US3816087A - Method of interconnecting glass parts by passing through electric current - Google Patents

Method of interconnecting glass parts by passing through electric current Download PDF

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Publication number
US3816087A
US3816087A US00188614A US18861471A US3816087A US 3816087 A US3816087 A US 3816087A US 00188614 A US00188614 A US 00188614A US 18861471 A US18861471 A US 18861471A US 3816087 A US3816087 A US 3816087A
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United States
Prior art keywords
edges
glass
electric current
passing
glass parts
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Expired - Lifetime
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US00188614A
Inventor
Duuren K Van
A Verhoeven
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US Philips Corp
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US Philips Corp
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Publication date
Priority to NL6902027A priority Critical patent/NL6902027A/xx
Priority to DE19702004338 priority patent/DE2004338C3/en
Priority to GB5513/70A priority patent/GB1241525A/en
Priority to FR7004258A priority patent/FR2030382B1/fr
Application filed by US Philips Corp filed Critical US Philips Corp
Priority to US00188614A priority patent/US3816087A/en
Application granted granted Critical
Publication of US3816087A publication Critical patent/US3816087A/en
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    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B23/00Re-forming shaped glass
    • C03B23/20Uniting glass pieces by fusing without substantial reshaping
    • C03B23/207Uniting glass rods, glass tubes, or hollow glassware
    • C03B23/217Uniting glass rods, glass tubes, or hollow glassware for the production of cathode ray tubes or similarly shaped tubes
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J5/00Details relating to vessels or to leading-in conductors common to two or more basic types of discharge tubes or lamps
    • H01J5/20Seals between parts of vessels
    • H01J5/22Vacuum-tight joints between parts of vessel
    • H01J5/24Vacuum-tight joints between parts of vessel between insulating parts of vessel
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J2893/00Discharge tubes and lamps
    • H01J2893/0033Vacuum connection techniques applicable to discharge tubes and lamps
    • H01J2893/0037Solid sealing members other than lamp bases
    • H01J2893/0038Direct connection between two insulating elements, in particular via glass material
    • H01J2893/0039Glass-to-glass connection, e.g. by soldering

Definitions

  • the invention relates to a method of interconnecting glass parts by fusing their edges together, in which the joined, preheated edges are heated and caused to fuse together by the passage of electric current with the aid of current supply points arranged along the outer circumference.
  • British Pat. specification No. 985,422 proposes to surround the gas flame conveying the electric current by flow of nonionized gas, for example, cold air, However, this method is complicated.
  • FIG. 1 is a schematic cross sectional view and H6.
  • 2 is a schematic longitudinal sectional view of an assembly for interconnecting glass parts of the bulb of an electron tube.
  • reference numeral 1 designates the glass cone of an electron tube, to which a flat glass window 2 has to be sealed.
  • the cone 1 is clamped in a holder and the glass plate 2 in a holder 111, which holders can be caused to rotate.
  • a rare gas in this case argon is supplied to the copper tubes 5 by means of the hoses 6 of insulating material, while an alternating voltage is applied to the tubes 5 by means of the conductors 9.
  • the tubes 5 are adjusted previously by means of the clamping connection 8 so that their mouthpieces are at a distance of about 0.5 to 2 cm from the glass edges of the bulb parts 1 and 2 to be sealed.
  • the argon stream is sufficiently conductive in the cold state for conveying the electric current to the pre-heated glass edges.
  • the argon gas is rapidly heated so that an arc 12 is struck as in the case of the current supply via a gas flame in the known methods.
  • the bulb 1 has a wall thickness of 2 mm
  • the window 2 has a thickness of 4 mm.
  • the alternating voltage is initially about 7,000 V.cm with an arc length of about 0.5 cm on either side of the window 2 and after heating of the argon stream and the glass it drops to about 1,500 V. These values correspond approximately with those involved in the use of a gas flame for current supply.
  • the argon stream has in this case a sectional area of 1 mm, whilst about 2 litres of argon are consumed per minute at each supply point.
  • the current strength through the arcsand the glass edges is initially 8 Amp. but it is afterwards raised to about 14 Amp. at which the glass becomes thin liquid.
  • the electric current as well as the supply of argon are interrupted in order to avoid that a cold stream of argon strikes the hot weld, after which the weld is after-heated in a conventional manner by means of the burners 3 and 4 and is subsequently cooled slowly.
  • the holder 11, in which the window plate 2 is held, for example, by subatmospheric pressure, can be moved up and down in a conventional manner so that during the preheating process the glass edges of the parts 1 and 2 can be held at a given distance from each other and heating of the outer and inner sides is more uniform. For sealing the edges together, they are simply brought into contact with each other.
  • the invention is suitable both for sealing together thick glass wall parts, for example, the window and the cone of television display tubes and for interconnecting thin-walled parts, for example, the neck and the cone of such a display tube.
  • the length of the arc and the current strength are, of course, adapted to the thickness of the glass as well as the diameter and the rate of flow of the argon if necessary.
  • argon is found to provide the best results.
  • three or more supply points may be used in a conventional manner, in which case threeor multi-phase alternating current is used. If desired, the glass parts may be sealed together whilst they are standing still with respect to the current supply points,
  • the ignition voltage and the arc voltage may be reduced by producing an auxiliary discharge in the gas supply duct or closely in front of the gas outlet aperture so that the gas stream is pre-ionized.
  • A- method of interconnecting glass parts by sealing their edges to each other comprising the steps of:

