US3929627A - Magnetic beneficiation for magnesite ores - Google Patents
Magnetic beneficiation for magnesite ores Download PDFInfo
- Publication number
- US3929627A US3929627A US530395A US53039574A US3929627A US 3929627 A US3929627 A US 3929627A US 530395 A US530395 A US 530395A US 53039574 A US53039574 A US 53039574A US 3929627 A US3929627 A US 3929627A
- Authority
- US
- United States
- Prior art keywords
- ore
- magnesite
- crushed
- concentrate
- further step
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03C—MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03C1/00—Magnetic separation
- B03C1/005—Pretreatment specially adapted for magnetic separation
- B03C1/01—Pretreatment specially adapted for magnetic separation by addition of magnetic adjuvants
Definitions
- the increase of the magnetic properties of the ore or mineral to be separated is achieved by selective absorption on the surface of one or more constituents of the ore or mineral of a finely divided, highly magnetic substance such as a magnetite or a ferrosilicon.
- the thusly conditioned ore or mineral therefore has increased magnetic properties.
- Such selective absorption is achieved by conditioning the crushed ore or mineral in an aqueous mixture of suitable reagents for activating the surface of the constituents to be magnetically separated.
- the crushed ore or mineral is again conditioned in an aqueous suspension of a finely divided, strongly magnetic material such as magnetite or ferrosilicon.
- This strongly magnetic material is selectively absorbed on the surface of one or more constituents of the ore or mineral and thus increases their magnetic properties.
- the constituents of the ore or mineral that have absorbed the strongly magnetic material are then separated from the remainder of the constituents by means of a magnetic separat r so as to obtain a concentrate of the remainder of the constituents.
- recovery of the finely ground magnetic material from the surface of the ore or mineral constituents is carried out with water under pressure or with the use of detergents, or by agitation in another magnetic field.
- the ore or mineral is crushed into small particles, as for example less than 15 mm., although particles larger than 15 mm. may be subjected to the present process.
- the crushed ore or mineral is then thoroughly washed and the various sized particles may be classified into fractions of less than 1 mm., 1 mm. to 15 mm., and greater than 15 mm.
- Each of the fractions are then conditioned for about 10 to 20 minutes in an aqueous mixture of suitable reagents for activation of the surface of the constituents thereof to be magnetically removed. After undergoing such conditioning the material is drained and fed into a second conditioner of a suspension of finely ground magnetite or ferrosilicon materials and is stirred for about 5 to minutes.
- the material is drained and then fed into wet and dry magnetic separators for separating the absorbed magnetic material from the remainder of the material so as to obtain a concentrate of this remainder of the separated material.
- crushed ore or mineral may be first subjected to a mechanical pre-concentration process to further ultimately effect a concentrate of the remainder of the constituents.
- This concentrate of non-magnetic material is washed and, according to its purity, constitutes the intermediate or final product.
- This concentrate can be further subjected to the beneficiation process as above described so as to improve its quality. This will depend on the quality of the first recovery treatment of the ore or mineral, or upon the specifications required of the final product.
- the particles which absorbed the magnetic material may be thoroughly washed with water under pressure or with the use of a detergent, or by agitation in a magnetic field, so that the absorbed film of the highly magnetic material may be removed.
- This recovery of the finely ground magnetic material from the surface of the ore or mineral constituents is carried out by known methods, as for example thickening, washing, magnetic separation or the use of a demagnetizing coil.
- a magnesite ore containing slightly magnetic serpentine and non-magnetic feldspars and silica was subjected to the beneficiation process as in the manner above-described.
- the first conditioning was carried out in an aqueous suspension of, by volume, 1 percent diesel oil and 0.15 percent of a mixture of a dialkyl quaternary ammonium chloride such as ARQUAD 2C-75 and primary amines such as ARMAC T and ARMAC C.
- the first conditioning lasted for ten minutes and the second conditioning step was carried out in an aqueous suspension of finely ground magnetite of 1 percent by volume.
