US3762025A - Method for producing metallic filaments - Google Patents

Method for producing metallic filaments Download PDF

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Publication number
US3762025A
US3762025A US00162989A US3762025DA US3762025A US 3762025 A US3762025 A US 3762025A US 00162989 A US00162989 A US 00162989A US 3762025D A US3762025D A US 3762025DA US 3762025 A US3762025 A US 3762025A
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metal
section
cross
filaments
tube
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Expired - Lifetime
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US00162989A
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A Gottlieb
G Majesko
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Carpenter Technology Corp
Wilbur B Driver Co
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Wilbur B Driver Co
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Assigned to CARPENTER TECHNOLOGY CORPORATION reassignment CARPENTER TECHNOLOGY CORPORATION ASSIGNMENT OF ASSIGNORS INTEREST. Assignors: AMAX INC., A CORP OF NEW YORK
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B1/00Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations
    • B21B1/16Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations for rolling wire rods, bars, merchant bars, rounds wire or material of like small cross-section
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21CMANUFACTURE OF METAL SHEETS, WIRE, RODS, TUBES OR PROFILES, OTHERWISE THAN BY ROLLING; AUXILIARY OPERATIONS USED IN CONNECTION WITH METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL
    • B21C37/00Manufacture of metal sheets, bars, wire, tubes or like semi-manufactured products, not otherwise provided for; Manufacture of tubes of special shape
    • B21C37/04Manufacture of metal sheets, bars, wire, tubes or like semi-manufactured products, not otherwise provided for; Manufacture of tubes of special shape of bars or wire
    • B21C37/047Manufacture of metal sheets, bars, wire, tubes or like semi-manufactured products, not otherwise provided for; Manufacture of tubes of special shape of bars or wire of fine wires
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S29/00Metal working
    • Y10S29/032Rolling with other step
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T29/00Metal working
    • Y10T29/49Method of mechanical manufacture
    • Y10T29/49002Electrical device making
    • Y10T29/49014Superconductor
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T29/00Metal working
    • Y10T29/49Method of mechanical manufacture
    • Y10T29/49801Shaping fiber or fibered material
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T29/00Metal working
    • Y10T29/49Method of mechanical manufacture
    • Y10T29/4981Utilizing transitory attached element or associated separate material

Abstract

A process for producing long continuous lengths of metallic filaments is disclosed which process comprises securing four flat plates of a first metal to each of the elongated sides of a billet of a second metal and having a cross section in shape of a rectangle, by edge welding each of the plates. The resulting assembly is essentially void free. The rectangular cross section of the billet is reduced while being elongated by hot rolling. The resulting elongated rectangular structure, having a core of the second metal and a cladding of the first metal over the elongated sides, is divided into a plurality of elements of the same lengths. The elements are inserted into a hollow metal tube open at both ends having a rectangular cross section in a manner to essentially eliminate the voids and with their longitudinal axes and the longitudinal axis of the tube essentially parallel. Ends of the tube are sealed and the sealed unit is reduced in cross section and elongated by hot rolling. The other materials are removed from the resulting filaments of the first metal yielding materials suitable for weaving into metal cloth.

