US3581512A - Liquid helium refrigeration apparatus and method - Google Patents

Liquid helium refrigeration apparatus and method Download PDF

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Publication number
US3581512A
US3581512A US829332A US3581512DA US3581512A US 3581512 A US3581512 A US 3581512A US 829332 A US829332 A US 829332A US 3581512D A US3581512D A US 3581512DA US 3581512 A US3581512 A US 3581512A
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United States
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mixture
liquid
superfluid
chamber
supply duct
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US829332A
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Frans Adrianus Staas
Adrianus Petrus Severijns
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US Philips Corp
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US Philips Corp
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    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25B—REFRIGERATION MACHINES, PLANTS OR SYSTEMS; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS
    • F25B9/00—Compression machines, plants or systems, in which the refrigerant is air or other gas of low boiling point
    • F25B9/12—Compression machines, plants or systems, in which the refrigerant is air or other gas of low boiling point using 3He-4He dilution

Definitions

  • the superfluid He is passed through asuperleak and combined with said mixture to dilute same in a mixing chamber, thus producing cold to cool an object disposable in the chamber.
  • An exhaust duct from the mixing chamber is proportioned so that the medium discharged therethrough exceeds its critical speed and thus flows turbulently.
  • the invention relates to a device for transporting thermal energy from a lower to a higher temperature level, which two temperature levels lie below the temperature of the A-point of He.
  • a known device of the type to which the present invention relates is described in Cryogenics, Apr. 1966, pp. 80- 88. This device is filled with a He-He-mixture and com prises a mixing chamber which is at a very low temperature, for example, 0. 1 K.
  • a communication duct which communicates, through a communication duct, with an evaporation reservoir which has a temperature of, for example, 0.8 K.
  • the vapor space of said reservoir communicates, through one or more counter-flow heat-exchangers, with the suction side of a diffusion pump operating at room temperature which sucks away vapor.
  • said vapor will mainly consist of He.
  • the vapor is then supplied, through the heat exchangers in which it cools in counter current with the vapor flowing towards the pump and one or more coolers in which it is further cooled to below its condensation temperature, to a further heat exchanger which is in thermal contact with the communication duct and the ex haust side of which communicates with the mixing chamber.
  • a substantially stationary quantity of He will be situated in the mixing chamber and in the communication duct, which quantity, de pendent upon the temperature, consists partly of superfluid and partly of normal He.
  • a phase separation takes place below 0.8 K, namely to a 3 He rich phase which behaves like a liquid and a phase which is poor in He which behaves like a gas.
  • This phase separation manifests itself in the mixing chamber.
  • evaporation takes place as it were and the transition heat required for this purpose (heat of evaporation provides a cooling effect.
  • the He will then expand in the quantity of superfluid He present in the communication duct during which a much larger quantity of cold is produced which, however, is substantially entirely required for cooling the He-stream towards the mixing chamber.
  • a drawback of this known device is that the He vapor from the evaporation reservoir is heated to room temperature and is then cooled again to the temperature of liquid helium. Of course, this is associated with losses, while the device struc turally is very complicated.
  • a further important drawback is that the diffusion pump operates at room temperature so that at the very low pressure prevailing of, for example, lO mm. Hg, only small quantities can be circulated so that the cold production will also be only small.
  • a superleak is to be understood to mean in the present ap' plication a mass of a material having the property that normal He cannot pass said mass and superfluid He can pass said mass without turbulence occurring during the flowing.
  • the rest of the circulation duct is constructed so that the medium therein exceeds its critical speed and turbulence oc curs.
