US3438618A - Vacuum heat treating furnace - Google Patents

Vacuum heat treating furnace Download PDF

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Publication number
US3438618A
US3438618A US577941A US3438618DA US3438618A US 3438618 A US3438618 A US 3438618A US 577941 A US577941 A US 577941A US 3438618D A US3438618D A US 3438618DA US 3438618 A US3438618 A US 3438618A
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Prior art keywords
shell
shields
retort
bars
work
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Karl H Seelandt
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Abar Ipsen Industries Inc
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Ikon Office Solutions Inc
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    • C—CHEMISTRY; METALLURGY
    • C21—METALLURGY OF IRON
    • C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00—General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/74—Methods of treatment in inert gas, controlled atmosphere, vacuum or pulverulent material
    • C21D1/773—Methods of treatment in inert gas, controlled atmosphere, vacuum or pulverulent material under reduced pressure or vacuum

Definitions

  • VACUUM HEAT TREATING FURNACE Filed Sept. 8 1966 Sheet ,3 of 13 W, 9m Oigfeelczfndd" dd WWWW ATTORIQSY April 15, 1969 Filed Sept. 8.. 1966 K. H. SEELANDT VACUUM HEAT TREATING FURNACE Sheet 4 of13 CRTTQWEY/ 6a r) 34. deelandf" April 15, 1969 K. H.'SEELANDT I 3, 38,6 8
  • the retort of a vacuum heat treating furnace is formed by two side-by-side and oppositely concave shells which are separable sidewise from one another to exposed workpieces in the chamber to quenching fluid and which are separa'ble endwise from one another to facilitate loading of the workpieces into the chamber.
  • correspondingly concave heating elements and reflecting shields are nested compactly within shells and are movable with the latter, the heating elements being formed by bars with an elliptical cross section and being located to radiate heat of high and substantially uniform intensity.
  • Cooling jackets surround each shell and insure positive circulation of cooling fluid around and in direct contact with the shell While providing reinforcing cold support for the shell.
  • This invention relates to heat treating furnaces and, more particularly, to furnaces of the type in which the treating chamber is defined in an enclosure or retort disposed within an outer vessel that may be evacuated to provide an artificial nonoxidizing atmosphere.
  • the retort is lined with a heat barrier such as a series of spaced reflecting shields for blocking the escape of heat as the work is heated in the retort by radiant elements distributed around the walls of the chamber, and the work subsequently is quenched by cooling fluid circulated through the chamber and around the work.
  • a general object of the present invention is to heat work loads rapidly with greater uniformity and to quench the heated Work in the retort more effectively than has been possible with prior furnaces of the foregoing character.
  • Another object is to facilitate the loading and unloading of the retort in such a furnace, particularly of delicate parts that require careful handling and placement.
  • a more specific object is to form the retort with two side-by-side and relatively movable shells fitted together to enclose the heating chamber and surround the work during heating, and separable from each other within the vacuum-tight vessel for the free circulation of gas through the retort during quenching.
  • Another object is to surround the work during heating with a compact array of closely and uniformly spaced heating elements on all sides of the work and to separate the heating elements along with the shells to expose the work for quenching.
  • a further object is to form both shells of the retort and the components therein with concave or U-shaped sides fitting together and closely around the work.
  • Still another object is to obtain greater uniformity of radiation intensity close to the heating elements where the intensity is greatest, in order to heat the work both rapidly and uniformly.
  • a related object is to provide a novel arrangement of spaced radiating surfaces and reflectors positioned outside the heating elements to obtain substantial uniformity of radiation intensity adjacent the inner sides of the elements.
  • a further object is to quench the work with cooling fluid injected into the open retort and directly against the work without prior contact with heated components of the furnace.
  • An additional object is to recirculate the quenching fluid after contact with the work as an incident to continued charging of the furnace with cold fluid or, alternatively, to recirculate and recool the quenching fluid on completion of such charging.
  • Another object is to simplify the mass production and servicing of such furnaces by making the two shells identical in shape for ready interchangeability of the shells and the parts therein.
  • Still another object is to support the components in each shell for quick and easy insertion and removal for repair and replacement of parts.
  • An additional object is to use thin and freely flexible sheet material as reflectors to reduce the mass of the shields, and to support the reflectors in a novel manner in the desired shape within the shells.
  • a further object is to cool the outer side of the retort more effectively than has been accomplished in prior furnaces, thereby positively preventing the escape of heat to the vessel, and to accomplish such cooling in a novel and relatively simple manner that insures the positive circulation of cooling fluid around and in direct contact with the shell while providing reinforcing cold support for the shell.
  • the invention also resides in the novel manner of nesting the reflecting shields and the heating elements compactly within each shell, and supporting the shields for movement relative to each other and to the shells during heating and cooling of the furnace.
  • FIG. 1 is a fragmentary side elevational view of a heat treating furnace embodying the novel features of the present invention.
  • FIG. 2 is an enlarged fragmentary cross sectional view taken substantially along line 2-2 of FIG. 3.
  • FIG. 3 is a fragmentary cross sectional view taken substantially along line 3-3 of FIG. 2.
  • FIG. 4 is an enlarged fragmentary cross sectional view taken substantially along line 44 of FIG. 3.
  • FIG. 5 is a perspective view of the retort.
  • FIG. 6 is an enlarged fragmentary cross sectional view taken along line 6-6 of FIG. 5.
  • FIGS. 7 and 8 are perspective views similar to FIG. 5 but showing the shells forming the retort in different moved positions.
  • FIG. 9 is an enlarged perspective view, partially in cross section, showing the supporting structure for one part of the retort, the retort being indicated in dot-dash mes.
  • FIGS. 10 and 11 are perspective views showing the internal construction of the two shells.
