WO2005042681B1 - Concrete surface retarders - Google Patents
Concrete surface retardersInfo
- Publication number
- WO2005042681B1 WO2005042681B1 PCT/US2004/032739 US2004032739W WO2005042681B1 WO 2005042681 B1 WO2005042681 B1 WO 2005042681B1 US 2004032739 W US2004032739 W US 2004032739W WO 2005042681 B1 WO2005042681 B1 WO 2005042681B1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- oil
- derivative
- salt
- cement
- coating composition
- Prior art date
Links
- 239000000203 mixture Substances 0.000 claims abstract 27
- 239000003921 oil Substances 0.000 claims abstract 11
- 239000010775 animal oil Substances 0.000 claims abstract 9
- 235000015112 vegetable and seed oil Nutrition 0.000 claims 18
- 239000008158 vegetable oil Substances 0.000 claims 18
- 239000004568 cement Substances 0.000 claims 16
- 239000008199 coating composition Substances 0.000 claims 14
- 150000003839 salts Chemical class 0.000 claims 13
- 239000011780 sodium chloride Substances 0.000 claims 13
- 230000000979 retarding Effects 0.000 claims 12
- 235000019198 oils Nutrition 0.000 claims 10
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims 6
- 235000014113 dietary fatty acids Nutrition 0.000 claims 6
- 239000000194 fatty acid Substances 0.000 claims 6
- 150000004665 fatty acids Chemical class 0.000 claims 6
- RGHNJXZEOKUKBD-SQOUGZDYSA-N Gluconic acid Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C(O)=O RGHNJXZEOKUKBD-SQOUGZDYSA-N 0.000 claims 4
- -1 crushed gravel Substances 0.000 claims 4
- 239000002253 acid Substances 0.000 claims 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 3
- BJHIKXHVCXFQLS-UYFOZJQFSA-N Fructose Natural products OC[C@@H](O)[C@@H](O)[C@H](O)C(=O)CO BJHIKXHVCXFQLS-UYFOZJQFSA-N 0.000 claims 2
- BJEPYKJPYRNKOW-UHFFFAOYSA-N Malic acid Chemical compound OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 claims 2
- GUBGYTABKSRVRQ-YOLKTULGSA-N Maltose Natural products O([C@@H]1[C@H](O)[C@@H](O)[C@H](O)O[C@H]1CO)[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 GUBGYTABKSRVRQ-YOLKTULGSA-N 0.000 claims 2
- FEWJPZIEWOKRBE-XIXRPRMCSA-N Mesotartaric acid Chemical compound OC(=O)[C@@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-XIXRPRMCSA-N 0.000 claims 2
- 239000011398 Portland cement Substances 0.000 claims 2
- 235000019484 Rapeseed oil Nutrition 0.000 claims 2
- SRBFZHDQGSBBOR-SQOUGZDYSA-N Xylose Natural products O[C@@H]1CO[C@@H](O)[C@@H](O)[C@@H]1O SRBFZHDQGSBBOR-SQOUGZDYSA-N 0.000 claims 2
- 150000001412 amines Chemical class 0.000 claims 2
- 239000011230 binding agent Substances 0.000 claims 2
- 150000001735 carboxylic acids Chemical class 0.000 claims 2
- 239000000969 carrier Substances 0.000 claims 2
- 239000003086 colorant Substances 0.000 claims 2
- 150000001875 compounds Chemical class 0.000 claims 2
- 239000000975 dye Substances 0.000 claims 2
- 150000002148 esters Chemical class 0.000 claims 2
- 150000002191 fatty alcohols Chemical class 0.000 claims 2
- 150000002193 fatty amides Chemical class 0.000 claims 2
- 239000000174 gluconic acid Substances 0.000 claims 2
- 235000012208 gluconic acid Nutrition 0.000 claims 2
- 229950006191 gluconic acid Drugs 0.000 claims 2
- 239000001630 malic acid Substances 0.000 claims 2
- 229940099690 malic acid Drugs 0.000 claims 2
- 235000011090 malic acid Nutrition 0.000 claims 2
- 239000011404 masonry cement Substances 0.000 claims 2
- 239000000463 material Substances 0.000 claims 2
- 239000004570 mortar (masonry) Substances 0.000 claims 2
- 239000000049 pigment Substances 0.000 claims 2
- 239000006254 rheological additive Substances 0.000 claims 2
- 239000004576 sand Substances 0.000 claims 2
- 239000004575 stone Substances 0.000 claims 2
- 239000003784 tall oil Chemical class 0.000 claims 2
- 239000011975 tartaric acid Substances 0.000 claims 2
- 229960001367 tartaric acid Drugs 0.000 claims 2
