US20130045322A1 - Edible oil composition - Google Patents

Edible oil composition Download PDF

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Publication number
US20130045322A1
US20130045322A1 US13/695,125 US201113695125A US2013045322A1 US 20130045322 A1 US20130045322 A1 US 20130045322A1 US 201113695125 A US201113695125 A US 201113695125A US 2013045322 A1 US2013045322 A1 US 2013045322A1
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US
United States
Prior art keywords
composition
oil
fat
fat particles
food product
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
US13/695,125
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English (en)
Inventor
Frank Emile Wubbolts
Lucia Izquierdo
Erik Johan Anton Schweitzer
Hangkam Man
Cynthia Akkermans
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Loders Croklaan BV
Feyecon Development and Implementation BV
Original Assignee
Loders Croklaan BV
Feyecon Development and Implementation BV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Loders Croklaan BV, Feyecon Development and Implementation BV filed Critical Loders Croklaan BV
Publication of US20130045322A1 publication Critical patent/US20130045322A1/en
Assigned to FEYECON DEVELOPMENT & IMPLEMENTATION B.V. reassignment FEYECON DEVELOPMENT & IMPLEMENTATION B.V. ASSIGNMENT OF ASSIGNORS INTEREST (SEE DOCUMENT FOR DETAILS). Assignors: AKKERMANS, CYNTHIA, IZQUIERDO, LUCIA, WUBBOLTS, FRANK EMILE
Assigned to LODERS CROKLAAN B.V. reassignment LODERS CROKLAAN B.V. ASSIGNMENT OF ASSIGNORS INTEREST (SEE DOCUMENT FOR DETAILS). Assignors: MAN, HANGKAM, Schweitzer, Erik Johan Anton
Abandoned legal-status Critical Current

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Classifications

    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
    • A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
    • A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
    • A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
    • A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
    • A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
    • A23D9/04—Working-up
    • A23D9/05—Forming free-flowing pieces

