US2792122A - Filtering device for use in the spinning of synthetic linear polymers - Google Patents
Filtering device for use in the spinning of synthetic linear polymers Download PDFInfo
- Publication number
- US2792122A US2792122A US342698A US34269853A US2792122A US 2792122 A US2792122 A US 2792122A US 342698 A US342698 A US 342698A US 34269853 A US34269853 A US 34269853A US 2792122 A US2792122 A US 2792122A
- Authority
- US
- United States
- Prior art keywords
- filter
- spinning
- plates
- opposite faces
- polymer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 229920000642 polymer Polymers 0.000 title claims description 26
- 238000009987 spinning Methods 0.000 title claims description 13
- 238000001914 filtration Methods 0.000 title description 5
- 239000007788 liquid Substances 0.000 claims description 7
- 239000000155 melt Substances 0.000 claims description 3
- 230000000694 effects Effects 0.000 claims description 2
- 230000002093 peripheral effect Effects 0.000 claims description 2
- 230000007423 decrease Effects 0.000 description 4
- 239000012535 impurity Substances 0.000 description 4
- 239000002184 metal Substances 0.000 description 3
- 239000007789 gas Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000004576 sand Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 229910000669 Chrome steel Inorganic materials 0.000 description 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- 239000004952 Polyamide Substances 0.000 description 1
- 239000004020 conductor Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 239000011810 insulating material Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 229920002647 polyamide Polymers 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 238000007669 thermal treatment Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Images
Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D1/00—Treatment of filament-forming or like material
- D01D1/10—Filtering or de-aerating the spinning solution or melt
- D01D1/106—Filtering
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/01—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with flat filtering elements
- B01D29/03—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with flat filtering elements self-supporting
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/44—Edge filtering elements, i.e. using contiguous impervious surfaces
- B01D29/46—Edge filtering elements, i.e. using contiguous impervious surfaces of flat, stacked bodies
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/50—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition
- B01D29/56—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition in series connection
- B01D29/58—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition in series connection arranged concentrically or coaxially
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2201/00—Details relating to filtering apparatus
- B01D2201/18—Filters characterised by the openings or pores
- B01D2201/184—Special form, dimension of the openings, pores of the filtering elements
Definitions
- the invention relates to a filtering device to be employed in the spinning of synthetic linear polymers from the melt.
- such spinning is efiected by extruding the molten polymer at a controlled rate through a suitable spinning nozzle. It is also known that it is necessary to place a suitable filter ahead of the spinning nozzle. Filters of various types are known such as filters consisting of stacks of nets having an increasing fine mesh towards the spinneret, or consisting of sand layers with a grain size that decreases in the same direction, with the sand being retained above the spinneret by nets.
- the filters according to the present invention accomplish with complete efiiciency both the above tasks.
- they comprise aseries of metal plates provided with through bores and grooves which, when the plates are juxtaposed define a plurality of narrow capillary channels which force the molten polymer to follow a sufficiently tortuous path in passing through said series of plates and which at the same time retain not only the solid impurities but also the gaseous bubbles, this being due-it is rbelievedto surface tension phenomena.
- the metal plates should preferably be made of a material that may be washed each time the filter becomes exhausted whereby it may then be re-used. Since this Washing is conveniently effected by means of nitric acid, in particular when the polymer to be filtered is a polyamide, it is convenient to make the plates of stainless steel, for example nickel-chrome steels.
- the dimensions of the bores and channels are naturally related to their shapes and to the characteristics of the polymer.
- Fig. 1 is a cross-sectional view and partly an elevational view of a filter according to an embodiment
- Fig. 2 is a plan view of an individual plate of the filter shown in Fig. 1;
- Fig. 3 is a cross-sectional view of the plate shown in Fig. 2.
- the numeral 10 denotes a casing which serves as a support for the filter to which the polymer is fed from conduit 18 and is provided with an outlet opening 13 for the filtered polymer.
- Bolts 11 and 12 lock the superimposed plates tightly against ring 19, and opening 13' thereof defines the inlet opening for the polymer to be filtered.
- the various plates are indicated by numeral 14, and one of the plates shown in Figs. 2 and 3.
- the plates are provided .with through bores 15 having a diameter of about 0.20 to 0.5 mm. and about 5 to 7 mm. long. Bores 15 are arranged along several concentric circles, as it is clearly seen in Fig. 2. Corresponding to each circle, there is a preferably semi-circular or like groove 16 which connects the entrances or the exits of all the through bores that are located on the same circle.
- the polymer which enters from conduit 18, after having passed through the bores 16 of the first plate, will have to flow along shorter or longer portions of the substantially circular capillary channels 17 defined by the grooves 16 of the lower face of the first plate and the corresponding grooves of the upper face of the second plate. Thereafter the polymer will cross the through bore of the second plate and so on.
- the diameters of the through bores are not the same for all plates, but decrease towards the spinneret.
- the plate adjacent the spinneret may have 0.20 mm. bores the immediately preceding plate 0.25 mm. bores and so on.
- the number of the bores depends on the amount of polymer spun in a unit of time.
