US732548A - Column for column-stills. - Google Patents

Column for column-stills. Download PDF

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Publication number
US732548A
US732548A US13280602A US1902132806A US732548A US 732548 A US732548 A US 732548A US 13280602 A US13280602 A US 13280602A US 1902132806 A US1902132806 A US 1902132806A US 732548 A US732548 A US 732548A
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Prior art keywords
column
plates
vertical
plate
stills
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Expired - Lifetime
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US13280602A
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Emile Guillaume
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/008Liquid distribution

Definitions

  • ATToRNExs TH Nunms PETERS co. moodnno.. wAsn-emown, D4 c.
  • My invention relates to a column for a colunIn-still,which column has inclined plates curved downward at their lower edges, each forming with a more or less vertical part a gutter open at the bottom.
  • the said vertical part may either be an attachment to or a part of a plate or it may be a separate piece, as I will describe with reference to the accompanying drawings, in which- Figure l is a cross-section through a rectangular column for a still fitted with plates according to my invention.
  • Fig. 2 is a similar section
  • Fig. 3 is a section on the line a b of Fig. 2 through a double column fitted with the plates
  • Fig. 4 is a vertical section through a cylindrical column fitted with the plates
  • Fig. 5 being a plan thereof.
  • a curved line (marked With arrowheads) indicates the direction of the vapor up the column, and the plates are shown attached to the sides of the column and inclined at a slight angle thereto.
  • the front portion 4 of each plate is curved downward, and there is fixed to the sides of the column a vertical plate 3, supported by braces 3', extending at an angle from the plate 3 to the inclined plate in front of each of the inclined plates and sufiiciently close thereto to form with the lower edge of the curved part 4 a narrow opening 2.
  • the liquid flows successively down the plates, and owing to the speed it acquires in iiowing down the inclined surface of the plate it impinges against the vertical surface 3 and fills the gutter formed between the latter and the curved portion 4.
  • Fig. l is a double column, the liquid being equally distributed'down each from the gutter 5.
  • the cylindrical column (shown in Figs. 4 and 5) has a central cylinder 6, which carries circular plates constructed like those already described and surrounded by vertical rings, as is obvious from the drawings. Between these plates are annular plates of the same form attach ed to the inner surface of the ou ter wall of the column. Vertical rings are arrangedv within the central openings of' these annular plates. As in the case of the rectangular columns these cylindrical columns can be duplicated, triplicated, the., and obviously a simple arrangement is fo make them concentric.
  • a column-still consisting of a vertical hollow column to the inner surface of whose walls are fixed inclinedl plates curved downward at their lower edges and extending into the column so that they compel the ascending Vapor to take a zigzag course, these 'inclined plates being combined with more or less Vertical plates which form by their juxtaposition with the lower edge and the inclined plates a gutter having a narrow opening at its bottom, substantially as described.
  • a column-still consisting of a Vertical hollow column to the inner surface of whose walls are fixed inclined plates curved downthe lower edges of the said inclined plates,

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electroluminescent Light Sources (AREA)
  • Treatment Of Fiber Materials (AREA)

