US20070006984A1 - Method for the treatment of fiber material - Google Patents

Method for the treatment of fiber material Download PDF

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Publication number
US20070006984A1
US20070006984A1 US10/523,063 US52306303A US2007006984A1 US 20070006984 A1 US20070006984 A1 US 20070006984A1 US 52306303 A US52306303 A US 52306303A US 2007006984 A1 US2007006984 A1 US 2007006984A1
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United States
Prior art keywords
refining
accordance
pulp
fibers
movement
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Abandoned
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US10/523,063
Inventor
Wolfgang Berger
Klaus Eibinger
Rudolf Eichinger
Dietmar Grueneis
Andrea Hierner
Walter Ruef
Ronald Sigl
Helmut Stark
Peter-Rigobert Winter
Erika Winter
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
INSTITUT fur PAPIER- ZELLSTOFF- und FASERTECHNIK DER TECHNISCHEN UNIVERSITAET GRAZ
NEUSIEDLER AG
NORSKE SKOG BRUCK GmbH
Mondi Frantschach GmbH
SCA Graphic Laakirchen AG
SAPPI PAPIER HOLDING AG
Voith Paper Fiber and Environmental Solutions GmbH and Co KG
Original Assignee
SAPPI PAPIER HOLDING AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SAPPI PAPIER HOLDING AG filed Critical SAPPI PAPIER HOLDING AG
Assigned to FRANTSCHACH PULP & PAPER AUSTRIA AG, SCA GRAPHIC LAAKIRCHEN AG, NEUSIEDLER AG, INSTITUT FUER PAPIER-, ZELLSTOFF- UND FASERTECHNIK DER TECHNISCHEN UNIVERSITAET GRAZ, SAPPI PAPIER HOLDING AG, VOITH PAPER FIBER SYSTEMS GMBH & CO. KG, NORSKE SKOG BRUCK GMBH reassignment FRANTSCHACH PULP & PAPER AUSTRIA AG ASSIGNMENT OF ASSIGNORS INTEREST (SEE DOCUMENT FOR DETAILS). Assignors: HIERNER, ANDREA, GRUENEIS, DIETMAR, WINTER, PETER-RIGOBERT (DECEASED) BY HIS HEIR WINTER, ERIKA, SIGL, RONALD, BERGER, WOLFGANG, RUEF, WALTER, EIBINGER, KLAUS, EICHINGER, RUDOLF, STARK, HELMUT
Publication of US20070006984A1 publication Critical patent/US20070006984A1/en
Abandoned legal-status Critical Current

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    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21DTREATMENT OF THE MATERIALS BEFORE PASSING TO THE PAPER-MAKING MACHINE
    • D21D1/00Methods of beating or refining; Beaters of the Hollander type
    • D21D1/20Methods of refining
    • D21D1/34Other mills or refiners
    • D21D1/36Other mills or refiners with vertical shaft
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21DTREATMENT OF THE MATERIALS BEFORE PASSING TO THE PAPER-MAKING MACHINE
    • D21D1/00Methods of beating or refining; Beaters of the Hollander type
    • D21D1/20Methods of refining
    • D21D1/34Other mills or refiners
    • D21D1/38Other mills or refiners with horizontal shaft

