US3904355A - Atmosphere isolating means in a continuous-type furnace - Google Patents

Atmosphere isolating means in a continuous-type furnace Download PDF

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US3904355A
US3904355A US489080A US48908074A US3904355A US 3904355 A US3904355 A US 3904355A US 489080 A US489080 A US 489080A US 48908074 A US48908074 A US 48908074A US 3904355 A US3904355 A US 3904355A
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furnace
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Susumu Takahashi
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    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B9/00Furnaces through which the charge is moved mechanically, e.g. of tunnel type; Similar furnaces in which the charge moves by gravity
    • F27B9/04Furnaces through which the charge is moved mechanically, e.g. of tunnel type; Similar furnaces in which the charge moves by gravity adapted for treating the charge in vacuum or special atmosphere
    • F27B9/045Furnaces with controlled atmosphere
    • F27B9/047Furnaces with controlled atmosphere the atmosphere consisting of protective gases
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/74Methods of treatment in inert gas, controlled atmosphere, vacuum or pulverulent material
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C8/00Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C8/06Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using gases

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  • the means comprises a plurality of curtain-like units suspended one after the other and freely over the articles being conveyed on a conveyor belt for heat-treatment. A proper sealing effect between the adjoining zones of the furnace is obtained so that the heat-treatment may be conducted under optimum atmospheric and thermal operating conditions.
  • This invention relates to an improved device for adjusting and maintaining the gas atmosphere in continuous-type furnaces such as a conveyor belt type gasatmosphcre heating furnace.
  • the progress of carburizing is affected adversely on account of carbon precipitation on the article surface at the heating zone.
  • the temperature has to he lowered from a carburizing temperature of 900C for example to the quenching temperature of 830C for example for the subsequent quenching operation. and if it is desired to diffuse the carbon deep from the surface of the article. the carbon potential at the diffusing zone must be lowered necessarily under that prescribed for the earburizing zone.
  • a certain possitive isolating device has to be provided between the zones. while the such device shall not prevent the free transferring movement of articlesv
  • the gas atmosphere must have a well-defined carbon potential for the re spective zones to heighten the accuracy in the carburizing depth.
  • FIG. is a schematic side elevation. partly in cross section. of the overall heating furnace
  • FIG. 2 is a front view of a curtain device which isolates adjacent zones
  • FIG. 3 is a sectional view taken on line lll lll of HG].
  • FIG. 4 is a graph showing dew points measured at several points within the furnace provided with this in vention isolating means.
  • FIG. 1 showing the overall continuoustype heating furnace A. 1 designates a conveyor belt of the mesh type for transporting the articles to be heat treated.
  • 2 an inlet for the carrier gas.
  • 3 an inlet for the carrier gas and the carburizing gas.
  • 4 an inlet for the carrier gas to be used in a diffusing zone t. 5 an agitator.
  • b heaters. 7 a quenching oil bath. a a heating zone. and I a earburizing Zone.
  • the furnace is provided with an inlet 9 and outlet 10. These inlet and outlet openings may be closed by pivotal doors (not shown).
  • the oil quenching bath 7 is provided with a conveyor 8 which takes out carhurized articles from the bath.
  • These curtains D are provided as isolating means between the heating zone a and the carburizing zone I). and between the carburizing zone b and the diffusion zone r. so that the supporting members 11 are secured at the upper part of the furnace A and the lower portions of the curtain are hung freely above the conveyor belt 1.
  • the respective zones u, h and r' are effectively divided from one another by these curtains D which are hung freely above the articles placed on the moving belt, so that these curtains D are flung open by the proceeding articles irrespective of the article size. and a proper sealing effect may be attained with these curtains D.
  • the gases in the zones u. b. L may be kept at the respective temperatures and compositions suited for the heat treatment to be conducted in the heating furance. Besides a more ac curate control of the carbon concentration and the depth of carbon penetration are possible with the above arrangement.
  • EXAMPLE A steel plate (SPCC) l mmv thick was used as a sample for carburizing and nitriding to obtain an HRV surface hardness higher than 770 and a depth of carbon penetration in the range of (H18 to (J. l 5 mm.
  • the carburizing zone Ii was kept at 8 lUC
  • a gas at a dew point of 4C was introduced from the inlet 2 as atmosphere in the heating zone.
  • a carrier gas at the dew point of 4C added with carburizing atmospheric gases of l percent of propane and 2 percent of ammonia was introduced from the inlets 3, 3.
  • a gas at the dew point of 4C was introduced from the inlet 4.
  • the oil quenching bath was maintained at 60C. Th test sample No.
  • a proper isolating effect between the adjoining zones is attained by the curtains D which may be flung open by the proceeding articles in conformity to the shape and size of the articles.
  • the carbon potential of the gas atmosphere may be adjusted and maintained at a highly accurate level so that the heat treatment may be conducted under the optimum operating conditions.
  • means for controlling and maintaining gas atmospheres for such zones comprising a plurality of curtains arranged one closely after the other, each said curtain comprising a plurality of sets of metal segments. which are all of the same height, the segments of each set being arranged in alignment laterally but being staggered relative to those of the next adjacent set, said curtains constituting isolating means between the adjacent zones, and being freely suspended above the conveyor means for isolating the atmospheres supplied to ssiad zones from one another and for allowing the articles to freely pass through the zones via said isolating means.

