zustands von ölen oder fetten |
Country Status (4)
Country | Link |
---|---|
US (1) | US7652490B2 (de) |
DE (1) | DE102004016957B4 (de) |
ES (1) | ES2332392B1 (de) |
WO (1) | WO2005098419A1 (de) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103196959A (zh) * | 2013-04-10 | 2013-07-10 | 明尼苏达矿业制造特殊材料(上海)有限公司 | 用于检测油或脂的品质的装置 |
CN103344675A (zh) * | 2013-06-20 | 2013-10-09 | 济南海能仪器股份有限公司 | 食用油极性有害组分传感器 |
US8829928B2 (en) | 2010-09-14 | 2014-09-09 | 3M Innovative Properties Company | Methods and devices for acquiring an oil sample and monitoring the quality thereof |
CN104819996A (zh) * | 2015-04-01 | 2015-08-05 | 天津工业大学 | 基于扫频复阻抗测量的油水两相流含水率计及其测量方法 |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE102006003733B3 (de) * | 2006-01-26 | 2007-03-29 | Testo Ag | Verfahren zur Prüfung eines Messgerätes |
DE102007036473A1 (de) | 2007-08-01 | 2009-02-05 | Testo Ag | Vorrichtung zum Messen des Zustands eines Messguts, insbesondere von Ölen oder Fetten |
DE102008014477B4 (de) | 2008-03-17 | 2018-08-30 | Testo Ag | Vorrichtung zum Messen des Zustands eines Messguts, insbesondere von Ölen oder Fetten |
CA2952739C (en) | 2014-06-30 | 2019-06-11 | Pitco Frialator, Inc. | System and method for sensing oil quality |
US9841394B2 (en) | 2015-11-16 | 2017-12-12 | Pitco Frialator, Inc. | System and method for sensing oil quality |
US10436730B2 (en) | 2015-12-21 | 2019-10-08 | Pitco Frialator, Inc. | System and method for sensing oil quality |
JP6993679B2 (ja) * | 2017-11-22 | 2022-01-13 | センスプロ株式会社 | 潤滑油センサヘッド、及びセンサシステム |
Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3746974A (en) * | 1971-03-25 | 1973-07-17 | Thexton Mfg Co | Oil permittivity sensor |
US4082997A (en) * | 1974-06-25 | 1978-04-04 | Japan Gasoline Co., Ltd. | Oil detecting device |
DE19947669A1 (de) * | 1999-10-04 | 2001-05-10 | Testo Gmbh & Co | Verfahren zur Bestimmung der Qualität von Fetten und Ölen und Vorrichtung zur Durchführung des Verfahrens |
US6282947B1 (en) * | 1996-07-09 | 2001-09-04 | Hydac Filtertechnik Gmbh | Arrangement for monitoring the useful properties of fluids |
US6469521B1 (en) * | 1999-04-22 | 2002-10-22 | Ebro Electronic Gmbh & Co. Kg | Method for measuring the state of oils or fats |
US20030155935A1 (en) * | 2001-12-28 | 2003-08-21 | Wolfgang Klun | Process and device for measuring the state of degradation of oils or fats |
US20040060344A1 (en) * | 2002-09-30 | 2004-04-01 | Kauffman Robert E. | Sensor device for monitoring the condition of a fluid and a method of using the same |
Family Cites Families (7)
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US3739265A (en) * | 1970-09-09 | 1973-06-12 | J Skildum | Test instrument and method for isolating and measuring the capacitance due to a particular functional group in a liquid |
JPS60188835A (ja) * | 1984-03-08 | 1985-09-26 | Sharp Corp | 感湿素子 |
KR960010689B1 (ko) * | 1991-08-28 | 1996-08-07 | 미쓰비시덴키 가부시키가이샤 | 연료의 유전율 검지센서 |
US5818731A (en) * | 1995-08-29 | 1998-10-06 | Mittal; Gauri S. | Method and apparatus for measuring quality of frying/cooking oil/fat |
