US3219265A - Centrifuges, e.g., ultracentrifuges for the separation of gases - Google Patents

Centrifuges, e.g., ultracentrifuges for the separation of gases Download PDF

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US3219265A
US3219265A US95683A US9568361A US3219265A US 3219265 A US3219265 A US 3219265A US 95683 A US95683 A US 95683A US 9568361 A US9568361 A US 9568361A US 3219265 A US3219265 A US 3219265A
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rotor
gas
plate
drum
mixture
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US95683A
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Los Johannes
Kelling Fridtjof
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Reactor Centrum Nederland
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Reactor Centrum Nederland
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B04—CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
    • B04B—CENTRIFUGES
    • B04B5/00—Other centrifuges
    • B04B5/08—Centrifuges for separating predominantly gaseous mixtures
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D59/00—Separation of different isotopes of the same chemical element
    • B01D59/20—Separation by centrifuging
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S494/00—Imperforate bowl: centrifugal separators
    • Y10S494/90—Imperforate bowl: centrifugal separators involving mixture containing one or more gases

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  • FIG.3 CENTRIFUGES, E.G. ULTRACENTRIFUGES FOR THE SEPARATION OF GASES Filed March 14, 1961 FIG.1 FIG.3
  • the invention relates to centrifuges and more particularly to ultracentrifuge for the separation of gas mix- 7 tures or mixtures of gaseous isotopes.
  • the centrifuges comprise a rotor mounted for rotation in a casing and means for the generation in the separating chamber of the rotor of a gas whirl transversely directed to the rotation.
  • a first means causes a temperature difference between the ends of the rotor.
  • Another means uses the momentum of the mixture supplied to the rotor and the way in which the components of the mixture are discharged.
  • a third means a stationary plate is placed within the closed rotor near one end thereof, said plate operating as a brake on the rotating gas, whereby the rotation of the gas in the neighborhood of said plate is considerably reduced, so that near said plate a smaller radial pressure gradient is produced and within the rotor local pressure differences occur which produce the desired whirl. All these means require special devices either for the production of a temperature gradient or for the supply of mixture and for the discharge of the separated components thereof, such devices being complicated and requiring measures difficult to realize.
  • the invention has for its object to provide a simple construction which is also adapted to produce the desired gas whirl and permits a simple supply of mixture and also a simple discharge of the components of said mixture.
  • the rotor is open at one of its ends and the separating chamber thereof is bounded at said open end by the stationary wall of said casing.
  • the wall of the casing acts as the stationary friction wall on the charge of the rotor, whereby the pressure ditferences required for the generation of the gas whirl are produced.
  • the generation of the whirl is facilitated, when the cylindrical wall of the rotor is bent towards the axis of the rotor in a marginal portion adjacent the open end of the rotor.
  • the part of the casing wall bounding the separating chamber at the open end of the rotor may be given a shape adapted to the suitable shape of the whirl by means of a special profile, e.g., the shape of an annular recess.
  • the portion of the casing wall bounding the separating chamber at the open end of the rotor may be provided with apertures.
  • the other end of the rotor may be closed by an end wall having apertures, through which the other component of the gaseous mixture may be discharged from the rotor. It is also possible to close the latter end of the rotor at some distance from the end of the cylindrical wall by a plate provided with apertures and to bend the marginal portion of the cylindrical wall of the rotor extending beyond said plate towards the axis of revolution.