  • a driving force is exerted on the helium in the circulation duct by means of the pump, which force upon starting while the temperature is still the same everywhere, results in a pressure difference across the part of the circulation duct in which no superleak is situated. No pressure difference will occur across the superleak as long as the temperature is the same on both sides.
  • Due to the pressure difference across the other part of the circulation duct the helium, both superfluid and normal helium, will start flowing therein. This means that with the normal helium, thermal energy will be conducted namely from one side of the superleak to the pump and the cooler present there.
  • the device according to the invention is characterized in that the device comprises a liquid pump the exhaust of which communicates, through one or more coolers, both with a first and a second supply duct.
  • the first supply duct communicates on its other side with the upper side of a mixing chamber, and the second supply duet comprises a superleak and empties on its other side in the lower part of the mixing chamber.
  • An exhaust duct communicates with the mixing chamber and is in heat-exchanging contact with the first supply duct and communicates on its other side with the suction side of the liquid pump.
  • the mixing chamber, the first and the second supply duct and the exhaust duct are insulated thermally; and the device is filled during operation with a mixture of He and He, a temperature prevailing during operation in the said cooler(s) which lies below the )t-point of the He He mixture on the entrance side of the first and second supply duct, so that inmixing of He and He occurs there,
  • the concentration of He in the first supply duct is higher than in the exhaust duct and the pump, the dimensions of the exhaust duct being so that the medium therein exceeds its critical speed and turbulence occurs.
  • the medium remains constantly in the liquid phase, so that no losses will occur due to heating to room temperature and subsequent cooling to the temperature of liquid helium as is the case in the known device. Furthermore, liquid is circulated by pumping in the device according to the invention, so that a large quantity can easily be transported.
  • unmixing of He and He is obtained by conveying the mixture compressed by the pump to a cooled place where the exhaust duct of the pump communicates with the first supply duct and the second supply duct in which the superleak is situated.
  • the cooled place is kept at a temperature which lies below the A-point of the mixture at that location.
  • the superfluid He can pass the superleak substantially unhindered, while the superleak has a great resistance to flow for He. As a result of this the He will flow to the first supply duct.
  • This first supply duct has a great impedance for the superfluid.
  • the thermal energy released upon unmixing is given off to the cooler.
  • the He in the first supply duct is further cooled by heat-exchange with medium in the exhaust duct.
  • the He is then added to the He, a large quantity of cold being produced at a very low temperature.
  • This cold may be used for cooling some object or others, thus termal energy being supplied to the medium.
  • the transfer of said thermal energy occurs by means of the "He flowing to the exhaust duct and normal He.
  • the He concentration in the exhaust duct will be lower than in the first supply duct. This is possible since the exhaust duct is proportioned so that turbulence occurs therein in the superfluid which gives rise to a pressure difference across the exhaust duct. As a result of this both He and normal He and super fluid He will flow through the exhaust duct. In this manner a device is obtained which structurally in simple and in which a large quantity of cold can be produced at a very low temperature with a comparatively good efficiency.
  • the liquid pump is a centrifugal pump.
  • the first and the second supply duct, the mixing chamber and the exhaust duct are arranged in a vacuum-insulated space, and the assembly is immersed in a reservoir containing liquid helium at a temperature which is lower than that of the )t-point ofHe.
  • a further device for transporting thermal energy from a lower to a higher temperature level is present, which two levels also lie below the temperature of the A-point of He, the coldest part of which device is in heat exchanging relationship with the first supply duct.
  • the medium in the first supply duct is cooled so that a lower tem perature can be reached in the mixing chamber.
  • FIGS. l and 2 are elevation views partially in cross section of two embodiments of the invention.
  • reference numeral 1 in FIG. 1 denotes a mixing chamber.
