US3476118A - Method of influencing tobacco smoke aroma - Google Patents

Method of influencing tobacco smoke aroma Download PDF

Info

Publication number
US3476118A
US3476118A US619058A US3476118DA US3476118A US 3476118 A US3476118 A US 3476118A US 619058 A US619058 A US 619058A US 3476118D A US3476118D A US 3476118DA US 3476118 A US3476118 A US 3476118A
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US
United States
Prior art keywords
tobacco
methoxy
hydroxy
influencing
tobacco smoke
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
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US619058A
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English (en)
Inventor
Werner Richard Gotthar Luttich
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
WERNER RICHARD GOTTHARD LUTTIC
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WERNER RICHARD GOTTHARD LUTTIC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
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Application filed by WERNER RICHARD GOTTHARD LUTTIC filed Critical WERNER RICHARD GOTTHARD LUTTIC
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Publication of US3476118A publication Critical patent/US3476118A/en
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Expired - Lifetime legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/28Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances

Definitions

  • the invention is more particularly applicable to natural tobaccos such as cigarette tobaccos, but can also be used in the case of synthetic tobaccos such as sheet made from tobacco waste products, or from a carrier substance, preferably not produced from the tobacco plant, which is impregnated with selected material so as to have the flavour of a natural tobacco when smoked. In this case it is important the carrier substance should not burn to produce materials which would impair the smoking quality.
  • German patent specification 1,131,580 makes the proposal of making synthetic or artificial tobacco fibres by selecting a suitable tobacco mixture, extracting it successively with water and alcohol, then producing a combined dry extract from the two extraction steps, and mixing the dry extract with a carrier substance such as cellulose or methyl-cellulose. The carrier substance is then made into fibres similar to those of natural tobacco.
  • synthetic tobacco which has aromaand flavour-producing materials from the natural tobacco so that it can be enjoyed by smokers. It is free from certain woody or cellulose materials of natural tobacco.
  • this previous invention does not relate to the systematic adjustment of the smoking flavour of a natural tobacco by adding or removing substances, a topic which is dealt with by the U.S. Patent 3,174,485.
  • This patent describes the addition to cigarette tobacco, the filter or wrapper of a controlled amount of specific flavor enhancers which may be derived from the volatile material distilled from a natural tobacco.
  • a further object of the invention is to provide a method of supplementing flavour-influencing substances already in a tobacco.
  • Yet a further object is to provide a method whereby more expensive components in a tobacco mixture may be decreased without the smoke flavour or aroma being impaired.
  • the present invention consists in a method of influencing the smoke flavour quality of a tobacco characterised by the step of adding to the unsmoked tobacco a flavour- Patented Nov'.-4, I969 ing material which occurs in the smoke natural tobacco, the compound having the general'formula' in which R, is hydroxy or methoxy, R is hydroxy or methoxy, or R R represent the group Those compounds having the desired flavor occur in natural tobacco and can be separated therefrom by steam distillation. In addition, they can also be produced synthetically.
  • the quantity of the materials added to the tobacco can vary within wide limits, for instance, between 5 and 800 p.p.m. or between 5 and 500 p.p.m., as may be required to influence the aroma or flavour of the tobacco in the re quired manner.
  • the flavouring substance added to the tobacco is a 3,4-vinylbenezne with substituents selected from the following group: hydroxy-, methoxy-, methylenedioxy-.
  • Vinylbeneznes can be used in which the vinyl group has been hydrated to the corresponding secondary alcohol group.
  • the following compounds can be used between 5 and 500 p.p.m. (preferably lO-l00 p.p.m.)
  • the quantity added tothe tobacco can also be as low as to be between 2 and ppm.
  • the isolation of the substances is preferably carried out by using steam distillation.
  • the substances are then separated from the distillate using known methods. Such for example, as described in the journal Helvetica Chimica Actu 50 68, 628 ff.
  • a method of influencing the smoke flavor of a tobacco characterized by the step of adding to the unsmoked tobacco a very small amount of a flavoring compound which occurs in the smoke of natural tobacco, the compound having the general formula in which R is hydroxy or methoxy, R is hydroxy or methoxy, or R -R represent the group 2.
  • flavouring compound is isolated from a tobacco steam distillate.

