US954451A - Desiccating apparatus. - Google Patents

Desiccating apparatus. Download PDF

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US954451A
US954451A US38602607A US1907386026A US954451A US 954451 A US954451 A US 954451A US 38602607 A US38602607 A US 38602607A US 1907386026 A US1907386026 A US 1907386026A US 954451 A US954451 A US 954451A
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conduit
chamber
air
desiccating
liquid
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US38602607A
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Irving S Merrell
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MERRELL-SOULE Co
MERRELL SOULE CO
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MERRELL SOULE CO
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/16Evaporating by spraying
    • B01D1/18Evaporating by spraying to obtain dry solids

Definitions

  • This system of desiccation requires the use of some form of atomizer or spraying device in which the liquid passalge is necessaril small and, therefore, easi y congested or c ogged by the constituent solids of the liquids, when heated moisture-absorbentis used unless some provision is made for kee ing the temperature of the liquid norma or below that of the heated moistureabsorbent while in transit through the atomizei' or spraying device to the desiccating chamber.
  • M v object therefore, is to insulate the liquid passage of the atomizer against the heat of the moisture-absorbing air passing therethrough so as to prevent the'concentration or thickenin of the liquid in tlie. liquid passage, and tiereby prevent congestion orstoppage of such passage and injury to the solids of the material.
  • I have sought to maintain an open liquid passage through the atomizer by new either insulating such passage from4 the heated moisture-absorbent, or by cooling .said passage by means of a circulating eooling agent surrounding same, or by both of these means, if necessary.
  • the discharge end of the conduit 2- of the atomizer is surrounded by a tubular cap. or shell -4- of greater cross sectional area than that of the liquid conduit -2- forming an intervening cooling chamber 5* which is closed at its inner end adjacent to the desiccating chamber -1- and is provided with an inlet conduit -6- and an outlet conduit .-7- for the circulation of a cooling agent, as water which is allowed to circulate freely around conduit -2- which is inclosed by the shell -flfso as to keep the temperature of the liquid passin through the conduit -2- normal, or su ciently below that of the iniowing heated air throii h the conduit w3h to prevent concentration or thickening of the liquid while in transit through the atomizer to the desiccatin chamber.
  • a cooling agent as water which is allowed to circulate freely around conduit -2- which is inclosed by the shell -flfso as to keep the temperature of the liquid passin through the conduit -2- normal, or su c
  • the conduit -3- for tie introduction of heated air'into the desiccating chamber is of somewhat greater diameter than the portion of the shell -4- which it incloses and iii order that the liquid passing through the conduit -2- may be further protected from the-heat of the moisture-absorbing air passing through the atomizer, a jacket -8- of heat-insulating material, such as asbestos or its equivalent, is interposed between the shells 4 and conduit 3 and 1s referably fitted closely upon the outer sur ace of the portion of the shell -4- surrounded by the air conduit -3- in such manner as to eHectively prevent the liquid from absorbing the heat from the air until after the liqthe portion of the r uid and air are commingled in the desiccating chamber, whereupon the air absorbs and carries od the moisture of the finely divided particles through a screen 9 in one side of the desiccating chamber, leaving the constituent solids in the form of a dry powder which is collected within the desiccating chamber
  • any means may be employed for heating the airA in the conduit -3-, and for this purpose.
  • ll have shown a heating chamber -10- inclosing a system of pipes or conduits -l1-, through which the circulating agent, as steam or hot water, may be introduced to heat the air in the chamber l0- which is provided with a supply pipe -12.- and outlet pipe -l3, the latter discharging into the conduit -3- of the atomizer.
  • this class of apparatus it is desirable to introduce the heated air into the desiccating chamber under ressure so as to split up or spray'the liquid) into the desiccating chamber2 where desiccation takes place, as previously stated.