Definitions

  • the invention relates to a method for treating pulp in accordance with the preamble of claim 1 .
  • Methods for treating pulp of the aforesaid type are generally also designated as refining processes. It has been known for a long time that pulp fibers have to be refined so that the paper later manufactured from them has the desired properties, in particular strengths, formation and surface.
  • the absolutely most used refining processes use such refining surfaces which are provided with rails known as blades.
  • the corresponding machines are mostly called blade refiners.
  • refining processes are also used in which at least one of the refining surfaces is bladeless so that the refining work is transmitted by frictional forces or shear forces.
  • the effect of the process can be controlled in a wide range by changing the refining parameters, with—in addition to the amount of the extraction—in particular a difference also being made as to whether a refining is desired which cuts more strongly or fibrillates more strongly. If pulp fibers are processed by the known refining processes, their dewatering resistance increases as the extraction increases. A customary measure for the dewatering resistance is the freeness according to Schopper-Riegler.
  • the refining parameters are selected such that the increase in freeness occurring to reach the required fiber quality is as low as possible.
  • the increase in the dewatering resistance which occurs in this process should be at least lower than with known refining processes.
  • the new refining process substantially works such that a refining shear loading of the pulp fibers is avoided to the largest extent.
  • Three important advantages are thereby substantially achieved with respect to the known refining processes:
  • FIG. 1 a simple example for the carrying out of the method in accordance with the invention
  • FIG. 2 schematically: an apparatus for the carrying out of the method
  • FIG. 3 a variation of the roll structure
  • FIG. 4 schematically in the position of use: a further apparatus for the carrying out of the method
  • FIG. 5 a qualitative strength diagram.
  • the representation in FIG. 1 can be considered as a view from above of part of an apparatus particularly suited for the carrying out of the method. However, no technical design details are shown.
  • the refining surface 1 is located in accordance with this representation on the outer periphery of a rotating refining body 9 .
  • the refining surface 2 as the inner side of a likewise rotating refining drum 8 , carries the pulp F to be refined, that is the watery suspension containing the paper fibers or pulp fibers, on its inner side. It is uniformly distributed on the refining surface 2 and rotates on and along with it due to the centrifugal forces.
  • the peripheral speed of the refining body 9 is indicated by a direction arrow 6 and that of the refining drum 8 is indicated by a direction arrow 7 .
  • the kinematics of these two refining surfaces in accordance with the invention is such that at the position 5 , at which the two refining surfaces approach one another the most, a very low speed arises between the pulp F and the refining surfaces in the direction of the main movements of the refining surfaces.
  • the main movement directions arise by movement of the refining surfaces due to the drive.
  • the refining body 9 in this process rolls off the inner side of the refining drum 8 .
  • the axis of rotation of the refining body 9 is parallel to that of the refining drum 8 and can be spatially fixed.
  • the actual refining zone 3 starts at the position at which the refining surface 1 dips into the layer of the pulp F.
  • the refining body 9 is pressed toward the refining surface 2 with the force P.
  • the refining effect can be adjusted by changing this force.
  • Line forces between 2 and 10 N/mm have proven advantageous.
  • the force is related to the width of the contacting refining bodies without taking into account the expansion of the contact surface in the running direction.
  • a fiber treatment thereby arises in the refining zone 3 with compression and crushing processes which flexibilize the fibers in a very gentle manner. No real shearing forces or even cutting forces are transmitted to the fibers.
  • the refining surface 1 is provided here with grooves 4 whose effect cannot be compared with that of blades of known blade refiners in which the blades are moved relative to one another at high speed.
  • the grooves 4 produce pressure pulses in cooperation with the counter surface which serve e.g. for the water absorption of the fibers. They also provide the transport of the pulp F through the refining zone 3 .
  • the grooves can extend over the full axial length of the refining body; however, they can also be interrupted.
  • the depth t and the width u should generally amount to at least 2 mm. Deviations from the rectangular structure shown here are also feasible, as FIG. 3 shows by way of example with reference to a trapezoidal structure.
  • FIG. 2 shows in the position of use.
  • a horizontally arranged refining drum 8 can be seen which is set into rotation via the drive 11 .
  • a plurality of refining bodies 9 are located inside this refining drum and—as has already been described—are moved such that a roll-off movement takes place at the contact positions to the refining drum 8 .
  • the refining bodies 9 are set into rotation by the drive 10 , with their axes of rotation being perpendicular and spatially fixed.
  • the added pulp F can be refined step-wise with such an apparatus and can be removed after the refining process as extracted pulp F′. If such an apparatus should be operated continuously, measures must be taken which effect a constant throughput of the pulp such that a uniform refining takes place.
  • FIG. 4 Another possibility of carrying out the method is shown in FIG. 4 in which the center lines of the refining drum 8 and of the refining bodies 9 are horizontal.
  • This apparatus allows continuous refining, which requires, however, that the desired extraction is already achieved with a few passages through a refining zone.
  • a broad layer of the pulp F to be refined is poured into the stationary refining drum 8 such that it runs down the inner wall of the refining drum due to gravity.
  • the refining body 9 rolls off the inner wall of the refining drum 8 in that the movement of rotation (direction arrow 6 ) of the refining body 9 about its axis is superimposed on a movement of rotation (direction arrow 6 ′) of the axis of the refining body 9 about the center line of the refining drum 8 .
  • such an apparatus includes a plurality of refining bodies 9 which are supported on a rotating rack. By selecting the addition and removal stations of the pulp F, its flow speed can be regulated. The refining bodies can run counter to the flow of the pulp (as drawn here) or follow it.
  • FIG. 5 The improvement which can be achieved by the new process is indicated in a schematic diagram in accordance with FIG. 5 .
  • This diagram shows the freeness (arrow 12 ), drawn over the tear length (arrow 13 ).
  • the curve 14 shows the result of a conventional blade refining and the curve 15 a result achieved with the new method. It can easily be seen that much lower freeness is produced to achieve a desired high tearing length in accordance with the new method.
  • This diagram is only intended to show a basic trend.

