WO2004108247A1 - Liquid purification installation - Google Patents

Liquid purification installation Download PDF

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Publication number
WO2004108247A1
WO2004108247A1 PCT/NL2004/000415 NL2004000415W WO2004108247A1 WO 2004108247 A1 WO2004108247 A1 WO 2004108247A1 NL 2004000415 W NL2004000415 W NL 2004000415W WO 2004108247 A1 WO2004108247 A1 WO 2004108247A1
Authority
WO
WIPO (PCT)
Prior art keywords
medium
gas lift
purification installation
bed
liquid
Prior art date
Application number
PCT/NL2004/000415
Other languages
English (en)
French (fr)
Inventor
Sjoerd Hubertus Josef Vellinga
Jelle Faber
Johannes Wilhelmus Wouters
Original Assignee
Paques B.V.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Paques B.V. filed Critical Paques B.V.
Priority to EP04748647A priority Critical patent/EP1658120A1/en
Publication of WO2004108247A1 publication Critical patent/WO2004108247A1/en

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D24/00Filters comprising loose filtering material, i.e. filtering material without any binder between the individual particles or fibres thereof
    • B01D24/28Filters comprising loose filtering material, i.e. filtering material without any binder between the individual particles or fibres thereof with the filter bed moving during the filtration
    • B01D24/30Translation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D24/00Filters comprising loose filtering material, i.e. filtering material without any binder between the individual particles or fibres thereof
    • B01D24/46Regenerating the filtering material in the filter
    • B01D24/4668Regenerating the filtering material in the filter by moving the filtering element
    • B01D24/4689Displacement of the filtering material to a compartment of the filtering device for regeneration