  • any suitable device may be employed for forcing the air 'through the chamber 10- and thence, through the conduit -3 into l the desiccating chamber, and for this purpose l have shown an ordinary air pump consisting of a cylinder 1dand piston --15-, the latterbeing actuated by any suitable mechanism, as a revolving crankarm -16- and connecting link -17- attached to the piston rod, said pump being provided with an inlet -18- having a check-valve -19-, and is also provided with an outlet 20 and a check-valve -21-, the check-valve -19- opening to admit air on the out-stroke of the piston and closing to prevent reflux on the downstroke of said piston while the other valve opens on the down-stroke to admit air to the heating chamber 10 and closes on .the upstroke of the piston to prevent reflux of the air from the heating chamber to the pump.
  • an ordinary air pump consisting of a cylinder 1dand piston --15-, the latterbeing actuated by any suitable mechanism, as a revol
  • the liquid may be forced through the conduit ⁇ -2- by any suitable means, preferably by gravity, and for this purpose l have shown a supply tank -22, as connected to the pipe -2- in a plane some distance above the outlet into the desiccating chamber.
  • the heated air and liquid are introduced simultaneously at'substantially the same point into the desiccatf ingI chamber, whereby the liquid is split up into a finely divided state, and the particles enveloped by the heated air which rapidly absorbs and carries of the moisture through the screen 9'- allowing the dry powdered solids to remain withln the desiccating chamber.
  • the conduit '-2 ⁇ which is surrounded by the heated air conduit -3-, is kept cool by @einer the circulation oi' a cooling agent through the chamber "Exand around the mouth of the conduit -2-, While at the same time the heat insulation -8- further protects the liquid passing through the conduit 2 of the atomizer against absorbing any the heat of the heated air in the conduit -3- until after the air and liquid have been liberated in the desiccating chamber.
  • a desiccating apparatus a desiccating chamber, a liquid supply conduit discharging into the desiccating chamber, a coolingchamber surrounding the discharge end of the liquid supply conduit and closed at its inner end nearest the desiccating chamber, a jacket of heat insulating material sur-v rounding the cooling chamber, and an air supply conduit surrounding said jacket and discharging into the desiccating chamber,
  • a desiccating apparatus a desiccatchamber being provided with an inlet and an outlet -for permitting the circulation or the cooling agent therethrough, a jacket oi" heat insulating material surrounding the cooling chamber, and an air conduit surrounding the jacket and having a tapering inner end discharging into the desiccating chamber.
  • a desiccating apparatus of the. class described a desiccating chamber, an air conduit discharging into the desiccating chamber, means for heating the air in transit thereto, a liquid conduit coterminating with the air conduit and discharging into the desiccating chamber, a cooling'chamber between the discharge end of the liquid conduit and the discharge end of the air conduit, and a jacket for heat insulation between thecooling chamber and the air conduit.
  • a desiccatingchamber an atomizer discharging into the desiccating chamber and comprising a liquid conduit and an air conduit, means for heating the air passing through the air conduit, and means including a jacket of heat insulating material between the liquid conduit and air conduit for preventing transmission of the heat from the air chamber to the liquid conduit at the point of discharge into the desiccating chaml ber.
  • a desiccating chamber an atomizer comprising a liquid conduit and an air Vconduit discharging at Vsubstantially the same point into the desiccating chamber, the air conduit having a tapering inner end whereby the liquid is s lit up into finely divided particles, means or heating the air in transit to the desiccating chamber, and means including a' cooling chamber and a jacket of heat insulating material, both located between the liquid conduit and air conduit for keeping the temperature of the liquid below that of the heated air while 1n transit to the desiccatin chamber.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Description

I. S. MERRELL.
DBSIGGATING APPARATUS,
APPLIOATION FILED JULY29,1907.
954,451 Patented Apr. 12, 1910.
UNITED STATES i PATENT OFFICE.
IRVING S. MERRELL, OF SYRACUSE, NEW' YORK, ASSIGNOR TO MERRELL-SOULE COM- PANY, F SYRACUSE, NEW YORK, .A CORPORATION 0F NEW YORK.
DESICCATING APPARATUS.
Specication of Letters Patent.
Patented Apr. 12, 1910.