  • a stationary discharge conduit or stripping tube may be so arranged as to open within the space bounded by said marginal wall portion.
  • FIG. 1 is an elevational sectional view of a centrifuge according to the invention
  • FIG. 2 is an elevational sectional view of a part of a centrifuge according to FIG. 1, having a slightly different upper part, and
  • FIG. 3 is an elevational sectional view of a part of a centrifuge according to FIG. 1 having a somewhat different lower part of the rotor.
  • a closed casing having a hollow cavity 2.
  • a rotor 3 which rests with a pintle 4 in a socket (not shown) provided in a block 5.
  • the rotor 3 is kept in a vertical position by an annular permanent magnet 6 attached to the upper part of the rotor and by a ring 7 of magnetic material mounted in the casing. Said ring may also be a permanent magnet.
  • the mixture to be separated e.g., a gas mixture or a mixture of gaseous isotopes, is supplied through a stationary tube 8 which extends into the rotor 3. It is of only slight importance and the invention is not concerned with the location at which the tube 8 opens in the rotor 2.
  • the upper end of the rotor is open and the separating chamber of the rotor is bounded at said end by a stationary Wall part 9 of the casing 1.
  • a screw-seal operating according to the principle of Holwecks molecular pump is designated by 10, said seal separating the upper part 11 of the space within the casing 1 from the space 2.
  • the wall 9 is provided with apertures or a gap 12, through which one of the components of the mixture to be separated may be led towards a chamber 13, from which it is discharged at 14.
  • a plate 15 provided with apertures 16 is mounted in the rotor.
  • the pintle 4 is fixed to said plate.
  • the end portion 17 of the rotor extending beyond the plate 15 is bent towards the axis of revolution.
  • stationary strip tubes 18 open, which are connected to a discharge tube 19.
  • the second component of the mixture is discharged through the latter tube.
  • the motor for driving the rotor is designated by 20 and 21.
  • FIG. 3 the lower end of the rotor is closed and provided with apertures 22. These apertures lead the relevant component of the mixture from the rotor into a chamber 23 separated from the space 2 by a screw-seal 24 operating in the manner of Holwecks molecular pump. Said component is discharged from the chamber 23 through a tube 25.
  • a gas whirl 26 improving the separating action of the centrifuge is produced and maintained by the braking operation of the stationary separating plate or body 9, 9a.
  • the separating plate has a braking influence on the revolving gas such that adjacent the plate the centrifugal force on the gas will be less than at greater distances from the plate so that there will be created an axially directed pressure gradient which will generate a gas whirl in the shape of a torus which is concentric with respect to the axis of revolution of the drum. Due to the plate the gas near the wall of the drum will flow towards the plate, while the gas near the axis of the drum will flow away from the plate.
  • the central supply of the mixture through the tube 8 also has a favorable action on said whirl due to the momentum of the mixture.
  • the curved shape of the upper boundary of the separating chamber of the rotor is better adapted to the shape of the whirl 26 than the plane shape thereof shown in FIG. 1.
  • An ultracentrifuge for the continuous separation of a gas mixture into light and heavy fractions comprising a stationary housing, a tubular elongated rotor drum having opposite ends one of which is open over substantially the entire cross-section of the drum while the other of the ends is a closed end, means supportingthe drum within said housing for rotation about a vertical axis with the open end of the drum facin-g upwardly, means for supplying the mixture to be separated into said drum, said stationary housing including a portion bounding said open end of the drum to close the same and exert a braking force on gas within the drum to create an axial gas whirl within the drum whereby the lighter fractions are accumulated at the lower end 25 gether with the inwardly curved portion of the drum defines a smooth inner curved surface at the upper end of the drum and means at said closed lower end of the drum for the discharge of the gas fraction accumulated thereat.