  • FIG. 12 is an enlarged fragmentary cross sectional view taken substantially along line 1212 of FIG. 3 and showing the construction of the hearth.
  • FIG. 13 is a perspective view of the hearth and its supporting structure.
  • FIG. 14 is an enlarged fragmentary cross sectional view taken through the hearth substantially along line 1414 of FIG. 4.
  • FIG. 15 is a perspective view of the heating elements of one of the shells, the lower shell herein.
  • FIG. 16 is a perspective view of the heating elements of the upper shell.
  • FIG. 17 is an enlarged cross sectional view of one of the heating elements.
  • FIG. 18 is an enlarged fragmentary cross sectional view taken along line 18-18 of FIG. 15 and showing the relationship of the heating elements to the innermost reflector and to the preferred position of the work load.
  • FIG. 18 is a perspective view of one of the shells illustrating the flow path of coolant therein.
  • FIG. 19 is an enlarged fragmentary view of part of FIG. 4 showing the interfitting relationship of the shells along one edge thereof and the manner of supporting the reflecting shields relative to each other.
  • FIG. 20 is an enlarged fragmentary cross sectional view taken along line 20-20 of FIG. 3 and showing a corner of the internal retort construction.
  • FIG. 21 is an enlarged view similar to another portion of FIG. 4 with additional parts shown in cross section and illustrating the support of the heating elements and reflecting shields of the lower shell.
  • FIG. 22 is a view similar to FIG. 21 but showing the manner of support in the upper shell.
  • FIG. 23 is an enlarged fragmentary cross sectional view taken substantially along line 2323 of FIG. 2 with additional parts broken away and shown in crosssection for clarity of illustration.
  • FIG. 24 is an enlarged fragmentary cross sectional view taken substantially along line 2424 of FIG. 2 with additional parts broken away and shown in crosssection.
  • FIGS. 25 and 26 are schematic perspective views of the two shells illustrating the flow paths of the coolant to and from the shells.
  • FIGS. 27 and 28 are views similar to FIGS. 25 and 26 but showing the conductors for carrying current to and from the shells.
  • FIG. 29 is a diagram showing the manner of connecting the different sets of heating elements.
  • FIG. 30 is a schematic perspective view of the retort with the shells thereof separated from each other, and illustrating the manner of charging and recirculating quenching fluid within the vessel.
  • FIG. 31 is a schematic perspective view of the retort and apparatus for recirculating and recooling the quenching fluid after the vessel has been charged.
  • the invention is embodied in a heat treating furnace of the type having a retort 11 (see FIGS. 25) enclosed in an outer vessel 12 and defining a heating chamber 13 in which a work load 14 is supported on a hearth 15 and heated by radiant heating elements 17-19 in the chamber.
  • the outer vessel is an open-ended cylinder supported on legs 20 adjacent its opposite ends and having outwardly dished circular heads 21 and 22 which close the ends of the vessel.
  • he head 21 at the front end is hinged at 23 on one side of the vessel to form a door for access to the interior of the vessel during loading and unloading of the retort and servicing of the furnace.
  • Suitable seals 24 (FIG. 3) are provided between the heads and the flanges 25 on the vessel ends to insure that the vessel is vacuum-tight when closed, and several clamps 27 hold the door tightly in place when it is closed.
  • the furnace 10 is evacuated by vacuum pumping apparatus 28 (FIG. 1) which herein is disposed along one side of the vessel and opens into the latter through a pipe 29 (FIG. 2) sealed to the vessel around an opening therein.
  • vacuum pumping apparatus 28 FIG. 1
  • FIG. 2 Various types of pumping apparatus may be used such as the combined arrangement shown in Patent No. 3,144,199 and comprising a mechanical pump connected by piping 31 to the lower, outlet end of an oil diffusion pump 32 communicating with the outlet pipe. The operation of such apparatus is well known to those skilled in the art and need not be described in detail herein.
  • the heating elements are energized to heat the work in the retort to a preselected temperature determined by the composition of the metal of the work and by the particular treatment to be performed. Then, after the work has been heated uniformly to the selected 4 temperature, it is cooled in quenching fluid such as an inert gas at a rate selected to obtain the physical properties desired in the finished product, the gas being circulated through the heating chamber 13 and around the work therein.
  • quenching fluid such as an inert gas
  • the present invention contemplates a new and improved furnace 10 of the foregoing character for heating work loads 14 rapidly with greater uniformity than has been possible with prior furnaces and quenching the heated work rapidly at closely controlled rates, and in which the work is loaded into and out of the retort 11 in a novel manner facilitating the handling and placement of the Work, particularly delicate parts such as brazing assemblies, without need for special handling equipment.
  • the retort comprises generally a pair of relatively movable shells 33 and 34 fitted together in side-by-side relation to define the enclosed heating chamber 13, and a unitary assembly is nested in each shell to provide an effective heat barrier between the shell and the chamber, including inner reflecting shields 35 and 37 lining the chamber, and also to provide an array of heating elements 17-19 uniformly spaced around the chamber and cooperating with the shields to produce substantially uniform radiation intensity on all sides of the work.
  • the shells 33 and 34 are separated to open the sides of the retort 11 and a charge of quenching fluid is injected into the chamber and directly against the work therein to reduce the temperature of the work quickly below the critical temperature.
  • a charge of quenching fluid is injected into the chamber and directly against the work therein to reduce the temperature of the work quickly below the critical temperature.
  • one of the shells is supported on the vessel for endwise movement away from the other shell and out through the door 21 into an extended position in which the work may be placed directly on the hearth 15. Then, as the shell is shifted back into the vessel, the work is carried into the heating chamber for the treating cycle.
  • the retort 11 is in the shape of an elongated box having six generally rectangular walls.
