US8555673B2 - Method and device for separating a mixture of at least hydrogen, nitrogen, and carbon monoxide by cryogenic distillation - Google Patents

Method and device for separating a mixture of at least hydrogen, nitrogen, and carbon monoxide by cryogenic distillation Download PDF

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US8555673B2
US8555673B2 US12/519,990 US51999007A US8555673B2 US 8555673 B2 US8555673 B2 US 8555673B2 US 51999007 A US51999007 A US 51999007A US 8555673 B2 US8555673 B2 US 8555673B2
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carbon monoxide
column
pressure
fraction
denitrogenation
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US20100071411A1 (en
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Arthur Darde
Antoine Hernandez
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Air Liquide SA
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
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Air Liquide SA
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    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0204—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the feed stream
    • F25J3/0223—H2/CO mixtures, i.e. synthesis gas; Water gas or shifted synthesis gas
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0228—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream
    • F25J3/0252—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream separation of hydrogen
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0228—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream
    • F25J3/0257—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream separation of nitrogen
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0228—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream
    • F25J3/0261—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream separation of carbon monoxide
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/70—Refluxing the column with a condensed part of the feed stream, i.e. fractionator top is stripped or self-rectified
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/74—Refluxing the column with at least a part of the partially condensed overhead gas
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2205/00—Processes or apparatus using other separation and/or other processing means
    • F25J2205/30—Processes or apparatus using other separation and/or other processing means using a washing, e.g. "scrubbing" or bubble column for purification purposes
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2240/00—Processes or apparatus involving steps for expanding of process streams
    • F25J2240/40—Expansion without extracting work, i.e. isenthalpic throttling, e.g. JT valve, regulating valve or venturi, or isentropic nozzle, e.g. Laval
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2270/00—Refrigeration techniques used
    • F25J2270/02—Internal refrigeration with liquid vaporising loop
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2270/00—Refrigeration techniques used
    • F25J2270/04—Internal refrigeration with work-producing gas expansion loop
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2270/00—Refrigeration techniques used
    • F25J2270/24—Quasi-closed internal or closed external carbon monoxide refrigeration cycle
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2280/00—Control of the process or apparatus
    • F25J2280/02—Control in general, load changes, different modes ("runs"), measurements
US12/519,990 2006-12-21 2007-12-12 Method and device for separating a mixture of at least hydrogen, nitrogen, and carbon monoxide by cryogenic distillation Active 2030-07-21 US8555673B2 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR0655770A FR2910602B1 (fr) 2006-12-21 2006-12-21 Procede et appareil de separation d'un melange comprenant au moins de l'hydrogene, de l'azote et du monoxyde de carbone par distillation cryogenique
FR0655770 2006-12-21
PCT/FR2007/052486 WO2008078040A2 (fr) 2006-12-21 2007-12-12 Procédé et appareil de séparation d'un mélange comprenant au moins de l'hydrogène, de l'azote et du monoxyde de carbone par distillation cryogénique

Publications (2)

Publication Number Publication Date
US20100071411A1 US20100071411A1 (en) 2010-03-25
US8555673B2 true US8555673B2 (en) 2013-10-15

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US12/519,990 Active 2030-07-21 US8555673B2 (en) 2006-12-21 2007-12-12 Method and device for separating a mixture of at least hydrogen, nitrogen, and carbon monoxide by cryogenic distillation

Country Status (5)

Country Link
US (1) US8555673B2 (fr)
EP (1) EP2140216B1 (fr)
CN (1) CN101568788B (fr)
FR (1) FR2910602B1 (fr)
WO (1) WO2008078040A2 (fr)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20100251765A1 (en) * 2009-04-01 2010-10-07 Air Products And Chemicals, Inc. Cryogenic Separation of Synthesis Gas
FR2959297B1 (fr) * 2010-04-22 2012-04-27 Air Liquide Procede et appareil de production d'azote par distillation cryogenique d'air
EP2562502A1 (fr) * 2011-06-24 2013-02-27 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Procédé et installation pour la fourniture d'un monoxyde de carbone gazeux par distillation cryogénique
FR3058996B1 (fr) * 2016-11-18 2022-01-07 Air Liquide Procede et installation de separation cryogenique d’un melange gazeux par lavage au methane
IT201700042150A1 (it) * 2017-04-14 2018-10-14 Cristiano Galbiati Separation equipment
CN107084594B (zh) * 2017-04-27 2022-07-26 杭州中泰深冷技术股份有限公司 一种液co循环制冷合成气制甲醇联产lng装置及其使用方法