  • a first supply duct 2 and a second supply duct 3 comprising a superleak 4 communicate with the mixing chamber 1; whereas the first supply duct opens into the upper part of the mixing chamber, the second supply duct opens into the lower part of the mixing chamber.
  • an exhaust duct 5 communicates with the lower part of the mixing chamber.
  • the first supply duct 2 and the exhaust duct 5 are in heat exchanging contact with each other by means of heat exchangers 7, 8 and 9 (of course the number of said heat exchangers may be increased or decreased, as is desired).
  • Each of these heat exchangers is constituted by a housing of a material which readily conducts heat, for example, copper, while said housing comprises two separate chambers 11 and 12, filled with balls of sintered copper which chambers form a part of the first supply duct 2 and the exhaust duct 5, respectively.
  • the mixing chamber 1, the first supply duct 2, and the exhaust duct 5, in which the heat exchangers 7, 8 and 9 are provided and the part of the second supply duct 3, in which the superleak 4 is situated are incorporated in a vacuum-insulated chamber 14.
  • the chamber 14 is surrounded by a bath 15 of liquid helium at a temperature of, for example, l.3 K.
  • the exhaust duct 5 On its side remote from the mixing chamber the exhaust duct 5 communicates with a liquid pump 16.
  • the exhaust duct 17 of said liquid pump 16 communicates through a cooler 18 with both the first supply duct 2 and the second supply duct 3.
  • a duct 20 With the suction side of the liquid pump 16 a duct 20 also communicates through which the mixture of He and He can be supplied.
  • the operation of this device is as follows: A mixture of He and He under pressure is supplied to the exhaust 17 by pump 16. Since the exhaust 17 is in heat exchanging relationship with the helium bath 15, the mixture will have a temperature of approximately l.3 K. Since the superleak 4 has a great resistance to the He, only superfluid He will flow through it.
  • the supply duct 2 is constructed so that it has a great resistance to the superfluid as compared with the superleak. So mainly He will flow through the duct 2, with only a few percent of He. In this manner, unmixing of the He and the He is obtained prior to the entrance in the supply ducts 2 and 3. Thermal energy is liberated which is conducted away to the liquid helium bath 15.
  • a temperature difierence will adjust, namely so that the temperature in the mixing chamber is lower than 1.3" K. and may be, for example, 0.6 K.
  • the He which flows through the supply duct 2 to the mixing chamber, is cooled in the heat exchangers 9, 8 and 7.
  • the He is again mixed with the He in the mixing chamber 1.
  • a quantity of cold is produced (transition heat plus expansion of He in He). This cold may be used effectively for cooling an object.
  • the thermal energy supplied is then transported, through the medium flowing through the exhaust duct 5 to the suction side of the pump, to a higher temperature level (l.3 K.) Cooling is obtained on the one hand by the transition from the He rich phase to the He poor phase and expansion of He in He, and on the other hand in that turbulence occurs in the exhaust duct in the superfluid, which results in a pressure difference across said duct and consequently normal He and He flow through the exhaust duct in addition to the superfluid, so that a heat current is obtained from the mixing chamber to the helium bath.
  • the "He may expand slightly further in the exhaust duct, in which cold is produced which can be used effectively for cooling the He in the supply duct 2.
  • FIG. 2 shows a device for transporting thermal energy between two temperature levels lying below the A-point of helium.
  • This device in part the same device as shown in FIG. 1.
  • the components of said device are denoted by the same reference numerals as in FIG. 1.
  • the device furthermore comprises a second cooling device which also supplies cold at a temperature which lies below the lt-point of helium.
  • This cooling device comprises a first superleak 25 which at its one side is in open communication with the liquid He bath l5 and at its other end communicates with a space 26 in the heat exchanger 9.
  • the space 26 communicates, through a duct 27 and a cooler 28, with a second superleak 29.
  • the superleak 29 is bounded at its upper side by a space 30 which comprises a heating device 31.
  • the space 30 furthermore communicates with the He bath through a duct 32.
  • This device is entirely incorporated in the vacuum space 14.