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Solid-Phase Diffusion Into Metallic Material Surfaces (AREA)
  • Tunnel Furnaces (AREA)

Abstract

Means for adjusting and maintaining the gas atmosphere in each zone of a continuous-type furnace. The means comprises a plurality of curtain-like units suspended one after the other and freely over the articles being conveyed on a conveyor belt for heat-treatment. A proper sealing effect between the adjoining zones of the furnace is obtained so that the heat-treatment may be conducted under optimum atmospheric and thermal operating conditions.

Description

United States Patent Takahashi 1 Sept. 9, 1975 1 1 ATMOSPHERE ISOLATING MEANS IN A 3.415.503 12/1968 Beck 432/152 x 3,467.366 9/1969 Westcren et a1. 432/152 X CONTINUOUS-TYPE FURNACE [76] Inventor: Susumu Takahashi, 12/21. S-chome.
Wakabaya. Setagaya-ku, Tokyo, Japan [22} Filed: July 17, 1974 [21] Appl. No.: 489,080
[52} U.S. Cl. 432/152; 34/142; 432/144 (51} Int. Cl.' F278 9/04 (58] Field of Search 432/152, 128. 143, 144; 34/242 [56] References Cited UNiTED STATES PATENTS 2.200.619 5/1940 Fallon 432/242 X 3.189.336 6/1965 Montagino 432/152 X Primary ExaminerJohn J. Camby Attorney, Agent, or FirmShlesinger, Fitzsimmons & Shlesinger [5 7] ABSTRACT Means for adjusting and maintaining the gas atmosphere in each zone ofa continuoustypc furnace. The means comprises a plurality of curtain-like units suspended one after the other and freely over the articles being conveyed on a conveyor belt for heat-treatment. A proper sealing effect between the adjoining zones of the furnace is obtained so that the heat-treatment may be conducted under optimum atmospheric and thermal operating conditions.
2 Claims, 4 Drawing Figures PATENTEU 9 W5 FIG. I
FIG. 3
ATMOSPHERE ISOLATING MEANS IN A CONTINUOUS-TYPE FURNACE This invention relates to an improved device for adjusting and maintaining the gas atmosphere in continuous-type furnaces such as a conveyor belt type gasatmosphcre heating furnace.
Heretofore. in this type of heating furnace wherein the conveyor belt is moved consecutively through the heating. carburizing and diffusing zones for continuous heat treatment operation. a so-called drop arch type unit is employed as a curtain for partitioning said zones from one another and separately controlling the atmo sphere in each of such zones. In order to minimize the gap between the arch and the articles to be processed. the arch must be shaped and sized to conform to the articles occasionally processed in the furnace. thus complicating the structure to the device and making it nccessary to use the different types of arch structure for each heat treating operation. In this known furnace. when the carbon potential ofthc gas atmosphere within the heating zone is equal to that of the gas atmosphere for the carhurizing zone. the progress of carburizing is affected adversely on account of carbon precipitation on the article surface at the heating zone. It shall be noted also that after carburizing. the temperature has to he lowered from a carburizing temperature of 900C for example to the quenching temperature of 830C for example for the subsequent quenching operation. and if it is desired to diffuse the carbon deep from the surface of the article. the carbon potential at the diffusing zone must be lowered necessarily under that prescribed for the earburizing zone. Hence, a certain possitive isolating device has to be provided between the zones. while the such device shall not prevent the free transferring movement of articlesv Moreover. in the case of carburizing to a shallower depth. the gas atmosphere must have a well-defined carbon potential for the re spective zones to heighten the accuracy in the carburizing depth.
Hence. it is the principal object of the present invention to provide a device for adjusting and maintaining the gas atmosphere in the carburizing furnace whereby the above inconvenience may be obviated.
The present invention will he described below by re ferring to the accompanying drawing showing a preferred embodiment thereof.
In the drawing:
FIG. is a schematic side elevation. partly in cross section. of the overall heating furnace;
FIG. 2 is a front view of a curtain device which isolates adjacent zones;
FIG. 3 is a sectional view taken on line lll lll of HG]; and
FIG. 4 is a graph showing dew points measured at several points within the furnace provided with this in vention isolating means.
Referring to FIG. 1 showing the overall continuoustype heating furnace A. 1 designates a conveyor belt of the mesh type for transporting the articles to be heat treated. 2 an inlet for the carrier gas. 3 an inlet for the carrier gas and the carburizing gas. 4 an inlet for the carrier gas to be used in a diffusing zone t. 5 an agitator. b heaters. 7 a quenching oil bath. a a heating zone. and I a earburizing Zone. The furnace is provided with an inlet 9 and outlet 10. These inlet and outlet openings may be closed by pivotal doors (not shown). The oil quenching bath 7 is provided with a conveyor 8 which takes out carhurized articles from the bath.