Description

[ 1 Oct. 2, 1973 METHOD FOR PRODUCING METALLIC FILAMENTS [75] Inventors: Arnold J. Gottlieb, Colonia; George A. Majesko, Glen Ridge, both of NJ.
[73] Assignee: Wilbur B. Driver Company, Newark,
[22] Filed: July 15, 1971 [21] Appl. No.: 162,989
Related US. Application Data [63] Continuation-impart of Ser. No. 820,556, April 30,
1969, abandoned.
2,077,682 4/1937 Everett 29/423 UX 2,711,966 6/1955 Watson et al. 29/470.9 UX 3,277,564 10/1966 Webber et al. 29/419 3,394,2l3 7/1968 Roberts et al. 29/419 X FOREIGN PATENTS OR APPLICATIONS 631,584 11/1949 Great Britain 29/l87.5
Primary Examiner-Charles W. Lanham Assistant Examiner-D. C. Reiley, lll Attorney-Norman J. OMalley et al.
[57] ABSTRACT A process for producing long continuous lengths of metallic filaments is disclosed which process comprises securing four flat plates of a first metal to each of the elongated sides of a billet of a second metal and having a cross section in shape of a rectangle, by edge welding each of the plates. The resulting assembly is essentially void free. The rectangular cross section of the billet is reduced while being elongated by hot rolling. The resulting elongated rectangular structure, having a core of the second metal and a cladding of the first metal over the elongated sides, is divided into a plurality of elements of the same lengths. The elements are inserted into a hollow metal tube open at both ends having a rectangular cross section in a manner to essentially eliminate the voids and with their longitudinal axes and the longitudinal axis of the tube essentially parallel. Ends of the tube are sealed and the sealed unit is reduced in cross section and elongated by hot rolling. The other materials are removed from the resulting filaments of the first metal yielding materials suitable for weaving into metal cloth.
3 Claims, 6 Drawing Figures 51 [3000 [J @1300 [3 DQEJ C] [HOOD p OBOE] Pmmmnmms 3,762,025
BOUQUET;
B00005? DDCIDEJC] I LDUUDUD:
INVENTORS. ARNOLD J. GOTTLIEB & GEORGE A. MAJESKO M cow ATTORNEY METHOD FOR PRODUCING METALLIC FILAMENTS CROSS REFERENCE TO RELATED APPLICATION This application is a continuation-in-part of Ser. No. 820,556, filed Apr. 30, 1969, now abandoned and assigned to the assignee of the present invention.
BACKGROUND OF THE INVENTION This invention relates to a multi-step process for producing metal filaments. More particularly it relates to a process utilizing hot rolling, in both steps.
Several processes are known for the production of metal fibers or filaments. For example, in US. Pat. No. 3,277,564 a process is disclosed wherein filaments are formed by forming a bundle of wires inside a sheath of a dissimilar metal, then drawing the bundle through a series of successive dies. Since round cross sectional shapes of the sheath are required in order to draw the bundle, any bundle has a relatively large portion thereof as voids. To obtain a reduction in the wire size, the total reduction in the cross-section of the bundle is relatively high.
U.S. Pat. No. 3,394,213 also discloses a process by which metal filaments are formed by construction of bundled wires or tubular elements by forming the bundled wires or elements into a billet and subjecting the billet successively to a hot forming constriction and subsequently drawing constriction. When the voids between the wires are not filled with a suitable particulate powder the billet is first compacted by axial shortening the billet, thus radially compacting the billet to reduce voids. Thereafter the billet is subject to hot extrusion.
It can be seen that the prior art methods each start with initial materials having a relatively large percentage of voids. Although the difficulties with voids are recognized, the solutions thereto either involve filling the voids with a filler material which inherently lowers the efiiciency of the process or compacting the initial billet which is an additional step and adds an inherent inefficiency.
Additionally, when core materials of a first metal having a circular cross-sectional area are sheathed with a second metal and are placed in contact with each other to form a billet inside a casing, the mutual contact of the sheathed material is along a line. When the billet is subjected to compaction or constriction pressures, there is a tendency for the sheath and the casing to flow into any voids thus reducing its thickness nonuniformly and can lead to sheath rupture. If the sheath thickness is insufficient to fill the voids the cores come into contact with each other and can weld to each other. These problems are intensified with hot rolling thus hot rolling is not practical if there is substantial voids in the billets.
It is believed, therefore, that a process using void free rectangular cross section metal fibers via hot rolling without compaction or use of filler materials is an advancement in the art.
SUMMARY OF THE INVENTION In our invention, the peripheral side surfaces of an elongated billet of uniform rectangular cross section of a second metal, for example, a billet, are each clad with a flat plate of a first metal. These plates are edge welded together to the member whereby an essentially void free assembly is formed.
The assembly is then hot rolled whereby it is reduced in cross section and is correspondingly elongated. The elongated member which has a rectangular cross section is cut into a plurality of like elements of the same length. Each element has a core of the second metal clad with the first metal.
A hollow tube of rectangular cross section with opposite open ends is formed of a metallic component which is dissimilar to the second metal and which can, but need not, be dissimilar to the first metal. This tube is filled with a plurality of said elements which have their longitudinal axes parallel with each other and with the longitudinal axis of the tube whereby the elements form an essentially void free bundle. The tube is then sealed and hot rolled. The individual elements are reduced in cross section and are elongated to form filaments of very small cross section imbedded in a metallic matrix.