  • the operation is as follows: By supplying current to the heating device 31, a higher temperature will prevail in the space 30 than in the cooler 28. As a result of this, a fountain pump effect occurs across the superleak 29 and superfluid helium will flow through the superleak 29 to the space 30, and then through the duct 32 to the helium bath. As a result of this a lower pressure will prevail in the cooler 28, so that the medium will flow from the space 26 through the duct 27 to the cooler 28.
  • the duct 27 is proportioned so that the medium therein exceeds its critical speed and turbulence occurs. This means that both superfluid and normal helium, flows through the duct 27.
  • a device for transporting thermal energy from a lower temperature level to a higher temperature level, which two temperature levels lie below the temperature of the lt-point of He wherein the device comprises a liquid pump, at least one cooler receiving liquid from the pump, a first supply duct communicating between the cooler and a mixing chamber, and a second supply duct comprising a superleak and, communicating between said cooler and emptying on its other side in the mixing chamber, an exhaust duct communicating between the mixing chamber and the suction side of the liquid pump, the mixing chamber, the first and the second supply duct and the exhaust duct being thermally insulated, and the device when being filled during operation with a mixture of He and He, having a temperature prevailing during operation in the said cooler which lies below the )t-point of the He-He mixture on the entrance side of the first and the second supply duct, so
  • the concentration of He in the first supply duct being higher than in the exhaust duct and the pump.
  • the dimensions of the exhaust duct being such that the medium therein exceeds its critical speed and turbulence occurs.
  • liquid pump is a centrifugal pump.
  • a device further comprising a reservoir containing liquid helium at a temperature which is lower than that of the )t-point of He the mixing chamber, the first and second supply duct and the exhaust duct being arranged in a vacuum-insulated space which is immersed in said reservoir.
  • a device further comprising an additional device for transporting thermal energy from a lower to a higher temperature level, which two levels also lie below the temperature of the )t-point of He, and the coldest part of which device is in heat exchanging relationship with the first supply duct.
  • Apparatus operating with a supply mixture of liquid heli urn for producing cold or cool an object comprising:
  • a. pump means for applying a pressure to flow the supply mixture of liquid helium
  • cooler means for cooling the flowing helium to a temperature below its A-point, with a resulting mixture of superfluid He, normal He, and liquid He components
  • a mixing chamber in which an object to be cooled is disposable, and into which flows said mixture of liquid He and liquid He from the supply duct which mixture is diluted in the chamber by superfluid He which flows into the chamber from the superleak, with a production of cold resulting in the chamber for cooling the object therein, and
  • exhaust duct means for discharge of the diluted fluid mixture from the mixing chamber.
  • Apparatus according to claim 5 further comprising a chamber containing a cooling bath of liquid He maintained below the A-point thereof 8.
  • Apparatus according to claim 5 further comprising a vacuum-insulated housing containing said mixing chamber, the superleak, the supply duct and exhaust duct.
  • Apparatus according to claim 5 wherein the fluid in the supply duct is a mixture of liquid He and He at a temperature below the A-point of said He-He mixture.
  • Apparatus according to claim 8 further comprising a reservoir for containing liquid He at a temperature below the A-point thereof in said vacuuminsulated housing immersed in the liquid He of said reservoir.
  • a method for cooling an object comprising the steps:
  • a method according to claim 11 wherein flowing said liquid helium He and He comprises pumping same with a pumsp means.
  • flowing the diluted mixture of liquid helium out of the mixing chamber comprises flowing same turbulently.
  • a method according to claim 11 further comprising insulating from heat transfer by using a vacuum chamber, said steps of (i) separating and flowing the superfluid He through a superleak, (ii) flowing the remaining mixture through a supply duct, (iii) mixing said flows from the superleak and the supply duct, and (iv) discharging the mixed helium from the mixing chamber.
  • a method according to claim 11 further comprising maintaining a quantity of liquid He about said vacuum chamber at below the )t-point temperature thereof.