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  • Paper (AREA)

Abstract

The method serves for the altering of suspended paper fibers or pulp fibers, in particular to increase the strength of the paper made from these fibers. Two refining surfaces are pressed toward one another and moved such that a relative speed prevails between the refining surfaces and the pulp in the refining zone which is as low as possible. The method can be carried out particularly easily with refining bodies which carry a refining surface and which are rolled off on the inner side of a refining drum carrying the refining surface.

Description

  • The invention relates to a method for treating pulp in accordance with the preamble of claim 1.
  • Methods for treating pulp of the aforesaid type are generally also designated as refining processes. It has been known for a long time that pulp fibers have to be refined so that the paper later manufactured from them has the desired properties, in particular strengths, formation and surface. The absolutely most used refining processes use such refining surfaces which are provided with rails known as blades. The corresponding machines are mostly called blade refiners. For special cases, refining processes are also used in which at least one of the refining surfaces is bladeless so that the refining work is transmitted by frictional forces or shear forces.
  • The effect of the process can be controlled in a wide range by changing the refining parameters, with—in addition to the amount of the extraction—in particular a difference also being made as to whether a refining is desired which cuts more strongly or fibrillates more strongly. If pulp fibers are processed by the known refining processes, their dewatering resistance increases as the extraction increases. A customary measure for the dewatering resistance is the freeness according to Schopper-Riegler.
  • Increasing the freeness has an unfavorable effect on the formation on the paper making machine, but is accepted, since the already named quality features of the pulp play an exceptional role for its usability. In many cases, the refining parameters are selected such that the increase in freeness occurring to reach the required fiber quality is as low as possible.
  • This influence possibility is, however, very limited. In addition, the refining can thereby become less favorable from a force-economic aspect.
  • It is the underlying object of the invention to provide a method for pulp treatment with which it is possible to alter pulp fibers or paper fibers such that the strengths of the paper made therefrom are increased. The increase in the dewatering resistance which occurs in this process should be at least lower than with known refining processes.
  • This object is satisfied by the features named in claim 1.
  • The new refining process substantially works such that a refining shear loading of the pulp fibers is avoided to the largest extent. Three important advantages are thereby substantially achieved with respect to the known refining processes:
    • 1. The fiber length is maintained substantially better.
    • 2. The fiber surface is not fibrillated or is fibrillated significantly less.
    • 3. The specific refining work to achieve the desired strengths is generally less.
  • Comparative trials with long fiber pulp have shown that to achieve a tear length of 8 km, 45° SR freeness occurred in a blade refining and with the new process only 18° SR. The required specific refining work was up to 50% lower.
  • It is to be assumed that the surface of the fibers is changed by the new refining process such that it is given an improved flexibility and binding capability without fibrils having to be removed from the outer surface of the fibers. The production of fines, that is of fiber fractions, can also be omitted.
  • If the process is used on recycled fibers, the advantages named under 1. and 2. play a special role. Recycled fibers have already undergone at least one, frequently even several refining processes so that any further crushing is willingly avoided.
  • The invention and its advantages will be explained with reference to drawings. There are shown:
  • FIG. 1 a simple example for the carrying out of the method in accordance with the invention;
  • FIG. 2 schematically: an apparatus for the carrying out of the method;
  • FIG. 3 a variation of the roll structure;
  • FIG. 4 schematically in the position of use: a further apparatus for the carrying out of the method;
  • FIG. 5 a qualitative strength diagram.
