US4871554A - Calcium fortified food product - Google Patents
Calcium fortified food product Download PDFInfo
- Publication number
- US4871554A US4871554A US07/084,680 US8468087A US4871554A US 4871554 A US4871554 A US 4871554A US 8468087 A US8468087 A US 8468087A US 4871554 A US4871554 A US 4871554A
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- Prior art keywords
- calcium
- beverage
- juice
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- concentrate
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/16—Inorganic salts, minerals or trace elements
Definitions
- This invention relates generally to a calcium fortified food product in the form of a ready-to-serve beverage, a frozen concentrate or a reconstitutable dry drink mix which provides between 10%-100% of the U.S. RDA of calcium per six ounce serving, which has a pH of not more than 4.5 and which has a Brix-acid ratio range of about 5:1 to 54:1.
- Calcium is the most abundant component of minerals present in the human body, comprising approximately two percent of total body weight. Calcium is continuously utilized by the body and is replenished by a variety of food sources.
- the several uses of calcium in the body include providing rigidity to the skeletal framework; serving as a catalyst for the conversion of prothrombin to thrombin, a compound necessary for blood clotting; increasing cell membrane permeability; activating a number of enzymes including lipase and adenosine triphosphatase; and acting as a component in the mechanisms of neural transmission and muscular contraction.
- a dietary calcium deficiency can have adverse effects on an individual's health which vary in degree depending upon age and sex.
- calcium deficiency can interfere with muscular contraction and can also result in depletion of skeletal calcium, resulting in thin and brittle bones.
- Osteoporosis is a deficiency disease, a condition in which there are varying degrees in the loss of bone density or actual bone loss.
- Adult bone loss is considered one of the most debilitating health problems for elderly people.
- women suffer more often and with more devastating effects. This is due in part to the fact that women, in general, have smaller skeletal structures than men and also undergo accelerated bone loss at menopause due to estrogen loss.
- This crippling disease affects approximately one out of four women over the age of 60. The bones become more susceptible to breaks; subsequent fractures have a lower chance of healing which often leads to fatal complications.
- Vitamin D active is the major regulator of intestinal absorption of calcium. Calcium intakes can therefore be more efficiently utilized when there is an abundant supply of vitamin D. Sunlight (ultraviolet light) is considered an important factor in the conversion of dietary precursors to vitamin D, especially for young people. The dietary sources of active vitamin D may become essential in elderly adults who are less likely to be exposed to sunlight.
- Acid solutions enhance the solubility of calcium salts.
- Much of the digestion of foods takes place in the duodenum where the pH of the gastric juices is low. Since calcium salts are more soluble in an acid pH, much of the absorption of calcium takes place in this segment of the gastrointestinal tract.
- Tricalcium phosphate, calcium lactate, calcium carbonate and many other calcium compounds have all been used as calcium sources in various calcium fortified products.
- calcium citrate is the preferred salt for calcium fortification in certain juices.
- Several commercially available products such as antacids disclose the use of calcium carbonate as a dietary calcium supplement.
- the recommended daily allowance (RDA) of a mineral is the gender-specific recommendation considered by scientific experts to be adequate to meet the need for that nutrient for virtually all healthy people in the population.
- the current RDA of calcium is 360 to 800 mg for children depending on age. 12.
- the RDA for teenagers from 11-15 years is 1200 mg and is 800 mg for adults.
- Pregnancy and lactation increase the recommended amount by about 400 mg per day.
- the U.S. Recommended Daily Allowances (U.S. RDA) are derived from the 1968 RDA and are standards specified by the Food and Drug Administration to simplify nutritional labelling.
- Dairy products are recognized as a rich source of dietary calcium, in some instances accounting for as much as 75% of an individual's dietary intake of calcium. Increased ingestion of dairy products, however, has several drawbacks which preclude their broad recommendation as a solution for dietary calcium deficiency. These drawbacks include lactose intolerance by some individuals; the high levels of cholesterol and cholesterol producing ingredients in dairy products; the high caloric yields of dairy products; and flavor off-tastes often experienced by elderly individuals.
- U.S. Pat. No. 3,227,562 discloses a citrus fruit juice concentrate having a low Brix to acid ratio.
- the Brix unit is a commonly used unit of measurement which expresses the concentration of dissolved solids in an aqueous solution.
- the acid unit is the citric acid concentration in the citrus juice.
- the Brix to acid ratio is the accepted measurement of the sweetness to tartness ratio used in the fruit juice industry.
- a Brix-Acid ratio is obtained by dividing the Brix value by the acid value for a given product which yields a ratio compared with unity which forms a comparative scale for acceptability for particular juice concentrates.