Application filed .Tuly 29, 1907. Serial No. 386,026.
i To all whom it 'may concern:
Be it known that I, lnvixc. S. MERRELL, of Syracuse, in the county of Ononda a, in the State of New York, have invente and useful Improvements in Desiccating Apparatus, of which the following, taken in connection with the accompanying drawings, is a full, clear, and exact description. Thisinvention relates to certain improvements in apparatus for desiccating the constituent solids of liquids, such as milk and other liquids containing a large amount of moisture. In this class of apparatus the liquid is introduced in a finely divided state or. spray, together with the moisture-absorbing gas, as air, into a suitable desiccating chamber where the moisture of the finely divided articles is rapidly taken up and .carried o by the absorbent gas or air, leaving the solids in the form of'a dry powder containing the same pro erties and characteristics as existed in t e original liquid and adapted to be collected separately from the moisture-laden air or gas. This system of desiccation requires the use of some form of atomizer or spraying device in which the liquid passalge is necessaril small and, therefore, easi y congested or c ogged by the constituent solids of the liquids, when heated moisture-absorbentis used unless some provision is made for kee ing the temperature of the liquid norma or below that of the heated moistureabsorbent while in transit through the atomizei' or spraying device to the desiccating chamber. Y
In my present apparatus which is employed iii carrying out the process described in in v pending application Serial No. 386.025. tiled July QS), 1907 I preferably eniplov heated air as the moisture-absorbent, which is introduced under ressure through the atomizer and into the dsiccating chamber simultaneously with the introduction of the liquid.
M v object, therefore, is to insulate the liquid passage of the atomizer against the heat of the moisture-absorbing air passing therethrough so as to prevent the'concentration or thickenin of the liquid in tlie. liquid passage, and tiereby prevent congestion orstoppage of such passage and injury to the solids of the material. In other words, I have sought to maintain an open liquid passage through the atomizer by new either insulating such passage from4 the heated moisture-absorbent, or by cooling .said passage by means of a circulating eooling agent surrounding same, or by both of these means, if necessary.
Other objects and uses relating to the s ecific construction of the atomizer and reg. tive arrangement of the Various parts of the apparatus. will be brought out in the following description.
In the drawings-I have shown a sectional view, partly in elevation, of an apparatus for cai'ryin out the objects hereinbefore stated, andg comprising essentially a desiccating chamber -1-; a liquid supply conduit -2- and an air conduit -3- sui'- roundiiig the li uid conduit --2, and together with sai liquid conduit constitutes an atomizer discharging into the desiccating chamber -1-.
The discharge end of the conduit 2- of the atomizer is surrounded by a tubular cap. or shell -4- of greater cross sectional area than that of the liquid conduit -2- forming an intervening cooling chamber 5* which is closed at its inner end adjacent to the desiccating chamber -1- and is provided with an inlet conduit -6- and an outlet conduit .-7- for the circulation of a cooling agent, as water which is allowed to circulate freely around conduit -2- which is inclosed by the shell -flfso as to keep the temperature of the liquid passin through the conduit -2- normal, or su ciently below that of the iniowing heated air throii h the conduit w3h to prevent concentration or thickening of the liquid while in transit through the atomizer to the desiccatin chamber.
The conduit -3- for tie introduction of heated air'into the desiccating chamber is of somewhat greater diameter than the portion of the shell -4- which it incloses and iii order that the liquid passing through the conduit -2- may be further protected from the-heat of the moisture-absorbing air passing through the atomizer, a jacket -8- of heat-insulating material, such as asbestos or its equivalent, is interposed between the shells 4 and conduit 3 and 1s referably fitted closely upon the outer sur ace of the portion of the shell -4- surrounded by the air conduit -3- in such manner as to eHectively prevent the liquid from absorbing the heat from the air until after the liqthe portion of the r uid and air are commingled in the desiccating chamber, whereupon the air absorbs and carries od the moisture of the finely divided particles through a screen 9 in one side of the desiccating chamber, leaving the constituent solids in the form of a dry powder which is collected within the desiccating chamber whence it may be removed at will.
