US3884841A - 2-n-butyl 4,4,6-trimethyl-1,3 dioxane perfume - Google Patents

2-n-butyl 4,4,6-trimethyl-1,3 dioxane perfume Download PDF

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Publication number
US3884841A
US3884841A US456317A US45631774A US3884841A US 3884841 A US3884841 A US 3884841A US 456317 A US456317 A US 456317A US 45631774 A US45631774 A US 45631774A US 3884841 A US3884841 A US 3884841A
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US
United States
Prior art keywords
weight
parts
trimethyl
butyl
perfume
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
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US456317A
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English (en)
Inventor
Jan Th M F Maessen
David Derijke
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Naarden International NV
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Naarden International NV
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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/0069—Heterocyclic compounds
    • C11B9/0073—Heterocyclic compounds containing only O or S as heteroatoms
    • C11B9/008—Heterocyclic compounds containing only O or S as heteroatoms the hetero rings containing six atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D319/00—Heterocyclic compounds containing six-membered rings having two oxygen atoms as the only ring hetero atoms
    • C07D319/04—1,3-Dioxanes; Hydrogenated 1,3-dioxanes
    • C07D319/06—1,3-Dioxanes; Hydrogenated 1,3-dioxanes not condensed with other rings

Definitions

  • flavour Green "floral, peppermintlike
  • Dependent on the type of composition the dosage 25 2j:n-Butyl-4.4.6-trimethyl-l.3- 160 parts by weight loxane may he between about 5 and about 15% by weight.
  • mgthylpmhalme 103 parts by weight a matter of fact in a perfumed product the final concen- 1000 Pans by weight tration will lie much lower.
  • 2-n-Butyl-4.4.6-trimethyl-1.3-dioxane may be prepared in the following way:
  • the evaporation residue is fractionated in a distillation apparatus with a 40 cm Vigreus-head, at which is obtained: 4 g fore-runnings, boiling point up to 81C/l mm Hg and 170 g 2-n-butyl-4.4 .6-trimethyl-l .3- dioxane boiling point 8l-82C/1 mm Hg; u 1,4295.
  • a perfume composition comprising from 5 to 16% of 2-n-butyl-4,4,6-trimethyl-1,3-dioxane in a perfume carrier.

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Cosmetics (AREA)
  • Fats And Perfumes (AREA)
  • Detergent Compositions (AREA)
  • Heterocyclic Compounds That Contain Two Or More Ring Oxygen Atoms (AREA)
US456317A 1973-04-18 1974-03-29 2-n-butyl 4,4,6-trimethyl-1,3 dioxane perfume Expired - Lifetime US3884841A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
NL7305487.A NL166187C (nl) 1973-04-18 1973-04-18 Werkwijze ter bereiding van reukstofcomposities door een 2-gesubstitueerd 4,4,6-trimethyl-1,3-dioxan te mengen met ten minste een andere reukstof en geparfu- meerde voorwerpen.

Publications (1)

Publication Number Publication Date
US3884841A true US3884841A (en) 1975-05-20

Family

ID=19818679

Family Applications (1)

Application Number Title Priority Date Filing Date
US456317A Expired - Lifetime US3884841A (en) 1973-04-18 1974-03-29 2-n-butyl 4,4,6-trimethyl-1,3 dioxane perfume

Country Status (9)

Country Link
US (1) US3884841A (ja)
JP (1) JPS505541A (ja)
BE (1) BE812847A (ja)
CH (1) CH601470A5 (ja)
DE (1) DE2415922C3 (ja)
FR (1) FR2226187B1 (ja)
GB (1) GB1465320A (ja)
IT (1) IT1050471B (ja)
NL (1) NL166187C (ja)