- Brix-acid ratios of concentrated citrus fruit juice, high grade fresh--frozen orange juice concentrate will usually have a range of Brix-acid ratios of about 12.5:1 to about 20:1 whereas a range for grapefruit juice would be about 7:1 to about 11:1.
- Brix-acid ratios for commercially available citrus fruit juice-containing drinks generally range from 17:1 to 54:1.
- High quality commercially available orange juice products usually have a Brix-acid ratio range of 16:1 or higher.
- the '562 patent attributes the characteristic aftertaste of its concentrate to a combination of salts comprising sodium chloride, magnesium chloride, calcium chloride and sodium silicate with a citrus concentrate comprised of orange, lemon grapefruit and lime.
- the level of calcium chloride contained in the concentrate of the '562 patent is in the range of 3 mg per 6 ounce serving with the bulk of the salt used to impart the pleasant aftertaste consisting of sodium chloride. This level provides an extremely low amount of calcium and will not deliver the requisite dietary amounts of calcium thought to be effective in the prevention of osteoporosis and the like.
- U.S. Pat. No. 3,657,424 discloses a citrus juice energy supplement which replenishes salts whose natural level in the body has been depleted, e.g., through exercise.
- This reference discloses the addition of a combination of salts, including sodium chloride, potassium chloride and calcium chloride, in amounts that do not exceed 0.2% percent by weight of the beverage.
- the calcium chloride present in the fruit juice disclosed in the '424 patent ranges from 0-0.04% by weight or approximately 30 mg of calcium per 6 ounce serving of fortified product.
- a calcium fortified food product in ready-to-serve and readily ingestible form which can provide a substantial amount and a readily absorbable form of the recommended daily allowance of calcium.
- a food product e.g., a beverage
- which can provide approximately 100 mg-1,000 mg of calcium per six ounce serving and which has a Brix-acid ratio of about 5:1 to about 54:1, preferably about 7:1 to about 20:1 for citrus products.
- a further object is the development of a food product which can be handled as a concentrate yet is fairly soluble in water and, when reconstituted, has a pH which does not exceed the upper levels for high acid food, e.g. about 4.5.
- a calcium fortified food product which provides between 10%-100% of the U.S. RDA of calcium.
- the food product of the present invention can comprise a ready-to-serve beverage, a frozen concentrate or a reconstitutable dry concentrate which provides between 10%-100% of the U.S. RDA of calcium per six ounce serving.
- a calcium-fortified beverage prepared in accordance with the present invention has a pH which does not exceed about 4.5 when it is reconstituted (i.e. in a single strength form) and Brix-acid ratio in a range of about 5:1 to about 54:1, preferably about 7:1 to 20:1 for citrus products.
- the beverage having these characteristics has distinct pleasant aftertaste and substantially no gritty mouth-feel.
- Any acidic fruit juice material, preferably citrus juices, can be used in the formulation of the concentrates and beverages of the invention.
- the source of calcium contained in the food product of the present invention is a salt blend of between about 50%-0% (by weight relative to total calcium from the salts) of tribasic calcium phosphate and about 20%-50% (by weight relative to total calcium from the salts) of calcium lactate.
- the quantity of salt blend present in the food product is that which yields from about 100 mg to about 1000 mg of calcium per six fluid ounces of beverage.
- a preferred salt blend ratio is about 65-75% of calcium phosphate and about 25-35% calcium lactate.
- a preferred quantity of salt blend yields about 300 mg of calcium per six fluid ounces of beverage.
- the present invention also relates to calcium fortified beverages which comprise about 70-97% water, about 2-28% by weight of concentrated fruit juice, and about 1-5% by weight of a salt blend of about 50-80% of tribasic calcium phosphate and about 20-50% of calcium lactate, by weight of total calcium.
- the calcium fortified beverages comprise about 70-80% water, about 12-25% concentrated fruit juice, and 2-4% of the calcium component.
- the present invention also relates calcium fortified beverage concentrates comprising water, concentrated fruit juice and the aforementioned calcium component.
- the concentrates comprise about 95-98% by weight of a mixture consisting of about 20-33% by weight of water and about 66-80% by weight of concentrated fruit juice, and about 2-5% by weight of the aforementioned calcium component.
- the calcium component is substantially dissolved to form a concentrate which is frozen.
- a salt blend of approximately 75% by weight, relative to total calcium, of tribasic calcium phosphate and about 25% by weight, relative to total calcium, of calcium lactate is added to a concentrated fruit juice according to the amounts listed in Table 1.
