WO1993023579A1 - Procede et dispositif de recuperation et de valorisation de composes metalliques - Google Patents
Procede et dispositif de recuperation et de valorisation de composes metalliques Download PDFInfo
- Publication number
- WO1993023579A1 WO1993023579A1 PCT/FR1993/000450 FR9300450W WO9323579A1 WO 1993023579 A1 WO1993023579 A1 WO 1993023579A1 FR 9300450 W FR9300450 W FR 9300450W WO 9323579 A1 WO9323579 A1 WO 9323579A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- heat treatment
- enclosure
- composite material
- constituents
- waste
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract description 17
- 150000001875 compounds Chemical class 0.000 title abstract description 3
- 238000011084 recovery Methods 0.000 title description 3
- 238000010438 heat treatment Methods 0.000 claims abstract description 23
- 239000002184 metal Substances 0.000 claims abstract description 20
- 229910052751 metal Inorganic materials 0.000 claims abstract description 20
- 239000000470 constituent Substances 0.000 claims abstract description 18
- 239000002131 composite material Substances 0.000 claims abstract description 17
- 239000000463 material Substances 0.000 claims abstract description 10
- 238000000926 separation method Methods 0.000 claims abstract description 7
- 239000006227 byproduct Substances 0.000 claims abstract description 6
- 238000000197 pyrolysis Methods 0.000 claims abstract description 4
- 239000011230 binding agent Substances 0.000 claims abstract description 3
- 239000000567 combustion gas Substances 0.000 claims abstract description 3
- 238000004806 packaging method and process Methods 0.000 claims abstract description 3
- 239000002699 waste material Substances 0.000 claims description 16
- 239000002245 particle Substances 0.000 claims description 10
- 238000004320 controlled atmosphere Methods 0.000 claims description 4
- 230000003750 conditioning effect Effects 0.000 claims description 3
- 230000001590 oxidative effect Effects 0.000 claims description 3
- 239000000047 product Substances 0.000 claims description 3
- 230000001066 destructive effect Effects 0.000 claims description 2
- 238000000605 extraction Methods 0.000 claims description 2
- 239000007789 gas Substances 0.000 claims description 2
- 238000005469 granulation Methods 0.000 claims description 2
- 230000003179 granulation Effects 0.000 claims description 2
- 238000000227 grinding Methods 0.000 claims description 2
- 238000000746 purification Methods 0.000 abstract 1
- 229910052802 copper Inorganic materials 0.000 description 9
- 239000010949 copper Substances 0.000 description 9
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 7
- 238000009434 installation Methods 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000002485 combustion reaction Methods 0.000 description 2
- 230000001143 conditioned effect Effects 0.000 description 2
- 238000005520 cutting process Methods 0.000 description 2
- 239000003822 epoxy resin Substances 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- LNEPOXFFQSENCJ-UHFFFAOYSA-N haloperidol Chemical compound C1CC(O)(C=2C=CC(Cl)=CC=2)CCN1CCCC(=O)C1=CC=C(F)C=C1 LNEPOXFFQSENCJ-UHFFFAOYSA-N 0.000 description 2
- 229920000647 polyepoxide Polymers 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 150000001879 copper Chemical class 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000003517 fume Substances 0.000 description 1
- 238000007499 fusion processing Methods 0.000 description 1
- 150000002736 metal compounds Chemical class 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000002341 toxic gas Substances 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B7/00—Working up raw materials other than ores, e.g. scrap, to produce non-ferrous metals and compounds thereof; Methods of a general interest or applied to the winning of more than two metals
- C22B7/001—Dry processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B17/00—Recovery of plastics or other constituents of waste material containing plastics
- B29B17/02—Separating plastics from other materials
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B15/00—Obtaining copper
- C22B15/0026—Pyrometallurgy
- C22B15/0056—Scrap treating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B17/00—Recovery of plastics or other constituents of waste material containing plastics
- B29B17/02—Separating plastics from other materials
- B29B2017/0213—Specific separating techniques
- B29B2017/0268—Separation of metals
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B17/00—Recovery of plastics or other constituents of waste material containing plastics
- B29B17/04—Disintegrating plastics, e.g. by milling
- B29B2017/0424—Specific disintegrating techniques; devices therefor
- B29B2017/0496—Pyrolysing the materials
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2705/00—Use of metals, their alloys or their compounds, for preformed parts, e.g. for inserts
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2705/00—Use of metals, their alloys or their compounds, for preformed parts, e.g. for inserts
- B29K2705/08—Transition metals
- B29K2705/10—Copper
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29L—INDEXING SCHEME ASSOCIATED WITH SUBCLASS B29C, RELATING TO PARTICULAR ARTICLES
- B29L2009/00—Layered products
- B29L2009/003—Layered products comprising a metal layer
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29L—INDEXING SCHEME ASSOCIATED WITH SUBCLASS B29C, RELATING TO PARTICULAR ARTICLES
- B29L2031/00—Other particular articles
- B29L2031/34—Electrical apparatus, e.g. sparking plugs or parts thereof
- B29L2031/3425—Printed circuits
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/62—Plastics recycling; Rubber recycling
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/80—Packaging reuse or recycling, e.g. of multilayer packaging
Definitions
- the present invention relates to a method and a device for ensuring the separation and recovery of metallic constituents and / or other recoverable constituents present in a composite material, in particular plastic-metal laminate.
