US1978945A - Apparatus for the distillation of coal - Google Patents

Apparatus for the distillation of coal Download PDF

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US1978945A
US1978945A US540608A US54060831A US1978945A US 1978945 A US1978945 A US 1978945A US 540608 A US540608 A US 540608A US 54060831 A US54060831 A US 54060831A US 1978945 A US1978945 A US 1978945A
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distillation
coal
fuel
grate
chamber
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US540608A
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Hereng Alfred Jean Andre
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    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10BDESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
    • C10B7/00Coke ovens with mechanical conveying means for the raw material inside the oven
    • C10B7/06Coke ovens with mechanical conveying means for the raw material inside the oven with endless conveying devices

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  • The, invention relates to apparatus for the dis- 5 tillation of fuels such as coal.
  • the coal to be treated is not in contact with the heating fluid and heat is transmitted through a partition.
  • the coal to be treated is heated internally by the heating fluid.
  • This invention relates to the second mentioned method, and, according thereto, the fuel to be treated, previously dried and heated up to about the softening point, is laid on a travelling grate pervious to fluids, as, for instance, on a power chain grate.
  • distillation chamber wherein the fuel is heated up to the above mentioned optimum temperature. Such heating may be ensured by combustion in the compartment of any available fuel, whether gaseous, liquid or solid.
  • One of the characteristic features of my invention consists in the possibility of heating the fuel to be distilled by means of the gas obtained from the distilling either by burning the same, since it is combustible, or through heating it up to an adequate temperature, say 700 C. 01 course radiation from the walls of said distillation chamber cooperates in heating the raw fuel that is laid on the 'metal grate or conveyor.
  • the links oi the chain are at a sufliciently high temperature, when they come again forwards after a complete revolution to cooperate in the heating of the fuel. Furthermore, said heating has the effect of freeing from dust the coal coming from. the drying device,
  • gaseous products of the distillation are 5 drawn under the fuel layer by suction chests,
  • the fuel layer is heated irom above, from below, and within its mass, said layer resting on a conveyor pervious to gases, the gaseous 49 products being drawnunderneath into suction chests or compartments.
  • the vapor products are partly condensable and include distillation gases having a high calorific power. These are the gases that can be used, as already stated, for heating the fuel in the distillation chamber.
  • the heavy tars laden with dust "withdrawn from the first condensation devices, are returned to the fuel in the distillation chamber; they 00- operate in reducing the amount of dust which passes through the grate, they are distilled anew in the fuel layer on contact with the nascent hydrocarbons and the distilled gases are sucked into the lower suction compartments or chests as above explained.
  • compartments which may be the combustion chamber of a boiler, or a quenching and cooling metal box for the semi colze; but w under this compartment extends the conveyor (that is to say the chain grate) that the fuel passes automatically from the first to the second compartment without interilerence from outside.
  • conveyor that is to say the chain grate
  • the semicolre passes from one compartment to the other at a temperature of approximately 509 C. and it is necessary only to draw air through compartments located under the conveyor in order readily to cause combustion.
  • Part of the we gases may, indeed, be utilized, as already stated, to ensure the heating of the distillation compartment through direct combustion.
  • heating of the fuel in the distllla- The'regenerator orgas heater' may be heated by any routine means (producer gas, etc.) and, especially, by hot gases from the boiler or even by.
  • regenerator should be so-selected as to minimize radiation losses, for instance,- directly above the distillation chamber.
  • the compactness of said semi colre may be increased in the course oi its travel through the distillation chamber by means of a loose chain, resting thereon and suitably weighted, and the slack side of which will ensure compression of the softened fuel down to hardening at the end of distillation, without interfering with the continuous travel oi the fuel.
  • Figs. 1 and 2 schematically illustrate apparatus in elevation with parts in section for performing the process
  • Fig. 3 is a top plan view showing the layer of coal on the endless grate.
  • Fig. 1 there are shown from left to right, the hopper, the drying device S, the distillation compartment D, the combustion chamber 0 and the boiler V. Underneath, the chain grate G.
  • the chain grate is the grate with which the boiler would be normally equipped, but it extends forward under the distillation compartment D and the drying device 8.
  • the drying device may be constituted by vertical channels through which the raw coal moves down by gravity and is heated by combustion gases from the boiler.
  • Gate E permits adjusting the amount of heat that the combustion chamber transmits by radiation to the distillation chamber. Said amount of heat, may, indeed, be sumcient alone to keep the combustion chamber at optimum temperature. i
  • the hydrocarbons obtained by the distillation are detarred and are drawn into the suction compartments H, and are ridoftheir liquid bydrocarbons by the usual means.
  • B is a tar separatorwherein the gases bubble in hot tar. .
  • the neavy tars, which settle down, are laden with dust; they are sent back, through L, into thedistillation chamber'D wherein they are freed of dust and I redistilled.
  • M is a rotary tar separator, M 21. petrol removing column.
  • the semi-coke passes into the quenching chamher '1.
  • An adjustably tensloned chain K presses down on the latter while this is soft, that is to say in the course of distillation. Said chain is free and is taken along by the motion of the fuel so that no relative movement is caused between the layer and the two chains K and G- On leaving grate G, the semicoke accumulates in hopper Ua' after having passed over a sieve U whereby the pea coke is. separated anddrops into hopper U1.
  • Apparatus for the low temperature distillation of coal comprising an endless chain grate pervious to gases, means for moving said grate, means for depositing coal in a layer on a first part of the .upper horizontal run of said grate, means for regulating' the thickness of the layer, a low temperature distillation chamber arranged above and around a second part of the upper run of the chain grate, heating means for distilling at low temperature the layer of coal in said distillation chamber, a suction compartment arranged against the under side of said second part of the upper run of said grate, means for exhausting the distillation gases from said distillation chamber through the layer of coal and said suction compartment, a tar separator into which said suction compartment discharges, means for circulating tar and coal dust from the bottom of said separator to the distillation chamber and discharging the tar and coal dust on the coal layer in the distillatio'n chamber, means for circulating at least one part of non-condensed gases from said tar separator to the distillation

