US605865A - Louis ernest fraipont - Google Patents

Louis ernest fraipont Download PDF

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US605865A
US605865A US605865DA US605865A US 605865 A US605865 A US 605865A US 605865D A US605865D A US 605865DA US 605865 A US605865 A US 605865A
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retorts
retort
gas
fraipont
superheater
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    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G9/00Thermal non-catalytic cracking, in the absence of hydrogen, of hydrocarbon oils
    • C10G9/02Thermal non-catalytic cracking, in the absence of hydrogen, of hydrocarbon oils in retorts
    • C10G9/04Retorts
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2400/00Products obtained by processes covered by groups C10G9/00 - C10G69/14
    • C10G2400/26Fuel gas

Definitions

  • the object of my invention is to provide a distilling and gasifying apparatus intended for reducing into gas by a series of successive fractional distillations and simultaneous gasifications all volatile substances contained in either crude or refined petroleum or in the fat. rock-oils, schistose oils, coal-tar oil, and generally in all hydrocarbons, the gases so obtained being fit for immediate use either for heating or lighting purposes. This complete gasification is more or less easy, according to the quality and specific gravity of the hydrocarbons used.
  • the fat, schistose, and coaltar oils leave after distillation considerable quantities of residue and are impracticable in the gas-generators now in use, which gasify the oil in one manipulation and almost instantaneously.
  • Every retort is provided With a drain-pipe penetrating to the bottom, whereby when the apparatus is in operation the residues of distillation can be evacuated by means of the pressure obtained in the retorts.
  • These drainpipes permit of crude hydrocarbons being burned and prevent an otherwise unavoidable fouling as also all formation of coke in the retorts.
  • the apparatus consists, essentially, of a series of retorts of any suitable number and shape intercommunicating by pipes. These retorts are heated independently from each other by a source of heat of any description, or, simpler still, they can be heated by the the nature of the oils used the lightest among these vapors are already reduced to gas. This mixture of vapor and gas passes into a third retort, where another part of vaporis reduced to gas, and so forth, the same operation being repeated in the subsequent retorts and recommenced as often as necessary to obtain the complete gasification of all distill able elements.
  • the non-distillable elements remain at the bottom of each retort, from where they are evacuated from time to time by means of the drain-pipes fitted to the retorts. In this manner a series of.successive distillations and gasifications are obtained, whereby hydrocarbons of any kind are reduced to gas in a complete manner, the non-distillable products being evacuated as soon as formed.
  • FIG. 1 shows the invention in elevation and partial longitudinal section.
  • FIG. 2 is a plan View of Fig. 1;
  • Fig. 3 a transverse section along the line 1 2 of Fig. 2 of a practical apparatus for gasifying ordinary fat oils.
  • the invention consists of a'first retort A, into which the hydrocarbons are fed up to the central part by means of the pipe 0, provided with a regulator consisting, as shown in Fig. 1, of a cylindrical chamber R, containing a movable ball a, which regulates by its displace;'-
  • the heavy vapors escaping from the retort A pass through the tube D into the retort A and successively through the tubes D D into the other retorts until A' is reached. In these successive retorts the vapors are overheated, and even the most volatile elements are 'gasified.
  • the retorts A A A are heated when the apparatus is in operation by means of the'burners P P, mounted on the tube S and fed by means of the gas produced by the apparatus itself.
  • This mixture of overheated vapors and gases already formed is fed in dry state into a gassuperheater F by means of the pipe E.
  • This superheater consists of three cylinders intercommunicating by means of the conduit-pipes 0, Figs. 2 and 3, and heated directly by means of the burners P, fed by the gas emerging from the superheater through the conduitpipes I T.
  • This construction of the superheater compels the vapors to pass in the first place through the two least-heated upper cylinders and lastly into the one most heated, because it is in direct contact with the flame from the heating-burners.
  • the retorts and cylinders are fitted on the inside with wings, serving to increase the heating-surface.
  • a drain-pipe X On top of the retort A is arranged a drain-pipe X, Figs. 2 and 3, penetrating to the bottom,with the object of efiecting while the apparatus is in operation by means of the pressure produced by the vaporization of the hydrocarbons the evacuation of the residues of crystallization.
  • the retorts are provided with a lid Z.
  • the pipes G X D D extend through these covers.
  • the body of the retort is kept pressed against the lid Z by a shaft V and a screw-nut Y.
  • This arrangement permits of the quick removal of the spherical part of the retort for the purpose of cleaning it without touching the other organs of the apparatus.
  • the same system of closure and .joint is applied to the cylinders. lhe gas produced on leaving the generator is delivered by the pipe V into a receiver, from where it can be distributed to the heating or lighting apparatuses of whatever kind for which it is destined.
  • the casin g the plurality of retorts connected in series, each being a complete retort in itself, means for feeding hydrocarbon to the first retort of the series, a drain-pipe connected with the retorts, a superheater connected with the last retort of the series and arranged to receive the volatilized hydrocarbon therefrom, a gas burner or jet beneath each retort and the superheater for independently heating said retorts and superheater, said burners being supplied with gas from the superheater, substantially as described.