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Manufacture Of Electron Tubes, Discharge Lamp Vessels, Lead-In Wires, And The Like (AREA)
  • Re-Forming, After-Treatment, Cutting And Transporting Of Glass Products (AREA)
  • Joining Of Glass To Other Materials (AREA)

Abstract

In sealing glass parts to each other by passing electric current through the preheated glass edges, the electric current is supplied to the glass edges via a stream of rare gas.

Description

United States Patent 1191 Van Duuren et al.
1 111 3,816,087 1 June 11, 1974 METHOD OF INTERCONNECTING GLASS PARTS BY PASSING THROUGH ELECTRIC CURRENT [75] lnventors: Kars Van Duuren; Adrianus Cornelis Johannes Verhoeven, both of Emmasingel, Eindhoven,
Netherlands [73] Assignee: U.S. Philips Corporation, New
York, NY.
[22] Filed: Oct. 12, 1971 [2]] App]. No.: 188,614
Related US. Application Data [63] Continuation of Ser. No. 8,325, Feb. 3, I970,
abandoned.
[30] Foreign Application Priority Data Netherlands 6902027 Feb. 8, 1969 [52] [1.8. CI. 65/40, 65/152, 219/121 P [51] Int. Cl C031) 29/00 [58] Field of Search 65/40, 152; 219/121 P [56] References Cited UNITED STATES PATENTS 12/1942 Guyer 65/40 10/1958 Gage 219/121 P x Primary Examiner-Robert L. Lindsay, Jr. Attorney, Agent, or FirmFrank R. Trifari [57] ABSTRACT In sealing glass parts to each other by passing electric current through the preheated glass edges, the electric current is supplied to the glass edges via a stream of rare gas.
3 Claims, 2 Drawing Figures 1 METHOD OF INTERCONNECTHNG GLASS PARTS BY PASSING THROUGH ELECTRIC C 1:
This application is a continuation of application Ser. No. 8,325, filed Feb. 3, 1970, now abandoned.
The invention relates to a method of interconnecting glass parts by fusing their edges together, in which the joined, preheated edges are heated and caused to fuse together by the passage of electric current with the aid of current supply points arranged along the outer circumference.
It is known, for example, from British Pat. specification No. 885,195 to use the flames of gas burners as current supply points. It has been found, however, that a few disadvantages may be involved. It may occur that the arc is unsteady so that a broader strip of glass is heated than required. Moreover, the arc may stand still for some time at a given point of the glass surface, although the glass surface is moved relatively to the current supply point. This gives rise to local overheating and decomposition of the glass.
In order to avoid these disadvantages British Pat. specification No. 985,422 proposes to surround the gas flame conveying the electric current by flow of nonionized gas, for example, cold air, However, this method is complicated.
It has been found that said disadvantages can be completely obviated by using in accordance with the invention as a current supply point a stream of a rare gas. It is preferred to use argon as a conductive gas for the electric current.
The invention will be described more fully with reference to an embodiment and to the drawing, in which FIG. 1 is a schematic cross sectional view and H6. 2 is a schematic longitudinal sectional view of an assembly for interconnecting glass parts of the bulb of an electron tube.
In the drawing reference numeral 1 designates the glass cone of an electron tube, to which a flat glass window 2 has to be sealed. The cone 1 is clamped in a holder and the glass plate 2 in a holder 111, which holders can be caused to rotate.