  • The representation in FIG. 1 can be considered as a view from above of part of an apparatus particularly suited for the carrying out of the method. However, no technical design details are shown. The refining surface 1 is located in accordance with this representation on the outer periphery of a rotating refining body 9. The refining surface 2, as the inner side of a likewise rotating refining drum 8, carries the pulp F to be refined, that is the watery suspension containing the paper fibers or pulp fibers, on its inner side. It is uniformly distributed on the refining surface 2 and rotates on and along with it due to the centrifugal forces. The peripheral speed of the refining body 9 is indicated by a direction arrow 6 and that of the refining drum 8 is indicated by a direction arrow 7. The kinematics of these two refining surfaces in accordance with the invention is such that at the position 5, at which the two refining surfaces approach one another the most, a very low speed arises between the pulp F and the refining surfaces in the direction of the main movements of the refining surfaces. The main movement directions arise by movement of the refining surfaces due to the drive. The refining body 9 in this process rolls off the inner side of the refining drum 8. The axis of rotation of the refining body 9 is parallel to that of the refining drum 8 and can be spatially fixed. The actual refining zone 3 starts at the position at which the refining surface 1 dips into the layer of the pulp F. To produce a compression force, the refining body 9 is pressed toward the refining surface 2 with the force P. The refining effect can be adjusted by changing this force. Line forces between 2 and 10 N/mm have proven advantageous. With this figure, the force is related to the width of the contacting refining bodies without taking into account the expansion of the contact surface in the running direction. A fiber treatment thereby arises in the refining zone 3 with compression and crushing processes which flexibilize the fibers in a very gentle manner. No real shearing forces or even cutting forces are transmitted to the fibers.
  • The refining surface 1 is provided here with grooves 4 whose effect cannot be compared with that of blades of known blade refiners in which the blades are moved relative to one another at high speed. The grooves 4 produce pressure pulses in cooperation with the counter surface which serve e.g. for the water absorption of the fibers. They also provide the transport of the pulp F through the refining zone 3. The grooves can extend over the full axial length of the refining body; however, they can also be interrupted. The depth t and the width u should generally amount to at least 2 mm. Deviations from the rectangular structure shown here are also feasible, as FIG. 3 shows by way of example with reference to a trapezoidal structure.
  • An apparatus for the carrying out of the method could generally be made such as FIG. 2 shows in the position of use. A horizontally arranged refining drum 8 can be seen which is set into rotation via the drive 11. A plurality of refining bodies 9 are located inside this refining drum and—as has already been described—are moved such that a roll-off movement takes place at the contact positions to the refining drum 8. The refining bodies 9 are set into rotation by the drive 10, with their axes of rotation being perpendicular and spatially fixed. The added pulp F can be refined step-wise with such an apparatus and can be removed after the refining process as extracted pulp F′. If such an apparatus should be operated continuously, measures must be taken which effect a constant throughput of the pulp such that a uniform refining takes place.
  • Another possibility of carrying out the method is shown in FIG. 4 in which the center lines of the refining drum 8 and of the refining bodies 9 are horizontal. This apparatus allows continuous refining, which requires, however, that the desired extraction is already achieved with a few passages through a refining zone. A broad layer of the pulp F to be refined is poured into the stationary refining drum 8 such that it runs down the inner wall of the refining drum due to gravity. The refining body 9 rolls off the inner wall of the refining drum 8 in that the movement of rotation (direction arrow 6) of the refining body 9 about its axis is superimposed on a movement of rotation (direction arrow 6′) of the axis of the refining body 9 about the center line of the refining drum 8. As a rule, such an apparatus includes a plurality of refining bodies 9 which are supported on a rotating rack. By selecting the addition and removal stations of the pulp F, its flow speed can be regulated. The refining bodies can run counter to the flow of the pulp (as drawn here) or follow it.
  • The improvement which can be achieved by the new process is indicated in a schematic diagram in accordance with FIG. 5. This diagram shows the freeness (arrow 12), drawn over the tear length (arrow 13). The curve 14 shows the result of a conventional blade refining and the curve 15 a result achieved with the new method. It can easily be seen that much lower freeness is produced to achieve a desired high tearing length in accordance with the new method. This diagram is only intended to show a basic trend.