Description

1934- A. J; A. HERENG 78,
APPARATUS FOR THE DISTILLATION OF COAL Original Filed Dec. 11, 1928 2 Sheets-Sheet 2,
REGENERA 70R namnr TAR M sip/um 70R INVENTOR A.J. A. Hm BY ATTORNEY Patented Oct. 30, 1934 'UNITED STATES APPARATUS roa 'rns msmmrron or /COAL Alfred Jean Anrlr He'reng, Paris, France Original application December 11, 1928, Serial No. 325,188. Divided and this application May 28, 1931, Serial No. 540,808. In France'Noyembcr 1 Claim.
This is a division of my copending application,
Serial No. 325,188, filed December 11, 1928, issued as Patent No. 1,909,956.
The, invention relates to apparatus for the dis- 5 tillation of fuels such as coal.
Persons skilled in the art are aware of the interest that attaches to extracting tars from fuels previous to combustion thereof and or the many processes or methods that have been put into operation with a view of obtaining the aforesaid result.
Said methods or processes may be classified in two main groups:
According to the processes of the first group,
the coal to be treated is not in contact with the heating fluid and heat is transmitted through a partition.
According to the processes of the second group, the coal to be treated is heated internally by the heating fluid.
This invention relates to the second mentioned method, and, according thereto, the fuel to be treated, previously dried and heated up to about the softening point, is laid on a travelling grate pervious to fluids, as, for instance, on a power chain grate.
It is a well-known iact that the best temperature for obtaining tars fromdistillation at a low temperature is included between 300 and 500 0.;
in front of and above the metal travelling grate, there is a distillation chamber wherein the fuel is heated up to the above mentioned optimum temperature. Such heating may be ensured by combustion in the compartment of any available fuel, whether gaseous, liquid or solid.
One of the characteristic features of my invention consists in the possibility of heating the fuel to be distilled by means of the gas obtained from the distilling either by burning the same, since it is combustible, or through heating it up to an adequate temperature, say 700 C. 01 course radiation from the walls of said distillation chamber cooperates in heating the raw fuel that is laid on the 'metal grate or conveyor.
On the other hand, the links oi the chain are at a sufliciently high temperature, when they come again forwards after a complete revolution to cooperate in the heating of the fuel. Furthermore, said heating has the effect of freeing from dust the coal coming from. the drying device,
thereby preventing coal dust from passing through the grate.
Another essential feature of my invention is that the gaseous products of the distillation are 5 drawn under the fuel layer by suction chests,
wherein a lower pressure is maintained than in the distillation chamber.
Therefore, the fuel layer is heated irom above, from below, and within its mass, said layer resting on a conveyor pervious to gases, the gaseous 49 products being drawnunderneath into suction chests or compartments.
The vapor products are partly condensable and include distillation gases having a high calorific power. These are the gases that can be used, as already stated, for heating the fuel in the distillation chamber.
The heavy tars laden with dust "withdrawn from the first condensation devices, are returned to the fuel in the distillation chamber; they 00- operate in reducing the amount of dust which passes through the grate, they are distilled anew in the fuel layer on contact with the nascent hydrocarbons and the distilled gases are sucked into the lower suction compartments or chests as above explained.
Beyond the distillation compartments, there is arranged another compartment, which may be the combustion chamber of a boiler, or a quenching and cooling metal box for the semi colze; but w under this compartment extends the conveyor (that is to say the chain grate) that the fuel passes automatically from the first to the second compartment without interilerence from outside.
As'will be readily realized, such a device permits:
(a) Either simply extracting the primary tars and tar oils and hydrocarbons such as henzol and toluol and burning the semi-colic and gases.
As a matter of fact, owing solely to the move-- on ments of the conveyor moving along, the semicolre passes from one compartment to the other at a temperature of approximately 509 C. and it is necessary only to draw air through compartments located under the conveyor in order readily to cause combustion.
The gases, are sent into the second compartment or combustion chamber wherein they co-= operate, jointly with the semi-collie, in heating,
for instance, a steam generator. Part of the we gases may, indeed, be utilized, as already stated, to ensure the heating of the distillation compartment through direct combustion.
(b) or else, extracting, as in the previous case,
the primary tars, burning the semi-coke in the combustion chamber, and, instead of sending back into the latter the collected gases, housing them in a gasorneter for industrial or domestic use.
In this case, heating of the fuel in the distllla- The'regenerator orgas heater'may be heated by any routine means (producer gas, etc.) and, especially, by hot gases from the boiler or even by.
a part of the rich gas produced. The location of the regenerator should be so-selected as to minimize radiation losses, for instance,- directly above the distillation chamber.