- Magnetic separation of for example the l to 3 mm. fraction yielded a product of pure magnesite with 0.72 percent SiO and 1.08 percent CaO, by volume, constituting a fraction of 36.4 percent of the magnesite ore feed which has an analysis of 16.92 percent SiO, and 4.9 percent CaO.
- the reagents used for activation of the surface of the constituents of the ore to be magnetically separated are the same as those used for the flotation process disclosed in commonly owned U.S. application Ser. No. 530,396, filed on even date herewith. Only very small quantities of these reagents are re; quired for the present process thereby rendering the first conditioning step quite economical.
- Another advantage with the use of the present process is that relatively coarse crushed ore can be used provided that the intended concentration can be carried out for such sized particles. The costly grinding operation normally required for flotation is therefore avoided.
- a process for the recovery of pure magnesite from magnesite ores containing magnesite, serpentine and other gangue material comprising:
Landscapes
- Manufacture And Refinement Of Metals (AREA)
- Separation Of Solids By Using Liquids Or Pneumatic Power (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GR362774 | 1974-01-29 |
Publications (1)
Publication Number | Publication Date |
---|---|
US3929627A true US3929627A (en) | 1975-12-30 |
Family
ID=10922932
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US530395A Expired - Lifetime US3929627A (en) | 1974-01-29 | 1974-12-06 | Magnetic beneficiation for magnesite ores |
Country Status (9)
Country | Link |
---|---|
US (1) | US3929627A (de) |
AT (1) | AT328387B (de) |
AU (1) | AU500249B2 (de) |
BR (1) | BR7500482A (de) |
CA (1) | CA1013709A (de) |
CS (1) | CS185672B2 (de) |
IN (1) | IN143918B (de) |
YU (1) | YU352374A (de) |
ZA (1) | ZA75612B (de) |
Cited By (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4147614A (en) * | 1976-06-10 | 1979-04-03 | Theodor Gambopoulos | Aqueous mixture of diesel oil, pine oil and diamine for conditioning of crushed magnesite ore in magnetic beneficiation process |
US4176054A (en) * | 1977-05-16 | 1979-11-27 | Kelley Joseph A | Waste paper recycling |
US4187170A (en) * | 1977-01-27 | 1980-02-05 | Foxboro/Trans-Sonics, Inc. | Magnetic techniques for separating non-magnetic materials |
US4219408A (en) * | 1978-04-27 | 1980-08-26 | Anglo-American Clays Corporation | Magnetic separation of minerals utilizing magnetic particulates |
US4225426A (en) * | 1975-10-01 | 1980-09-30 | Anglo-American Clays Corporation | Magnetic beneficiation of clays utilizing magnetic particulates |
US4225425A (en) * | 1975-10-01 | 1980-09-30 | Anglo-American Clays Corporation | Method for separating metallic minerals utilizing magnetic seeding |
US4298169A (en) * | 1979-09-26 | 1981-11-03 | The Regents Of The University Of Minnesota | Selective flocculation, magnetic separation, and flotation of ores |
US4526681A (en) * | 1983-10-31 | 1985-07-02 | Purdue Research Foundation | Magnetic separation method utilizing a colloid of magnetic particles |
US4643822A (en) * | 1985-02-28 | 1987-02-17 | The Secretary Of State For Trade And Industry In Her Britannic Majesty's Government Of The United Kingdom Of Great Britain And Northern Ireland | Method of separation of material from material mixtures |
US4657666A (en) * | 1981-10-26 | 1987-04-14 | W.S.R. Pty. Ltd. | Magnetic flotation |