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3966647A (en) * 1974-03-18 1976-06-29 Lever Brothers Company Perfume compositions containing monoalkyl-para-dioxanes
US4124541A (en) * 1976-06-28 1978-11-07 Henkel Kommanditgesellschaft Auf Aktien Dioxa bicyclo dodecane and -hexadecane perfume compositions
US4146506A (en) * 1976-10-23 1979-03-27 Henkel Kommanditgesellschaft Auf Aktien (Henkel Kgaa) Perfume compositions with 4-isopropyl-5,5-dimethyl-1,3-dioxane
US4198323A (en) * 1977-07-29 1980-04-15 Henkel Kommanditgesellschaft Auf Aktien (Henkel Kgaa) 2,2,5-Trimethyl-5-phenyl-1,3-dioxane and perfume compositions containing it
US4211674A (en) * 1978-04-10 1980-07-08 Polak's Frutal Works B.V. Cyclic acetals and ketals and their use in perfume compositions
US4372880A (en) * 1980-04-25 1983-02-08 Henkel Kommanditgesellschaft Auf Aktien Use of substituted 2-(1-methylbutyl)-1,3-dioxanes as perfuming agents
EP1316553A1 (de) * 2001-11-30 2003-06-04 Celanese Chemicals Europe GmbH Riechstoffe auf Basis cyclischer Acetale

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5939890A (ja) * 1982-08-26 1984-03-05 Neos Co Ltd フエニル置換２−（１−アルケニル）−４−イソプロピル−５，５−ジメチル−１，３−ジオキサン誘導体
EP3101112B1 (en) * 2012-01-18 2019-04-03 The Procter and Gamble Company Perfume systems
CA2908686A1 (en) * 2013-04-24 2014-10-30 The Procter & Gamble Company Perfume systems

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB981285A (en) * 1962-09-04 1965-01-20 Unilever Ltd Alkylated 1,3-dioxanes and their use as perfumes

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB981285A (en) * 1962-09-04 1965-01-20 Unilever Ltd Alkylated 1,3-dioxanes and their use as perfumes

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3966647A (en) * 1974-03-18 1976-06-29 Lever Brothers Company Perfume compositions containing monoalkyl-para-dioxanes
US4124541A (en) * 1976-06-28 1978-11-07 Henkel Kommanditgesellschaft Auf Aktien Dioxa bicyclo dodecane and -hexadecane perfume compositions
US4146506A (en) * 1976-10-23 1979-03-27 Henkel Kommanditgesellschaft Auf Aktien (Henkel Kgaa) Perfume compositions with 4-isopropyl-5,5-dimethyl-1,3-dioxane
US4198323A (en) * 1977-07-29 1980-04-15 Henkel Kommanditgesellschaft Auf Aktien (Henkel Kgaa) 2,2,5-Trimethyl-5-phenyl-1,3-dioxane and perfume compositions containing it
US4211674A (en) * 1978-04-10 1980-07-08 Polak's Frutal Works B.V. Cyclic acetals and ketals and their use in perfume compositions
US4372880A (en) * 1980-04-25 1983-02-08 Henkel Kommanditgesellschaft Auf Aktien Use of substituted 2-(1-methylbutyl)-1,3-dioxanes as perfuming agents
EP1316553A1 (de) * 2001-11-30 2003-06-04 Celanese Chemicals Europe GmbH Riechstoffe auf Basis cyclischer Acetale
EP1481974A1 (de) * 2001-11-30 2004-12-01 Celanese Chemicals Europe GmbH Riechstoffe auf Basis cyclischer Acetale

Also Published As

Publication number Publication date
IT1050471B (it) 1981-03-10
DE2415922A1 (de) 1974-11-07
NL166187C (nl) 1981-07-15
DE2415922C3 (de) 1978-06-08
CH601470A5 (ja) 1978-07-14
BE812847A (nl) 1974-09-26
NL7305487A (ja) 1974-10-22
FR2226187A1 (ja) 1974-11-15
DE2415922B2 (de) 1977-10-20
GB1465320A (en) 1977-02-23
JPS505541A (ja) 1975-01-21
FR2226187B1 (ja) 1978-01-20
NL166187B (nl) 1981-02-16

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