Definitions

  • the present invention relates to a purification installation for purifying a liquid, comprising: • a reactor vessel containing a bed of a granular medium;
  • the at least one gas lift system comprises a riser with a suction inlet located in the bed and a blow outlet, at a higher position, opening into the medium washer, as well as gas feed means for generating a gas lift in the riser that draws up medium and liquid at the suction inlet and feeds these upwards through the riser to the medium washer, wherein the medium washer has a medium outlet for returning washed medium to the bed.
  • the reactor vessel is conical at the base. The cone is usually deep, that is to say the bottom wall has a steep slope.
  • a gas lift system is arranged centrally in the known reactor vessel, h this known installation the gas lift system has a suction inlet that is close to the point of the conical base and a blow outlet that opens into a medium washer arranged centrally in the reactor vessel, hi the case of the known installation the granular medium is usually sand.
  • the gas lift system has a suction inlet that is close to the point of the conical base and a blow outlet that opens into a medium washer arranged centrally in the reactor vessel, hi the case of the known installation the granular medium is usually sand.
  • dirty sand drawn up from the bottom of the sand bed is fed upwards through the riser to the medium washer.
  • the sand is cleaned in the medium washer so as then, after cleaning, to drop back onto the top of the sand bed.
  • the liquid to be purified is fed into the sand bed in the reactor vessel.
  • the liquid On passing upwards through the sand bed, the liquid is cleaned, so as then to be discharged from the reactor vessel from the top. With this procedure the sand bed is in counter-current because dirty sand is always fed upwards from the bottom via the riser for cleaning and drops back onto the top of the sand bed after cleaning.
  • the supply of liquid to be purified and the distribution thereof over the sand bed is effected by means of outflow arms that run radially.
  • One disadvantage of the known purification installation is that the total height of the reactor vessel is large because of the cone required.
  • a further disadvantage is that the greater the reactor surface area the less effective is the suction of the medium for feeding upwards via the riser to the medium washer. This ineffectiveness is associated with a relatively high energy requirement for the gas lift system and a relatively large amount of wash liquid required for the medium washer.
  • the aim of the present invention is to provide an improved purification installation of the type mentioned in the preamble, which, in particular, overcomes one or more of the abovementioned disadvantages.
  • Said aim is achieved according to the invention by providing a purification installation of the type mentioned in the preamble, which is characterised in that the purification installation has a multiplicity of gas lift systems, the respective blow outlets of which emerge in the medium washer.
  • the purification installation has a multiplicity of gas lift systems, the respective blow outlets of which emerge in the medium washer.
  • an advantageous embodiment of the invention is characterised in that one medium washer is provided per two or more gas lift systems or even one medium washer is provided per reactor vessel. The number of components susceptible to fouling and wear can be reduced in this way.
  • the medium washer viewed in the horizontal direction, is provided centrally with respect to the associated gas lift systems.
  • the risers of the associated gas lift systems can as far as possible be of approximately equal length, which is advantageous in order as far as possible to be able to utilise the reactor vessel uniformly over the reactor surface area - viewed horizontally.
  • the medium washer is provided centrally in the reactor vessel.
  • each gas lift system is provided at the bottom with a bowl, such as a cone, that opens at the top.
  • a cone at the bottom of each gas lift system promotes effective suction of medium by the gas lift system.
  • each bowl is integral with the respective gas lift system, such that each respective gas lift system can be fitted or removed as a unit together with the respective bowl in each case.
  • integral with is understood to mean that the bowl and the gas lift system, or at least the bottom section thereof, have already been fixed to one another outside the reactor vessel. This can be effected, for example, by making the inlet end of the gas lift system and the bowl from an injection moulding made of plastic or optionally a metal.
  • the bowl is fixed to the inlet end of the gas lift system by means of assembly means such as screws or bolt or snap-fit connections.
  • the purification installation according to the invention has a liquid feed system for feeding the liquid to be purified into the bed.
  • the liquid feed system comprises a multiplicity of parallel distribution arms that are equipped for feeding liquid into the bed over the length of the distribution arms.
  • Such distribution arms can consist of elongated caps that are open at the bottom and at one end are mounted on a feed line for the liquid. The liquid fed underneath the cap will enter the bed of medium via the open lower end of the cap.
  • the cap ensures that there is a hollow space in the bed via which the liquid can flow into the bed, distributed over the bed.
  • distribution arms are known per se from the state of the art.
  • the distribution arms are arranged radially. This has the significant disadvantage that in the case of larger reactor vessel diameters the distribution of liquid over the reactor vessel at the radial outer side differs from that in the centre of the reactor vessel.
  • Positioning the distribution arms parallel with one another in accordance with the present invention now makes it possible to ensure that the feed of the liquid to be purified is uniform at all points over the entire reactor surface area.
  • these parallel distribution arms can also highly advantageously be used with purification installations already known from the state of the art, i.e. separately from the multiple gas lift systems.
  • the present invention therefore also relates to a purification installation for purifying a liquid, comprising:
  • the gas lift system comprises a riser with a suction inlet located in the bed and a blow outlet that is located higher and opens into the medium washer, as well as gas feed means for generating a gas lift in the riser that draws in medium, liquid and gas at the suction inlet and feeds these upwards through the riser to the medium washer; • wherein the medium washer has a medium outlet for returning the washed medium to the bed; characterised in that the liquid feed system comprises a multiplicity of parallel distribution arms that are equipped for feeding liquid into the bed over the length of the distribution arms.
  • the distribution arms can be constructed as is known from the state of the art, for example by means of the caps open at the bottom, which have already been mentioned above.
  • the characterising clause of Claim 1 and Claims 2 - 10 of this application can be linked as dependent claims to the purification installation according to the second aspect.
  • the purification installation according to the invention has a control system equipped for mutually independent control of the gas feed to the respective gas lift systems.
  • the reactor vessel of the purification installation according to the invention can have a base that is essentially flat.
  • the distance from the distribution arms to the base can be reduced to 60 to 90 cm, whilst this is approximately 2 to 3 m in the state of the art.
  • the flat base enables very easy positioning of the gas lift systems.
  • FIG. 1 shows, diagrammatically, a vertical longitudinal sectional view of a purification installation according to the invention
  • Fig. 1A shows the detail la from Figure 1;
  • Fig. 2 shows the upper section of the purification installation, likewise in vertical longitudinal section, according to the arrows II in Fig. 1;
  • Fig. 3 shows, diagrammatically, a horizontal section according to the arrows in in
  • FIG. 4 shows, diagrammatically, a horizontal section according to arrows IV.
  • Figure 1 shows a reactor vessel with a bed 3 of granular medium therein.
  • This granular medium can be of diverse types. For example, consideration can be given to filter sand.