US4735707A (en) * | 1985-06-01 | 1988-04-05 | The British Petroleum Company P.L.C. | Removing mineral matter from solid carbonaceous fuels |
US4765486A (en) * | 1983-06-21 | 1988-08-23 | The United States Of America As Represented By The Secretary Of Agriculture | Method for obtaining a purified fraction from a mixture using a magnetic fluid |
US4810368A (en) * | 1985-04-10 | 1989-03-07 | Electro Minerals (Canada) Inc. | Automatic method for separating and cleaning silicon carbide furnace materials |
US6098810A (en) * | 1998-06-26 | 2000-08-08 | Pueblo Process, Llc | Flotation process for separating silica from feldspar to form a feed material for making glass |
US20080164140A1 (en) * | 2007-01-05 | 2008-07-10 | Cytec Technology Corp. | Process for the removal of impurities from carbonate minerals |
WO2009124015A2 (en) * | 2008-03-31 | 2009-10-08 | Mba Polymers, Inc. | Methods, systems, and devices for separating materials using magnetic and frictional properties |
Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US861782A (en) * | 1905-03-20 | 1907-07-30 | Internat Separator Company | Process of separating ore. |
US933717A (en) * | 1909-01-11 | 1909-09-07 | Alfred Arthur Lockwood | Process of treating ores. |
US989239A (en) * | 1907-03-18 | 1911-04-11 | Polygraph Duplicating Typewriter Company | Redproducing and imitating machine. |
US1043851A (en) * | 1912-04-29 | 1912-11-12 | Murex Magnetic Company Ltd | Process of separating ores, &c. |
US2240718A (en) * | 1938-08-13 | 1941-05-06 | Schiffman Le Roy Edgar | Concentration of ores |
US2269912A (en) * | 1939-01-04 | 1942-01-13 | Raymond B Ladoo | Method of treating ores |
US2828010A (en) * | 1956-06-07 | 1958-03-25 | Gompper Johannes | Seed separation |
US3032189A (en) * | 1958-11-17 | 1962-05-01 | Int Minerals & Chem Corp | Beneficiation of phosphatic ores |
-
1974
- 1974-11-27 AT AT948974A patent/AT328387B/de not_active IP Right Cessation
- 1974-12-06 US US530395A patent/US3929627A/en not_active Expired - Lifetime
- 1974-12-20 CA CA216,594A patent/CA1013709A/en not_active Expired
- 1974-12-20 IN IN2821/CAL/74A patent/IN143918B/en unknown
- 1974-12-24 AU AU76858/74A patent/AU500249B2/en not_active Expired
- 1974-12-31 YU YU03523/74A patent/YU352374A/xx unknown
-
1975
- 1975-01-23 BR BR482/75A patent/BR7500482A/pt unknown
- 1975-01-29 CS CS7500000587A patent/CS185672B2/cs unknown
- 1975-01-29 ZA ZA00750612A patent/ZA75612B/xx unknown
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US861782A (en) * | 1905-03-20 | 1907-07-30 | Internat Separator Company | Process of separating ore. |
US989239A (en) * | 1907-03-18 | 1911-04-11 | Polygraph Duplicating Typewriter Company | Redproducing and imitating machine. |
US933717A (en) * | 1909-01-11 | 1909-09-07 | Alfred Arthur Lockwood | Process of treating ores. |
US1043851A (en) * | 1912-04-29 | 1912-11-12 | Murex Magnetic Company Ltd | Process of separating ores, &c. |
US2240718A (en) * | 1938-08-13 | 1941-05-06 | Schiffman Le Roy Edgar | Concentration of ores |
US2269912A (en) * | 1939-01-04 | 1942-01-13 | Raymond B Ladoo | Method of treating ores |
US2828010A (en) * | 1956-06-07 | 1958-03-25 | Gompper Johannes | Seed separation |
US3032189A (en) * | 1958-11-17 | 1962-05-01 | Int Minerals & Chem Corp | Beneficiation of phosphatic ores |
Cited By (20)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4225426A (en) * | 1975-10-01 | 1980-09-30 | Anglo-American Clays Corporation | Magnetic beneficiation of clays utilizing magnetic particulates |