  • the shell 33 is disposed beneath the shell 34 and is formed by an upright wall 38 constituting the front of the retort, a horizontal lower wall 39 (see FIG. 4), and elongated rectangular lower sidewalls 40 extending upwardly from the sides of the lower wall half way to the top of the retort.
  • the upper shell is the same shape as the lower shell but is inverted and fitted over the latter with the depending end wall 38 closing the open rear end of lower shell and the depending sidewalls 40 extending downwardly from the sides of the upper wall 39 and cooperating with the lower sidewalls to close the sides of the retort.
  • Each shell is composed of suitable sheet material such as stainless steel, the end walls being welded to a one-piece U-shaped section forming the pr mary part of each shell.
  • the lower shell 33 is supported in the vessel 12 for horizontal movement relative to the upper shell 34 on a telescoping horizontal frame 41 (FIGS. 1-4) which is slidably mounted on the bottom of the vessel on two parallel rods 42.
  • the latter extend from front to rear in the vessel along the tops of two spaced rows of pads or brackets 43 fastened to the bottom of the furnace.
  • Each slide rod 42 is supported on the associated row of pads by studs 44 threaded upwardly into the underside of the rod and extending downwardly through holes in the alined pads.
  • Lock nuts threaded on each stud on opposite sides of the pad hold the stud in place. It will be seen that this arrangement makes it possible to adjust the level of the rods relative to the pads and lock the rod in the selected position.
  • each slide rod 42 Telescoped onto each slide rod 42 are two bearing sleeves 45 (FIGS. 1, 3 and 4) which are fast in bores in blocks 47 fast on the underside of the telescoping frame 41 thereby supporting the frame for free in-and-out sliding along the rods.
  • the blocks and the bearing sleeves are split (see FIG. 4) to for-m clearance slots in their undersides for passing the studs 44 as the sleeves move along the rods.
  • the two sleeves on each rod are secured to the rear portion of the telescoping frame which thus projects outwardly or forwardly, cantilever fashion, beyond the ends of the slide rods when the two forward sleeves are at the front ends of the rods.
  • End flanges 48 on the rods abut against the sleeves to prevent the latter from riding off the rods.
  • two additional sets of bearing sleeves 45 are mounted in bores in blocks 47 fast on top of the telescoping frame 41 adjacent the forward end thereof, with two upper slide rods 42 slidably supported in these sleeves in parallel relation with the lower rods 42. Studs 44 threaded into the tops of the upper rods extend upwardly through alined holes in two channel-shaped supports 49 paralleling the rods, and are fastened to the supports. The upper sides of the upper sleeves and blocks also are split to form slots permitting movement of the studs past the sleeves. Above the studs, the channel-shaped supports are welded to a series of parallel transverse channels '50 which, in turn, are welded to the underside of the lower shell 33.
  • the upper slide rods slide through the upper bearing sleeves as the shell is pulled outwardly toward the door until the rear sleeve on each rod abuts against an end flange 4-8 on the rear end of the rod. Then the continued outward motion of the shell pulls the telescoping frame outwardly along the lower slide rods to the position shown in FIG. 1. Accordingly, the shell may be pulled completely out of the vessel 12 for loading and unloading. Even in the fully extended position, however, the telescoping cantilever support holds the shell firmly in place.
  • End flanges 48 on the front ends of the upper slide rods limit inward motion of the latter through the upper bearings and similar end flanges on the lower slide rods limit inward motion of the lower bearings.
  • latch arms 51 are pivoted on headed pins 52 projecting forwardly from the lower slide rods and are swingable upwardly from the broken-line positions in FIG. 2 into the positions shown in full in which the notched free end portions of the arms interlock with headed pins 53 on the upper slide rods. This latches both the upper rods and the telescoping frame to the fixed lower rods.
  • the upper shell 34 is supported in the vessel 12 on a horizontal frame 54 which is suspended on the lower end of an elevator rod 55 extending downwardly from a vertical elevator cylinder 57 mounted on a ring 58 sealed in an opening (see FIG. 3) in the top of the vessel.
  • a piston (not shown) guided in the cylinder for vertical movement in response to the admission of pressure fluid into the opposite ends of the cylinder.
  • a pump 59 is mounted on top of the vessel beside the cylinder and is driven by a selectively operable motor 60, the pump delivering pressure fluid to the cylinder through a control valve 61 which directs the pump output to the appropriate end of the cylinder.
  • the elevator mechanism raises and lowers the upper shell to open and close the retort when the lower shell is in place within the furnace.
  • the horizontal frame 54 connected to the elevator rod 55 is formed by a series of parallel transverse channels 62 (see FIG. 9) joined together by two elongated, front-to-rear rails 63, one of the channels being fastened to a block 64 on the lower end of the rod to fasten the frame to the elevator mechanism.
  • two cross-bars 65 on the upper sides of the frame rails support sleeves 67 having center bores receiving vertical guides 68 depending from the top of the vessel through the sleeves and on through alined holes in the cross-bars beneath the sleeves.
  • the guides and the sleeves cooperate to maintain the frame horizontal at all times.
  • the upper ends of these guides are fastened to the upper end walls of tubular fittings 69 sealed in the top of the furnace.
  • the upper shell 34 also is supportedfor sliding out of the vessel 12 through the open door 21.
  • two parallel slide rods 70 are mounted on the frame and the shell is slidably supported on the rods by hearing sleeve carried in bars 71 projecting horizontally from brackets 72 upstanding from the top of the shell.
  • the rods extend from front to rear along the top of the shell and are adjustably secured to the frame 54 by two rows of studs 73 similar to the lower studs 44, the sleeves and the supporting bars having split lower sides to move along the rods past the studs.
  • the illustrative embodiment of the invention comprises two shells forming a box with rectangular sides
  • the U-shaped sections can be semicylindrical rather than semi-rectangular, particularly if the work load is to be cylindrical, and that the shells may be of other shapes that fit together to form an enclosure within the vacuum vessel.