Thereafter, the composite (which if necessary can be further reduced by cold drawing and annealing) can be immersed in acid media which will not attack the second metal but which will etch away all material other than the first metal, leaving only the filaments. These filaments form metallic yarn which can be used in weaving or the like.
Alternatively, the composite need not be etched but can be used without further processing as a fiber reinforced structure.
BRIEF DESCRIPTION OF THE DRAWINGS FIG. 1 illustrates the initial step in cladding the first component;
FIG. 2 is an end view of the billet showing location of longitudinal welds;
FIG. 3 is a perspective view of the billet showing location of the end welds;
FIG. 4 shows in cross section the shape of the clad billet after hot rolling;
FIG. 5 is a cross sectional view of the geometry employed in further step of our process; and
FIG. 6 illustrates the member obtained after still a further step in our process.
DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS For a better understanding of the present invention, together with other and further objects, advantages, and capabilities thereof, reference is made to the following disclosure and appended claims in connection with the above-described drawings.
Referring now to FIGS. l7, there is shown a first component 10 of 304 stainless steel with a cross section in the form of a square two and one half inches on a side. Flat steel side plates 12 are secured to the flat, cleaned and ground sides of the billet 13 by longitudinal comer welds l4 and end welds 16.
The steel plate covered billet was then processed in the following manner. It was first hot rolled at a temperature of 2,000 F through a succession of diamond and oval passes to reduce the cross section of the plate covered billet, for example, to a square 0.25 inch on a side as shown at 20.
A succession of segments of like length were cut from the above. After descaling, these lengths were then packed in a hollow steel tube 24 of 3 X 3 inch cross section having a one-fourth inch thick wall. The void space is essentially eliminated when segments of square cross section are used.
This tube was then sealed and again hot rolled as before whereby the individual cores of element 20 form elongated filaments 26 of small cross section, imbedded in a metallic matrix 28. Illustratively, the composite can have a diameter of 0.25 inch at this stage.
Thereafter the composite was cold drawn and annealed to reduce the diameter of the individual filaments to a desired value as for example 0.0005 inch. The drawn composite can then be treated as for example by dipping into a dilute nitric acid bath until the steel is etched away leaving only the fine filaments of stainless steel which can be used in weaving, knitting or the like.
Alternatively, this last step can be omitted whereby the composite can be used in applications where reinforced structures are of interest.
The portions of our process relating to the steps associated with FIGS. 4-7 can be repeated as often as necessary to increase the number of filaments.
We have found that by using rectangular shaped materials throughout, the difficulties of the prior art are avoided.
As previously mentioned the prior art methods each start with initial materials having a relatively large percentage of voids. Although the difi'lculties with voids are recognized, the solutions thereto either involve filling the voids with a filler material which inherently lowers the efficiency of the process or compacting the initial billet which is an additional step and adds an inherent inefficiency.
Additionally, when core materials of a first metal having a circular cross-sectional area are sheathed with a second metal and are placed in contact with each other to form a billet inside a casing, the mutual contact of the sheathed material is along a line. When the billet is subjected to compaction or constriction pressures, there is a tendency for the sheath and the casing to flow into any voids thus reducing its thickness nonuniformly and can lead to sheath rupture. If the sheath thickness is insufficient to fill the voids, the core members come into contact with each other and can weld to each other. These problems are intensified with hot rolling, thus hot rolling is not practical if there is substantial voids in the billets.
By using the special geometric shapes as defined herein the foregoing problems are overcome. For example, excessive spreading during hot rolling is eliminated, the sheathing is uniform, no voids are present, therefore, no sheath rupture or core welding occurs and hot rolling is used throughout to produce the fibers.
While we have described our invention with particular reference to the drawings, our protection is to be limited only by the terms of the claims which follow.
What is claimed is:
l. A method for producing long continuous lengths of metallic filaments comprising the steps of:
securing four flat plates of a first metal to each of the elongated flat outer sides of a billet of a second metal and having a cross section in the shape of a rectangle by edge welding, the resulting assembly being essentially free of voids;
reducing said assembly in cross section while elongating same by hot rolling to an elongated structure having a rectangular cross section;
dividing said elongated structure into a plurality of elements of the same length each having a longitudinal axis;
inserting said elements into a hollow tube open at both ends and having a cross section in rectangular shape in a manner to essentially eliminate the voids and having the longitudinal axes of the element mutually parallel and parallel with the longitudinal axis of said tube, said tube being composed of a metallic component which is dissimilar to the second metal and can, but need not be dissimilar to the first metal;
sealing said element carrying tube at both ends; and
reducing said sealed tube in cross section while elongating same by hot rolling whereby filaments of small cross section composed of said second metal are imbedded in a metallic matrix.
2. A method as set forth in claim 1 further including the additional step of removing said matrix from said filaments whereby the filaments are exposed.
3. A method as set forth in claim 1 wherein said rectangle is a square.