After the edges of the bulb parts 1 and 2 to be sealed together have been heated by means of gas burners 3 and tat about 600C, a rare gas, in this case argon is supplied to the copper tubes 5 by means of the hoses 6 of insulating material, while an alternating voltage is applied to the tubes 5 by means of the conductors 9. The tubes 5 are adjusted previously by means of the clamping connection 8 so that their mouthpieces are at a distance of about 0.5 to 2 cm from the glass edges of the bulb parts 1 and 2 to be sealed. The argon stream is sufficiently conductive in the cold state for conveying the electric current to the pre-heated glass edges. By this electric current the argon gas is rapidly heated so that an arc 12 is struck as in the case of the current supply via a gas flame in the known methods. In the embodiment shown, the bulb 1 has a wall thickness of 2 mm, the window 2 has a thickness of 4 mm. The alternating voltage is initially about 7,000 V.cm with an arc length of about 0.5 cm on either side of the window 2 and after heating of the argon stream and the glass it drops to about 1,500 V. These values correspond approximately with those involved in the use of a gas flame for current supply. The argon stream has in this case a sectional area of 1 mm, whilst about 2 litres of argon are consumed per minute at each supply point.
In contrast to the known methods, in which the are passed along a gas flame reciprocates unsteadily, the arc struck via an argon stream is almost completely already and does not tend to stick to given points of the weld so that burned-in dots in the weld are avoided.
The current strength through the arcsand the glass edges is initially 8 Amp. but it is afterwards raised to about 14 Amp. at which the glass becomes thin liquid. After the edges of the bulb parts 1 and 2 have fused together, the electric current as well as the supply of argon are interrupted in order to avoid that a cold stream of argon strikes the hot weld, after which the weld is after-heated in a conventional manner by means of the burners 3 and 4 and is subsequently cooled slowly. The holder 11, in which the window plate 2 is held, for example, by subatmospheric pressure, can be moved up and down in a conventional manner so that during the preheating process the glass edges of the parts 1 and 2 can be held at a given distance from each other and heating of the outer and inner sides is more uniform. For sealing the edges together, they are simply brought into contact with each other.
The invention is suitable both for sealing together thick glass wall parts, for example, the window and the cone of television display tubes and for interconnecting thin-walled parts, for example, the neck and the cone of such a display tube. The length of the arc and the current strength are, of course, adapted to the thickness of the glass as well as the diameter and the rate of flow of the argon if necessary.
Although only argon is mentioned herein, the other rare gases: neon, helium, krypton and xenon may also be employed. However, argon is found to provide the best results.
Instead of using two current supply points three or more supply points may be used in a conventional manner, in which case threeor multi-phase alternating current is used. If desired, the glass parts may be sealed together whilst they are standing still with respect to the current supply points,
The ignition voltage and the arc voltage may be reduced by producing an auxiliary discharge in the gas supply duct or closely in front of the gas outlet aperture so that the gas stream is pre-ionized.
What is claimed is:
1. A- method of interconnecting glass parts by sealing their edges to each other comprising the steps of:
preheating the edges of the glass parts;
bringing the preheated edges in contact with each other;
passing an electric current through at least two streams of ionized rare gas, said streams being arranged circumferential to the edges to be sealed and directed at said edges;
and rotating said edges relative to the streams to uniformly heat said edges by said current to provide an evenly fused glass seal between said edges.
2. A method as claimed in claim 1, wherein said rare gas is argon.
3. A method as claimed in claim 2 wherein the gas stream is pre-ionized by an auxiliary discharge.