  • the concept may be applied to vertically loaded furnaces with modifications to suit this type of furnace.
  • the heat barrier within each shell 33, 34 is formed by a set of reflecting shields 35 and 37 that are formed in the same shape as the shells and nested therein in spaced relation with the shells and with each other to reflect radiation from the heating elements 17-19 back into the heating chamber 13, the shields 35 being U-shaped in cross section to cover the U-shaped portions of the shells and the shields 37 being flat.
  • Both types of shields are composed of suitable high-temperature metal such as molybdenum, tungsten or tantalum, depending upon the temperature levels to be developed in the furnace, and are made as thin as is practical to minimize the mass of the shielding and reduce the heat stored therein during the heating operation.
  • molybdenum sheet material on the order of .003 of an inch thick is used, several strips of such foil being disposed in side-by-side overlapping relation to form each shield.
  • Molybdenum parts including the heating elements, may be used in a vacuum where the work is to be heated to about 2400 degrees F. From 2400 to somewhat above 3000 degrees, tantalum parts are used, and tungsten parts are used in temperatures up to about 4000 degrees.
  • a basket 77 (see FIGS. 10 and 11) composed of relatively heavy screen material such as No. 4 mesh Inconel which is stiff enough to be formed into the shape of the shells and thereafter retain its shape as the shields and associated parts are assembled into the baskets.
  • the baskets comprise generally rectangular end walls and shallow sections of U- shaped cross-section for fitting into the U-shaped portions of the shells, and are sufficiently smaller than the shells to leave a small clearance space inside the shells.
  • the shields are supported on the baskets primarily by a plurality of pin 78 (see FIGS.
  • each pin On the inner end of each pin is a washer 80 abutting against the exposed surface of the innermost shield and held on the pin by a head 81.
  • a washer 82 On the outer end of the pin, which preferably is pointed as shown in FIGS. 19 and 20, is a washer 82 which frictionally grips the pin to tie the assembly together.
  • the spacer rings are telescoped loosely onto the pins and the holes in the shields around the pins are made substantially-larger than the thickness of the pins themselves, thereby permitting the shields and the rings to move relative to the pins during heating and cooling of the furnace.
  • the spacer rings, the pins and the washers on the pins all are composed of high-temperature metal selected for the temperatures to be attained in the furnace, molybdenum in this instance.
  • the supporting pins 78 are distributed liberally around the basket to hold the shields in the desired shape and in properly spaced relation.
  • the strips of the innermost shield are laid out and the pins are insorted through the inner washers 80 and upwardly through the strips.'Then a spacer 79 is dropped onto each pin and the strips of the next shield are laid over the inner shield so that the pins pass through the pre-punched holes and the second shield comes to rest against the spacers. Successive shields are placed in this manner until the preselected number of shields are in place.
  • six shields are used.
  • the shields become progressively smaller from the outer shield inwardly, and that the strips are sized and the pin holes are positioned to provide the appropriate radius at the junctions of the upright sidewalls with the horizontal walls.
  • the sidewalls may be brought into their proper positions simply by raising the horizontal walls and allowing the sidewalls to hang downwardly therefrom.
  • a suitable frame (not shown) may be disposed beneath the central portion of the shields during assembly and then lifted upwardly to raise the central portion.
  • a basket 77 is fitted over the assembly and the pins 78 are passed through the screen material to mount the shields in the basket. Additional spacers 79 on the pins between each basket and the outer shield space the latter from the basket. It is possible to spring the basket walls outwardly sufiiciently to pass over the shields and then release them to close around the shields. After the lock washers 82 have been slipped onto the pins, the flexible shields are held in shape by the pins which are held in place by the basket.
  • the sets of flat shields 37 for the end walls 28 of the shells are held together in the same manner (see FIG. 20) by pins 78, spacers 79 and washers 80 and 82.
  • the ends of the shields are stepped as shown in FIG. 20 with the outer three flat shields overlying the ends of the outer three U-shaped shields and with the inner three shields of each type foreshortened so that the inner three fiat shields overlie the ends of the inner three U- shaped shields.
  • hanger pins 84 are secured to each basket in two rows adjacent the free edges of the U-shaped portion and to the end wall in selected locations, each pin extending inwardly through a series of alined holes in the shields and supporting on 8 its inner end a heating element clamp 85.
  • Each such clamp comprises a pair of bars (see FIGS. 15 and 16) disposed in side-by-side relation on opposite sides of two heating elements which are notched to receive the clamp bars.
  • the heating elements are elongated solid bars forming electrical resistors and are composed of molybdenum. As shownmost clearly in FIGS.
  • each such grid comprises three long bars 18 covering the central portion of .the shield and tWo shorter bars 19, approximately half as .long as the central bars, positioned along opposite sides of the shield.
  • the heating element clamps 85 in each shell 33, 34 are electrical conductors and cooperate with the bars 17-19 and with additional clamps 87 and 88, to define a single series path for the flow of electricity in the two grids.
  • the clamps 85 extend in opposite directions from the opposite ends of each bar to connect the barelectrically to the two adjacent bars.
  • the U-shaped bar at the right or inner end of the lower shell is supported at one end by a singlebar clamp 87 and at the other end by a double-bar clamp 85 that also supports the second heating bar.
  • the other end of the second bar is held by a double-bar clamp that also holds the third bar.
  • This alternating arrangement of clamps continues to the left end of the grid where the last U-shaped bar is held by a curved clamp 88 that turns the corner and also holds the upper end of the lower short bar 19, thereby electrically connecting the two grids.
  • the lower end of the short bar shares a double-bar clamp 85 with the lower end of the adjacent long bar 18, and the series connections continue across the flat grid to the lower end of the upper short bar 19 which is held in a single-bar clamp 87.