Claims (14)

1. A method of altering paper fiber or pulp fibers in a watery suspension, in which the pulp (F) is guided through at least one refining zone (3) which lies between refining surfaces (1, 2), in which the refining surfaces (1, 2) are moved relative to one another and are pressed toward one another, whereby mechanical refining work is transmitted to the fibers such that the strengths of the paper made therefrom change, characterized in that,
the relative speed between the pulp (F) and the refining surfaces, considered in the main direction of movement of the refining surfaces, is at most 10% of the absolute speed of the refining surface driven the fastest at the position (5) at which two refining surfaces (1, 2) are closest in the refining zone (3), such that no shear forces, or at most very low shear forces, are transmitted to the fibers in the refining zone (3).
2. A method in accordance with claim 1, characterized in that the relative speed between the pulp (F) and the refining surfaces, considered in the main direction of movement of the refining surfaces, is lower than 5% of the absolute speed of the refining surface driven the fastest at the position (5) at which two refining surfaces (1, 2) are closest in the refining zone (3).
3. A method in accordance with claim 1, characterized in that the relative movement of the refining surfaces (1, 2) is a roll-off movement.
4. A method in accordance with claim 1, characterized in that the mechanical refining work is transmitted by compressing the pulp.
5. A method in accordance with claim 1, characterized in that a refining surface (1) is provided with grooves (4, 4′) which extend transversely to the main direction of movement of the moved refining surface.
6. A method in accordance with claim 5, characterized in that the grooves (4, 4″) have a depth (t) of at least 2 mm and an extent (u) in the direction of movement of the moved refining surfaces of at least 2 mm.
7. A method in accordance with claim 5, characterized in that the second refining surface (2) is not provided with transversely extending grooves.
8. A method in accordance with claim 1, characterized in that one refining surface (1) is located outwardly on a cylindrical refining body (9) whose center line is moved relative to a refining drum (8) which includes the other refining surface (2) on its inner side.
9. A method in accordance with claim 8, characterized in that a plurality of refining bodies (9) are used in a refining drum (8).
10. A method in accordance with claim 1, characterized in that the pulp (F) is not moved relative to one of the refining surfaces (1, 2) in the refining zone (3).
11. A method in accordance with claim 1, characterized in that the fibers are present in a suspension with at most 10% solid content.
12. A method in accordance with claim 11, characterized in that the solid content amounts to at most 6%.
13. A method in accordance with claim 1, characterized in that the absolute speed of at least one refining surface (1, 2) is kept to a value between 8 and 30 m/sec.
14. A method in accordance with claim 1, characterized in that the refining surfaces (1, 2) are pressed toward one another such that a line force arises in the refining zone (3) between 2 and 10 N/mm.
US10/523,063 2002-08-13 2003-07-30 Method for the treatment of fiber material Abandoned US20070006984A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE10236962A DE10236962A1 (en) 2002-08-13 2002-08-13 Papermaking process compresses slow-speed fibers between a roller with shallow transverse grooves and a smooth interface
DE102-36-962.3 2002-08-13
PCT/EP2003/008445 WO2004022843A1 (en) 2002-08-13 2003-07-30 Method for the treatment of fiber material

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US20070006984A1 true US20070006984A1 (en) 2007-01-11

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US (1) US20070006984A1 (en)
EP (1) EP1521883A1 (en)
JP (1) JP2005535799A (en)
CN (1) CN1697902A (en)
AU (1) AU2003258551A1 (en)
BR (1) BR0305765A (en)
DE (1) DE10236962A1 (en)
NO (1) NO20041310L (en)
RU (1) RU2309211C2 (en)
WO (1) WO2004022843A1 (en)

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WO2016091968A1 (en) * 2014-12-10 2016-06-16 Clumpkens Mathias Johannes Method for refining fibres for paper making and apparatus suitable for said process