Description

No. 732,548. PATENTBD JUNE 30, 1903.
E. GUILLAUME. COLUMN FOR COLUMN STILLS.
APPLIGATION FILED Nov. 25, 1902. No 'MODEL s SHEETS-SHEET 1.
A'rroRNsYs INV-E NTOR me News uns co, vnormlwojwnmmou, n L.
WITNasbke No. 732,548. PATLNITLD'JUNLSO, 1903;
' E. GUILLAUME.
COLUMN FOR COLUMN STILLS.y
A APPLIUATION FILED Nov. 2 5, 1902. v j No noDnL. a'sHsBTs-snnz'r 2.
Lk j
wnT-Nassas INvELNTOR TNE Nom-us PETERS cufwwomfLlTHo. wnswmuon. u. c.
PATBNTBD JUNE 30, 190s.
` E. GUILLAUME.
COLUMN PoR coLUMN sTILLs.
APPLICATION FILED NOV. 25, 1902.
3 SHEETS-SHEET 3.
N0 MODEL.
ATToRNExs TH: Nunms PETERS co. moodnno.. wAsn-emown, D4 c.
UNITED STATESv Patented D' une 30, 1903.
PATENT EEICE. i
lCOLUMN FOR COLUMN-STILLS.
SPECIFICATION forming part of Letters Patent No. 732,548, dated June 30, 1903..
Application led November 25, 1902. Serial No. 1-32,806. (No model.)
To all whom t may concern.-
Be it known that I, EMILE GUILLAUME, a citizen of the French Republic, residing in Paris, in the Republic of France, have invented certain new and useful Improvements in Columns for Column-Stills, (for which I have obtained a patent in France, No. 320, 850, bearing date May 2, 1902,) of which the following is a specification. p
My invention relates to a column for a colunIn-still,which column has inclined plates curved downward at their lower edges, each forming with a more or less vertical part a gutter open at the bottom. The said vertical part may either be an attachment to or a part of a plate or it may be a separate piece, as I will describe with reference to the accompanying drawings, in which- Figure l is a cross-section through a rectangular column for a still fitted with plates according to my invention. Fig. 2 is a similar section, and Fig. 3 is a section on the line a b of Fig. 2 through a double column fitted with the plates, and Fig. 4 is a vertical section through a cylindrical column fitted with the plates, Fig. 5 being a plan thereof.
In Fig'l a curved line (marked With arrowheads) indicates the direction of the vapor up the column, and the plates are shown attached to the sides of the column and inclined at a slight angle thereto. The front portion 4 of each plate is curved downward, and there is fixed to the sides of the column a vertical plate 3, supported by braces 3', extending at an angle from the plate 3 to the inclined plate in front of each of the inclined plates and sufiiciently close thereto to form with the lower edge of the curved part 4 a narrow opening 2. As indicated, the liquid flows successively down the plates, and owing to the speed it acquires in iiowing down the inclined surface of the plate it impinges against the vertical surface 3 and fills the gutter formed between the latter and the curved portion 4. It thus acquires a head sufficient to carry it through the opening 2 in the form of a continuous sheet onto the succeeding plate against the pressure created by the upward passage of the vapor. It will be obvious that the extent to which the gutter l becomes filled depends on the adjustment of the distance between plate 3 and the curved changes its direction.
able them to accompany the vapor when it It is found to some advantage to Inake the lower edge vertical plates 3 extend slightly below the lower edge of the curved portion 4, this favoring .the formation of sheets. It is unnecessary to lay down any directions as to the proportions of the plates or their vertical distances apart, as these obviously depend upon the purpose for which the column is to be applied andthe height available for construction of' the column.
The description given above with reference to Fig. l applies also to Fig. 2, which is a double column, the liquid being equally distributed'down each from the gutter 5.
The cylindrical column (shown in Figs. 4 and 5) has a central cylinder 6, which carries circular plates constructed like those already described and surrounded by vertical rings, as is obvious from the drawings. Between these plates are annular plates of the same form attach ed to the inner surface of the ou ter wall of the column. Vertical rings are arrangedv within the central openings of' these annular plates. As in the case of the rectangular columns these cylindrical columns can be duplicated, triplicated, the., and obviously a simple arrangement is fo make them concentric.
Having thus described the nature of this invention and the best means I know of carrying the same into practical effect, I claiml'. In a coluInn-still, inclined plates each curved downward at its lower edge and combined with a more or less vertical plate, so arranged that .its juxtaposition with the' lower edge of the said inclined plate forms'a gutter having a narrow opening at its' bottom, substantially as described.
2. In a column-still, inclined plates each curved downwardat its lower edge and combined with a more or less verticalV plate, so arranged that its juxtaposition with the lower edge of the said inclined plate forms a gutter having a narrow opening at its bottom, the
ICO
lower edge of the said more or less Vertical plate extending a little below the lower edge of the said inclined plate, substantially as described.
3. A column-still consisting of a vertical hollow column to the inner surface of whose walls are fixed inclinedl plates curved downward at their lower edges and extending into the column so that they compel the ascending Vapor to take a zigzag course, these 'inclined plates being combined with more or less Vertical plates which form by their juxtaposition with the lower edge and the inclined plates a gutter having a narrow opening at its bottom, substantially as described.
4e. A column-still consisting of a Vertical hollow column to the inner surface of whose walls are fixed inclined plates curved downthe lower edges of the said inclined plates,
substantially as described.
In witness whereoll I have hereunto set my hand in presence of two witnesses.
EMILE GUILLAUME.
Vitnesses:
EDWARD I. MACLEAN, JULES FAYoLLE'r.
US13280602A 1902-11-25 1902-11-25 Column for column-stills. Expired - Lifetime US732548A (en)

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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2805845A (en) * 1953-02-17 1957-09-10 Berry Jean-Luc Fractionating distilling apparatus
US3083148A (en) * 1960-10-10 1963-03-26 Mojonnier Bros Co Fractionation column
US4543219A (en) * 1982-11-24 1985-09-24 Nippon Kayaku Kabushiki Kaisha Baffle tray tower
US20110210457A1 (en) * 2007-08-16 2011-09-01 Jgc Corporation Contactor
RU2446872C2 (en) * 2007-08-16 2012-04-10 ДжейДжиСи КОРПОРЕЙШН Contact device
US9993760B2 (en) * 2015-08-07 2018-06-12 Big Heart Pet, Inc. Particle separator systems and processes for improving food safety
US20220072446A1 (en) * 2018-12-28 2022-03-10 Neste Oyj Apparatus and Method for heat treating a feedstock comprising a lipid material
US20220331727A1 (en) * 2021-04-20 2022-10-20 Mag Aerospace Industries, Llc Air / waste water separator

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2805845A (en) * 1953-02-17 1957-09-10 Berry Jean-Luc Fractionating distilling apparatus
US3083148A (en) * 1960-10-10 1963-03-26 Mojonnier Bros Co Fractionation column
US4543219A (en) * 1982-11-24 1985-09-24 Nippon Kayaku Kabushiki Kaisha Baffle tray tower
US20110210457A1 (en) * 2007-08-16 2011-09-01 Jgc Corporation Contactor
RU2446872C2 (en) * 2007-08-16 2012-04-10 ДжейДжиСи КОРПОРЕЙШН Contact device
US8240640B2 (en) 2007-08-16 2012-08-14 Jgc Corporation Contactor
US9993760B2 (en) * 2015-08-07 2018-06-12 Big Heart Pet, Inc. Particle separator systems and processes for improving food safety
US20220072446A1 (en) * 2018-12-28 2022-03-10 Neste Oyj Apparatus and Method for heat treating a feedstock comprising a lipid material
US12102945B2 (en) * 2018-12-28 2024-10-01 Neste Oyj Apparatus and method for heat treating a feedstock comprising a lipid material
US20220331727A1 (en) * 2021-04-20 2022-10-20 Mag Aerospace Industries, Llc Air / waste water separator
US12090434B2 (en) * 2021-04-20 2024-09-17 Mag Aerospace Industries, Llc Air / waste water separator

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