  • the arrangement for the upper grids is similar, as shown in FIG. 16, the U-shaped bar 17 at the left and the lower end of the upper short bar 19 being held in single-bar clamps 87 at the opposite ends of the series.
  • each pin comprises an elongated stud 90 (See FIGS. 21 and 22) extending at its inner end through alined holes formed in the clamp bars between the two heating bars held thereby, and a nut 91 is threaded onto the inner end and tightened against the inner clamp bar.
  • a ceramic sleeve 92 Telescoped snugly over the intermediate portion of the stud is a ceramic sleeve 92 which extends loosely through the six shields and projects somewhat beyond the inner and outer shields.
  • a tube 93 which fits snugly into a counterbore in the inner end of the sleeve and is held by the counterbore in coaxial relation with the stud.
  • the inner end of this tube which herein is composed of molybdenum, is seated in a counterbore in the clamp bar and thus cooperates with the nut 91 in holding the clamp together.
  • a washer 94 is telescoped loosely over the stud 90 inside the screen 77 and an insulating plug 95 is slipped onto the stud through a clip or bracket 96, 97 which is used to support the basket on the shell.
  • a flange 98 on the insulating plug is pressed tightly against the clip by a nut 99 that is threaded onto the outer end of the stud to draw the entire hanger assembly together, clamping the clip against the screen and securing the hanger both to the clip and to the screen.
  • a dished washer 100 is telescoped snugly on the tube 93 adjacent the inner end of the ceramic sleeve to prevent coating of the sleeve by metallic vapor that could conduct current to the shields,
  • each lead-in bar is an elongated and relatively heavy rod that may be composed of molybdenum, abutting at its inner end against the heating element and extending outwardly through an insulating ceramic sleeve 103 which extends through the shell 33 or 34, the reflecting shields 35 or 37, and the basket 77.
  • a stud 104 extending through the lead-in bar has nuts 105 threaded on its opposite ends to hold the heating bar firmly against the lead-in bar.
  • the clips 96 and 97 spaced along the edges of the U-shaped portions engage elongated rails 107 (FIGS. 4, 21 and 22) fastened to the sidewalls of the shells, the rails and clips being arranged to permit the baskets to be slipped quickly into and out of the shells.
  • the clips 97 on the upper basket See FIGS. 4,
  • 11 and 22 are inverted U-shaped pieces each having a depending leg or tab hooked over and into an upwardly opening groove defined between an inwardly offset upper portion of the adjacent upper rail 107.
  • the latter is welded to the upper shell and preferably extends along substantially the full length of the shell.
  • the lower rails are the same as the upper rails and receive downwardly extending legs or tabs of the lower clips 96 which are Z-shaped as shown in'FIGS. 4, 10 and 21.
  • the upper basket may be slid endwise into the upper shell through the open front end of the latter, and the lower basket may be lowered into the lower shell through the top, both sets of clips and rails becoming engaged during such assembly.
  • two channels 108 are fastened to the underside of the lower basket to rest on the bottom of the lower shell, and a similar channel 109 (FIGS. 4 and 11) is fastened to the top of the upper basket and formed with oppositely projecting flanges 110 fitting over the downwardly offset portions of two spaced parallel rails 111 fastened to the upper wall of the shell.
  • the end walls of the basket preferably are supported independently of the U-shaped portions by elements (See FIG. 10) similar to the clips 96.
  • the lead-in bars 101 are fastened to bus bars 112-115 (FIGS. 1-3, 27 and 28) which extend around the shells to suitable electrical connections as shown most clearly in FIGS. 27 and 28.
  • bus bars 112-115 FIGS. 1-3, 27 and 28
  • FIGS. 24 and 28 it will be seen that the lead-in bar projecting through the front end wall 38 of the lower shell is fastened to the bus bar 112 which bends around the shell to the left side and carries a rearwardly facing contact plate 117 engageable with a similar forwardly facing plate 118 that is supported on the adjacent side 'of the vessel 12.
  • the lead-in bar exiting through the rear portion of the lower shell is fastened to the bus bar 113 which extends forwardly along the right side of the shell, then across the front and downwardly to a level below the bus bar 112, and finally rearwardly beneath the other bar, terminating in another rearwardly facing contact plate 117 engageable with a similar forwardly facing plate 118 supported on the vessel beside the left side of the retort.
  • the outer end portion of the front lead-in bar 101 is clamped between the legs of a split conductor 119 upstanding from the bus bar 112, the latter being fastened to the front of the shell by means of a block 120 Welded to the shell and carrying an insulating plate 121 which is fastened separately to the bus bar and to the supporting block by bolts 122.
  • the contact plates 117 are fastened to the out-turned ends of the bus bars to face rearwardly along the side of the shell and toward the plates 118 which are carried on the front ends of two rods 123 connected at 124 to cables 125 and 126 fastened to connectors 135 and 127, respectively, passing through the vessel wall, the rods being supported for limited front-to-rear slidIng on brackets 128 (See FIG. 24) welded to the inside of the vessel.
  • the rods and plates are urged forwardly by springs 129 acting between the plates and backing plates 130 bolted to ceramic insulating blocks 131 bolted, in turn, to the supporting brackets.
  • the lead-in bars 101 are connected to the bus bars 114 and 115 (FIGS. 2 and 27) which extend around the back of the shell to the left side where cables 133 and 134 connect the bars to another set of connectors 135 and 127, respectively, passing through the vessel.
  • the cables accommodate up-anddown movement of the shell during normal furnace operation, and may be disconnected when the upper shell is to be slide out through the front door during servicing.
  • the cables 125 and 133 are hot lines and the cables 126 and 134 are grounded. This is indicated in FIG. 29 wherein the four heating grids' are shown schematically as resistors connected through the cables 125 and 133 to hot terminals 135 and through cables 126 and 134 to a common ground terminal 127.