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DE10337921A1 (en) * 2003-08-18 2005-03-17 Voith Paper Patent Gmbh Refining assembly, for a suspension of papermaking paper/cellulose fibers, forms a fiber layer on the inner surface of the rotating drum with beater rollers pressed against it and a constant liquid flow in and out of the layer
DE10337922A1 (en) * 2003-08-18 2005-03-17 Voith Paper Patent Gmbh Refining assembly, for a suspension of papermaking paper/cellulose fibers, forms a fiber layer on the inner surface of the rotating drum with beater rollers pressed against it and a constant liquid flow in and out of the layer
US20060186235A1 (en) * 2003-08-18 2006-08-24 Voith Paper Patent Gmbh Method for refining paper or cellulose fibers in an aqueous suspension
DE102005016318A1 (en) * 2005-04-09 2006-10-12 Voith Paper Patent Gmbh Process for grinding aqueous suspended paper or pulp fibers and grinding device for its implementation
WO2006108508A1 (en) * 2005-04-15 2006-10-19 Voith Patent Gmbh Method for preparing paper-fibre raw material
EP1728918A3 (en) 2005-05-12 2006-12-13 Voith Patent GmbH Proces for removing impurities from an aqueous fibrous suspension
ATE468434T1 (en) * 2005-12-17 2010-06-15 Voith Patent Gmbh METHOD FOR REMOVAL OF INTERFERENTS FROM AN AQUEOUS FIBER SUSPENSION
DE102007003964A1 (en) * 2007-01-26 2008-01-24 Voith Patent Gmbh Wood-pulping equipment for paper- or card manufacture, employs compression refiner to complete fiber hydration and separation without damage
US9879361B2 (en) * 2012-08-24 2018-01-30 Domtar Paper Company, Llc Surface enhanced pulp fibers, methods of making surface enhanced pulp fibers, products incorporating surface enhanced pulp fibers, and methods of making products incorporating surface enhanced pulp fibers
ES2756299T3 (en) 2014-02-21 2020-04-27 Domtar Paper Co Llc Improved pulp fibers on a substrate surface
WO2015127233A1 (en) 2014-02-21 2015-08-27 Domtar Paper Company Llc Surface enhanced pulp fibers in fiber cement
WO2018026804A1 (en) 2016-08-01 2018-02-08 Domtar Paper Company, Llc Surface enhanced pulp fibers at a substrate surface
WO2018075627A1 (en) 2016-10-18 2018-04-26 Domtar Paper Company, Llc Method for production of filler loaded surface enhanced pulp fibers
WO2019152969A1 (en) 2018-02-05 2019-08-08 Pande Harshad Paper products and pulps with surface enhanced pulp fibers and increased absorbency, and methods of making same
CN109183489A (en) * 2018-09-25 2019-01-11 福建锐信合成革有限公司 A kind of release paper quetsch
US11608596B2 (en) 2019-03-26 2023-03-21 Domtar Paper Company, Llc Paper products subjected to a surface treatment comprising enzyme-treated surface enhanced pulp fibers and methods of making the same
FR3137398A1 (en) * 2022-06-30 2024-01-05 Centre Technique Du Papier METHOD FOR PROCESSING CELLULOSIC FIBERS BY MECHANICAL COMPRESSION, PARTICULARLY FOR PAPER PULP

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2016091968A1 (en) * 2014-12-10 2016-06-16 Clumpkens Mathias Johannes Method for refining fibres for paper making and apparatus suitable for said process
NL2013950B1 (en) * 2014-12-10 2016-10-11 Johannes Clumpkens Mathias Method for refining fibres for paper making and apparatus suitable for said process.

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NO20041310L (en) 2004-03-30
AU2003258551A1 (en) 2004-03-29
WO2004022843A1 (en) 2004-03-18
BR0305765A (en) 2004-10-05
JP2005535799A (en) 2005-11-24
AU2003258551A8 (en) 2004-03-29
RU2005106869A (en) 2005-10-10
CN1697902A (en) 2005-11-16
EP1521883A1 (en) 2005-04-13
RU2309211C2 (en) 2007-10-27
DE10236962A1 (en) 2004-02-26

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