- the invention applies in particular, without being limited to such an application, to the recovery of copper contained in laminate plates for printed circuits.
- laminate plates for printed circuits consisting of a glass fabric support bonded by epoxy resins on which is deposited a coating of copper of very high purity, it is necessary to cut to the desired format of relatively large plates significant, which results in falls comprising a significant proportion of very high purity copper (of the order of 99.95%).
- very high purity copper of the order of 99.95%).
- the present invention has set itself the objective of carrying out the separation of metallic compounds and in particular copper, contained in a composite material by means of a process which does not have the drawbacks mentioned above of the prior techniques.
- the invention relates to a process for separating recoverable metal constituents such as in particular glass-resin-metal contained in a composite material, in particular plastic-metal laminate, characterized in that it consists in:
- the atmosphere controlled during the heat treatment can be oxidizing or reducing.
- the temperature of this heat treatment is approximately 400 ° C.
- the invention also relates to a device for implementing the method as specified above.
- a heat treatment chamber supplied with waste of composite material and in which the pyrolysis of this waste is carried out at a temperature between 350 and 450 ° C, preferably about 400 ° C, the combustion gases of the binders contained in the material composite being evacuated from said enclosure to be treated and purified by conventional means;
- - grinding means receiving the material from the heat treatment enclosure; - means ensuring the separation of recoverable metal constituents from the by-products and;
- said heat treatment enclosure is produced in the form of an enclosure with heat transfer particles, which may for example be of the particle rain, fluidized bed or vibrated bed type.
- the waste of said composite material previously reduced to the necessary dimensions is brought on a continuous conveyor of various types, carpet, vibrator, etc. and in this case a rotary drum positioned in said heat treatment enclosure and more particularly in the bed of particles, the feeding of said drum being carried out using a feed screw placed at one of its ends and the extraction and evacuation of the treated waste being carried out using a system conventional lifter provided at the other end of said drum.
- this process is essentially characterized by the fact that the waste of composite material containing a recoverable metallic constituent, in particular a red metal such as copper, is treated in a heat treatment enclosure. in which is maintained a temperature between 350 and 450 ° C, preferably 400 ° C, a controlled atmosphere being maintained in said enclosure so as to avoid any ignition of the products resulting from the combustion of flammable materials.
- a recoverable metallic constituent in particular a red metal such as copper
- the treated material undergoes a sorting operation in order to separate the recoverable metal component, the latter then being conditioned.
- the single figure represents, by way of nonlimiting example an installation making it possible to ensure the implementation of the method according to the invention.
- This installation comprises a feed hopper 10 in which the waste of the composite material is stored (for example waste resulting from the cutting of printed circuit boards), these having been previously conditioned, for example by cutting them to the desired dimensions.
- This hopper 10 feeds, by means of conventional dosing and weighing devices not shown in the drawing, the heat treatment chamber 12 in which a temperature between about 350 and 450 ° C. is maintained as well as a controlled atmosphere can be oxidizing or reducing.
- This "heat treatment chamber 12 is preferably a particle oven, for example a fluidized bed, vibrated bed or particle rain oven.
- the waste coming from the hopper of storage 10 are brought to a conveyor and, in this case in a rotary drum placed in the particle bed, the feeding of this drum being carried out by any conventional means, in particular a conveyor screw placed at one end of said drum and the treated waste is removed using conventional lifting systems positioned at the other end of this drum.
- a conveyor screw placed at one end of said drum and the treated waste is removed using conventional lifting systems positioned at the other end of this drum.
- the treated waste coming from the furnace 12 is brought into a hopper 14 supplying a crusher 16 from which this treated waste and reduced to the desired dimensions is
- the valuable metal components are fed into a scrubber 26 to be subsequently stored after treatment in a hopper 28 feeding a packaging installation 5 30.
- This conditioning can be performed so as to perform a compacting granulation of the recovered metallic component which is then packaged and evacuated.
- the installation naturally includes conventional means for purifying and dedusting the fumes extracted from the pyrolysis furnace 12 (these installations of well known type have not been shown in the drawing). It also includes a system for purifying and filtering the air from the separator 18 and the purifier 26. Here still these are systems well known to those skilled in the art and for this reason, they will not be described here.
- the invention allows under particularly advantageous economic conditions to recover metallic components of high purity contained in composite materials, in particular plastic-metal laminates. This is how this invention makes it possible to recover the copper contained in waste originating from the production of printed circuit boards.