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  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture Of Tobacco Products (AREA)
  • Filling Or Emptying Of Bunkers, Hoppers, And Tanks (AREA)
US619058A 1966-03-05 1967-02-27 Method of influencing tobacco smoke aroma Expired - Lifetime US3476118A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DER0042755 1966-03-05

Publications (1)

Publication Number Publication Date
US3476118A true US3476118A (en) 1969-11-04

Family

ID=7406745

Family Applications (1)

Application Number Title Priority Date Filing Date
US619058A Expired - Lifetime US3476118A (en) 1966-03-05 1967-02-27 Method of influencing tobacco smoke aroma

Country Status (9)

Country Link
US (1) US3476118A (xx)
BE (1) BE694958A (xx)
CH (1) CH491610A (xx)
DE (1) DE1692938A1 (xx)
GB (2) GB1175442A (xx)
LU (1) LU53121A1 (xx)
NL (1) NL6703164A (xx)
NO (1) NO118357B (xx)
SE (1) SE343465B (xx)

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US20060247446A1 (en) * 2003-07-25 2006-11-02 Samuel Neto Multi-metal oxide containing silver, vanadium and a promoter metal and use thereof
US20080019892A1 (en) * 2004-06-15 2008-01-24 Basf Aktiengesellschaft Multimetal Oxide Containing Silver, Vanadium And A Phosphor Group Element And The Use Thereof
US20100037903A1 (en) * 2008-08-14 2010-02-18 R. J. Reynolds Tobacco Company Method for Preparing Flavorful and Aromatic Compounds
US20100300463A1 (en) * 2009-06-02 2010-12-02 R.J. Reynolds Tobacco Company Thermal treatment process for tobacco materials
WO2011088171A2 (en) 2010-01-15 2011-07-21 R. J. Reynolds Tobacco Company Tobacco-derived components and materials
WO2011133633A1 (en) 2010-04-21 2011-10-27 R. J. Reynolds Tobacco Company Tobacco seed-derived components and materials
WO2012021683A2 (en) 2010-08-12 2012-02-16 R. J. Reynolds Tobacco Company Thermal treatment process for tobacco materials
WO2012083127A1 (en) 2010-12-17 2012-06-21 R. J. Reynolds Tobacco Company Tobacco-derived syrup composition
WO2012103435A1 (en) 2011-01-28 2012-08-02 R. J. Reynolds Tobacco Company Tobacco-derived casing composition
WO2012148996A1 (en) 2011-04-27 2012-11-01 R. J. Reynolds Tobacco Company Tobacco-derived components and materials
WO2012158915A2 (en) 2011-05-19 2012-11-22 R. J. Reynolds Tobacco Company Molecularly imprinted polymers for treating tobacco material and filtering smoke from smoking articles
WO2013074315A1 (en) 2011-11-17 2013-05-23 R.J. Reynolds Tobacco Company Method for producing triethyl citrate from tobacco
WO2013148810A1 (en) 2012-03-28 2013-10-03 R. J. Reynolds Tobacco Company Smoking article incorporating a conductive substrate
WO2014004648A1 (en) 2012-06-28 2014-01-03 R. J. Reynolds Tobacco Company Reservoir and heater system for controllable delivery of multiple aerosolizable materials in an electronic smoking article
WO2014037794A2 (en) 2012-09-04 2014-03-13 R. J. Reynolds Tobacco Company Electronic smoking article comprising one or more microheaters
WO2014058837A1 (en) 2012-10-09 2014-04-17 R. J. Reynolds Tobacco Company Tobacco-derived o-methylated flavonoid composition
WO2014058678A1 (en) 2012-10-08 2014-04-17 R. J. Reynolds Tobacco Company An electronic smoking article and associated method
WO2014120479A1 (en) 2013-01-30 2014-08-07 R. J. Reynolds Tobacco Company Wick suitable for use in an electronic smoking article
WO2014138223A1 (en) 2013-03-07 2014-09-12 R.J. Reynolds Tobacco Company Method for producing lutein from tobacco
WO2014150247A1 (en) 2013-03-15 2014-09-25 R. J. Reynolds Tobacco Company Heating control arrangement for an electronic smoking article and associated system and method
WO2014150926A1 (en) 2013-03-14 2014-09-25 R. J. Reynolds Tobacco Company Sugar-enriched extract derived from tobacco
WO2014159617A1 (en) 2013-03-14 2014-10-02 R. J. Reynolds Tobacco Company Protein-enriched tobacco-derived composition