  • Medium washer 2 is. provided centrally in the reactor vessel 1. Furthermore, several, three in this example drawn, gas lift systems 4, 5 are provided in the reactor vessel. Each gas lift system has a riser 4 with a suction inlet 6 located in the bed 3 and a blow outlet 7 that is at a higher position and opens into the medium washer 2, as well as gas feed means 20 for generating a gas lift in the riser 4. This gas lift sucks medium from the bed, as well as liquid contained in the bed, and feeds these upwards through the riser to the medium washer 2. The medium of the bed is then washed in the medium washer 2 so as, after having been washed, to be returned to the bed via a medium outlet 8 of the medium washer.
  • the liquid to be purified in the reactor vessel is fed via liquid distribution system 10 into the bed 3 in the reactor vessel.
  • Liquid to be purified is introduced via the liquid feed system 10 into the reactor vessel 1.
  • This feed of the liquid to be purified takes place in particular in the bed of granular medium 3.
  • the liquid introduced into the bed 3 passes upwards through the bed 3 and is purified during this passage.
  • a discharge 14, 15 for purified liquid is provided at the top of the reactor vessel 1.
  • this discharge 14, 15 here consists of an overflow trough 14 with a discharge line 15.
  • Broken line 16 indicates the level of the liquid at the top of the reactor vessel.
  • the bed of granular medium 3 is subjected to a downward flow in that the granular medium is drawn up at the bottom by the gas lift systems - this is one gas lift system in the state of the art - and fed upwards to the medium washer 2.
  • the cleaned granular material then drops back onto the top of the bed 3 from the medium washer 2.
  • the bed 3 slopes at the top, as indicated by the broken lines 17 in Figure 1.
  • the medium washer 2 will now be described with reference to Figure 2. Before discussing the medium washer 2 in more detail, it is pointed out that dirt is also already dissociated from the medium in the gas lift, in particular in the risers 4. Further impurities are then removed from the medium in a medium washer.
  • the medium washer 2 comprises a space delimited by a peripheral wall 21.
  • the blow outlets 7 of the risers 4 open into the top of this space.
  • a discharge for liquid to be washed is provided centrally in the chamber 22.
  • This discharge comprises a discharge line 23 and a central inlet pipe section 24.
  • An inlet opening 25 has been made in the top of the inlet pipe section 24.
  • the top end of the pipe section 24 is also provided with a slider 26, by means of which the bottom of this can be set with opening 25.
  • a partition 27 is provided around the top end of the inlet pipe section 24. The reason for this is to form an inlet chamber for the gas lift systems that is separated from the inlet of the inlet pipe section 24. This prevents medium fed upwards with the gas lift being discharged directly from the medium washer via the inlet 24 and the discharge 23.
  • the medium fed into the medium washer via the risers 4 drops down into the medium discharge channel 28 under the influence of gravity.
  • Baffles 29 are provided in the medium discharge channel 28 such that a labyrinth is produced in the discharge channel 28.
  • the liquid feed system 10 comprises a distribution pipe 30 on which a number of- in this example four — connection stubs 32 for pipe sections 31 are provided.
  • the pipe sections 31 extend through the wall of the reactor vessel.
  • the pipe section 31 and the connection stubs 32 are connected to one another by means of flange joints and optionally can also be dismantled.
  • the pipe sections 31 open into the longitudinal ends of each cap 33.
  • the various caps 33 are arranged parallel to one another in the reactor vessel, preferably with a mutual spacing D.
  • the caps 33 are closed off from above, at the longitudinal side edges - preferably also at the longitudinal ends - and are open at the undersides.
  • the caps 33 are generally referred to as so-called distribution arms.
  • the distribution arms can also be constructed in a different way. In the state of the art it is customary to make the distribution arms run in a radial pattern, which has the disadvantage that the spacing between the distribution arms at the radial outer ends is greater than in the centre, which, in turn, is inherently associated with a non-uniform distribution of the liquid over the reactor surface area.
  • Uniform distribution can be achieved by constructing the distribution arms not so much as straight distribution arms but rather as rings or segments of a circle and providing adjacent rings/segments of a circle with a fixed radial spacing in the reactor vessel.
  • this is a relatively complex construction which, moreover, has the disadvantage that a liquid feed system then always has to be designed depending on the diameter of the reactor vessel.
  • the distribution arms straight and positioning them parallel to one another in accordance with the invention, an appreciably simplified liquid feed system is possible.
  • the length of the distribution arms can easily be adapted depending on the distance to be spanned in the reactor vessel. If use is made of a distribution pipe 30 with rigid connection stubs 32, then it is only the manifold 30 that has to be adapted. However, this can easily be overcome by providing flexible lines between the pipes 31 and connection stubs 32 and optionally closing off superfluous connection stubs 32.
  • the gas lift systems comprise a riser 4.
  • This riser can be made of metal and can be rigid, but can also be a flexible line made of, for example, plastic.
  • An air chamber 35, into which a nozzle 7 for blowing in air emerges, is at the bottom of the riser 4.
  • the nozzle 7 for blowing in air is provided with air via the air feed line 20.
  • the air chamber 35 is located concentrically around the bottom end 60 of the riser 4.
  • the air chamber is essentially closed.
  • the air passes from the air chamber 35 into the riser 60, 4 via passages, such as slits. With this arrangement the lift action sucks in liquid and medium via the open bottom end 61.
  • Each gas lift system is provided with a cone 9 at the bottom of the riser 4.
  • the cone 9 is provided with a plate 37 at the bottom and, for the purposes of stable support, bears on the plate 37 via a cylindrical part 36.
  • the cone is connected to the gas chamber 6 by means of arms 38.
  • the gas chamber 6 as such can be connected to the riser 4. This connection can already be made before assembly in the reactor vessel. In this way it becomes possible to lower the whole into the reactor vessel and to fix it in a desired position on the base of the reactor vessel.
  • the broken lines 42 and 43 show, diagrammatically, an interface in the bed of granular material 3 along which the granular medium sinks into the respective cones 9.
  • the portion of the granular medium that is below the broken lines 42 and 43 will then essentially form a sort of dead zone that remains unutilised.
  • the construction height needed in the reactor vessel for the cones 9 of the gas lift systems according to the invention is appreciably less that the construction height in the case of a cone for a reactor vessel according to the state of the art.
  • the dead spaces also termed stagnant zones, are relatively small and do not interfere with, or barely interfere with, the process. Said additional bottom wall sections are then not really necessary.
  • the gas used for the gas lift systems can be air or another suitable gas.
  • Figure 1 also shows, diagrammatically, a control system 50 that via signal leads 54, 55 can control a control valve 51, 52 in each of the feed lines 20 to a gas lift system.
  • the control valves 51, 52 can preferably be controlled independently of one another to allow a specific quantity of gas that has been supplied via line 53 to pass through.
  • the present invention can be employed, inter alia, in: polishing filtration of effluent, on its own or combined with biofiltration; treatment of surface water, groundwater or cooling water, to remove the suspended particles or - after flocculation - dissolved substances.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
PCT/NL2004/000415 2003-06-11 2004-06-11 Liquid purification installation WO2004108247A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
EP04748647A EP1658120A1 (en) 2003-06-11 2004-06-11 Liquid purification installation