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)

Description

(No Model.)
L. E. FRAIPONT. APPARATUS FOR VAPORIZING OILS.
Patented June 21, 1898.
I7z ifazzto 7";
7:11.: vworrgs m: NORRIS PETERS co, Pum'uuiun, WASHINGTON, u. c.
UNTTED STATES PATENT I rETcE.
LOUIS ERNEST FRAIPONI, OF PARIS, FRANCE.
APPARATUS FOR VAPORIZING OILS.
SPECIFICATION forming part of Letters Patent No. 605,865, dated June 21, 1898.
Application filed May 20, 1897. Serial No. 687,890. (No model.) Patented in France September 4, 1896, No. 259,439.
To all whom it may concern.-
Be it known that I, LoUIs ERNEST FRAI- PONT, a citizen of the Republic of France, residing at Paris, in the Department of the Seine, France, have invented a certain new and Improved Apparatus for the Vaporizing of Petroleum, Heavy Oils, Tar-Oils, and Hydrocarbons Generally, of which the following is a full, clear, and exact specification.
The invention has been patented in France, No. 259,439, dated September 4, 1896.
The object of my invention is to provide a distilling and gasifying apparatus intended for reducing into gas by a series of successive fractional distillations and simultaneous gasifications all volatile substances contained in either crude or refined petroleum or in the fat. rock-oils, schistose oils, coal-tar oil, and generally in all hydrocarbons, the gases so obtained being fit for immediate use either for heating or lighting purposes. This complete gasification is more or less easy, according to the quality and specific gravity of the hydrocarbons used. The fat, schistose, and coaltar oils leave after distillation considerable quantities of residue and are impracticable in the gas-generators now in use, which gasify the oil in one manipulation and almost instantaneously. It happens, in fact, that after a very short time the heaviest substances, which do not volatilize at ordinary temperatures, condense on the pipes and finally foul them. In my system the gasification is effected gradually and can be divided in any desired number of fractions, according to the nature of the oil used, in order to obtain the gasification of the whole product.
Every retort is provided With a drain-pipe penetrating to the bottom, whereby when the apparatus is in operation the residues of distillation can be evacuated by means of the pressure obtained in the retorts. These drainpipes permit of crude hydrocarbons being burned and prevent an otherwise unavoidable fouling as also all formation of coke in the retorts.
The apparatus consists, essentially, of a series of retorts of any suitable number and shape intercommunicating by pipes. These retorts are heated independently from each other by a source of heat of any description, or, simpler still, they can be heated by the the nature of the oils used the lightest among these vapors are already reduced to gas. This mixture of vapor and gas passes into a third retort, where another part of vaporis reduced to gas, and so forth, the same operation being repeated in the subsequent retorts and recommenced as often as necessary to obtain the complete gasification of all distill able elements. The non-distillable elements remain at the bottom of each retort, from where they are evacuated from time to time by means of the drain-pipes fitted to the retorts. In this manner a series of.successive distillations and gasifications are obtained, whereby hydrocarbons of any kind are reduced to gas in a complete manner, the non-distillable products being evacuated as soon as formed.
For the better understanding of the specification I will now refer to the accompanying drawings, in which- Figure 1 shows the invention in elevation and partial longitudinal section. Fig. 2 is a plan View of Fig. 1; Fig. 3, a transverse section along the line 1 2 of Fig. 2 of a practical apparatus for gasifying ordinary fat oils.
The same referencecharacters are applied to the same elements in the different figures.