  • the internal components of the retort 11, including the shields 35 and 37 and the heating elements 1719 are mounted compactly within the baskets 77 for quick and easy removal from the associated shells for servicing or for replacement by other assemblies.
  • the two heating grids in each shell are replaceable as units without disturbing the shields.
  • the two shells, the shields therein, and the heating grids are made identical in size and shape thereby reducing the number of different fabrication parts and facilitating mass production, and also simplifying the servicing of the furnace.
  • each of the heating bars is elliptical in cross-section to provide oppositely facing convex side surfaces (FIGS, 17 and 18) facing inwardly toward the work and outwardly toward the shield, and the elements are spaced preselected distances from each other and from the shields to heat spaced areas of the work primarily by direct radiation and heat the intervening areas at substantially the same rate with the assistance of reflected radiation.
  • FIGS. 17 and 18 The optimum elliptical shape is shown in FIGS. 17 and 18 wherein it will be seen that the width of the bars is substantially greater than twice the thickness, and that the center of curvature a (FIG. 17) of each bar side surface 140 is spaced a substantial distance beyond the opposite side of the bar.
  • FIGURE 18 it will be seen that the shields are placed close to the lines defined by the centers of curvature of the inwardly facing sides 140 of each row of bars, about one-half the bar width from the outwardlyfacing side, and that adjacent bars of each grid are spaced apart a distance the same as the bar width.
  • the heaters are centered between the shields and the work load 14.
  • the intensity drops sharply as the distance from the source increases (specifically, in accordance with the square of the distance), and also decreases as the angle of incidence of the radiation is reduced. Consequently, the area of the work beside the central portion of each bar, and closest to the bar as indicated by the length of the arrows 141 in FIG. 18, will be heated directly to the greatest extent as a result of both the close spacing and the angle of incidence. The areas of the work opposite the side portions of the bar will be heated directly to a lesser extent due to the increasing distance from the convex radiating surface 140, and also due to the decreasing angle of incidence. By making the radiating surface relatively flat (as compared to a cylindrical surface of equal thickness), this variation in direct radiation, in areas opposite the bars, is minimized.
  • the combination of the substantially flat shields with the convex outside radiating surfaces 140 results in the heating of the intermediate areas of the work by reflected heat that combines with the direct radiation to bring these intermediate areas quickly up to substantially the same temperature as the areas directly opposite the bars.
  • the radiation from the outer surfaces considered as traveling along straight lines from point sources on the surfaces, is dispersed in the manner indicated by the arrows 142 and 143 in FIG. 18 and reflected back between the bars as at 144 and 145 to cover the intermediate areas of the Work.
  • the result is greater uniformity close to the grids where the intensity is greatest and where the work may be heated rapidly to the desired temperature, this arrangement thus approximating the heating effect of a solid-sheet resistor.
  • FIGS. 17 and 18 illustrate the optimum configuration and spacing of the bars, and that it is possible to obtain improved heating uniformity with elliptical bars of somewhat different curvature-for example, with sides formed with a larger radius of curvature-and also with bars spaced somewhat farther apart and from the shields.
  • intensity falls off sharply so that more time must be spent in heating.
  • the resistance is relatively low, and a low-voltage source is used to produce a high rate of current flow and generate heat at the desired rate.
  • the input voltage may be on the order of 60 volts derived through a step-down transformer (not shown) from the usual 220 volt supply.
  • the large radiating surface area provided by the grids in each shell maintains a low power density at the surfaces of the elements.
  • the hearth (See FIGS. 3, 4 and 13) for supporting the work in the heating chamber 13 comprises a series of elongated hearth bars that are spaced above the level of the horizontal portions of the lower U-shaped heating bars 17 and have upper surfaces disposed in a common horizontal plane.
  • the hearth bars are composed of high-temperature metal, herein molybdenum, and are provided with ceramic caps 147 for applications in which there is a danger of damage as a result of placement of metal workbaskets directly on the metal bars.
  • such caps may take the form of elongated blocks of the same width as the hearth bars, and formed with rounded upper surfaces for engaging the workbasket and depending longitudinal ribs 148 (FIGS.
  • the posts comprise central molybdenum tubes 151 fitting at their up per ends into recesses in the undersides of the hearth bars adjacent the ends thereof and telescoped at their lower ends into upright sleeves 152 of suitable high-temperature metal.
  • Each such sleeve is welded to a square plate 153 that is fitted into one of the elongated upwardly opening channels 108 fastened to the underside of the basket.
  • each channel is formed with flanges 154 that abut against the bottom of the basket 77, and pins 155 having heads 157 below the flanges extend upwardly therethrough with washers 158 locked on the pins above the screen.
  • the two channels support two rows of hearth posts beneath the opposite end portions of the hearth bars, the supporting plates 153 being spot-welded to the channels to hold each post in a centered position between two heating bars 17.
  • an insulating ceramic sleeve 159 is telescoped onto the upper portion of each tube and covers the latter between the hearth bars 15 and the supporting sleeves 152, the ceramic sleeves extending through the innermost shield 35 and preferably somewhat farther into the shielding.
  • a washer 160 on the insulating sleeve above the inner shield covers the clearance left between the shields and the post to permit shifting of the shields during heating and cooling, and a ceramic washer 164 in the bottom of the supporting sleeve prevents metal-to-metal contact between the tube and the plate 153, thereby spreading and distributing the heat couducted through the tube and the plate to the shell 33.
  • conduits 161 (FIG. 6) having open, relatively wide sides facing toward and covered by the shells whereby the conduits carry separated flows of cooling fluid around the shells in direct contact with a major portion of each shell.
  • the conduits are V-shaped grooves formed by corrugations 162, 163, in a sheet of imperferate material laid over the outer sides of the shell and substantially coextensive with the shell sides with one generally rectangular sheet covering each end wall of the retort and one U-shaped sheet covering the remainder of the shell.