WO2014159250A1 (en) 2013-03-12 2014-10-02 R. J. Reynolds Tobacco Company An electronic smoking article having a vapor-enhancing apparatus and associated method
US8910639B2 (en) 2012-09-05 2014-12-16 R. J. Reynolds Tobacco Company Single-use connector and cartridge for a smoking article and related method
WO2015017613A1 (en) 2013-08-02 2015-02-05 R.J. Reynolds Tobacco Company Process for producing lignin from tobacco
WO2015021137A1 (en) 2013-08-08 2015-02-12 R. J. Reynolds Tobacco Company Tobacco-derived pyrolysis oil
US8991403B2 (en) 2009-06-02 2015-03-31 R.J. Reynolds Tobacco Company Thermal treatment process for tobacco materials
US9078473B2 (en) 2011-08-09 2015-07-14 R.J. Reynolds Tobacco Company Smoking articles and use thereof for yielding inhalation materials
WO2015109085A1 (en) 2014-01-17 2015-07-23 R.J. Reynolds Tobacco Company Process for producing flavorants and related materials
US9220302B2 (en) 2013-03-15 2015-12-29 R.J. Reynolds Tobacco Company Cartridge for an aerosol delivery device and method for assembling a cartridge for a smoking article
US9277770B2 (en) 2013-03-14 2016-03-08 R. J. Reynolds Tobacco Company Atomizer for an aerosol delivery device formed from a continuously extending wire and related input, cartridge, and method
US9451791B2 (en) 2014-02-05 2016-09-27 Rai Strategic Holdings, Inc. Aerosol delivery device with an illuminated outer surface and related method
US9491974B2 (en) 2013-03-15 2016-11-15 Rai Strategic Holdings, Inc. Heating elements formed from a sheet of a material and inputs and methods for the production of atomizers
WO2017040789A1 (en) 2015-09-02 2017-03-09 R.J. Reynolds Tobacco Company Method for monitoring use of a tobacco product
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WO2017044558A1 (en) 2015-09-09 2017-03-16 R. J. Reynolds Tobacco Company Flavor delivery article
US9597466B2 (en) 2014-03-12 2017-03-21 R. J. Reynolds Tobacco Company Aerosol delivery system and related method, apparatus, and computer program product for providing control information to an aerosol delivery device via a cartridge
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WO2017093941A1 (en) 2015-12-03 2017-06-08 Niconovum Usa, Inc. Multi-phase delivery compositions and products incorporating such compositions
US9833019B2 (en) 2014-02-13 2017-12-05 Rai Strategic Holdings, Inc. Method for assembling a cartridge for a smoking article
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US9839238B2 (en) 2014-02-28 2017-12-12 Rai Strategic Holdings, Inc. Control body for an electronic smoking article
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US10031183B2 (en) 2013-03-07 2018-07-24 Rai Strategic Holdings, Inc. Spent cartridge detection method and system for an electronic smoking article
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WO2022053982A1 (en) 2020-09-11 2022-03-17 Nicoventures Trading Limited Alginate-based substrates
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DE2752787A1 (de) 1976-11-23 1978-05-24 Naarden International Nv Substituierte cyclohexanone als riech- und geschmacksstoffe
US20060247446A1 (en) * 2003-07-25 2006-11-02 Samuel Neto Multi-metal oxide containing silver, vanadium and a promoter metal and use thereof
US7462727B2 (en) 2003-07-25 2008-12-09 Basf Aktiengesellschaft Multimetal oxide containing silver, vanadium and a promoter metal and use thereof
US20080019892A1 (en) * 2004-06-15 2008-01-24 Basf Aktiengesellschaft Multimetal Oxide Containing Silver, Vanadium And A Phosphor Group Element And The Use Thereof
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CH491610A (de) 1970-06-15
NL6703164A (xx) 1967-09-06
DE1692938A1 (de) 1972-03-16
GB1175442A (en) 1969-12-23
BE694958A (xx) 1967-08-14
SE343465B (xx) 1972-03-13
LU53121A1 (xx) 1967-05-03
NO118357B (xx) 1969-12-15
GB1175441A (en) 1969-12-23

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