- the concentrated fruit juice chosen in this embodiment is orange juice, although any other single fruit juices such as juice from grapefruit, lemons, limes, tangerines, grapes, apples, nectarines, peaches, pears, cherries, cranberries, strawberries, mangos, bananas, kiwis, plums, blueberries, and the like can be used.
- Citrus fruits could be used and would still result in a beverage product having an acceptable pH, such as less than 4.5. This pH maintains the product as a high acid food.
- composition of the salt blend can also be preferably varied between 65%-75% by weight of tribasic calcium phosphate and 25%-35% by weight of calcium lactate.
- the pH of the food product of the present invention does not exceed about 4.5 even at 100% of the U.S. RDA calcium fortification levels.
- Preparation of the especially preferred calcium fortified orange juice of the present invention involves the steps of determining the U.S. RDA level of calcium desired; addition of the calcium salt blend to water; gentle agitation of the solution of salt blend and water until partial solubility of the salt blend in water is achieved; addition of preblended orange juice concentrate and flavoring components and continued agitation until the salt blend is completely dispersed.
- the salt therein can be mixed with a portion of the fresh juice, and then with continued agitation, the remaining portion can be added.
- the preferred salt blend and fruit juice concentrate containing the ingredients listed in Table I provides a beverage which contains about 300 mg of calcium per six ounce serving. This preferred beverage will deliver approximately 30% of the U.S. RDA for calcium.
- the calcium is present, at least partially, in organically complexed forms. These forms help promote absorption of calcium in the gut.
- a six fluid ounce serving of the preferred calcium fortified orange juice or citrus juice product provides about 100% of the U.S. RDA for ascorbic acid.
- Another feature of the present invention is that the indigenous nutrients present in orange or citrus juice are not significantly affected by calcium salt addition.
- the blend of calcium phosphate, calcium lactate and citrus juice according to the invention is also essentially free from harsh or bitter taste, effervescence during manufacture or when consumed, calcium salt precipitation and calcium salt overnote flavor.
- blends of other calcium salts and citrus juice usually exhibit such undesirable qualities and produce the characteristic bitter overnote of a calcium salt taste.
- the characteristic sharp, clean, fruity, citrus taste of the beverage according to the invention is, therefore, surprising.
- the preferred calcium fortified orange or citrus juice product also contains significant quantities of other essential nutrients including folic acid, thiamine and potassium.
- a comparison of the nutrients contained in ordinary orange juice and those contained in the preferred fortified orange juice of the present invention is set forth in Table II.
- the beverage of the invention is substantially similar to ordinary juice beverages.
- a calcium fortified juice product manufactured in accordance with the present invention exhibits good solids distribution. It is desirable, however, to shake the product well in order to distribute pulp and other solids. It is also a characteristic of the calcium fortified orange juice of the present invention that the salt blend does not markedly increase sedimentation in spite of the well-known phenomenon of calcium citrate precipitation. Those undissolved materials which do form a sediment (usually natural citrus juice solids) can be readily redistributed throughout the juice by shaking or stirring before drinking. Accordingly, it is believed that the natural pectins present in standard orange or citrus juice serve as chelating or complexing agents to distribute and suspend the calcium salts. For those products made in accordance with the present invention that contain substantially little or no pectin and pulp at low viscosities, a stabilizer such as algin, pectin or dextrin may be incorporated to suspend the calcium salts.
- Tables III-V set forth exemplary compositions of other forms of the calcium fortified food product of the present invention.
- solubility of solids contained in a beverage manufactured in accordance with the present invention is dependent upon the calcium blend or individual calcium salt used.
- the calcium yield of each salt utilized varies slightly from batch to batch but an average yield could generally be expected and used in preparing formulations for manufacture.
- the addition of calcium to a standard single strength orange juice (11.8% to 12.0% soluble solids) increased the soluble solids to 12.2% to 13.7%, depending on the calcium salt selected and the enrichment level.
- the soluble, solids in frozen concentrated orange juice increased to about 43.0% to 49.0% soluble solids, as based on the use of calcium carbonate (at 40.04% calcium content, the compound which was highest in calcium) and calcium gluconate (at 9.31% calcium content, the compound which was lowest in calcium) as single sources of calcium.
- calcium carbonate at 40.04% calcium content, the compound which was highest in calcium
- calcium gluconate at 9.31% calcium content, the compound which was lowest in calcium
- Other salts either individually or in blends had harsh tastes, caused precipitates and/or masked the citrus juice flavor of the beverage being formulated.
- a highly desirable taste can be achieved by variation of the percentages of the two salts present so that the bland taste of one balances the tangy taste of the other.
- Table VII illustrates the changes in orange juice when equivalent amounts of calcium are added, i.e., 300 mg of calcium per 6 fluid ounces.
