WO2003066562A3 - PROCEDE DE PREPARATION DE COMPOSES ω-BROMOALKYLCARBOXYLIQUES - Google Patents

PROCEDE DE PREPARATION DE COMPOSES ω-BROMOALKYLCARBOXYLIQUES Download PDF

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Publication number
WO2003066562A3
WO2003066562A3 PCT/FR2003/000262 FR0300262W WO03066562A3 WO 2003066562 A3 WO2003066562 A3 WO 2003066562A3 FR 0300262 W FR0300262 W FR 0300262W WO 03066562 A3 WO03066562 A3 WO 03066562A3
Authority
WO
WIPO (PCT)
Prior art keywords
bromoalkylcarboxylic
preparing
solvent
compounds
acid
Prior art date
Application number
PCT/FR2003/000262
Other languages
English (en)
Other versions
WO2003066562A2 (fr
Inventor
Christophe Ruppin
Philippe Gillet
Original Assignee
Atofina
Christophe Ruppin
Philippe Gillet
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Atofina, Christophe Ruppin, Philippe Gillet filed Critical Atofina
Priority to AU2003222342A priority Critical patent/AU2003222342A1/en
Publication of WO2003066562A2 publication Critical patent/WO2003066562A2/fr
Publication of WO2003066562A3 publication Critical patent/WO2003066562A3/fr

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/09—Preparation of carboxylic acids or their salts, halides or anhydrides from carboxylic acid esters or lactones
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

L'invention concerne un procédé de préparation d'acide ω-bromoolkylcarboxyliques et de leurs esters, les ω-bromoalcanoates d'alkyle qui consiste à faire réagir HBr gazeux avec une lactone en absence de solvant à une température supérieure à la température de fusion du milieu réactionnel puis à estérifier l'acide ω-bromoalkylcarboxylique avec un alcool en milieu solvant et sans ajout de catalyseur, de façon à extraire l'eau sous forme d'un héteroazéotrope ternaire eau / solvant / alcool par distillation extractive.
PCT/FR2003/000262 2002-02-06 2003-01-28 PROCEDE DE PREPARATION DE COMPOSES ω-BROMOALKYLCARBOXYLIQUES WO2003066562A2 (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
AU2003222342A AU2003222342A1 (en) 2002-02-06 2003-01-28 Method for preparing $g(v)-bromoalkylcarboxylic compounds

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR02/01392 2002-02-06
FR0201392A FR2835524A1 (fr) 2002-02-06 2002-02-06 Procede de preparation de composes omega -bromoalkylcarboxyliques

Publications (2)

Publication Number Publication Date
WO2003066562A2 WO2003066562A2 (fr) 2003-08-14
WO2003066562A3 true WO2003066562A3 (fr) 2004-04-01

Family

ID=27619926

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/FR2003/000262 WO2003066562A2 (fr) 2002-02-06 2003-01-28 PROCEDE DE PREPARATION DE COMPOSES ω-BROMOALKYLCARBOXYLIQUES

Country Status (3)

Country Link
AU (1) AU2003222342A1 (fr)
FR (1) FR2835524A1 (fr)
WO (1) WO2003066562A2 (fr)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100340538C (zh) * 2005-11-03 2007-10-03 复旦大学 5－溴戊酸的制造方法
CN1319926C (zh) * 2005-11-03 2007-06-06 复旦大学 4－溴丁酸的制造方法
CN114736119B (zh) * 2022-05-09 2024-02-06 迈奇化学股份有限公司 一种4-溴丁酸乙酯的一步制备法
CN117865802A (zh) * 2024-03-11 2024-04-12 山东顺成化学有限公司 一种4-溴丁酸乙酯的制备方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB753686A (en) * 1953-03-16 1956-07-25 Celanese Corp Production of haloacids
US3917618A (en) * 1972-06-30 1975-11-04 Wyeth John & Brother Ltd {68 -(1-Piperidino)thiocarproamides
US5902895A (en) * 1996-05-04 1999-05-11 Huels Aktiengesellschaft Method for the continuous production of esters of thermally unstable acids

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB753686A (en) * 1953-03-16 1956-07-25 Celanese Corp Production of haloacids
US3917618A (en) * 1972-06-30 1975-11-04 Wyeth John & Brother Ltd {68 -(1-Piperidino)thiocarproamides
US5902895A (en) * 1996-05-04 1999-05-11 Huels Aktiengesellschaft Method for the continuous production of esters of thermally unstable acids

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
BROWN, G. B. ET AL: "The Preparation of Ethyl epsilon-Bromocaproate", JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, vol. 66, 1944, pages 839, XP002248688 *

Also Published As

Publication number Publication date
AU2003222342A8 (en) 2003-09-02
AU2003222342A1 (en) 2003-09-02
FR2835524A1 (fr) 2003-08-08
WO2003066562A2 (fr) 2003-08-14

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