US4225425A (en) * | 1975-10-01 | 1980-09-30 | Anglo-American Clays Corporation | Method for separating metallic minerals utilizing magnetic seeding |
US4147614A (en) * | 1976-06-10 | 1979-04-03 | Theodor Gambopoulos | Aqueous mixture of diesel oil, pine oil and diamine for conditioning of crushed magnesite ore in magnetic beneficiation process |
US4187170A (en) * | 1977-01-27 | 1980-02-05 | Foxboro/Trans-Sonics, Inc. | Magnetic techniques for separating non-magnetic materials |
US4176054A (en) * | 1977-05-16 | 1979-11-27 | Kelley Joseph A | Waste paper recycling |
US4219408A (en) * | 1978-04-27 | 1980-08-26 | Anglo-American Clays Corporation | Magnetic separation of minerals utilizing magnetic particulates |
US4298169A (en) * | 1979-09-26 | 1981-11-03 | The Regents Of The University Of Minnesota | Selective flocculation, magnetic separation, and flotation of ores |
US4657666A (en) * | 1981-10-26 | 1987-04-14 | W.S.R. Pty. Ltd. | Magnetic flotation |
US4765486A (en) * | 1983-06-21 | 1988-08-23 | The United States Of America As Represented By The Secretary Of Agriculture | Method for obtaining a purified fraction from a mixture using a magnetic fluid |
US4526681A (en) * | 1983-10-31 | 1985-07-02 | Purdue Research Foundation | Magnetic separation method utilizing a colloid of magnetic particles |
US4643822A (en) * | 1985-02-28 | 1987-02-17 | The Secretary Of State For Trade And Industry In Her Britannic Majesty's Government Of The United Kingdom Of Great Britain And Northern Ireland | Method of separation of material from material mixtures |
US4810368A (en) * | 1985-04-10 | 1989-03-07 | Electro Minerals (Canada) Inc. | Automatic method for separating and cleaning silicon carbide furnace materials |
US4735707A (en) * | 1985-06-01 | 1988-04-05 | The British Petroleum Company P.L.C. | Removing mineral matter from solid carbonaceous fuels |
US6098810A (en) * | 1998-06-26 | 2000-08-08 | Pueblo Process, Llc | Flotation process for separating silica from feldspar to form a feed material for making glass |
US20080164140A1 (en) * | 2007-01-05 | 2008-07-10 | Cytec Technology Corp. | Process for the removal of impurities from carbonate minerals |
US8066885B2 (en) * | 2007-01-05 | 2011-11-29 | Cytec Technology Corp. | Process for the removal of impurities from carbonate minerals |
WO2009124015A2 (en) * | 2008-03-31 | 2009-10-08 | Mba Polymers, Inc. | Methods, systems, and devices for separating materials using magnetic and frictional properties |
WO2009124015A3 (en) * | 2008-03-31 | 2010-01-14 | Mba Polymers, Inc. | Methods, systems, and devices for separating materials using magnetic and frictional properties |
US20100078362A1 (en) * | 2008-03-31 | 2010-04-01 | Mba Polymers, Inc. | Methods, Systems, and Devices for Separating Materials Using Magnetic and Frictional Properties |
US8056728B2 (en) | 2008-03-31 | 2011-11-15 | Mba Polymers, Inc. | Methods, systems, and devices for separating materials using magnetic and frictional properties |
Also Published As
Publication number | Publication date |
---|---|
AU500249B2 (en) | 1979-05-17 |
CA1013709A (en) | 1977-07-12 |
ZA75612B (en) | 1976-01-28 |
CS185672B2 (en) | 1978-10-31 |
AU7685874A (en) | 1976-06-24 |
IN143918B (de) | 1978-02-25 |
ATA948974A (de) | 1975-06-15 |
BR7500482A (pt) | 1975-11-04 |
YU352374A (en) | 1982-02-28 |
AT328387B (de) | 1976-03-25 |
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