- 235000002906 tartaric acid Nutrition 0.000 claims 2
- 239000002383 tung oil Substances 0.000 claims 2
- 239000004034 viscosity adjusting agent Substances 0.000 claims 2
- 239000000341 volatile oil Substances 0.000 claims 2
- 238000005406 washing Methods 0.000 claims 2
- WQZGKKKJIJFFOK-VFUOTHLCSA-N β-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 claims 2
- 235000019489 Almond oil Nutrition 0.000 claims 1
- 210000000988 Bone and Bones Anatomy 0.000 claims 1
- 241000207199 Citrus Species 0.000 claims 1
- 240000002268 Citrus limon Species 0.000 claims 1
- 235000005979 Citrus limon Nutrition 0.000 claims 1
- 240000000560 Citrus x paradisi Species 0.000 claims 1
- 241000252203 Clupea harengus Species 0.000 claims 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N D-Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims 1
- WQZGKKKJIJFFOK-QTVWNMPRSA-N D-mannopyranose Chemical compound OC[C@H]1OC(O)[C@@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-QTVWNMPRSA-N 0.000 claims 1
- 239000005715 Fructose Substances 0.000 claims 1
- GUBGYTABKSRVRQ-UUNJERMWSA-N Lactose Natural products O([C@@H]1[C@H](O)[C@H](O)[C@H](O)O[C@@H]1CO)[C@H]1[C@@H](O)[C@@H](O)[C@H](O)[C@H](CO)O1 GUBGYTABKSRVRQ-UUNJERMWSA-N 0.000 claims 1
- 235000019482 Palm oil Nutrition 0.000 claims 1
- 235000019483 Peanut oil Nutrition 0.000 claims 1
- 235000019495 Pecan oil Nutrition 0.000 claims 1
- 235000004347 Perilla Nutrition 0.000 claims 1
- 240000003877 Perilla frutescens Species 0.000 claims 1
- 235000004348 Perilla frutescens Nutrition 0.000 claims 1
- 241001125046 Sardina pilchardus Species 0.000 claims 1
- CZMRCDWAGMRECN-GDQSFJPYSA-N Sucrose Natural products O([C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O1)[C@@]1(CO)[C@H](O)[C@@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-GDQSFJPYSA-N 0.000 claims 1
- 235000019486 Sunflower oil Nutrition 0.000 claims 1
- 235000009470 Theobroma cacao Nutrition 0.000 claims 1
- 240000000280 Theobroma cacao Species 0.000 claims 1
- 235000019498 Walnut oil Nutrition 0.000 claims 1
- 229960003487 Xylose Drugs 0.000 claims 1
- 239000008168 almond oil Substances 0.000 claims 1
- 235000021302 avocado oil Nutrition 0.000 claims 1
- 239000008163 avocado oil Substances 0.000 claims 1
- 235000019519 canola oil Nutrition 0.000 claims 1
- 239000000828 canola oil Substances 0.000 claims 1
- 239000004359 castor oil Substances 0.000 claims 1
- 235000019438 castor oil Nutrition 0.000 claims 1
- 235000020971 citrus fruits Nutrition 0.000 claims 1
- 235000019864 coconut oil Nutrition 0.000 claims 1
- 239000003240 coconut oil Substances 0.000 claims 1
- 235000012716 cod liver oil Nutrition 0.000 claims 1
- 239000003026 cod liver oil Substances 0.000 claims 1
- 235000005687 corn oil Nutrition 0.000 claims 1
- 239000002285 corn oil Substances 0.000 claims 1
- 239000008121 dextrose Substances 0.000 claims 1
- 239000000686 essence Substances 0.000 claims 1
- 239000000945 filler Substances 0.000 claims 1
- 235000021323 fish oil Nutrition 0.000 claims 1
- 239000008103 glucose Substances 0.000 claims 1
- 239000008169 grapeseed oil Substances 0.000 claims 1
- 239000010460 hemp oil Substances 0.000 claims 1
- 235000019514 herring Nutrition 0.000 claims 1
- 239000008101 lactose Substances 0.000 claims 1
- GUBGYTABKSRVRQ-XLOQQCSPSA-N lactose Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@H](O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-XLOQQCSPSA-N 0.000 claims 1
- 239000010699 lard oil Substances 0.000 claims 1
- 235000021388 linseed oil Nutrition 0.000 claims 1
- 239000000944 linseed oil Substances 0.000 claims 1
- 239000010697 neat foot oil Substances 0.000 claims 1
- 235000019488 nut oil Nutrition 0.000 claims 1
- 239000010466 nut oil Substances 0.000 claims 1
- 235000008390 olive oil Nutrition 0.000 claims 1