- the dimensions of grooves 16 and therefore of channels 17 may also decrease in a like manner towards the spinneret.
- a filter of this type is perfectly effective for retaining both the impurities and the gaseous bubbles.
- Another advantage of this filter is that it is made of a material that is a good heat conductor and that may be heated by conduction and that at any rate is excellently adapted to keep the temperature of the polymer and therefore the spinning viscosity at the desired level. This makes it possible to avoid the excessively severe thermal treatments which were necessary to bring the polymer to such a temperature as to cause it to reach the spinneret while still having the required fluidity even after passing through filters made of insulating materials.
- Spinning filter for use in the spinning of synthetic linear polymers from the melt, comprising a casing having an inlet opening for the liquid polymer to be filtered and an outlet opening for the filtered liquid polymer, the centers of said inlet and outlet openings defining a general axis of the filter, a plurality of metal plates having each a cylindrical peripheral surface and two plane parallel opposite faces, said plates being assembled within said casing coaxilly with and perpendicularly to said general axis of the filter and with their parallel opposite faces in juxtaposed contacting relationship, said parallel opposite faces being sufiiciently smooth to effect a seal against the liquid polymer when in contact with one another, said plates being further provided with through bore disposed along concentric circles centered about said general axis of the filter and having circular grooves on their parallel opposite faces, each groove connecting the openings of those of said through bores being disposed on the same one of said concentric circles, and locking means tightly holding said plates within said casing in the aforementioned assembled relationship the through bores of adjacent plates being staggered 3
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Textile Engineering (AREA)
- Spinning Methods And Devices For Manufacturing Artificial Fibers (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
IT735788X | 1952-03-28 |
Publications (1)
Publication Number | Publication Date |
---|---|
US2792122A true US2792122A (en) | 1957-05-14 |
Family
ID=11315330
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US342698A Expired - Lifetime US2792122A (en) | 1952-03-28 | 1953-03-16 | Filtering device for use in the spinning of synthetic linear polymers |
Country Status (4)
Country | Link |
---|---|
US (1) | US2792122A (cs) |
FR (1) | FR1072897A (cs) |
GB (1) | GB735788A (cs) |
NL (2) | NL177215B (cs) |
Cited By (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2923970A (en) * | 1960-02-09 | genovese | ||
US2999274A (en) * | 1958-04-14 | 1961-09-12 | Phillips Petroleum Co | Dispersing solid additives in plastics |
US3050774A (en) * | 1957-09-03 | 1962-08-28 | Du Pont | Spinneret assembly |
US3245113A (en) * | 1963-06-10 | 1966-04-12 | American Cyanamid Co | Apparatus for forming multi-component fibers |
US3320633A (en) * | 1965-08-25 | 1967-05-23 | Du Pont | Apparatus for forming two component yarns |
US3407437A (en) * | 1965-07-15 | 1968-10-29 | Barmag Barmer Maschf | Spinning head for high pressure melt spinning |
US3516119A (en) * | 1967-05-22 | 1970-06-23 | Vickers Zimmer Ag | Spinning device |
US3737036A (en) * | 1970-08-26 | 1973-06-05 | Bendix Corp | Filter for polymer processing and method of manufacture |
FR2345286A1 (fr) * | 1976-03-24 | 1977-10-21 | Gellert Jobst | Filtre de moulage par injection |
US4061462A (en) * | 1974-06-17 | 1977-12-06 | Montedison S.P.A. | Apparatus for extruding thermoplastic material |
US4728502A (en) * | 1984-05-02 | 1988-03-01 | Hamill Brendan J | Apparatus for the chemical synthesis of oligonucleotides |
US4918807A (en) * | 1988-10-19 | 1990-04-24 | A. Ahlstrom Corporation | Screen and method of manufacture |
DE19643425C2 (de) * | 1996-10-22 | 1999-12-02 | Geb Schroeder Beeck | Sandlose Spinndüse |
US6033609A (en) * | 1997-10-28 | 2000-03-07 | Basf Corporation | Device and method to prevent spinneret hole contamination |
US20220203272A1 (en) * | 2020-12-29 | 2022-06-30 | Metal Industries Research & Development Centre | Tangential flow filtration module and tangential flow filtration assembly |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2971219A (en) * | 1956-08-14 | 1961-02-14 | Du Pont | Mixer distribution plate |
Citations (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE257144C (cs) * | ||||
US1262317A (en) * | 1917-11-12 | 1918-04-09 | John H V Finney | Carbureter attachment. |