Or again, extracting the primary tars, as above indicated, storing the rich gas in a gasometenand quenching the semi-coke so as to prevent combustion thereof, and utilizi this solid fuel for some ulterior, industrial or domestic use. a
The compactness of said semi colre may be increased in the course oi its travel through the distillation chamber by means of a loose chain, resting thereon and suitably weighted, and the slack side of which will ensure compression of the softened fuel down to hardening at the end of distillation, without interfering with the continuous travel oi the fuel. Y
, of air in accordance with the routine water-gas or air-gas manufacturing methods.
In order to make my invention more clearly understood I have illustrated two embodiments thereof in the drawings appended hereto and wherein:
Figs. 1 and 2 schematically illustrate apparatus in elevation with parts in section for performing the process, and Fig. 3 is a top plan view showing the layer of coal on the endless grate.
In Fig. 1 there are shown from left to right, the hopper, the drying device S, the distillation compartment D, the combustion chamber 0 and the boiler V. Underneath, the chain grate G.
As will be apparent, the chain grate is the grate with which the boiler would be normally equipped, but it extends forward under the distillation compartment D and the drying device 8.
The drying device, indicated as an example, may be constituted by vertical channels through which the raw coal moves down by gravity and is heated by combustion gases from the boiler.
Dried and heated, the coal falls down on to the grate whereon the thickness of the layer is regulated by the gate P. The fuel travels freely through chamber D,.heated up to GOT-650. "C. and is distilled. The semi-coke passes into the combustion chamber C wherein it is burnt by air blown into suction compartments or chests A.
Gate E permits adjusting the amount of heat that the combustion chamber transmits by radiation to the distillation chamber. Said amount of heat, may, indeed, be sumcient alone to keep the combustion chamber at optimum temperature. i
The hydrocarbons obtained by the distillation are detarred and are drawn into the suction compartments H, and are ridoftheir liquid bydrocarbons by the usual means. B is a tar separatorwherein the gases bubble in hot tar. .The neavy tars, which settle down, are laden with dust; they are sent back, through L, into thedistillation chamber'D wherein they are freed of dust and I redistilled. M is a rotary tar separator, M 21. petrol removing column.
, The gases, deterred and rid of their liquid hydrocarbons, are sent to the burners 0 where complete or partial combustion thereof is caused depending on the extra heat to be provided for the distillation chamber. Excess gases pass under baiiie E and are burnt in combustion chamber C.
. In the device illustrated by-Fig. 2, it is contemplated to extract semi-coke in agglomerated form. on issuing from the condensation apparatus (not shown but like M1 in Fig. 1), the cooled distillation gas is led to suction chamber '1, passes through the conveyor and the semi-coke layer which gives up thereto its actual heat and is cooled. The gas thus partly heated goes to regenerator R and goes through the same cycle as in the foregoing case.
The semi-coke passes into the quenching chamher '1.
An adjustably tensloned chain K, of the same width as the fuel layer, presses down on the latter while this is soft, that is to say in the course of distillation. Said chain is free and is taken along by the motion of the fuel so that no relative movement is caused between the layer and the two chains K and G- On leaving grate G, the semicoke accumulates in hopper Ua' after having passed over a sieve U whereby the pea coke is. separated anddrops into hopper U1.
What I claim is: Apparatus for the low temperature distillation of coal comprising an endless chain grate pervious to gases, means for moving said grate, means for depositing coal in a layer on a first part of the .upper horizontal run of said grate, means for regulating' the thickness of the layer, a low temperature distillation chamber arranged above and around a second part of the upper run of the chain grate, heating means for distilling at low temperature the layer of coal in said distillation chamber, a suction compartment arranged against the under side of said second part of the upper run of said grate, means for exhausting the distillation gases from said distillation chamber through the layer of coal and said suction compartment, a tar separator into which said suction compartment discharges, means for circulating tar and coal dust from the bottom of said separator to the distillation chamber and discharging the tar and coal dust on the coal layer in the distillatio'n chamber, means for circulating at least one part of non-condensed gases from said tar separator to the distillation chamber, a loose endless grate of the same 'width as the layer of coal arranged in the distillation chamber with its bottom run loosely hung upon the layer and pressing on the same, whereby the distilled coal is agglomerated in said distillation cham er, and a second 140 chamber adjacent the discharge end of the upper run of the endless chain grate for receiving the distilled and agglomerated coke residue.
US540608A 1928-12-11 1931-05-28 Apparatus for the distillation of coal Expired - Lifetime US1978945A (en)