Definitions

  • This invention relates to an edible oil composition, to a method for its preparation and to a method of making a food product using the composition.
  • Oils and fats are important components of many food products and they can contribute structure, texture and flavour to the products as well as acting as a source of energy. Often, food products that contain liquid oils also contain a structuring agent. Structuring agents are generally fats that are solid at room temperature (20° C.) and that provides structure to the oil phase.
  • WO 2009/090416 discloses a confectionery water-in-oil emulsion comprising a fat phase; an emulsifier; and an aqueous phase; wherein the fat phase comprises a first fat, such as cocoa butter, that can exist in more than one crystal form, present substantially in a single crystal form having a first melting point; and a second fat, such as palm oil, having a second melting point lower than the first melting point.
  • a first fat such as cocoa butter
  • a second fat such as palm oil
  • U.S. Pat. No. 5,858,445 describes a margarine fat blend comprising 5 to 14% of a structuring agent, also termed a hardstock.
  • the hardstock is a stearin fraction of an interesterified mixture of 25 to 65% unhardened lauric fat stearin and 75 to 35% unhardened C16+ fat stearin.
  • EP-A-1795257 describes a method of stabilising an edible dispersion comprising oil using a micronized fat powder.
  • the micronized fat powder acts as a structuring agent.
  • WO 2010/053360 describes a dispersion of a structuring agent.
  • the present invention provides a method of preparing an edible oil composition, suitable for use in the preparation of a food product, comprising mixing from 1% to 15% by weight of fat particles with a liquid oil and storing the resulting composition for up to 10 weeks, wherein the mixing and storing conditions provide the composition in a form after storage that is pourable.
  • the invention provides a pourable edible oil composition, suitable for use in the preparation of a food product, comprising from 1% to 15% by weight of fat particles dispersed in a liquid oil, having a pourability of from 0.2 to 0.6 cm/g and/or a viscosity of less than 30,000 cP as determined using a Brookfield viscometer after 10 seconds using a spindle S-64, at a speed of 1.5 rpm.
  • Yet another aspect of the invention is a method of making a food product comprising mixing the edible oil composition of the invention with one or more additional edible components.
  • a further aspect of the invention is the use of the edible oil composition of the invention in the manufacture of a food product.
  • the method of the invention provides a dispersion or suspension of a structuring agent in a liquid oil that remains pourable.
  • the composition after storage has a pourability of from 0.2 to 0.6 cm/g, more preferably from 0.30 to 0.55 cm/g, as determined by the method described in the examples section below.
  • the pourability of the composition after storage may be defined in other ways, for example, the composition after storage preferably has a viscosity of less than 30,000 cP as determined using a Brookfield viscometer after 10 seconds using a spindle S-64, at a speed of 1.5 rpm.
  • the fat is in the solid state (or substantially in the solid state) in the edible oil composition of the invention.
  • the fat may be any edible fat that is solid at 20° C. and is capable of acting as a structuring agent in a food product.
  • the fat is: a cocoa butter equivalent (CBE) (such as shea stearin); or cocoa butter; or palm oil stearin.
  • CBE cocoa butter equivalent
  • the liquid oil may be any liquid oil (i.e., an oil that is liquid at 20° C.) containing triglycerides that is useful in a food product.
  • suitable liquid oils include soybean oil, rapeseed oil, sunflower oil, safflower oil, corn oil and mixtures thereof. Sunflower oil and safflower oil, and their mixtures, are particularly preferred
  • the liquid oil comprises sunflower oil.
  • the fat particles are micronized fat.
  • the fat particles may be produced by a method which comprises spraying a mixture of liquid fat containing a gas in a liquefied or supercritical state. Suitable methods are disclosed in EP-A-1795257 and in WO 2010/053360.
  • the fat particles may be produced by a method comprising: providing the fat in the liquid state together with a gas in a liquefied or supercritical state, and optionally water, at elevated pressure; and spraying the mixture to a lower pressure to form the fat particles.
  • the fat particles are produced in the solid state and this may require cooling.
  • the fat particles are not produced by a method comprising: providing the fat in the liquid state together with a gas in a liquefied or supercritical state, and water, at elevated pressure; and spraying the mixture to a lower pressure to form the fat particles.
  • the fat particles preferably have at least one dimension of less than 1 ⁇ m.