D t'lesignates a curtain comprising more than two overlapped sets of steel plates or segments d. each said set consisting of a plurality of the aligned or juxtaposed segments (1 each of which is formed as a thin band of heating resistant steel. These sets of steel segments (1 are so placed that the individual segments ofone set are staggered relative to those of the other set of the segments (1. These segments d are secured at the upper ends to a support member 11 so that their lower ends are left loose and depend in the form of a blind or a rope curtain. These curtains D are provided as isolating means between the heating zone a and the carburizing zone I). and between the carburizing zone b and the diffusion zone r. so that the supporting members 11 are secured at the upper part of the furnace A and the lower portions of the curtain are hung freely above the conveyor belt 1.
in the heat treating operation. the respective zones u, h and r' are effectively divided from one another by these curtains D which are hung freely above the articles placed on the moving belt, so that these curtains D are flung open by the proceeding articles irrespective of the article size. and a proper sealing effect may be attained with these curtains D. Thus. the gases in the zones u. b. L may be kept at the respective temperatures and compositions suited for the heat treatment to be conducted in the heating furance. Besides a more ac curate control of the carbon concentration and the depth of carbon penetration are possible with the above arrangement.
Next. the present invention will he explained in connection with the following numerical example.
EXAMPLE A steel plate (SPCC) l mmv thick was used as a sample for carburizing and nitriding to obtain an HRV surface hardness higher than 770 and a depth of carbon penetration in the range of (H18 to (J. l 5 mm. The carburizing zone Ii was kept at 8 lUC A gas at a dew point of 4C was introduced from the inlet 2 as atmosphere in the heating zone. A carrier gas at the dew point of 4C added with carburizing atmospheric gases of l percent of propane and 2 percent of ammonia was introduced from the inlets 3, 3. A gas at the dew point of 4C was introduced from the inlet 4. The oil quenching bath was maintained at 60C. Th test sample No. l was designed to pass through the carburizing Zone in 30 minutes. while the test sample No. 2 was designed to pass through the same zone in fill minutes. as tabulated in the following Table with the test results. The transition in the dew points as measured at various points inside the furnace is shown graphically in the chart of FIG. 4, in which ordinate indicates the temperature (C) of dew points and abscissa indicates measuring points in the furnace.
Penetration 1mm) Tenip.1C) Timelminutes) No l (Llll-(l l4 8H) 30 Table-Continued Test Sample Number of samples Surface Hardncss(HR\/J It will be seen from FIG. 4 and the above Table that the arrangement of this invention enables the tempera tures and dew points of the respective zones of the furnace to be demarcated definitely from one another in accordance with the requirement for the carburizing operation being conducted in the furnace.
According to this invention. a proper isolating effect between the adjoining zones is attained by the curtains D which may be flung open by the proceeding articles in conformity to the shape and size of the articles. Moreover. the carbon potential of the gas atmosphere may be adjusted and maintained at a highly accurate level so that the heat treatment may be conducted under the optimum operating conditions.
What is claimed is:
1. In combination with a continuous-type furnace in which articles to be treated are transferred by conveyor means through a plurality of treating zones. means for controlling and maintaining gas atmospheres for such zones comprising a plurality of curtains arranged one closely after the other, each said curtain comprising a plurality of sets of metal segments. which are all of the same height, the segments of each set being arranged in alignment laterally but being staggered relative to those of the next adjacent set, said curtains constituting isolating means between the adjacent zones, and being freely suspended above the conveyor means for isolating the atmospheres supplied to ssiad zones from one another and for allowing the articles to freely pass through the zones via said isolating means.
2. Isolating means as claimed in claim 1, in which the segments are thermally resistive thin metallic strips.