- 239000004006 olive oil Substances 0.000 claims 1
- 239000002540 palm oil Substances 0.000 claims 1
- 239000000312 peanut oil Substances 0.000 claims 1
- 239000010470 pecan oil Substances 0.000 claims 1
- 239000001794 pinus palustris tar oil Substances 0.000 claims 1
- 239000010491 poppyseed oil Substances 0.000 claims 1
- 235000005713 safflower oil Nutrition 0.000 claims 1
- 239000003813 safflower oil Substances 0.000 claims 1
- 235000019512 sardine Nutrition 0.000 claims 1
- 235000011803 sesame oil Nutrition 0.000 claims 1
- 239000008159 sesame oil Substances 0.000 claims 1
- 239000011492 sheep wool Substances 0.000 claims 1
- 239000002904 solvent Substances 0.000 claims 1
- 235000012424 soybean oil Nutrition 0.000 claims 1
- 239000003549 soybean oil Substances 0.000 claims 1
- 239000005720 sucrose Substances 0.000 claims 1
- 125000000185 sucrose group Chemical group 0.000 claims 1
- 239000002600 sunflower oil Substances 0.000 claims 1
- 239000003760 tallow Substances 0.000 claims 1
- 239000008170 walnut oil Substances 0.000 claims 1
Abstract
Surface retarder compositions of the invention comprise at least one surface retarder active suspended in a vegatable oil or derivative thereof, an animal oil or derivative thereof, or mixtures thereof. Methods involving use of the compositions are also described.
Claims
1. A method for treating the surface of a hydratable cementitious composition, comprising: providing a hydratable cementitious composition having a surface to be etched, said hydratable cementitious composition comprising a hydratable cement binder comprising Portland cement, masonry cement, or mortar cement, and water; said hydratable cementitious composition further comprising an aggregate selected from the group consisting of sand, crushed gravel, and stone; applying a coating composition onto a surface of said cementitious composition, said coating composition comprising at least one cement set retarding active component dispersed in a vegetable oil or derivative thereof, an animal oil or derivative thereof, or a mixture of said oils or derivatives thereof; and washing away a portion of said surface of said cementitious composition coated with said coating composition using a pressure-washer or hose, thereby revealing an etched portion in said cementitious composition comprising said aggregate.
2. The method of claim 1 wherein said vegetable oil, said animal oil, or mixture or derivative thereof is present in an amount not less than 1 % and not greater than 98% based on total weight of said coating composition.
3. The method of claim 1 wherein said vegetable oil, said animal oil, or mixture or derivative thereof is present in an amount not less than 25% and not greater than 92% based on total weight of said coating composition.
4. The method of claim 1 wherein said vegetable oil, said animal oil, or mixture or derivative thereof is present in an amount not less than 50% and not greater than 90% based on total weight of said coating composition
5. The method of claim 4 wherein said at least one cement set retarding active component is dispersed in a vegetable oil.
6. The method of claim 5 wherein said vegetable oil is selected from the group consisting of rapeseed oil, sunflower oil, soy bean oil, castor oil, peanut oil, grape seed oil, corn oil, canola oil, coconut oil, linseed oil, sesame oil, olive oil, palm oil, almond oil, avocado oil, china wood oil, cocoa oil, safflower oil, hemp seed oil, walnut oil, poppy seed oil, oiticaca oil, palm nut oil, perilla oil, pecan oil, tung oil, and pine tar oil.
7. The method of claim 1 wherein said vegetable oil comprises at least 50% by total weight of rapeseed oil.
8. The method of claim 1 wherein said at least one cement set retarding active component is dispersed in a vegetable oil or derivative thereof.