  • the fat particles may be in the form of platelets or having a thickness of less than 1 ⁇ m, such as from 0.01 to 0.5 ⁇ m or bubbles having a wall thickness of less than 1 ⁇ m, such as from 0.01 to 0.5 ⁇ m.
  • At least 95% of the fat particles have at least one dimension of less than 1 ⁇ m.
  • at least 95% of the fat particles may be in the form of platelets having a thickness of less than 1 ⁇ m, such as from 0.01 to 0.5 ⁇ m or bubbles having a wall thickness of less than 1 ⁇ m, such as from 0.01 to 0.5 ⁇ m.
  • the fat particles and the liquid oil are mixed under low shear.
  • the fat particles and the liquid oil are mixed at a temperature of from 5° C. to 40° C., more preferably from 10° C. to 30° C.
  • the composition is stored at a temperature of from 6° C. to 35° C., more preferably from 10° C. to 30° C.
  • the composition is stored for up to 10 weeks, for example from 1 day to 8 weeks or from 2 days to 6 weeks, such as from 2 days to 3 weeks.
  • the composition is subjected to continuous or intermittent stirring during storage as this has been found to be beneficial to stability on storage.
  • compositions may be stored at a higher temperature than the mixing temperature.
  • the fat particles are present in the edible oil composition in an amount of from 1 to 15% by weight, preferably from 2 to 13% by weight, such as from 5 to 12% or from 6 to 11% by weight.
  • the composition that is produced by the method of the invention is a pourable edible oil composition, suitable for use in the preparation of a food product, comprising from 1% to 15% by weight of fat particles dispersed in a liquid oil, having a pourability of from 0.2 to 0.6 cm/g and/or a viscosity of less than 30,000 cP as determined using a Brookfield viscometer after 10 seconds using a spindle S-64, at a speed of 1.5 rpm.
  • compositions of the invention optionally contain an emulsifier, such as lecithin, more preferably in an amount of up to 2% by weight (or up to 1% by weight) of the composition.
  • an emulsifier such as lecithin
  • the emulsifier is incorporated in (or otherwise associated with) the fat particles.
  • the fat particles preferably comprise an emulsifier prior to mixture with the liquid oil.
  • the food product may be in the form of an emulsion, such as a water-in-oil or oil-in-water emulsion.
  • an emulsifier such as lecithin
  • emulsifier will also be present to stabilise the emulsion.
  • the food product is preferably a confectionery product.
  • Confectionery products include fillings and coatings.
  • the edible oil composition of the invention preferably constitutes the fat in the filling or the coating.
  • Confectionery products typically comprise one or more confectionery additives.
  • the confectionery products preferably comprise, in addition to the edible oil composition of the invention, one or more confectionery additives selected from sugar, cocoa powder, milk powder, yoghurt powder, flavouring and emulsifier.
  • the confectionery products comprise at least sugar and cocoa powder and, optionally, one or more of the other components.
  • Other confectionery products comprise at least sugar and flavouring and, optionally, one or more of the other components. Additional components such as colouring agents and preservatives may optionally be present in the compositions.
  • Sugar includes sucrose, dextrose and fructose (preferably sucrose).
  • Flavourings include, for example, strawberry, raspberry, vanilla, mint, orange, lemon, lime, coffee and the like.
  • the confectionery products may contain nut solids (e.g., from peanuts, almonds, hazelnuts, walnuts, cashew nuts, pistachio nuts, macadamia nuts and pecan nuts), such as nut paste.
  • nut solids e.g., from peanuts, almonds, hazelnuts, walnuts, cashew nuts, pistachio nuts, macadamia nuts and pecan nuts
  • the confectionery product may be an emulsion, such as a water-in-oil emulsion.
  • the confectionery products are preferably adapted to be stored and/or sold and/or consumed at ambient temperature i.e., 10° C. to 30° C.
  • the confectionery products may be frozen products such as ice cream.
  • the confectionery product may comprise a substrate such as a biscuit, sponge or wafer, to which a coating or filling is applied, and may be impregnated into the wafers.
  • the biscuits, sponges or wafers can be present as single layers or in multiple layers.
  • the confectionery products may comprise a filling covered with an outer layer of chocolate, either when applied on biscuits, sponges or wafers, or when not so applied.
  • a preferred confectionery product comprises a chocolate outer layer filled with a filling, optionally comprising a biscuit, sponge or wafer in association with the filling.
  • the outer layer of chocolate will encapsulate the filling and the biscuit or wafer, if present.
  • the confectionery product may be a bar, optionally divided into segments. The segments may be adapted to allow part of the product to be broken off by the user and consumed separately from the remainder of the product.
  • the confectionery product may be a filling or coating that forms part of a bakery product.
