WO2004061887A1 - Dispositifs alimentes par des batteries a l'etat solide et procedes de fabrication associes - Google Patents

Dispositifs alimentes par des batteries a l'etat solide et procedes de fabrication associes Download PDF

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Publication number
WO2004061887A1
WO2004061887A1 PCT/US2003/041739 US0341739W WO2004061887A1 WO 2004061887 A1 WO2004061887 A1 WO 2004061887A1 US 0341739 W US0341739 W US 0341739W WO 2004061887 A1 WO2004061887 A1 WO 2004061887A1
Authority
WO
WIPO (PCT)
Prior art keywords
substrate
battery
film
switch
source
Prior art date
Application number
PCT/US2003/041739
Other languages
English (en)
Other versions
WO2004061887A9 (fr
Inventor
Mark L. Jenson
Jody J. Klaassen
Stuart K. Shakespeare
James R. Sullivan
Richard E. Billion
Charles A. Lemaire
Original Assignee
Cymbet Corporation
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US10/336,621 external-priority patent/US7294209B2/en
Priority claimed from US10/336,619 external-priority patent/US20040131760A1/en
Priority claimed from US10/336,662 external-priority patent/US7603144B2/en
Priority claimed from US10/336,620 external-priority patent/US6906436B2/en
Application filed by Cymbet Corporation filed Critical Cymbet Corporation
Priority to AU2003300153A priority Critical patent/AU2003300153A1/en
Priority to CNB2003801100863A priority patent/CN100403477C/zh
Priority to EP03800408A priority patent/EP1590823A4/fr
Priority to JP2004564923A priority patent/JP2006515952A/ja
Publication of WO2004061887A1 publication Critical patent/WO2004061887A1/fr
Publication of WO2004061887A9 publication Critical patent/WO2004061887A9/fr

Links

Classifications

    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01H—ELECTRIC SWITCHES; RELAYS; SELECTORS; EMERGENCY PROTECTIVE DEVICES
    • H01H35/00—Switches operated by change of a physical condition
    • H01H35/14—Switches operated by change of acceleration, e.g. by shock or vibration, inertia switch
    • H01H35/145—Switches operated by change of acceleration, e.g. by shock or vibration, inertia switch operated by a particular acceleration-time function
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01H—ELECTRIC SWITCHES; RELAYS; SELECTORS; EMERGENCY PROTECTIVE DEVICES
    • H01H83/00—Protective switches, e.g. circuit-breaking switches, or protective relays operated by abnormal electrical conditions otherwise than solely by excess current
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01H—ELECTRIC SWITCHES; RELAYS; SELECTORS; EMERGENCY PROTECTIVE DEVICES
    • H01H1/00—Contacts
    • H01H1/0036—Switches making use of microelectromechanical systems [MEMS]
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/04—Construction or manufacture in general
    • H01M10/0436—Small-sized flat cells or batteries for portable equipment
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/058—Construction or manufacture
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/42—Methods or arrangements for servicing or maintenance of secondary cells or secondary half-cells
    • H01M10/425—Structural combination with electronic components, e.g. electronic circuits integrated to the outside of the casing
    • H01M10/4257—Smart batteries, e.g. electronic circuits inside the housing of the cells or batteries
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M6/00—Primary cells; Manufacture thereof
    • H01M6/40—Printed batteries, e.g. thin film batteries
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
    • H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
    • H01G11/08—Structural combinations, e.g. assembly or connection, of hybrid or EDL capacitors with other electric components, at least one hybrid or EDL capacitor being the main component
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
    • H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
    • H01G11/84—Processes for the manufacture of hybrid or EDL capacitors, or components thereof
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01H—ELECTRIC SWITCHES; RELAYS; SELECTORS; EMERGENCY PROTECTIVE DEVICES
    • H01H37/00—Thermally-actuated switches
    • H01H2037/008—Micromechanical switches operated thermally
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01H—ELECTRIC SWITCHES; RELAYS; SELECTORS; EMERGENCY PROTECTIVE DEVICES
    • H01H35/00—Switches operated by change of a physical condition
    • H01H35/14—Switches operated by change of acceleration, e.g. by shock or vibration, inertia switch
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/056—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes
    • H01M10/0561—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes the electrolyte being constituted of inorganic materials only
    • H01M10/0562—Solid materials
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M2004/026—Electrodes composed of, or comprising, active material characterised by the polarity
    • H01M2004/027—Negative electrodes
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M2004/026—Electrodes composed of, or comprising, active material characterised by the polarity
    • H01M2004/028—Positive electrodes
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M2300/00—Electrolytes
    • H01M2300/0017—Non-aqueous electrolytes
    • H01M2300/0065—Solid electrolytes
    • H01M2300/0068—Solid electrolytes inorganic
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M2300/00—Electrolytes
    • H01M2300/0017—Non-aqueous electrolytes
    • H01M2300/0065—Solid electrolytes
    • H01M2300/0068—Solid electrolytes inorganic
    • H01M2300/0071—Oxides
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/52—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
    • H01M4/525—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M50/00—Constructional details or processes of manufacture of the non-active parts of electrochemical cells other than fuel cells, e.g. hybrid cells
    • H01M50/10—Primary casings; Jackets or wrappings
    • H01M50/102—Primary casings; Jackets or wrappings characterised by their shape or physical structure
    • H01M50/11—Primary casings; Jackets or wrappings characterised by their shape or physical structure having a chip structure, e.g. micro-sized batteries integrated on chips
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/50—Manufacturing or production processes characterised by the final manufactured product