US5824889A (en) * | 1997-03-06 | 1998-10-20 | Kavlico Corporation | Capacitive oil deterioration and contamination sensor |
GB9709290D0 (en) * | 1997-05-07 | 1997-06-25 | Collister Christopher J | Electrical measurement apparatus for oil |
US6746974B1 (en) * | 1999-03-10 | 2004-06-08 | 3M Innovative Properties Company | Web material comprising a tackifier |
-
2004
- 2004-04-06 DE DE102004016957A patent/DE102004016957B4/de not_active Expired - Fee Related
-
2005
- 2005-03-30 WO PCT/EP2005/003322 patent/WO2005098419A1/de active IP Right Grant
- 2005-03-30 ES ES200650068A patent/ES2332392B1/es not_active Expired - Fee Related
- 2005-03-30 US US11/547,761 patent/US7652490B2/en active Active
Patent Citations (7)
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US3746974A (en) * | 1971-03-25 | 1973-07-17 | Thexton Mfg Co | Oil permittivity sensor |
US4082997A (en) * | 1974-06-25 | 1978-04-04 | Japan Gasoline Co., Ltd. | Oil detecting device |
US6282947B1 (en) * | 1996-07-09 | 2001-09-04 | Hydac Filtertechnik Gmbh | Arrangement for monitoring the useful properties of fluids |
US6469521B1 (en) * | 1999-04-22 | 2002-10-22 | Ebro Electronic Gmbh & Co. Kg | Method for measuring the state of oils or fats |
DE19947669A1 (de) * | 1999-10-04 | 2001-05-10 | Testo Gmbh & Co | Verfahren zur Bestimmung der Qualität von Fetten und Ölen und Vorrichtung zur Durchführung des Verfahrens |
US20030155935A1 (en) * | 2001-12-28 | 2003-08-21 | Wolfgang Klun | Process and device for measuring the state of degradation of oils or fats |
US20040060344A1 (en) * | 2002-09-30 | 2004-04-01 | Kauffman Robert E. | Sensor device for monitoring the condition of a fluid and a method of using the same |
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IRION E ET AL: "Oil-Quality and Oil-Level Detection with the TEMIC QLT-Sensor Leads to Variable Maintenance Intervals", SAE TECHNICAL PAPER SERIES, SOCIETY OF AUTOMOTIVE ENGINEERS, WARRENDALE, PA, US, no. 970847, 1997, pages 105 - 110, XP002968686, ISSN: 0148-7191 * |
U. DEMISCH, M. MUHL: "Electronic nose for detection of the deterioration of frying fat- comparative stdies for a new quick test", 3RD INTERNATIONAL SYMPOSIUM ON DEEP FAT FRYING, 20 March 2000 (2000-03-20), HAGEN, pages 11 - 12, XP002330509 * |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US8829928B2 (en) | 2010-09-14 | 2014-09-09 | 3M Innovative Properties Company | Methods and devices for acquiring an oil sample and monitoring the quality thereof |
CN103196959A (zh) * | 2013-04-10 | 2013-07-10 | 明尼苏达矿业制造特殊材料(上海)有限公司 | 用于检测油或脂的品质的装置 |
CN103344675A (zh) * | 2013-06-20 | 2013-10-09 | 济南海能仪器股份有限公司 | 食用油极性有害组分传感器 |
CN104819996A (zh) * | 2015-04-01 | 2015-08-05 | 天津工业大学 | 基于扫频复阻抗测量的油水两相流含水率计及其测量方法 |
Also Published As
Publication number | Publication date |
---|---|
US7652490B2 (en) | 2010-01-26 |
US20080186033A1 (en) | 2008-08-07 |
DE102004016957B4 (de) | 2007-05-03 |
ES2332392A1 (es) | 2010-02-03 |
DE102004016957A1 (de) | 2005-10-27 |
ES2332392B1 (es) | 2010-09-08 |
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