US1456438A (en) * | 1922-07-28 | 1923-05-22 | Hesselman Knut Jonas Elias | Liquid filter |
FR666474A (fr) * | 1928-12-28 | 1929-10-02 | Régulateur-filtre pour carburateur d'automobile | |
GB324034A (en) * | 1928-10-13 | 1930-01-13 | Albert Schrempp | Improved filter device |
US1788412A (en) * | 1922-01-24 | 1931-01-13 | Sperry Dev Co | Oil engine |
US1983330A (en) * | 1928-07-06 | 1934-12-04 | Celanese Corp | Manufacture of artificial filaments, threads, films, or the like |
US2266363A (en) * | 1938-11-10 | 1941-12-16 | Du Pont | Apparatus for the production of filaments |
US2266368A (en) * | 1938-11-10 | 1941-12-16 | Du Pont | Apparatus for the production of artificial structures |
US2284787A (en) * | 1938-04-08 | 1942-06-02 | Winkler Jack | Filter |
US2345014A (en) * | 1941-10-20 | 1944-03-28 | Stamsvik Mfg Corp | Filtration unit |
US2449809A (en) * | 1939-01-12 | 1948-09-21 | Johnson & Johnson | Corrugated disk filter |
US2507355A (en) * | 1946-01-17 | 1950-05-09 | Sola Giuseppe | Filter for injectors for combustion engines |
-
0
- NL NL96182D patent/NL96182C/xx active
- NL NLAANVRAGE7210499,A patent/NL177215B/xx unknown
-
1953
- 1953-03-12 FR FR1072897D patent/FR1072897A/fr not_active Expired
- 1953-03-16 GB GB7240/53A patent/GB735788A/en not_active Expired
- 1953-03-16 US US342698A patent/US2792122A/en not_active Expired - Lifetime
Patent Citations (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE257144C (cs) * | ||||
US1262317A (en) * | 1917-11-12 | 1918-04-09 | John H V Finney | Carbureter attachment. |
US1788412A (en) * | 1922-01-24 | 1931-01-13 | Sperry Dev Co | Oil engine |
US1456438A (en) * | 1922-07-28 | 1923-05-22 | Hesselman Knut Jonas Elias | Liquid filter |
US1983330A (en) * | 1928-07-06 | 1934-12-04 | Celanese Corp | Manufacture of artificial filaments, threads, films, or the like |
GB324034A (en) * | 1928-10-13 | 1930-01-13 | Albert Schrempp | Improved filter device |
FR666474A (fr) * | 1928-12-28 | 1929-10-02 | Régulateur-filtre pour carburateur d'automobile | |
US2284787A (en) * | 1938-04-08 | 1942-06-02 | Winkler Jack | Filter |
US2266363A (en) * | 1938-11-10 | 1941-12-16 | Du Pont | Apparatus for the production of filaments |
US2266368A (en) * | 1938-11-10 | 1941-12-16 | Du Pont | Apparatus for the production of artificial structures |
US2449809A (en) * | 1939-01-12 | 1948-09-21 | Johnson & Johnson | Corrugated disk filter |
US2345014A (en) * | 1941-10-20 | 1944-03-28 | Stamsvik Mfg Corp | Filtration unit |
US2507355A (en) * | 1946-01-17 | 1950-05-09 | Sola Giuseppe | Filter for injectors for combustion engines |
Cited By (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2923970A (en) * | 1960-02-09 | genovese | ||
US3050774A (en) * | 1957-09-03 | 1962-08-28 | Du Pont | Spinneret assembly |
US2999274A (en) * | 1958-04-14 | 1961-09-12 | Phillips Petroleum Co | Dispersing solid additives in plastics |
US3245113A (en) * | 1963-06-10 | 1966-04-12 | American Cyanamid Co | Apparatus for forming multi-component fibers |
US3407437A (en) * | 1965-07-15 | 1968-10-29 | Barmag Barmer Maschf | Spinning head for high pressure melt spinning |
US3320633A (en) * | 1965-08-25 | 1967-05-23 | Du Pont | Apparatus for forming two component yarns |
US3516119A (en) * | 1967-05-22 | 1970-06-23 | Vickers Zimmer Ag | Spinning device |
US3737036A (en) * | 1970-08-26 | 1973-06-05 | Bendix Corp | Filter for polymer processing and method of manufacture |
US4061462A (en) * | 1974-06-17 | 1977-12-06 | Montedison S.P.A. | Apparatus for extruding thermoplastic material |
FR2345286A1 (fr) * | 1976-03-24 | 1977-10-21 | Gellert Jobst | Filtre de moulage par injection |
US4728502A (en) * | 1984-05-02 | 1988-03-01 | Hamill Brendan J | Apparatus for the chemical synthesis of oligonucleotides |
US4918807A (en) * | 1988-10-19 | 1990-04-24 | A. Ahlstrom Corporation | Screen and method of manufacture |
DE19643425C2 (de) * | 1996-10-22 | 1999-12-02 | Geb Schroeder Beeck | Sandlose Spinndüse |
US6033609A (en) * | 1997-10-28 | 2000-03-07 | Basf Corporation | Device and method to prevent spinneret hole contamination |
US20220203272A1 (en) * | 2020-12-29 | 2022-06-30 | Metal Industries Research & Development Centre | Tangential flow filtration module and tangential flow filtration assembly |
US11684874B2 (en) * | 2020-12-29 | 2023-06-27 | Metal Industries Research & Development Centre | Tangential flow filtration module and tangential flow filtration assembly |
Also Published As
Publication number | Publication date |
---|---|
GB735788A (en) | 1955-08-31 |
FR1072897A (fr) | 1954-09-16 |
NL177215B (nl) | |
NL96182C (cs) |
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