Definitions

  • a system includes a substrate, a circuit connected to the substrate, and a thin-film battery connected to the substrate and connected to the circuit.
  • the thin-film battery powers the circuit.
  • An acceleration-enabled switch is also connected to the substrate for electrically activating the circuit.
  • the acceleration-enabled switch is a MEMS device.
  • the acceleration-enabled switch includes at least one cantilevered beam.
  • the acceleration-enabled switch includes at least one cantilevered beam and an electrical contact. The at least one cantilevered beam contacts the electrical contact in response to an acceleration.
  • FIG. 2B is a flowchart of one embodiment of a fabrication process according to the teachings of the present invention.
  • FIG. 2C is a flowchart of one embodiment of a fabrication process according to the teachings of the present invention.
  • FIG. 3 A is a diagram of a device for fabricating a thin-film battery according to the teachings of the present invention.
  • FIG. 8H shows an elevation view of the partially built device of FIG. 8C.
  • FIG. 8M shows a schematic of the device of FIG. 8E at a radio-wave-recharging station.
  • FIG. 24A shows an embodiment of a shipping label that uses an RFID device.
  • FIG. 24B shows an embodiment of a product label that uses an RFID device.
  • FIG. 1A shows an embodiment of an energy-storage device 50 according to the present invention.
  • a substrate 55 is provided, on which is formed a contact film 57.
  • Contact film 57 acts as a current collector and is connected to a lead 58, which, in some embodiments, connects one pole of the energy storage device 50 to an external circuit.
  • the electronic circuit is attached to the battery as formed. In other embodiments, the circuit may be remote from the battery, for example, not attached to the battery as formed.
  • An electrode film 59 is formed on the contact film 57. hi some embodiments, the electrode film 59 substantially covers a surface of the contact film 57 so as to minimize resistance by maximizing the area of the interface between the films.
  • the energized particles are energized ions.
  • the energized ions include a material that is different than the electrode material.
  • the energized particles or the ion beam assist in controlling growth of the structure of the electrode material at the location.
  • process operation 255 is used to form a cathode film or layer 59 for a solid-state, thin-film battery.
  • the cathode film 59 is in electrical and physical contact with the cathode contact.
  • An electrolyte film 61 is deposited, process operation 257, on the cathode film 59.
  • An anode film 63 is deposited, process operation 259, on the electrolyte film.
  • the crystalline structure of a thin film formed according to the teachings herein has a higher order than those achieved by conventional cathode film forming techniques.
  • FIG. 2C shows one embodiment of a method 250C for fabricating an energy-storage device.
  • Process operations 251, 253, 257, 261, and 263 are substantially similar to the process operations described above with reference to Figure 2A.
  • Process operation 255C is a process operation for depositing a cathode film at least partially on the cathode contact film.
  • the cathode film is deposited as described above with reference to Figure 2A.
  • the cathode film is deposited according to other deposition processes known in the art.
  • Process operation 259D is a process operation for depositing an electrode material to a location at least partially on the electrolyte film, while simultaneously supplying energized particles to the electrode material.
  • the energy range in a further embodiment is about 65 eN to about 75 eN.
  • the energy range in a further embodiment is about 10 eN to about 100 eN.
  • the energy range in a further embodiment is about 10 eN to about 90 eN.
  • the energy range in a further embodiment is about 30 eN to about 300 eN.
  • the energy range is in the range of about 60 eN to 150 eN.
  • the energy of the ions from the secondary source is about 70 eN.