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Environmental & Geological Engineering (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Processing Of Solid Wastes (AREA)
- Manufacture And Refinement Of Metals (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR92/05697 | 1992-05-11 | ||
| FR9205697A FR2690928A1 (fr) | 1992-05-11 | 1992-05-11 | Procédé et dispositif de récupération et de valorisation de composés métalliques. |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| WO1993023579A1 true WO1993023579A1 (fr) | 1993-11-25 |
Family
ID=9429672
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PCT/FR1993/000450 WO1993023579A1 (fr) | 1992-05-11 | 1993-05-10 | Procede et dispositif de recuperation et de valorisation de composes metalliques |
Country Status (4)
| Country | Link |
|---|---|
| AU (1) | AU4074693A (enrdf_load_stackoverflow) |
| FR (1) | FR2690928A1 (enrdf_load_stackoverflow) |
| TW (1) | TW221830B (enrdf_load_stackoverflow) |
| WO (1) | WO1993023579A1 (enrdf_load_stackoverflow) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2000009771A1 (en) * | 1998-08-12 | 2000-02-24 | Corenso United Oy Ltd. | Liquid carton waste material recycling process and apparatus for recycling liquid carton waste material |
| US6511656B2 (en) | 2000-07-12 | 2003-01-28 | L'oreal S.A. | Compositions for coloring the skin comprising at least one flavylium salt which is unsubstituted in position 3 and at least one organomodified silicone |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE4418562A1 (de) * | 1993-06-29 | 1995-01-12 | Leybold Durferrit Gmbh | Verfahren und Vorrichtung zur Behandlung von im wesentlichen aus Kunststoff oder Gummi bestehendem Gut |
| FR2938457B1 (fr) * | 2008-11-14 | 2011-01-07 | Terra Nova | Procede de recuperation des metaux contenus dans les dechets electroniques |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3821026A (en) * | 1971-11-05 | 1974-06-28 | E Swartz | Scrap metal recovery method and apparatus |
| FR2226362A1 (enrdf_load_stackoverflow) * | 1973-04-19 | 1974-11-15 | Lonza Ag | |
| EP0239227A1 (en) * | 1986-02-19 | 1987-09-30 | Camlaw Limited | Fluidised bed process for the recovery of finely divided metals |
| EP0274059A2 (en) * | 1986-12-12 | 1988-07-13 | Recytec S.A. | Process for the recycling of electrical batteries, assembled printed circuit boards and electronic components |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS62103325A (ja) * | 1985-10-31 | 1987-05-13 | Hiroshi Soma | 金属−プラスチツク複合材料から当該金属を回収する方法およびその装置 |
| DD292676A5 (de) * | 1985-12-13 | 1991-08-08 | Kombinat Lew "Hans Beimler",De | Verfahren zur kontinuierlichen metallrueckgewinnung von metallkaschierten schichtpressstoffplattenabfaellen |
-
1992
- 1992-05-11 FR FR9205697A patent/FR2690928A1/fr active Pending
-
1993
- 1993-05-10 AU AU40746/93A patent/AU4074693A/en not_active Abandoned
- 1993-05-10 WO PCT/FR1993/000450 patent/WO1993023579A1/fr active Application Filing
- 1993-06-19 TW TW82103544A patent/TW221830B/zh active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3821026A (en) * | 1971-11-05 | 1974-06-28 | E Swartz | Scrap metal recovery method and apparatus |
| FR2226362A1 (enrdf_load_stackoverflow) * | 1973-04-19 | 1974-11-15 | Lonza Ag | |
| EP0239227A1 (en) * | 1986-02-19 | 1987-09-30 | Camlaw Limited | Fluidised bed process for the recovery of finely divided metals |
| EP0274059A2 (en) * | 1986-12-12 | 1988-07-13 | Recytec S.A. | Process for the recycling of electrical batteries, assembled printed circuit boards and electronic components |
Non-Patent Citations (3)
| Title |
|---|
| DATABASE WPI Week 2, 1992 Derwent Publications Ltd., London, GB; AN 92-008156 * |
| JOM vol. 44, no. 7, Juillet 1992, WARRENDALE US pages 43 - 48 JAMES E. HOFFMAN 'Recovering Precious Metals from Electronic Scrap' * |
| PATENT ABSTRACTS OF JAPAN vol. 11, no. 317 (C-452)15 Octobre 1987 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2000009771A1 (en) * | 1998-08-12 | 2000-02-24 | Corenso United Oy Ltd. | Liquid carton waste material recycling process and apparatus for recycling liquid carton waste material |
| WO2000009770A1 (en) * | 1998-08-12 | 2000-02-24 | Foster Wheeler Energia Oy | Process and apparatus for recovering metal material from waste material |
| US6401635B1 (en) | 1998-08-12 | 2002-06-11 | Corenso United Oy Ltd. | Liquid carton waste material recycling process and apparatus for recycling liquid carton waste material |
| US6409798B1 (en) | 1998-08-12 | 2002-06-25 | Foster Wheeler Energia Oy | Process for recovering metal material from waste material |
| US6511656B2 (en) | 2000-07-12 | 2003-01-28 | L'oreal S.A. | Compositions for coloring the skin comprising at least one flavylium salt which is unsubstituted in position 3 and at least one organomodified silicone |
Also Published As
| Publication number | Publication date |
|---|---|
| FR2690928A1 (fr) | 1993-11-12 |
| TW221830B (enrdf_load_stackoverflow) | 1994-03-21 |
| AU4074693A (en) | 1993-12-13 |
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