Claims (3)

1. A method of interconnecting glass parts by sealing their edges to each other comprising the steps of: preheating the edges of the glass parts; bringing the preheated edges in contact with each other; passing an electric current through at least two streams of ionized rare gas, said streams being arranged circumferential to the edges to be sealed and directed at said edges; and rotating said edges relative to the streams to uniformly heat said edges by said current to provide an evenly fused glass seal between said edges.
2. A method as claimed in claim 1, wherein said rare gas is argon.
3. A method as claimed in claim 2 wherein the gas stream is pre-ionized by an auxiliary discharge.
US00188614A 1969-02-08 1971-10-12 Method of interconnecting glass parts by passing through electric current Expired - Lifetime US3816087A (en)

Priority Applications (5)

Application Number Priority Date Filing Date Title
NL6902027A NL6902027A (en) 1969-02-08 1969-02-08
DE19702004338 DE2004338C3 (en) 1969-02-08 1970-01-30 Method for connecting glass parts by carrying out an electric current
GB5513/70A GB1241525A (en) 1969-02-08 1970-02-05 Methods of sealing glass parts
FR7004258A FR2030382B1 (en) 1969-02-08 1970-02-06
US00188614A US3816087A (en) 1969-02-08 1971-10-12 Method of interconnecting glass parts by passing through electric current

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
NL6902027A NL6902027A (en) 1969-02-08 1969-02-08
US832570A 1970-02-03 1970-02-03
US00188614A US3816087A (en) 1969-02-08 1971-10-12 Method of interconnecting glass parts by passing through electric current

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FR (1) FR2030382B1 (en)
GB (1) GB1241525A (en)
NL (1) NL6902027A (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4118618A (en) * 1976-04-14 1978-10-03 Les Cables De Lyon Device for welding optical fibres end to end
US4691090A (en) * 1980-06-27 1987-09-01 Npk Za Kontrolno Zavarachni Raboti Method and device for plasma cutting of non-metallic materials
US5322542A (en) * 1991-11-22 1994-06-21 Toyo Glass Company Limited Method of and apparatus for chamfering edge of glass vessel
CN110254839A (en) * 2019-06-05 2019-09-20 杭州电子科技大学 A kind of Reagent Tube rotates heat-sealing device and its heat-sealing method automatically

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2306054A (en) * 1938-02-19 1942-12-22 Corning Glass Works Glass heating and working
US2858411A (en) * 1955-10-11 1958-10-28 Union Carbide Corp Arc torch and process

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2306054A (en) * 1938-02-19 1942-12-22 Corning Glass Works Glass heating and working
US2858411A (en) * 1955-10-11 1958-10-28 Union Carbide Corp Arc torch and process

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4118618A (en) * 1976-04-14 1978-10-03 Les Cables De Lyon Device for welding optical fibres end to end
US4691090A (en) * 1980-06-27 1987-09-01 Npk Za Kontrolno Zavarachni Raboti Method and device for plasma cutting of non-metallic materials
US5322542A (en) * 1991-11-22 1994-06-21 Toyo Glass Company Limited Method of and apparatus for chamfering edge of glass vessel
CN110254839A (en) * 2019-06-05 2019-09-20 杭州电子科技大学 A kind of Reagent Tube rotates heat-sealing device and its heat-sealing method automatically
CN110254839B (en) * 2019-06-05 2021-04-20 杭州电子科技大学 Automatic rotating heat sealing device and method for reagent tube

Also Published As

Publication number Publication date
NL6902027A (en) 1970-08-11
FR2030382A1 (en) 1970-11-13
FR2030382B1 (en) 1974-03-15
DE2004338A1 (en) 1970-09-03
DE2004338B2 (en) 1976-04-22
GB1241525A (en) 1971-08-04

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