  • the ions provide energy in a range of about 45 eN to about 95 eN.
  • An electrolyte third film e.g., films 61, 61 C or 73, having ionic transport qualities but not being electrically conductive (an electrolyte) is deposited so as to completely overlay the second deposited film.
  • the third film is deposited using a first deposition source and a secondary source supplying energetic ions to the growing film.
  • the first deposition source is a physical vapor deposition source.
  • the secondary source is an ion source with the capability of supplying energetic ions having energy greater than 5eV.
  • the energy range is about 5eV to about 3,000eV. In some embodiments, the energy range of is about 5 eV to about l,000eV.
  • Figure 8C shows a plan view of the substrate of Figure 8B after placing and wiring a separately fabricated chip 2440 connected by wires 2441, 2442, and 2443 to the integrated battery 2320 and device 2430 sharing common terminal 2324.
  • Figure 8H shows an elevation view of the partially built device of Figure 8C.
  • FIG. 21 A shows an embodiment of a wireless tagging system 2100.
  • the system includes a Radio Frequency Identification (RFID) device 2170 and a remote RF device 2160 for communicating with the RFID device.
  • RFID device 2170 includes a battery 2120 deposited on a flexible substrate 2110, electronic circuit 2130 placed on the battery 2120 and operatively coupled to the battery 2120 in order for the battery 2120 to provide power to the electronic circuit 2130, an RF antenna 2140 deposited on the battery 2120 and coupled to the electronic circuit 2130, and an adhesive layer 2150 deposited on the side of the flexible substrate that is opposite the battery 2120 and electronic circuit 2130 layer.
  • wiring 2131 connects electronic circuit 2130 to battery 2120 and antenna 2140.
  • Timing circuit 2336 is optionally used to prevent the patient or caregiver from administering doses too often.
  • a caregiver optionally uses the remote RF device to transmit RF energy to initiate a delivery of a bolus of drug, or to interrogate the RFID device to determine the history of drug therapy provided by the device.
  • the RFID device is activated when the RF device activates an RF-actuated switch. In other embodiments, the RFID device is switch-activated when the RFID portion of the device is attached to the drug reservoir portion of the device.
  • the substrate 2809 includes an elastomer, polymer, paper and or plastic web or sheet on which the energy-storage device is fabricated.
  • Substrate 2809 being elongate, allows a plurality of energy-storage devices to be deposited on successive locations of the substrate, thereby improving the rate of energy device production.
  • a plurality of deposition stations 2811 are provided to simultaneously deposit a plurality of films at different locations on the substrate 2809.

Landscapes

  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microelectronics & Electronic Packaging (AREA)
  • Physics & Mathematics (AREA)
  • Electromagnetism (AREA)
  • Battery Mounting, Suspending (AREA)
  • Charge And Discharge Circuits For Batteries Or The Like (AREA)
  • Secondary Cells (AREA)
  • Switches Operated By Changes In Physical Conditions (AREA)
  • Battery Electrode And Active Subsutance (AREA)

Abstract

L'invention concerne un système comprenant une batterie à couches minces (50) et un commutateur à activité activée. Ledit système est placé sur un substrat (55) au moyen d'un support adhésif. Dans des modes de réalisation de l'invention, le substrat est flexible. Un circuit électrique est également formé sur le substrat, lequel comprend des dispositifs électroniques. Ledit commutateur à activité activée place ladite batterie à couches minces en communication électronique avec le circuit et les dispositifs électroniques. La batterie et le circuit sont formés sur le substrat et peuvent comprendre une pluralité de couches déposées.
PCT/US2003/041739 2003-01-02 2003-12-31 Dispositifs alimentes par des batteries a l'etat solide et procedes de fabrication associes WO2004061887A1 (fr)