Claims (2)

1. In combination with a continuous-type furnace in which articles to be treated are transferred by conveyor means through a plurality of treating zones, means for controlling and maintaining gas atmospheres for such zones comprising a plurality of curtains arranged one closely after the other, each said curtain comprising a plurality of sets of metal segments, which are all of the same height, the segments of each set being arranged in alignment laterally but being staggered relative to those of the next adjacent set, said curtains constituting isolating means between the adjacent zones, and being freely suspended above the conveyor means for isolating the atmospheres supplied to ssiad zones from one another and for allowing the articles to freely pass through the zones via said isolating means.
2. Isolating means as claimed in claim 1, in which the segments are thermally resistive thin metallic strips.
US489080A 1974-07-17 1974-07-17 Atmosphere isolating means in a continuous-type furnace Expired - Lifetime US3904355A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4193761A (en) * 1977-10-07 1980-03-18 Enzo Mantegani Kiln
US4867677A (en) * 1989-05-03 1989-09-19 Bethlehem Steel Corporation Curtain door for metal reheating furnace
US20020160909A1 (en) * 2001-04-25 2002-10-31 Emmanuel Auer Process and apparatus for the thermal treatment of pulverulent substances
US11186108B1 (en) 2020-10-16 2021-11-30 Photo U.S.A. Corporation Sublimation printing on to dark surfaces
US11548307B2 (en) 2020-07-29 2023-01-10 Photo U.S.A. Corporation Sublimation printing production line and automated sublimation printing method for cylindrical workpieces

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2200619A (en) * 1938-07-12 1940-05-14 Fallon John Means for sealing the charging and discharging apertures of continuous or intermittent furnaces
US3189336A (en) * 1962-11-15 1965-06-15 Midland Ross Corp Metallurgical heating furnace
US3415503A (en) * 1967-08-18 1968-12-10 Btu Eng Corp Conditioned atmosphere furnace muffle
US3467366A (en) * 1967-10-02 1969-09-16 Hayes Inc C I Furnace construction having atmosphere curtain

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2200619A (en) * 1938-07-12 1940-05-14 Fallon John Means for sealing the charging and discharging apertures of continuous or intermittent furnaces
US3189336A (en) * 1962-11-15 1965-06-15 Midland Ross Corp Metallurgical heating furnace
US3415503A (en) * 1967-08-18 1968-12-10 Btu Eng Corp Conditioned atmosphere furnace muffle
US3467366A (en) * 1967-10-02 1969-09-16 Hayes Inc C I Furnace construction having atmosphere curtain

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4193761A (en) * 1977-10-07 1980-03-18 Enzo Mantegani Kiln
US4867677A (en) * 1989-05-03 1989-09-19 Bethlehem Steel Corporation Curtain door for metal reheating furnace
US20020160909A1 (en) * 2001-04-25 2002-10-31 Emmanuel Auer Process and apparatus for the thermal treatment of pulverulent substances
US7288501B2 (en) * 2001-04-25 2007-10-30 Umicore Ag & Co., Kg Process and apparatus for the thermal treatment of pulverulent substances
US11548307B2 (en) 2020-07-29 2023-01-10 Photo U.S.A. Corporation Sublimation printing production line and automated sublimation printing method for cylindrical workpieces
US11186108B1 (en) 2020-10-16 2021-11-30 Photo U.S.A. Corporation Sublimation printing on to dark surfaces

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