The invention consists of a'first retort A, into which the hydrocarbons are fed up to the central part by means of the pipe 0, provided with a regulator consisting, as shown in Fig. 1, of a cylindrical chamber R, containing a movable ball a, which regulates by its displace;'-
ment the admission of hydrocarbons and prevents them being driven back by the pressure coming from the apparatus- The heavy vapors escaping from the retort A pass through the tube D into the retort A and successively through the tubes D D into the other retorts until A' is reached. In these successive retorts the vapors are overheated, and even the most volatile elements are 'gasified. The retorts A A A are heated when the apparatus is in operation by means of the'burners P P, mounted on the tube S and fed by means of the gas produced by the apparatus itself.
This mixture of overheated vapors and gases already formed is fed in dry state into a gassuperheater F by means of the pipe E. This superheater consists of three cylinders intercommunicating by means of the conduit-pipes 0, Figs. 2 and 3, and heated directly by means of the burners P, fed by the gas emerging from the superheater through the conduitpipes I T. This construction of the superheater compels the vapors to pass in the first place through the two least-heated upper cylinders and lastly into the one most heated, because it is in direct contact with the flame from the heating-burners.
The retorts and cylinders are fitted on the inside with wings, serving to increase the heating-surface. On top of the retort A is arranged a drain-pipe X, Figs. 2 and 3, penetrating to the bottom,with the object of efiecting while the apparatus is in operation by means of the pressure produced by the vaporization of the hydrocarbons the evacuation of the residues of crystallization. By means of these drain-pipes, which prevent all foulin g and all formation of coke, it becomes possible to burn crude hydrocarbons.
The retorts are provided with a lid Z. The pipes G X D D extend through these covers. The body of the retort is kept pressed against the lid Z by a shaft V and a screw-nut Y. This arrangement permits of the quick removal of the spherical part of the retort for the purpose of cleaning it without touching the other organs of the apparatus. The same system of closure and .joint is applied to the cylinders. lhe gas produced on leaving the generator is delivered by the pipe V into a receiver, from where it can be distributed to the heating or lighting apparatuses of whatever kind for which it is destined.
I claim 1. In combination, the casin g, the plurality of retorts connected in series, each being a complete retort in itself, means for feeding hydrocarbon to the first retort of the series, a drain-pipe connected with the retorts, a superheater connected with the last retort of the series and arranged to receive the volatilized hydrocarbon therefrom, a gas burner or jet beneath each retort and the superheater for independently heating said retorts and superheater, said burners being supplied with gas from the superheater, substantially as described.
2. In combination, the casing, the plurality of retorts, each complete in itself, said retorts being connected in series, means for feeding hydrocarbon to the first retort of the series, a drain-pipe connected with the retorts, the superheater comprising three tubes, two above and one centrally below and connected in series, connections from the last retort of the series to one of the upper tubes, the gas flowing thence through the second upper tube and finally into the lower one, the gas-jet beneath each retort, the jets beneath the superheater adapted to impinge against the said lower tube, and the pipe connections from the superheater to the burners, substantially as described.
In witness whereof I have hereunto set my hand in presence of two witnesses.
LOUIS ERNEST FRAIPONT.
Witnesses:
EDWARD P. MACLEAN, J ULEs FAYOLLET.
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