Priority Applications (4)

Application Number Priority Date Filing Date Title
AU2003300153A AU2003300153A1 (en) 2003-01-02 2003-12-31 Solid-state battery-powered devices and manufacturing methods
CNB2003801100863A CN100403477C (zh) 2003-01-02 2003-12-31 固态电池供电装置及其制造方法
EP03800408A EP1590823A4 (fr) 2003-01-02 2003-12-31 Dispositifs alimentes par des batteries a l'etat solide et procedes de fabrication associes
JP2004564923A JP2006515952A (ja) 2003-01-02 2003-12-31 ソリッドステートのバッテリー給電の装置と製法

Applications Claiming Priority (8)

Application Number Priority Date Filing Date Title
US10/336,619 2003-01-02
US10/336,621 US7294209B2 (en) 2003-01-02 2003-01-02 Apparatus and method for depositing material onto a substrate using a roll-to-roll mask
US10/336,619 US20040131760A1 (en) 2003-01-02 2003-01-02 Apparatus and method for depositing material onto multiple independently moving substrates in a chamber
US10/336,662 2003-01-02
US10/336,620 2003-01-02
US10/336,662 US7603144B2 (en) 2003-01-02 2003-01-02 Active wireless tagging system on peel and stick substrate
US10/336,620 US6906436B2 (en) 2003-01-02 2003-01-02 Solid state activity-activated battery device and method
US10/336,621 2003-01-02

Publications (2)

Publication Number Publication Date
WO2004061887A1 true WO2004061887A1 (fr) 2004-07-22
WO2004061887A9 WO2004061887A9 (fr) 2004-08-26

Family

ID=32719457

Family Applications (1)

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PCT/US2003/041739 WO2004061887A1 (fr) 2003-01-02 2003-12-31 Dispositifs alimentes par des batteries a l'etat solide et procedes de fabrication associes

Country Status (6)

Country Link
EP (1) EP1590823A4 (fr)
JP (1) JP2006515952A (fr)
KR (1) KR20050092384A (fr)
CN (1) CN100403477C (fr)
AU (1) AU2003300153A1 (fr)
WO (1) WO2004061887A1 (fr)

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EP2202767A1 (fr) * 2008-12-24 2010-06-30 STMicroelectronics (Rousset) SAS Dispositif de surveillance de la température d'un élément
EP2328223A1 (fr) * 2009-11-30 2011-06-01 Broadcom Corporation Batterie avec récepteur de puissance sans fil intégré et/ou RFID
US8410637B2 (en) 2009-11-30 2013-04-02 Broadcom Corporation Wireless power system with selectable control channel protocols
US8525370B2 (en) 2009-11-30 2013-09-03 Broadcom Corporation Wireless power circuit board and assembly
WO2014027220A1 (fr) * 2012-08-15 2014-02-20 Nokia Corporation Appareil et procédés pour récolte d'énergie électrique et/ou communication sans fil
US9099410B2 (en) 2003-10-13 2015-08-04 Joseph H. McCain Microelectronic device with integrated energy source
US9590444B2 (en) 2009-11-30 2017-03-07 Broadcom Corporation Device with integrated wireless power receiver configured to make a charging determination based on a level of battery life and charging efficiency
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DE102010028868B4 (de) * 2010-05-11 2019-11-14 Robert Bosch Gmbh Halbleitersubstratbasierte Anordnung für eine RFID-Einrichtung, RFID-Einrichtung und Verfahren zur Herstellung einer solchen halbleitersubstratbasierten Anordnung
CN110663135A (zh) * 2017-05-31 2020-01-07 Tdk电子股份有限公司 混合式能量供应电路、混合式能量供应电路的应用和用于制造混合式能量供应电路的方法
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EP1590823A4 (fr) 2007-05-30
CN100403477C (zh) 2008-07-16
JP2006515952A (ja) 2006-06-08
AU2003300153A1 (en) 2004-07-29
WO2004061887A9 (fr) 2004-08-26
EP1590823A1 (fr) 2005-11-02
CN1757086A (zh) 2006-04-05
KR20050092384A (ko) 2005-09-21

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