Description

Nov. 23, 1965 J. LOS ETAL 3,219,265
CENTRIFUGES, E.G. ULTRACENTRIFUGES FOR THE SEPARATION OF GASES Filed March 14, 1961 FIG.1 FIG.3
United States Patent 3,219,265 CENTRIFUGES, e.g., ULTRACENTRIFUGES FQR THE SEPARATION OF GASES Johannes Los and Fridtjof Kelling, Amsterdam, Netherlands, assignors to Reactor Centrurn Nederland, The Hague, Netherlands Filed Mar. 14, 1961, Ser. No. 95,683
, Claims priority, application Netherlands, Mar. 17, N60,
249,508 1 Claim. 01. 233-27 The invention relates to centrifuges and more particularly to ultracentrifuge for the separation of gas mix- 7 tures or mixtures of gaseous isotopes.
The centrifuges comprise a rotor mounted for rotation in a casing and means for the generation in the separating chamber of the rotor of a gas whirl transversely directed to the rotation.
The separating action of a gas centrifuge is very much improved, when in the rotor a gas whirl is produced, which is directed transversely to the rotation. For the generation of said gas whirl various means are known. A first means causes a temperature difference between the ends of the rotor. Another means uses the momentum of the mixture supplied to the rotor and the way in which the components of the mixture are discharged. According to a third means a stationary plate is placed within the closed rotor near one end thereof, said plate operating as a brake on the rotating gas, whereby the rotation of the gas in the neighborhood of said plate is considerably reduced, so that near said plate a smaller radial pressure gradient is produced and within the rotor local pressure differences occur which produce the desired whirl. All these means require special devices either for the production of a temperature gradient or for the supply of mixture and for the discharge of the separated components thereof, such devices being complicated and requiring measures difficult to realize.
The invention has for its object to provide a simple construction which is also adapted to produce the desired gas whirl and permits a simple supply of mixture and also a simple discharge of the components of said mixture. According to the invention the rotor is open at one of its ends and the separating chamber thereof is bounded at said open end by the stationary wall of said casing. In this case the wall of the casing acts as the stationary friction wall on the charge of the rotor, whereby the pressure ditferences required for the generation of the gas whirl are produced.
The generation of the whirl is facilitated, when the cylindrical wall of the rotor is bent towards the axis of the rotor in a marginal portion adjacent the open end of the rotor. Also the part of the casing wall bounding the separating chamber at the open end of the rotor may be given a shape adapted to the suitable shape of the whirl by means of a special profile, e.g., the shape of an annular recess.
For the discharge of one of the components of the gaseous mixture the portion of the casing wall bounding the separating chamber at the open end of the rotor may be provided with apertures.
The other end of the rotor may be closed by an end wall having apertures, through which the other component of the gaseous mixture may be discharged from the rotor. It is also possible to close the latter end of the rotor at some distance from the end of the cylindrical wall by a plate provided with apertures and to bend the marginal portion of the cylindrical wall of the rotor extending beyond said plate towards the axis of revolution. A stationary discharge conduit or stripping tube may be so arranged as to open within the space bounded by said marginal wall portion.
Patented Nov. 23, 1965 For the elucidation of the invention reference is made to the accompanying drawing, therein:
FIG. 1 is an elevational sectional view of a centrifuge according to the invention,
FIG. 2 is an elevational sectional view of a part of a centrifuge according to FIG. 1, having a slightly different upper part, and
FIG. 3 is an elevational sectional view of a part of a centrifuge according to FIG. 1 having a somewhat different lower part of the rotor.
In the drawing 1 is a closed casing, having a hollow cavity 2. Mounted for rotation centrally in said casing is a rotor 3 which rests with a pintle 4 in a socket (not shown) provided in a block 5. The rotor 3 is kept in a vertical position by an annular permanent magnet 6 attached to the upper part of the rotor and by a ring 7 of magnetic material mounted in the casing. Said ring may also be a permanent magnet. The mixture to be separated, e.g., a gas mixture or a mixture of gaseous isotopes, is supplied through a stationary tube 8 which extends into the rotor 3. It is of only slight importance and the invention is not concerned with the location at which the tube 8 opens in the rotor 2.
According to the invention the upper end of the rotor is open and the separating chamber of the rotor is bounded at said end by a stationary Wall part 9 of the casing 1. A screw-seal operating according to the principle of Holwecks molecular pump is designated by 10, said seal separating the upper part 11 of the space within the casing 1 from the space 2. The wall 9 is provided with apertures or a gap 12, through which one of the components of the mixture to be separated may be led towards a chamber 13, from which it is discharged at 14.