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  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Thermal Sciences (AREA)
  • General Engineering & Computer Science (AREA)
US829332A 1968-06-05 1969-06-02 Liquid helium refrigeration apparatus and method Expired - Lifetime US3581512A (en)

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NL6807902A NL6807902A (es) 1968-06-05 1968-06-05

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US (1) US3581512A (es)
AT (1) AT289730B (es)
BE (1) BE734083A (es)
CH (1) CH508847A (es)
DE (1) DE1924786A1 (es)
DK (1) DK130490B (es)
FR (1) FR2010177B1 (es)
GB (1) GB1270675A (es)
NL (1) NL6807902A (es)
SE (1) SE354347B (es)

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3678704A (en) * 1969-10-16 1972-07-25 Philips Corp Device for transporting thermal energy at temperatures lying below the {80 -temperature of helium
US3835662A (en) * 1972-03-18 1974-09-17 Philips Corp Device for transporting heat from a lower to a higher temperature level
US3896630A (en) * 1972-03-17 1975-07-29 Philips Corp Method for starting a {hu 3{b He-{hu 4{b He dilution refrigerator
US3922881A (en) * 1973-11-13 1975-12-02 Philips Corp Helium 3-helium 4 dilution refrigerator
US3992893A (en) * 1974-02-22 1976-11-23 Commissariat A L'energie Atomique Method for the production of superfluid helium under pressure at very low temperature and an apparatus for carrying out said method
US4134037A (en) * 1976-10-28 1979-01-09 Alsthom-Atlantique Current lead-in device for superconducting rotary electrical machines
US4297856A (en) * 1979-03-14 1981-11-03 U.S. Philips Corporation 3 He-4 He Dilution refrigerator
EP0089391A1 (en) * 1982-03-23 1983-09-28 International Business Machines Corporation Method and dilution refrigerator for cooling at temperatures below 1K
US4485640A (en) * 1982-04-01 1984-12-04 Commissariat A L'energie Atomique Device for automatically regulating the superfluid helium level in a tank
US4991401A (en) * 1988-02-02 1991-02-12 Centre National D'etudes Spatiales Process and apparatus for obtaining very low temperatures
CN112325498A (zh) * 2020-11-06 2021-02-05 格物致寒(苏州)科学仪器有限公司 一种稀释制冷系统及方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3195322A (en) * 1961-09-22 1965-07-20 Atomic Energy Authority Uk Refrigerator employing helium
US3376712A (en) * 1966-03-16 1968-04-09 Atomic Energy Authority Uk Refrigerators operating at very low temperatures
US3472038A (en) * 1967-04-22 1969-10-14 Philips Corp Apparatus and method for transferring heat from a lower temperature level to a higher temperature level

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3195322A (en) * 1961-09-22 1965-07-20 Atomic Energy Authority Uk Refrigerator employing helium
US3376712A (en) * 1966-03-16 1968-04-09 Atomic Energy Authority Uk Refrigerators operating at very low temperatures
US3472038A (en) * 1967-04-22 1969-10-14 Philips Corp Apparatus and method for transferring heat from a lower temperature level to a higher temperature level

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3678704A (en) * 1969-10-16 1972-07-25 Philips Corp Device for transporting thermal energy at temperatures lying below the {80 -temperature of helium
US3896630A (en) * 1972-03-17 1975-07-29 Philips Corp Method for starting a {hu 3{b He-{hu 4{b He dilution refrigerator
US3835662A (en) * 1972-03-18 1974-09-17 Philips Corp Device for transporting heat from a lower to a higher temperature level
US3922881A (en) * 1973-11-13 1975-12-02 Philips Corp Helium 3-helium 4 dilution refrigerator
US3992893A (en) * 1974-02-22 1976-11-23 Commissariat A L'energie Atomique Method for the production of superfluid helium under pressure at very low temperature and an apparatus for carrying out said method
US4134037A (en) * 1976-10-28 1979-01-09 Alsthom-Atlantique Current lead-in device for superconducting rotary electrical machines
US4297856A (en) * 1979-03-14 1981-11-03 U.S. Philips Corporation 3 He-4 He Dilution refrigerator
EP0089391A1 (en) * 1982-03-23 1983-09-28 International Business Machines Corporation Method and dilution refrigerator for cooling at temperatures below 1K
US4485640A (en) * 1982-04-01 1984-12-04 Commissariat A L'energie Atomique Device for automatically regulating the superfluid helium level in a tank
US4991401A (en) * 1988-02-02 1991-02-12 Centre National D'etudes Spatiales Process and apparatus for obtaining very low temperatures
CN112325498A (zh) * 2020-11-06 2021-02-05 格物致寒(苏州)科学仪器有限公司 一种稀释制冷系统及方法

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AT289730B (de) 1971-05-10
NL6807902A (es) 1969-12-09
FR2010177A1 (es) 1970-02-13
CH508847A (de) 1971-06-15
GB1270675A (en) 1972-04-12
DE1924786A1 (de) 1970-01-08
FR2010177B1 (es) 1973-05-25
BE734083A (es) 1969-12-04
DK130490C (es) 1975-07-21
SE354347B (es) 1973-03-05
DK130490B (da) 1975-02-24

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