- Calcium carbonate was considered as a source of calcium. Its utilization in the invention, however, was considered unacceptable due to off-flavors, excessive foaming and effervescence during blending and an excessive increase in pH with a corresponding decrease in titrable acidity.
- a blend of two or more calcium salts was necessary. Though strict flavor equivalency was not obtained due to changes in the pH and perceived sensory texture, very acceptable prototypes were developed varying in degrees in flavor difference from the control. The various calcium blends developed and their characteristics are presented in Table VIII.
- the blends containing tribasic and monobasic calcium phosphate were found to be possibly drinkable, but tended to add a harsh character to the flavor of the beverage. As previously discussed, even limited usage of calcium carbonate tended to cause excessive foaming and effervescence. When prescribed amounts of calcium carbonate were are to the concentrated orange juice product, the foaming was unacceptable and posed problems for industrial production.
- the blend found to develope the desired flavor and taste characteristics, to facilitate preparation of beverages and to minimize cost was calcium phosphate (tribasic) and calcium lactate.
- the range of percent of total calcium for this blend is from about 50% to about 80% calcium phosphate and about 20% to about 50% calcium lactate.
- the preferred ratio range is from about 65% to about 75% by weight of the calcium from calcium phosphate and the remaining fraction of calcium (25% to 35% by weight) from calcium lactate.
- the pH of the calcium fortified orange juice helps maintain the product in the high acid condition. Calcium salts were blended so that the pH of the fortified juice product was less than 4.5 and the Brix-acid ratio was about 12.5:1 to about 20:1, (7:1 to 11:1 for grapefruit and other higher acid juices).
- the two orange juice samples used in the study contained a 75/25 weight percent blend (calcium basis) of tricalcium phosphate: calcium lactate; and a 80/20 weight percent blend (calcium basis) of tricalcium phosphate: monocalcium phosphate.
- Indirect measurements of intestinal calcium absorption expressed as increments in urinary calcium were made and the results are listed in Table IX.
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Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
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US07/084,680 US4871554A (en) | 1987-08-12 | 1987-08-12 | Calcium fortified food product |
CA000571798A CA1323793C (fr) | 1987-08-12 | 1988-07-12 | Produit alimentaire enrichi en calcium |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US07/084,680 US4871554A (en) | 1987-08-12 | 1987-08-12 | Calcium fortified food product |
Publications (1)
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US4871554A true US4871554A (en) | 1989-10-03 |
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Application Number | Title | Priority Date | Filing Date |
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US07/084,680 Expired - Fee Related US4871554A (en) | 1987-08-12 | 1987-08-12 | Calcium fortified food product |
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US (1) | US4871554A (fr) |
CA (1) | CA1323793C (fr) |
Cited By (63)
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EP0507157A1 (fr) * | 1991-04-05 | 1992-10-07 | Eckes-Granini GmbH & Co. Kommanditgesellschaft | Jus de fruit isotonique enrichi avec des minéraux |
US5389387A (en) * | 1991-12-26 | 1995-02-14 | The Procter & Gamble Company | Storage stable calcium-supplemented beverage concentrates |
US5401524A (en) * | 1992-10-21 | 1995-03-28 | The Proctor & Gamble Company | Storage stable calcium-supplemented beverage premix concentrates and syrups |
US5422128A (en) * | 1991-12-26 | 1995-06-06 | The Procter & Gamble Company | Storage stable calcium-supplemented beverage concentrates |
US5424082A (en) * | 1994-03-03 | 1995-06-13 | The Proctor & Gamble Company | Calcium and vitamin C containing beverage products with improved color stability |
US5445837A (en) * | 1992-10-21 | 1995-08-29 | The Procter & Gamble Company | Sweetener supplement fortified with a concentrated bioavailable calcium source and process of making |
US5468506A (en) * | 1992-10-21 | 1995-11-21 | The Procter & Gamble Company | Concentrated bioavailable calcium source |
US5474793A (en) * | 1994-05-10 | 1995-12-12 | Meyer; Larry E. | Process for preparing calcium-supplemented not-from-concentrate fruit juice beverages |
US5500232A (en) * | 1994-10-06 | 1996-03-19 | Bristol-Myers Squibb Company | Calcium fortified beverages |
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US5928691A (en) * | 1997-05-01 | 1999-07-27 | Nestec S.A. | Calcium complex and a process of making a food fortified with calcium |
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WO2000028838A1 (fr) * | 1998-11-18 | 2000-05-25 | Abbott Laboratories | Supplement nutritionnel a base de jus enrichi de calcium |
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US20080274264A1 (en) * | 2006-06-09 | 2008-11-06 | John Godber | Calcium fortification substance for clear beverages |
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