  • the corrugations 163 in the end sheets are vertical and have open upper and lower ends communicating with headers 164 formed by transverse horizontal ridges in the corrugated sheet extending across the upper and lower edge portions of the sheet, which is sealed to the end wall by continuous, fluid-tight marginal welds and also is sealed around the lead-in holes 102 and spot-welded to the sheet at spaced points along the inner ridges 165 abutting against the shell between adjacent conduits, as illustrated in FIG. 6. These ridges need not be perfectly sealed to the shell.
  • the corrugations 162 in the U- shaped sheet define conduits extending along U-shaped paths from near one side edge around the shell to the other side edge and having open ends opening into headers 167 formed by transverse or horizontal ridges extending along the side edges, this sheet also being sealed to the shell around its edges and around the holes 102 and spot-welded along the inner ridges 165 abutting against the shell.
  • Each header 164 and 167 is'provided with a flow pipe 168 for connection to an outside circulation system for forcing a suitable coolant, usually water, through the jackets at a relatively high rate to cool the shells during heat treating. For example, 3040 gallons per minute may be forced through each shell.
  • the circulation system is shown as including supply and return pipes 169 and 170, respectively, for the lower shell 33 entering the vessel 12 on the lower right side.
  • the supply pipe feeds two flexible hoses 171 and 172 carrying water to the inlet headers which are at the lower edge of the front end wall and at the right side of the U-shaped section.
  • the flexible supply hoses lead into pipes 173 and 174 leading to the flow pipes on the headers, and are connected to the supply pipe by joints at 175 (see FIG. 26) which enable the operator to disconnect the hoses manually in a simple and rapid operation preparatory to sliding of the lower shell out of the furnace.
  • the return pipe 170 receives water from two flexible return hoses 177 fastened to the pipe at quick-disconnect joints 178 and communicating through piping 179 with the flow pipes of the outlet headers, the upper header on the end wall and the left header on the U-shaped section.
  • water forced into the vessel through the supply pipe 169 fills the two inlet headers and flows through the conduits to the outlet pipes thereon.
  • Water for cooling the upper shell 34 enters and leaves the vessel 12 through pipes passing through the rear head 22.
  • One pipe 180 (FIGS. 3 and 25) feeds water into a flexible and extensible hose 181 fastened to the lower flow pipe 168 on the rear wall 38 of the retort 11 to flow upwardly to the upper header 164 from which it exits into a hose 182 and a pipe 183.
  • Another supply pipe 184 feeds the header 167 on the right, as viewed in FIG. 2, with water that flows around the U-shaped section and out of the other header through a hose 185 at the front of the header and a return pipe 187 extending to the rear and out through the head 22.
  • the conduits are divided into banks of several conduits each and means are provided for directing the coolant from one bank to the next to flow back and forth along zigzag paths from one header to the other while progressing from the inlet pipe to the outlet pipe, this being indicated by the arrows in FIG. 18
  • this is accomplished by dams or weirs 167 partially or fully closing the headers between adjacent banks of conduits and staggered longitudinally of the shell in a manner similar to the arrangement of the heating bar clamps 85.
  • the flow from the inlet pipe on the right in FIG. 18 fills the first bank of conduits with water which crosses the shell to the other header and then flows into the next bank to recross the shell, continuing in this manner to the opposite end of the shell and the flow pipe communicating with the header on the left side.
  • the flow path may be designed for the entry and exit of coolant on the same side of the shell, if desired, and that other variations are possible.
  • an up-and-down zigzag flow is provided in each end wall jacket.
  • the corrugated sheets reinforce and provide cold support for the entire shell structure, and distribute the flows of coolant over virtually all of the outer surface of each shell for a positive cooling action. Accordingly, the shells are effectively maintained at low temperatures during heating, and this facilitates the rapid cooling of the work during quenching.
  • the effective internal cooling eliminates the need for direct cooling of the vessel and its heads.
  • the retort 11 is opened by raising the upper shell 34 away from the lower shell 33 and thereby forming elongated circulation ports 188 (FIGS. 7, 30 and 31) along both sidewalls and ports 189 across both end walls, and quenching fluid is injected into the retort and directly against the work therein.
  • an elongated spray pipe 190 is disposed along each side of the retort as shown in FIGS. 2, 4 and 30 and centered on the spaces between the shells when the retort is open, each pipe being formed with longitudinally spaced nozzles 191 (see FIG. 4) for directing jets of fluid into the chamber 13 and against the work 14.
  • the quenching fluid argon for example, is stored under pressure in a bottle or tank (not shown) outside the furnace and preferably is maintained in liquid state for delivery to the spray pipes 190 through inlet pipes 192 extending through the opposite sides of the vessel.
  • the inlet pipes deliver the fluid to the spray pipes at the longitudinal midpoints thereof, and suitable valving (not shown) controls the flow from the source into the inlet pipes.
  • the liquid When quenching gas in the liquid state is directed into the evacuated furnace 10 through the spray pipes 190, the liquid immediately vaporizes as it enters the retort 11 and circulates around the work 14. In changing phase from liquid to gas, of course, the quenching fluid becomes substantially cooler than its storage temperature. Thus, even if the liquid is stored at room temperature, the temperature of the expanding gas as it is about to impinge against the work may be as low as 80 degrees F. For an even lower initial quenching temperature, the liquid may be refrigerated in storage and delivered to the retort at a temperature considerably below room temperature. In this manner, the temperature of the work is reduced rapidly below the critical range by cold gas impinging against and circulating around the work in the retort.
  • a flanged tube 193 (FIGS. 2 and 30) is disposed between the inner end portion of each inlet pipe and the associated spray pipe to receive the flow of coolant from the inlet pipe and guide the liquid into the spray pipe.