Any means may be employed for heating the airA in the conduit -3-, and for this purpose. ll have shown a heating chamber -10- inclosing a system of pipes or conduits -l1-, through which the circulating agent, as steam or hot water, may be introduced to heat the air in the chamber l0- which is provided with a supply pipe -12.- and outlet pipe -l3, the latter discharging into the conduit -3- of the atomizer. 1n this class of apparatus it is desirable to introduce the heated air into the desiccating chamber under ressure so as to split up or spray'the liquid) into the desiccating chamber2 where desiccation takes place, as previously stated. v
Any suitable device may be employed for forcing the air 'through the chamber 10- and thence, through the conduit -3 into l the desiccating chamber, and for this purpose l have shown an ordinary air pump consisting of a cylinder 1dand piston --15-, the latterbeing actuated by any suitable mechanism, as a revolving crankarm -16- and connecting link -17- attached to the piston rod, said pump being provided with an inlet -18- having a check-valve -19-, and is also provided with an outlet 20 and a check-valve -21-, the check-valve -19- opening to admit air on the out-stroke of the piston and closing to prevent reflux on the downstroke of said piston while the other valve opens on the down-stroke to admit air to the heating chamber 10 and closes on .the upstroke of the piston to prevent reflux of the air from the heating chamber to the pump.
The liquid may be forced through the conduit `-2- by any suitable means, preferably by gravity, and for this purpose l have shown a supply tank -22, as connected to the pipe -2- in a plane some distance above the outlet into the desiccating chamber. i
It now appears that the heated air and liquid are introduced simultaneously at'substantially the same point into the desiccatf ingI chamber, whereby the liquid is split up into a finely divided state, and the particles enveloped by the heated air which rapidly absorbs and carries of the moisture through the screen 9'- allowing the dry powdered solids to remain withln the desiccating chamber. During this feedingof the liquid and air into the desiccating chamber, the conduit '-2` which is surrounded by the heated air conduit -3-, is kept cool by @einer the circulation oi' a cooling agent through the chamber "Exand around the mouth of the conduit -2-, While at the same time the heat insulation -8- further protects the liquid passing through the conduit 2 of the atomizer against absorbing any the heat of the heated air in the conduit -3- until after the air and liquid have been liberated in the desiccating chamber.
What claim ist l. ln combination with a desiccating chamber, a liquid supply conduit d1scharging into the desiccating chamber, a cooling chamber surrounding the discharge end of the liquid supply conduit, a acket of heat insulating material surrounding the cooling chamber, and an air conduit surrounding the jacket andalso discharging into the desiccating chamber. j
2. ln a desiccating apparatus,a desiccating chamber, a liquid supply conduit discharging into the desiccating chamber, a coolingchamber surrounding the discharge end of the liquid supply conduit and closed at its inner end nearest the desiccating chamber, a jacket of heat insulating material sur-v rounding the cooling chamber, and an air supply conduit surrounding said jacket and discharging into the desiccating chamber,
3. ln a desiccating apparatus, a desiccatchamber being provided with an inlet and an outlet -for permitting the circulation or the cooling agent therethrough, a jacket oi" heat insulating material surrounding the cooling chamber, and an air conduit surrounding the jacket and having a tapering inner end discharging into the desiccating chamber.
4. ln a desiccating apparatus of the. class described, a desiccating chamber, an air conduit discharging into the desiccating chamber, means for heating the air in transit thereto, a liquid conduit coterminating with the air conduit and discharging into the desiccating chamber, a cooling'chamber between the discharge end of the liquid conduit and the discharge end of the air conduit, and a jacket for heat insulation between thecooling chamber and the air conduit.
5. In a desiccating apparatus of the class described, a desiccatingchamber, an atomizer discharging into the desiccating chamber and comprising a liquid conduit and an air conduit, means for heating the air passing through the air conduit, and means including a jacket of heat insulating material between the liquid conduit and air conduit for preventing transmission of the heat from the air chamber to the liquid conduit at the point of discharge into the desiccating chaml ber.
described, a desiccating chamber, an atomizer comprising a liquid conduit and an air Vconduit discharging at Vsubstantially the same point into the desiccating chamber, the air conduit having a tapering inner end whereby the liquid is s lit up into finely divided particles, means or heating the air in transit to the desiccating chamber, and means including a' cooling chamber and a jacket of heat insulating material, both located between the liquid conduit and air conduit for keeping the temperature of the liquid below that of the heated air while 1n transit to the desiccatin chamber. 15
In witness whereof Ighave hereunto set my hand this 27th day of July 1907.