9. The method of claim 8 wherein said vegetable oil derivative comprises one or more materials selected from the group consisting of mono and diglycerides of C6-C30 fatty acids, esters of C.6-C30 fatty acids, ethoxylated compounds of C6-C30 fatty acids, C6-C30 fatty alcohols, C6-C30 fatty amines, O-C30 fatty amides, and tall oil derivatives.
10. The method of claim 1 wherein said at least one cement set retarding active component is dispersed in a vegetable oil or derivative thereof/ and said vegetable oil or derivative being an essential oil.
11. The method of claim 1 wherein said essential oil is selected from the . essences of orange, grapefruit, lemon, citrus, and pinetree.
12. The method of claim 1 wherein said at least one cement set retarding active component is dispersed in an animal oil selected from the group consisting of lard oil, bone oil, herring oil, cod liver oil, neatsfoot oil, sardine oil, lanoline oil, fish oil, sheep wool oil, and tallow oil.
13. The method of claim 12 wherein said animal oil contains a material selected from the group consisting of mono and diglycerides of C6-C30 fatty acids, esters of C6-C30 fatty acids, ethoxylated compounds of C6-C30 fatty acids, C6-C30 fatty alcohols, C6-C30 fatty amines, C.6-C30 fatty amides, and tall oil derivatives.
14. The method of claim 1 wherein said composition comprises at least two different vegetable oils, or a vegetable oil and a vegetable oil derivative.
15. The method of claim 1 wherein said at least one cement set retarding active component is a sugar, or an acid or salt thereof.
17
16. The method of claim 15 wherein said at least one cement set retarding active component is present in an amount not less than 1% and not greater than 20% by total weight of the composition.
17. The method of claim 16 wherein said at least one cement set retarding active component is selected from the group consisting of carboxylic acid or its salt, malic acid or its salt, tartaric acid or its salt, citric acid or its salt, gluconic acid or its salt, heptagluconic acid or its salt.
18. The method of claim 16 wherein said at least one cement set retarding active component is a sugar.
19. The method of claim 18 wherein said sugar is selected from the group consisting of sucrose, roferose, dextrose, maltose, lactose, xylose, fructose, mannose, and glucose.
20. The method of claim 1 further comprising water or petroleum- based solvent. -
21. The method of claim 1 further comprising a pigment, colorant, dye, Jiller, rheology modifier, viscosity modifier, or mixture thereof.
22. > The method of claim 3 wherein said coating composition comprises mixture of said vegetable oil or derivative thereof and said animal oil or derivative thereof.
23. A method for treating the surface of a hydratable cementitious composition, comprising:
(A) providing a hydratable cementitious composition having a surface to be etched, said hydratable cementitious composition comprising a hydratable cement binder comprising Portland cement, masonry cement, or mortar cement, and water; said hydratable cementitious composition further comprising an aggregate selected from the group consisting of sand, crushed gravel, and stone;
(B) applying a coating composition onto a surface of said cementitious composition, wherein said coating composition comprises at least one cement set retarding active component present in an amount not less than 1 %
18 and not greater than 20% by total weight of said coating composition, said at least one cement set retarding active component being dispersed in an oil carrier which is present in an amount not less than 25% and not greater than 92% based on total weight of said coating composition, and said oil carrier comprising at least two different vegetable oils or a vegetable oil and a vegetable oil derivative, and at least one animal oil; said at least one cement set retarding active component being selected from the group consisting of carboxylic acid or its salt, malic acid or its salt, tartaric acid or its salt, citric acid or its salt, gluconic acid or its salt, heptagluconic acid or its salt; and said coating composition further comprising a pigment, colorant, dye, or mixture thereof, and said coating composition further comprising a filler, rheology modifier, viscosity modifier, or mixture thereof ;: and
(C) washing away a portion of said surface of said cementitious composition coated with said coating composition using a pressure-washer or hose, thereby revealing an etched portion in said cementitious composition comprising said aggregate.