  • the action of the liquid entering the flanged and flared end 194 of the tube draws or aspirates gas from outside the retort back into the latter through the tube.
  • a pressure relief valve 195 is mounted on the vessel to release gas to the outside when the pressure attains a level on the order of 25 p.s.i.
  • the furnace may be charged with gas in the manner described above to cool the work quickly below the critical range as the vaporizin-g fluid is sprayed on the work, and the gas leaving the retort is collected in an outlet duct 197 (FIGS. 1, 2 and 31), cooled in a heat exchanger 198 outside the vessel 12 and then returned to the retort by an outside blower 199 through a diffuser 200 for directing the cooled gas through the rear port 189 and against the work.
  • the outlet duct opens into the top of the vessel adjacent the front end thereof (see FIG. 1) and leads rearwardly to the upper end of the heat exchanger which is housed in a vertical cylindrical case at the rear end of the furnace.
  • suitable heat transfer components not shown
  • the inner wall of the cylindrical case which is formed as a water jacket.

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  • Physics & Mathematics (AREA)
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  • Crystallography & Structural Chemistry (AREA)
  • Mechanical Engineering (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Muffle Furnaces And Rotary Kilns (AREA)
  • Furnace Details (AREA)
US577941A 1966-09-08 1966-09-08 Vacuum heat treating furnace Expired - Lifetime US3438618A (en)

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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3730502A (en) * 1969-04-16 1973-05-01 Us Army Apparatus for vacuum brazing-gas quenching non-ferrous and ferrous alloys
US3752456A (en) * 1971-03-15 1973-08-14 Asea Ab Vertical tubular furnace for high operating pressures
US4713124A (en) * 1983-06-22 1987-12-15 Schmetz Gmbh & Co. Kg Unternehmensverwaltung Method for cooling a charge after thermal treatment
US4753192A (en) * 1987-01-08 1988-06-28 Btu Engineering Corporation Movable core fast cool-down furnace
WO1991009976A1 (en) * 1989-12-21 1991-07-11 Cambridge Vacuum Engineering Ltd. Apparatus and method for cooling a furnace load
US5524020A (en) * 1994-08-23 1996-06-04 Grier-Jhawar-Mercer, Inc. Vacuum furnace with movable hot zone
US6349108B1 (en) 2001-03-08 2002-02-19 Pv/T, Inc. High temperature vacuum furnace
US20150226377A1 (en) * 2012-08-03 2015-08-13 Benito Andres De Orte Glaria High pressure vessel for withstanding fatigue operating cycles

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1706010A (en) * 1928-06-11 1929-03-19 Robert J Walker Electric furnace
US2568653A (en) * 1946-09-06 1951-09-18 Mojonnier Bros Co Heat exchange receptacle
US2756032A (en) * 1952-11-17 1956-07-24 Heater
US2987788A (en) * 1958-03-06 1961-06-13 Gen Electric Crucible assembly for electric arc furnace
US3033547A (en) * 1957-07-01 1962-05-08 Sunbeam Equip Vacuum furnace
FR1391240A (fr) * 1964-03-10 1965-03-05 Degussa Four à vide
US3185460A (en) * 1963-08-15 1965-05-25 Pacific Scientific Co Vacuum furnace
US3197975A (en) * 1962-08-24 1965-08-03 Dunham Bush Inc Refrigeration system and heat exchangers

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1706010A (en) * 1928-06-11 1929-03-19 Robert J Walker Electric furnace
US2568653A (en) * 1946-09-06 1951-09-18 Mojonnier Bros Co Heat exchange receptacle
US2756032A (en) * 1952-11-17 1956-07-24 Heater
US3033547A (en) * 1957-07-01 1962-05-08 Sunbeam Equip Vacuum furnace
US2987788A (en) * 1958-03-06 1961-06-13 Gen Electric Crucible assembly for electric arc furnace
US3197975A (en) * 1962-08-24 1965-08-03 Dunham Bush Inc Refrigeration system and heat exchangers
US3185460A (en) * 1963-08-15 1965-05-25 Pacific Scientific Co Vacuum furnace
FR1391240A (fr) * 1964-03-10 1965-03-05 Degussa Four à vide

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3730502A (en) * 1969-04-16 1973-05-01 Us Army Apparatus for vacuum brazing-gas quenching non-ferrous and ferrous alloys
US3752456A (en) * 1971-03-15 1973-08-14 Asea Ab Vertical tubular furnace for high operating pressures
US4713124A (en) * 1983-06-22 1987-12-15 Schmetz Gmbh & Co. Kg Unternehmensverwaltung Method for cooling a charge after thermal treatment
US4753192A (en) * 1987-01-08 1988-06-28 Btu Engineering Corporation Movable core fast cool-down furnace
WO1991009976A1 (en) * 1989-12-21 1991-07-11 Cambridge Vacuum Engineering Ltd. Apparatus and method for cooling a furnace load
US5524020A (en) * 1994-08-23 1996-06-04 Grier-Jhawar-Mercer, Inc. Vacuum furnace with movable hot zone
US6349108B1 (en) 2001-03-08 2002-02-19 Pv/T, Inc. High temperature vacuum furnace
US6529544B2 (en) 2001-03-08 2003-03-04 Lennie L. Ashburn Vacuum heat treating furnace
US20030165177A1 (en) * 2001-03-08 2003-09-04 Ashburn Lennie L. Cooling system for heat treating furnace
US6947467B2 (en) 2001-03-08 2005-09-20 Pv/T, Inc. Cooling system for heat treating furnace
US20150226377A1 (en) * 2012-08-03 2015-08-13 Benito Andres De Orte Glaria High pressure vessel for withstanding fatigue operating cycles

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DE1974060U (de) 1967-12-07
DE1583325A1 (de) 1970-08-06

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