IRVING S. MERRELL.
lrVitnesses M ILDRED M. VNo'r'r,
HOWARD P. DENNIsoN.
US38602607A 1907-07-29 1907-07-29 Desiccating apparatus. Expired - Lifetime US954451A (en)

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Cited By (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2478779A (en) * 1945-03-07 1949-08-09 American Dyewood Company Spray drying apparatus
US2652593A (en) * 1951-01-31 1953-09-22 Sinclair Refining Co Treatment of pitch
US2664671A (en) * 1951-04-04 1954-01-05 Int Harvester Co Receiving mechanism for drawn glass strands
US2833345A (en) * 1953-05-06 1958-05-06 Norton Co Spray drying apparatus
US3038533A (en) * 1956-03-19 1962-06-12 Purdue Research Foundation Drying process and apparatus for heatsensitive materials
US3399511A (en) * 1966-02-15 1968-09-03 American Hydrotherm Corp Jet compressor
US3430289A (en) * 1965-11-01 1969-03-04 Toho Zinc Co Ltd Apparatus for preparing high purity fine powder of low-melting metals
US4705467A (en) * 1984-11-28 1987-11-10 Shell Oil Company Method and apparatus for filtering the air outlet of a solid sulphur particle production apparatus
US4946481A (en) * 1984-11-28 1990-08-07 Shell Oil Company Filter screen apparatus for the air outlet of a particle production apparatus
US5216898A (en) * 1992-01-14 1993-06-08 Astec Industries, Inc. Cooling apparatus
US6460831B2 (en) * 1996-11-29 2002-10-08 Fuji Bc Engineering Co., Ltd. Cutting liquid coater
US6659370B1 (en) 1998-05-25 2003-12-09 Fuji Bc Engineering Co., Ltd. Liquid spray device and cutting method
US6773212B2 (en) 2000-10-26 2004-08-10 Fuji Koeki Co., Ltd. Cutting-oil coater and cutting device

Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2478779A (en) * 1945-03-07 1949-08-09 American Dyewood Company Spray drying apparatus
US2652593A (en) * 1951-01-31 1953-09-22 Sinclair Refining Co Treatment of pitch
US2664671A (en) * 1951-04-04 1954-01-05 Int Harvester Co Receiving mechanism for drawn glass strands
US2833345A (en) * 1953-05-06 1958-05-06 Norton Co Spray drying apparatus
US3038533A (en) * 1956-03-19 1962-06-12 Purdue Research Foundation Drying process and apparatus for heatsensitive materials
US3430289A (en) * 1965-11-01 1969-03-04 Toho Zinc Co Ltd Apparatus for preparing high purity fine powder of low-melting metals
US3399511A (en) * 1966-02-15 1968-09-03 American Hydrotherm Corp Jet compressor
US4705467A (en) * 1984-11-28 1987-11-10 Shell Oil Company Method and apparatus for filtering the air outlet of a solid sulphur particle production apparatus
US4946481A (en) * 1984-11-28 1990-08-07 Shell Oil Company Filter screen apparatus for the air outlet of a particle production apparatus
US5216898A (en) * 1992-01-14 1993-06-08 Astec Industries, Inc. Cooling apparatus
US6460831B2 (en) * 1996-11-29 2002-10-08 Fuji Bc Engineering Co., Ltd. Cutting liquid coater
US6679484B2 (en) 1996-11-29 2004-01-20 Fuji Bc Engineering Co., Ltd. Cutting liquid coater
US6659370B1 (en) 1998-05-25 2003-12-09 Fuji Bc Engineering Co., Ltd. Liquid spray device and cutting method
US6773212B2 (en) 2000-10-26 2004-08-10 Fuji Koeki Co., Ltd. Cutting-oil coater and cutting device

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