Near the lower end of the rotor a plate 15 provided with apertures 16 is mounted in the rotor. The pintle 4 is fixed to said plate. The end portion 17 of the rotor extending beyond the plate 15 is bent towards the axis of revolution. In the annular space bounded by the bent portion 17 and the plate 15 stationary strip tubes 18 open, which are connected to a discharge tube 19. The second component of the mixture is discharged through the latter tube. The motor for driving the rotor is designated by 20 and 21.
The difference between the embodiment illustrated in FIG. 2 and that according to FIG. 1 is that the upper part of the cylindrical rotor wall is bent towards the axis of revolution and the wall 9a has a predetermined profile which in the drawing is curved.
In FIG. 3 the lower end of the rotor is closed and provided with apertures 22. These apertures lead the relevant component of the mixture from the rotor into a chamber 23 separated from the space 2 by a screw-seal 24 operating in the manner of Holwecks molecular pump. Said component is discharged from the chamber 23 through a tube 25.
In each of the illustrated centrifuge drums, a gas whirl 26 improving the separating action of the centrifuge is produced and maintained by the braking operation of the stationary separating plate or body 9, 9a. The separating plate has a braking influence on the revolving gas such that adjacent the plate the centrifugal force on the gas will be less than at greater distances from the plate so that there will be created an axially directed pressure gradient which will generate a gas whirl in the shape of a torus which is concentric with respect to the axis of revolution of the drum. Due to the plate the gas near the wall of the drum will flow towards the plate, while the gas near the axis of the drum will flow away from the plate. As a result of the diffusion of the gas molecules dhe to the centrifugal force, the axial gas flow towards the braking plate will become gradually heavier and the axial gas '2) flow away from the plate will become gradually lighter. Consequently, the heavier gas components will be discharged at the upper end of the drum adjacent plate 9, 9a, and the lighter components will be discharged at the lower end of the drum. The central supply of the mixture through the tube 8 also has a favorable action on said whirl due to the momentum of the mixture. The curved shape of the upper boundary of the separating chamber of the rotor is better adapted to the shape of the whirl 26 than the plane shape thereof shown in FIG. 1.
What we claim is:
An ultracentrifuge for the continuous separation of a gas mixture into light and heavy fractions, said ultracentrifuge comprising a stationary housing, a tubular elongated rotor drum having opposite ends one of which is open over substantially the entire cross-section of the drum while the other of the ends is a closed end, means supportingthe drum within said housing for rotation about a vertical axis with the open end of the drum facin-g upwardly, means for supplying the mixture to be separated into said drum, said stationary housing including a portion bounding said open end of the drum to close the same and exert a braking force on gas within the drum to create an axial gas whirl within the drum whereby the lighter fractions are accumulated at the lower end 25 gether with the inwardly curved portion of the drum defines a smooth inner curved surface at the upper end of the drum and means at said closed lower end of the drum for the discharge of the gas fraction accumulated thereat.
References Cited by the Examiner UNITED STATES PATENTS 533,316 1/1895 Naylor 233-46 X 1,061,656 5/1913 Black 233-28 X 2,228,816 1/1941 Doran 233-21 2,553,936 5/1951 Patrick 233-46 X 2,563,550 8/1951 Quist 233-21 1 2,733,857 2/1956 Beams 23324 3,108,955 10/1963 Boyland 23324 X FOREIGN PATENTS 572,830 11/1958 Belgium. 1,224,098 2/1960 France.
833,487 3/1952 Germany.
87,740 3/ 1958 Netherlands. 156,091 9/1956 Sweden.
OTHER REFERENCES Beams: The Ultracentrifuge, published in Science in Progress, second series, pages 232-264, copyright 1940, by Yale University Press. A copy can be found in the Scientific Library or in Division 32, Class 233/1 (publications).
M. CARY NELSON, Primary Examiner.
HERBERT L. MARTIN, HARRY B. THORNTON,
Examiners.
US95683A 1960-03-17 1961-03-14 Centrifuges, e.g., ultracentrifuges for the separation of gases Expired - Lifetime US3219265A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3282035A (en) * 1963-12-30 1966-11-01 Steinberg Robert Molecular beam velocity selector
US3780937A (en) * 1970-02-27 1973-12-25 Tokyo Shibaura Electric Co Centrifugal gas separator with electric motor drive
US3902657A (en) * 1972-05-19 1975-09-02 Stichting Reactor Centrum Centrifugal separator for cryogenic gaseous mixtures
US4182480A (en) * 1976-06-28 1980-01-08 Ultra Centrifuge Nederland N.V. Centrifuge for separating helium from natural gas
CN107138293A (en) * 2017-06-30 2017-09-08 吴素贞 A kind of teaching experiment centrifuge