  • Baked products include bread, cakes, biscuits and sponges.
  • a baked product may comprise a biscuit, sponge or wafer comprising two or more layers of biscuit, sponge or wafer, with the filling between adjacent layers.
  • the bakery product may comprise two layers of biscuit, sponge or wafer with the filling sandwiched between the layers.
  • the filled confectionery products will generally be packaged, for example in a wrapper, for sale.
  • Confectionery fillings and coatings may be made by combining one or more confectionery additives selected from sugar, cocoa powder, milk powder, yoghurt powder, flavouring and emulsifier, with the composition of the invention.
  • the components will be mixed at a temperature of greater than 40° C., such as from 50-80° C.
  • Confectionery products may be made, for example, by filling an edible substrate with a filling according to methods well known in the art.
  • Suitable edible substrates include biscuits, wafers and chocolate shells.
  • the fat particles in the edible oil composition preferably comprise cocoa butter or a cocoa butter equivalent (CBE) such as shea stearin.
  • CBE cocoa butter equivalent
  • a preferred composition of the invention is a pourable edible oil composition, suitable for use in the preparation of a confectionery product, comprising from 1% to 15% by weight of particles of cocoa butter or a cocoa butter equivalent (CBE) dispersed in a liquid oil, having a pourability of from 0.2 to 0.6 cm/g and/or a viscosity of less than 30,000 cP as determined using a Brookfield viscometer after 10 seconds using a spindle S-64, at a speed of 1.5 rpm.
  • CBE cocoa butter equivalent
  • the food product may be a margarine or a spread.
  • composition of the invention is a pourable edible oil composition, suitable for use in the preparation of a margarine or spread, comprising from 1% to 15% by weight of particles of palm oil stearin dispersed in a liquid oil comprising sunflower oil, having a pourability of from 0.2 to 0.6 cm/g and/or a viscosity of less than 30,000 cP as determined using a Brookfield viscometer after 10 seconds using a spindle S-64, at a speed of 1.5 rpm.
  • the pourability measurement is carried out following the steps showed below.
  • This procedure is repeated at least three times for each sample in order to obtain several values and to calculate the mean value.
  • Fat powder was produced from a palm oil stearin having an iodine value (IV) of 14 (available from Loders Croklaan BV, Wormerveer, The Netherlands) by ScMM (Supercritical Melt Micronization) technique operated on a continuous basis at 20 weight % CO 2 in fat at 300 bar and a pre-expansion temperature of 50° C. using a 340 ⁇ m Spraying Systems SK series spray drying nozzle.
  • the oil employed for the production of the samples was sunflower oil.
  • Samples were produced by heating up/cooling down the oil to the desired temperature and blending the appropriate amount of fat powder in the oil using a spoon (low shear). Once the samples were produced, they were stored at the desired temperature in storage cabinets for 3 weeks. Processing conditions and compositions of the samples are shown in the table below.
  • Fat content, mixing and storage temperatures of the samples Fat in Oil* Mixing Temperature Storage Temperature Sample (wt %) (° C.) (° C.) A-2-A 5 10 10 A-2-B 5 10 30 A-3-A 10 10 10 A-3-B 10 10 30 B-2 5 30 30 B-3 10 30 30 C-1 2.5 40 40 C-2 5 40 40 C-3 10 40 40 D-2 5 20 20 D-3 10 20 20 *Lecithin content of all samples is 0.7 wt %
  • Viscosity of the fat-in-oil blends was measured after 3-week storage using a Brookfield viscometer. The measurement was realized after 10 seconds using a spindle S-64, at a speed of 1.5 r.p.m.
  • Fat-in-oil blends were stored at a certain temperature for 3 weeks. Stability of the samples was assessed by visual examination and analysis of the oil exudation.
  • FIG. 2 shows the pourability of the fat-in-oil blends immediately after their production:
  • FIG. 2 a 2.5 wt % fat in oil
  • FIG. 2 b 5 wt % fat in oil
  • FIG. 2 c 10 wt % fat in oil
  • FIG. 2 d 15 wt % fat in oil.
  • FIG. 3 shows a comparison between the pourability of the samples immediately after their preparation (week 0) and after 3 weeks' storage.
  • FIG. 3 a 5 wt % fat in oil
  • FIG. 3 b 10 wt % fat in oil.
  • FIGS. 3 a ) and 3 b ) show a surprising effect of the invention, namely that the pourability passes through a minimum as temperature increases. This unexpected effect shows the importance of selecting the correct storage temperature for a given type of fat particles. The pourability may be too low for commercial acceptability of the composition if the storage temperature is within the range of the minimum of the pourability value.
  • samples stored at 40° C. are less stable than samples stored at lower temperatures. This might be due to the fact that at 40° C. the percentage of solid fat is 78% while at lower temperatures this percentage is above 89%.
  • the samples look whiter and more opaque.