19
Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2006535546A JP5127227B2 (en) | 2003-10-20 | 2004-10-05 | Concrete surface retarder |
| AU2004285109A AU2004285109B2 (en) | 2003-10-20 | 2004-10-05 | Concrete surface retarders |
| NZ546380A NZ546380A (en) | 2003-10-20 | 2004-10-05 | Concrete surface retarders for treating the surface of a hydratable cementitious composition |
| KR1020067006817A KR101136355B1 (en) | 2003-10-20 | 2004-10-05 | Concrete surface retarders |
| CA002543441A CA2543441C (en) | 2003-10-20 | 2004-10-05 | Concrete surface retarders |
| HK07103169.2A HK1097564A1 (en) | 2003-10-20 | 2007-03-23 | Concrete surface retarders |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10/689,925 | 2003-10-20 | ||
| US10/689,925 US7037367B2 (en) | 2003-10-20 | 2003-10-20 | Concrete surface retarders |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| WO2005042681A2 WO2005042681A2 (en) | 2005-05-12 |
| WO2005042681A3 WO2005042681A3 (en) | 2005-12-29 |
| WO2005042681B1 true WO2005042681B1 (en) | 2006-02-09 |
Family
ID=34394524
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PCT/US2004/032739 WO2005042681A2 (en) | 2003-10-20 | 2004-10-05 | Concrete surface retarders |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US7037367B2 (en) |
| EP (1) | EP1526120B8 (en) |
| JP (1) | JP5127227B2 (en) |
| KR (1) | KR101136355B1 (en) |
| CN (1) | CN100537685C (en) |
| AU (1) | AU2004285109B2 (en) |
| CA (1) | CA2543441C (en) |
| ES (1) | ES2569519T3 (en) |
| HK (1) | HK1097564A1 (en) |
| NZ (1) | NZ546380A (en) |
| WO (1) | WO2005042681A2 (en) |
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| US5912283A (en) * | 1995-07-19 | 1999-06-15 | Toyo Aluminium Kabushiki Kaisha | Surface-treated color pigment, colored substrate particles and production process thereof |
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| US5728209A (en) * | 1995-11-13 | 1998-03-17 | Mbt Holding Ag | Unitized cement admixture |
| JP3291180B2 (en) * | 1995-11-13 | 2002-06-10 | 株式会社ブリヂストン | Method for producing sheet-like material and method for producing concrete product using the same |
| US5794401A (en) * | 1997-06-03 | 1998-08-18 | Shaw; Lee A. | Durable architectural flooring and method of fabricating the same |
| JPH11277043A (en) * | 1998-03-30 | 1999-10-12 | Seikitokyu Kogyo Co Ltd | Method and apparatus for reclaiming asphalt concrete mass |
| US6187382B1 (en) * | 1998-10-09 | 2001-02-13 | Donald V. Lightcap, Jr. | Liquid membrane-forming curing composition and method of curing fresh concrete |
| DE69936462T2 (en) * | 1998-11-24 | 2008-03-13 | Commodore International Ltd., Birkenhead | PROCESS FOR REMOVING CEMENT |
| JP2001031452A (en) * | 1999-07-19 | 2001-02-06 | Takenaka Komuten Co Ltd | Hardening retarder for washing finish of concrete surface and washing finish technique |
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| JP4391033B2 (en) * | 2001-03-23 | 2009-12-24 | サカタインクス株式会社 | Offset printing ink composition |
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-
2003
- 2003-10-20 US US10/689,925 patent/US7037367B2/en not_active Expired - Lifetime
-
2004
- 2004-10-05 WO PCT/US2004/032739 patent/WO2005042681A2/en active Application Filing
- 2004-10-05 NZ NZ546380A patent/NZ546380A/en not_active IP Right Cessation
- 2004-10-05 JP JP2006535546A patent/JP5127227B2/en not_active Expired - Fee Related
- 2004-10-05 CA CA002543441A patent/CA2543441C/en not_active Expired - Lifetime
- 2004-10-05 CN CNB2004800309293A patent/CN100537685C/en not_active Expired - Fee Related
- 2004-10-05 AU AU2004285109A patent/AU2004285109B2/en not_active Ceased
- 2004-10-05 KR KR1020067006817A patent/KR101136355B1/en not_active IP Right Cessation
- 2004-10-20 ES ES04256447.6T patent/ES2569519T3/en not_active Expired - Lifetime
- 2004-10-20 EP EP04256447.6A patent/EP1526120B8/en not_active Expired - Lifetime
-
2007
- 2007-03-23 HK HK07103169.2A patent/HK1097564A1/en not_active IP Right Cessation
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