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US325188A US1909956A (en) 1928-11-08 1928-12-11 Process of coal distillation
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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2531998A (en) * 1945-09-20 1950-11-28 George W Wallace Carbonization apparatus
US2621151A (en) * 1947-05-27 1952-12-09 Ingeniorsbyran Fredca Aktiebol Coal and the like
US2955991A (en) * 1955-02-24 1960-10-11 Wood Associates Inc Apparatus for heating agglutinating coal
US3226212A (en) * 1962-01-02 1965-12-28 Mcdowell Wellman Eng Co Apparatus for the production of combustible gases from solid carbonaceous materials
US3432397A (en) * 1965-02-23 1969-03-11 Clyde H O Berg Method of retorting solids
US3475279A (en) * 1966-07-01 1969-10-28 Kenneth Ralph Bowman Recovery process and apparatus
US4395309A (en) * 1980-11-03 1983-07-26 Esztergar Ernest P Fractional distillation of hydrocarbons from coal

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2531998A (en) * 1945-09-20 1950-11-28 George W Wallace Carbonization apparatus
US2621151A (en) * 1947-05-27 1952-12-09 Ingeniorsbyran Fredca Aktiebol Coal and the like
US2955991A (en) * 1955-02-24 1960-10-11 Wood Associates Inc Apparatus for heating agglutinating coal
US3226212A (en) * 1962-01-02 1965-12-28 Mcdowell Wellman Eng Co Apparatus for the production of combustible gases from solid carbonaceous materials
US3432397A (en) * 1965-02-23 1969-03-11 Clyde H O Berg Method of retorting solids
US3475279A (en) * 1966-07-01 1969-10-28 Kenneth Ralph Bowman Recovery process and apparatus
US4395309A (en) * 1980-11-03 1983-07-26 Esztergar Ernest P Fractional distillation of hydrocarbons from coal

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