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Edible Oils And Fats (AREA)
  • Confectionery (AREA)
US13/695,125 2010-04-30 2011-04-21 Edible oil composition Abandoned US20130045322A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP10250865 2010-04-30
EP10250865.2 2010-04-30
PCT/EP2011/002033 WO2011134627A1 (en) 2010-04-30 2011-04-21 Edible oil composition

Publications (1)

Publication Number Publication Date
US20130045322A1 true US20130045322A1 (en) 2013-02-21

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US13/695,125 Abandoned US20130045322A1 (en) 2010-04-30 2011-04-21 Edible oil composition

Country Status (6)

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US (1) US20130045322A1 (es)
EP (1) EP2563156A1 (es)
JP (1) JP5767317B2 (es)
KR (1) KR20130114568A (es)
AU (1) AU2011247400B2 (es)
WO (1) WO2011134627A1 (es)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10729155B2 (en) * 2014-05-08 2020-08-04 Conopco, Inc. Method for manufacturing a frozen confection
WO2020260628A1 (en) * 2019-06-28 2020-12-30 Firmenich Sa Fat blends, emulsions thereof, and related uses

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EP2636312B1 (en) 2012-03-08 2019-05-08 Bunge Loders Croklaan B.V. Glyceride composition
DK2636313T3 (en) 2012-03-08 2018-12-03 Bunge Loders Croklaan B V Glyceride composition obtainable from shea oil
CN104812250A (zh) 2012-11-28 2015-07-29 帝斯曼知识产权资产管理有限公司 粉状制剂
EP3054776B1 (en) * 2013-10-07 2018-06-13 Unilever N.V. Process for preparing emulsifier-free edible fat-continuous emulsions
CN106536696B (zh) 2014-07-22 2023-12-29 日清奥利友集团株式会社 粉末油脂组合物、包含粉末油脂组合物的食品及它们的制造方法
EP3262950A4 (en) * 2015-02-26 2018-10-24 The Nisshin OilliO Group, Ltd. Powdered chocolate
WO2017051910A1 (ja) 2015-09-24 2017-03-30 日清オイリオグループ株式会社 粉末油脂組成物及びその製造方法
JP6208921B1 (ja) 2016-01-21 2017-10-04 日清オイリオグループ株式会社 液状成分の増粘剤
JP6178950B1 (ja) 2016-01-21 2017-08-09 日清オイリオグループ株式会社 液状成分の増粘剤
EP3406695A4 (en) 2016-01-21 2019-09-11 The Nisshin OilliO Group, Ltd. POWDER TRANSFORMATION AGENT FOR LIQUID COMPONENT
US11241020B2 (en) 2016-01-21 2022-02-08 The Nisshin Oillio Group, Ltd. Powderizing agent for liquid component

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US2875065A (en) * 1955-05-11 1959-02-24 Lever Brothers Ltd Fluid shortening composition
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US3047402A (en) * 1959-11-06 1962-07-31 Lever Brothers Ltd Fluid shortening
US3325292A (en) * 1965-12-02 1967-06-13 Armour & Co Preparation of liquid shortening and product
US3528823A (en) * 1966-08-04 1970-09-15 Lever Brothers Ltd Fluid shortening
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US4385076A (en) * 1979-06-13 1983-05-24 The Procter & Gamble Company Fat or oil composition containing microfine particles of flavor enhancer
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10729155B2 (en) * 2014-05-08 2020-08-04 Conopco, Inc. Method for manufacturing a frozen confection
WO2020260628A1 (en) * 2019-06-28 2020-12-30 Firmenich Sa Fat blends, emulsions thereof, and related uses
CN113423287A (zh) * 2019-06-28 2021-09-21 弗门尼舍有限公司 脂肪混合物、其乳液和相关用途
US20220167642A1 (en) * 2019-06-28 2022-06-02 Firmenich Sa Fat blends, emulsions thereof, and related uses

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WO2011134627A8 (en) 2012-12-06
AU2011247400A1 (en) 2012-11-15
JP5767317B2 (ja) 2015-08-19
EP2563156A1 (en) 2013-03-06
KR20130114568A (ko) 2013-10-17
AU2011247400B2 (en) 2013-09-12
JP2013524820A (ja) 2013-06-20
WO2011134627A1 (en) 2011-11-03

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