Citations (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3756036A (en) * 1971-04-20 1973-09-04 Phillips Petroleum Co Demethanizing method and apparatus
US3886756A (en) * 1972-05-10 1975-06-03 Air Prod & Chem Separation of gases
US4478621A (en) * 1982-04-28 1984-10-23 Linde Aktiengesellschaft Process for the extraction of carbon monoxide from gas streams
US4969338A (en) * 1989-08-21 1990-11-13 The Boc Group, Inc. Method and apparatus of producing carbon dioxide in high yields from low concentration carbon dioxide feeds
DE19541339A1 (de) 1995-11-06 1997-05-07 Linde Ag Verfahren zum Gewinnen von Kohlenmonoxid
US5992175A (en) * 1997-12-08 1999-11-30 Ipsi Llc Enhanced NGL recovery processes
US6062042A (en) * 1998-01-13 2000-05-16 Air Products And Chemicals, Inc. Seperation of carbon monoxide from nitrogen-contaminated gaseous mixtures
US6073461A (en) * 1998-01-13 2000-06-13 Air Products And Chemicals, Inc. Separation of carbon monoxide from nitrogen-contaminated gaseous mixtures also containing hydrogen and methane
US20050126220A1 (en) * 2003-12-15 2005-06-16 Ward Patrick B. Systems and methods for vaporization of liquefied natural gas
US20060016216A1 (en) * 2004-07-23 2006-01-26 Tonkovich Anna L Distillation process using microchannel technology
FR2879595A1 (fr) * 2006-01-26 2006-06-23 Air Liquide Procede d'integration d'une unite de deazotation sur une boite froide produisant du monoxyde de carbone
US7107788B2 (en) * 2003-03-07 2006-09-19 Abb Lummus Global, Randall Gas Technologies Residue recycle-high ethane recovery process
US20070056319A1 (en) * 2004-04-07 2007-03-15 Jean Billy Process and installation for providing a fluid mixture containing at least 10% carbon monoxide
US20120145529A1 (en) * 2010-12-14 2012-06-14 Chevron U.S.A. Inc. Apparatus, process and system for delivering fluid to a distillation column or reactor

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2718428B1 (fr) * 1994-04-11 1997-10-10 Air Liquide Procédé et installation de production de monoxyde de carbone.
DE4433114A1 (de) * 1994-09-16 1996-03-21 Linde Ag Verfahren zum Gewinnen einer Kohlenmonoxid-Reinfraktion
FR2754541B1 (fr) * 1996-10-15 1998-12-24 Air Liquide Procede et installation pour la separation d'un melange d'hydrogene et/ou d'au moins un hydrocarbure et/ou d'azote et/ou d'oxyde de carbone
EP1479990A1 (fr) * 2003-05-19 2004-11-24 L'Air Liquide Société Anonyme à Directoire et Conseil de Surveillance pour l'Etude et Exploitation des Procédés Georges Claude Procédé et installation pour la production d'un mélange contenant au moins 10% de monoxyde de carbone

Patent Citations (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3756036A (en) * 1971-04-20 1973-09-04 Phillips Petroleum Co Demethanizing method and apparatus
US3886756A (en) * 1972-05-10 1975-06-03 Air Prod & Chem Separation of gases
US4478621A (en) * 1982-04-28 1984-10-23 Linde Aktiengesellschaft Process for the extraction of carbon monoxide from gas streams
US4969338A (en) * 1989-08-21 1990-11-13 The Boc Group, Inc. Method and apparatus of producing carbon dioxide in high yields from low concentration carbon dioxide feeds
DE19541339A1 (de) 1995-11-06 1997-05-07 Linde Ag Verfahren zum Gewinnen von Kohlenmonoxid
US5992175A (en) * 1997-12-08 1999-11-30 Ipsi Llc Enhanced NGL recovery processes
US6062042A (en) * 1998-01-13 2000-05-16 Air Products And Chemicals, Inc. Seperation of carbon monoxide from nitrogen-contaminated gaseous mixtures
US6073461A (en) * 1998-01-13 2000-06-13 Air Products And Chemicals, Inc. Separation of carbon monoxide from nitrogen-contaminated gaseous mixtures also containing hydrogen and methane
US7107788B2 (en) * 2003-03-07 2006-09-19 Abb Lummus Global, Randall Gas Technologies Residue recycle-high ethane recovery process
US20050126220A1 (en) * 2003-12-15 2005-06-16 Ward Patrick B. Systems and methods for vaporization of liquefied natural gas
US20070056319A1 (en) * 2004-04-07 2007-03-15 Jean Billy Process and installation for providing a fluid mixture containing at least 10% carbon monoxide
US20060016216A1 (en) * 2004-07-23 2006-01-26 Tonkovich Anna L Distillation process using microchannel technology
FR2879595A1 (fr) * 2006-01-26 2006-06-23 Air Liquide Procede d'integration d'une unite de deazotation sur une boite froide produisant du monoxyde de carbone
US20120145529A1 (en) * 2010-12-14 2012-06-14 Chevron U.S.A. Inc. Apparatus, process and system for delivering fluid to a distillation column or reactor

Non-Patent Citations (5)

* Cited by examiner, † Cited by third party
Title
"Process and Apparatus for Separation of Nitrogen From Carbon Monixide" Research Disclosure, Mason Publications, Hampshire, GB, No. 426, Oct. 1999, pp. 1335-1336.
Berninger, R., "Fortschritte Bei Der H2/CO-Tieftemperaturzerlegung" Berichte Aus Technik Und Wissenschaft, Linde AG. Wiesbaden, DE, vol. 62, 1988, pp. 18-23.
Berninger, R., "Progress in H2/CO Low-Temperature Separation", Linde Reports on Science and Technology, vol. 62, 1988, pp. 18-23.
English translation of abstract for FR2879595. *
Search Report for PCT/FR2007/052486.

Also Published As

Publication number Publication date
CN101568788A (zh) 2009-10-28
US20100071411A1 (en) 2010-03-25
CN101568788B (zh) 2011-11-02
WO2008078040A3 (fr) 2009-05-22
FR2910602B1 (fr) 2012-12-14
FR2910602A1 (fr) 2008-06-27
EP2140216A2 (fr) 2010-01-06
WO2008078040A2 (fr) 2008-07-03
EP2140216B1 (fr) 2017-11-08

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