Claims (3)

1. A method for producing long continuous lengths of metallic filaments comprising the steps of: securing four flat plates of a first metal to each of the elongated flat outer sides of a billet of a second metal and having a cross section in the shape of a rectangle by edge welding, the resulting assembly being essentially free of voids; reducing said assembly in cross section while elongating same by hot rolling to an elongated structure having a rectangular cross section; dividing said elongated structure into a plurality of elements of the same length each having a longitudinal axis; inserting said elements into a hollow tube open at both ends and having a cross section in rectangular shape in a manner to essentially eliminate the voids and having the longitudinal axes of the element mutually parallel and parallel with the longitudinal axis of said tube, said tube being composed of a metallic component which is Dissimilar to the second metal and can, but need not be dissimilar to the first metal; sealing said element carrying tube at both ends; and reducing said sealed tube in cross section while elongating same by hot rolling whereby filaments of small cross section composed of said second metal are imbedded in a metallic matrix.
2. A method as set forth in claim 1 further including the additional step of removing said matrix from said filaments whereby the filaments are exposed.
3. A method as set forth in claim 1 wherein said rectangle is a square.
US00162989A 1971-07-15 1971-07-15 Method for producing metallic filaments Expired - Lifetime US3762025A (en)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3844021A (en) * 1972-07-17 1974-10-29 Nippon Seisen Co Ltd Method of simultaneously drawing a plurality of wires and apparatus therefor
US3882587A (en) * 1972-12-06 1975-05-13 Rau Fa G Method of producing a fibre-reinforced material
US4333216A (en) * 1981-03-23 1982-06-08 United Technologies Corporation Method for manufacturing a sandwich panel structure
US6112395A (en) * 1997-11-12 2000-09-05 Usf Filtration And Separations Group, Inc. Process of making fine and ultra fine metallic fibers
WO2012143668A1 (en) * 2011-04-18 2012-10-26 Cladinox International Limited Methods for the production of clad steel products
US9005767B2 (en) 2009-10-22 2015-04-14 Cladinox International Limited Corrosion resistant metal products

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2050298A (en) * 1934-04-25 1936-08-11 Thos Firth & John Brown Ltd Metal reducing method
US2077682A (en) * 1935-05-17 1937-04-20 Thos Firth & John Brown Ltd Drawing process
GB631584A (en) * 1947-12-31 1949-11-04 Colvilles Ltd Improvements relating to the manufacture of composite metal billets and of lined tubes therefrom
US2711966A (en) * 1949-12-01 1955-06-28 Lukens Steel Co Parting composition
US3277564A (en) * 1965-06-14 1966-10-11 Roehr Prod Co Inc Method of simultaneously forming a plurality of filaments
US3394213A (en) * 1964-03-02 1968-07-23 Roehr Prod Co Inc Method of forming filaments

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2050298A (en) * 1934-04-25 1936-08-11 Thos Firth & John Brown Ltd Metal reducing method
US2077682A (en) * 1935-05-17 1937-04-20 Thos Firth & John Brown Ltd Drawing process
GB631584A (en) * 1947-12-31 1949-11-04 Colvilles Ltd Improvements relating to the manufacture of composite metal billets and of lined tubes therefrom
US2711966A (en) * 1949-12-01 1955-06-28 Lukens Steel Co Parting composition
US3394213A (en) * 1964-03-02 1968-07-23 Roehr Prod Co Inc Method of forming filaments
US3277564A (en) * 1965-06-14 1966-10-11 Roehr Prod Co Inc Method of simultaneously forming a plurality of filaments

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3844021A (en) * 1972-07-17 1974-10-29 Nippon Seisen Co Ltd Method of simultaneously drawing a plurality of wires and apparatus therefor
US3882587A (en) * 1972-12-06 1975-05-13 Rau Fa G Method of producing a fibre-reinforced material
US4333216A (en) * 1981-03-23 1982-06-08 United Technologies Corporation Method for manufacturing a sandwich panel structure
US6112395A (en) * 1997-11-12 2000-09-05 Usf Filtration And Separations Group, Inc. Process of making fine and ultra fine metallic fibers
US6497029B1 (en) 1997-11-12 2002-12-24 Pall Filtration And Separations Group Inc. Process for making fine and ultra fine metallic fibers
US9005767B2 (en) 2009-10-22 2015-04-14 Cladinox International Limited Corrosion resistant metal products
WO2012143668A1 (en) * 2011-04-18 2012-10-26 Cladinox International Limited Methods for the production of clad steel products
CN103476519A (en) * 2011-04-18 2013-12-25 克拉迪劳斯国际有限公司 Methods for the production of clad steel products
US9346093B2 (en) 2011-04-18 2016-05-24 Cladinox International Limited Methods for the production of clad steel products

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Free format text: ASSIGNMENT OF ASSIGNORS INTEREST.;ASSIGNOR:AMAX INC., A CORP OF NEW YORK;REEL/FRAME:004284/0609

Effective date: 19840427