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB964169A (en) * 1963-06-21 1964-07-15 Shell Int Research Apparatus for separating gas and liquid from a gas/liquid mixture
FR2182586B1 (en) * 1972-01-19 1979-08-10 Commissariat Energie Atomique
JPS517859B2 (en) * 1973-01-20 1976-03-11

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Publication number Priority date Publication date Assignee Title
BE572830A (en) * 1957-11-14
NL87740C (en) *
US533316A (en) * 1895-01-29 Fruit-juice extractor
US1061656A (en) * 1906-02-19 1913-05-13 Joseph L Black Separator for mechanical mixtures of gases.
US2228816A (en) * 1939-01-05 1941-01-14 Gen Electric Apparatus for separating fluids
US2553936A (en) * 1948-07-02 1951-05-22 Ben F Patrick Reclaiming machine
US2563550A (en) * 1951-08-07 Gaseous fluid centrifuge
DE833487C (en) * 1939-06-18 1952-03-10 Linde Eismasch Ag Method and device for the separation of gas and liquid mixtures in centrifuges
US2733857A (en) * 1956-02-07 beams
FR1224098A (en) * 1957-12-27 1960-06-22 Reactor Centrum Nederland Ultracentrifuge for continuous separation of a two-component gas mixture
US3108955A (en) * 1947-02-26 1963-10-29 Gen Electric Co Ltd Hollow rotors and centrifuges

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Publication number Priority date Publication date Assignee Title
DE157674C (en) *
AT211288B (en) * 1957-11-28 1960-09-26 Degussa Gas centrifuge

Patent Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL87740C (en) *
US533316A (en) * 1895-01-29 Fruit-juice extractor
US2563550A (en) * 1951-08-07 Gaseous fluid centrifuge
US2733857A (en) * 1956-02-07 beams
US1061656A (en) * 1906-02-19 1913-05-13 Joseph L Black Separator for mechanical mixtures of gases.
US2228816A (en) * 1939-01-05 1941-01-14 Gen Electric Apparatus for separating fluids
DE833487C (en) * 1939-06-18 1952-03-10 Linde Eismasch Ag Method and device for the separation of gas and liquid mixtures in centrifuges
US3108955A (en) * 1947-02-26 1963-10-29 Gen Electric Co Ltd Hollow rotors and centrifuges
US2553936A (en) * 1948-07-02 1951-05-22 Ben F Patrick Reclaiming machine
BE572830A (en) * 1957-11-14
FR1224098A (en) * 1957-12-27 1960-06-22 Reactor Centrum Nederland Ultracentrifuge for continuous separation of a two-component gas mixture

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3282035A (en) * 1963-12-30 1966-11-01 Steinberg Robert Molecular beam velocity selector
US3780937A (en) * 1970-02-27 1973-12-25 Tokyo Shibaura Electric Co Centrifugal gas separator with electric motor drive
US3902657A (en) * 1972-05-19 1975-09-02 Stichting Reactor Centrum Centrifugal separator for cryogenic gaseous mixtures
US4182480A (en) * 1976-06-28 1980-01-08 Ultra Centrifuge Nederland N.V. Centrifuge for separating helium from natural gas
CN107138293A (en) * 2017-06-30 2017-09-08 吴素贞 A kind of teaching experiment centrifuge

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GB921350A (en) 1963-03-20
CH381647A (en) 1964-09-15
NL103433C (en)
DK103284C (en) 1965-12-06
NL249508A (en)

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