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
NL1023641 2003-06-11
NL1023641A NL1023641C2 (nl) 2003-06-11 2003-06-11 Zuiveringsinstallatie.

Publications (1)

Publication Number Publication Date
WO2004108247A1 true WO2004108247A1 (en) 2004-12-16

Family

ID=33509740

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/NL2004/000415 WO2004108247A1 (en) 2003-06-11 2004-06-11 Liquid purification installation

Country Status (4)

Country Link
EP (1) EP1658120A1 (nl)
CN (1) CN1822889A (nl)
NL (1) NL1023641C2 (nl)
WO (1) WO2004108247A1 (nl)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2617779C1 (ru) * 2015-12-10 2017-04-26 Закрытое Акционерное Общество "Аквафор Продакшн" (Зао "Аквафор Продакшн") Устройство очистки жидкости

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS55132612A (en) * 1979-04-02 1980-10-15 Hitachi Chem Co Ltd Moving bed type filter device
US5727908A (en) * 1992-07-14 1998-03-17 Andritz Sprout-Bauer, Inc. Air lift pump for wet particulates
US6471857B1 (en) * 1999-10-27 2002-10-29 Koyo Engineering Co., Ltd. Filter apparatus with sand filter bed

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS55132612A (en) * 1979-04-02 1980-10-15 Hitachi Chem Co Ltd Moving bed type filter device
US5727908A (en) * 1992-07-14 1998-03-17 Andritz Sprout-Bauer, Inc. Air lift pump for wet particulates
US6471857B1 (en) * 1999-10-27 2002-10-29 Koyo Engineering Co., Ltd. Filter apparatus with sand filter bed

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
DATABASE WPI Week 198048, 15 October 1980 Derwent World Patents Index; AN 1980-85130C *
PATENT ABSTRACTS OF JAPAN vol. 005, no. 004 (C - 038) 13 January 1981 (1981-01-13) *

Also Published As

Publication number Publication date
EP1658120A1 (en) 2006-05-24
CN1822889A (zh) 2006-08-23
NL1023641C2 (nl) 2004-12-14

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