US1689895A - Method of spinning artificial silk - Google Patents
Method of spinning artificial silk Download PDFInfo
- Publication number
- US1689895A US1689895A US180994A US18099427A US1689895A US 1689895 A US1689895 A US 1689895A US 180994 A US180994 A US 180994A US 18099427 A US18099427 A US 18099427A US 1689895 A US1689895 A US 1689895A
- Authority
- US
- United States
- Prior art keywords
- spinning
- artificial silk
- carbon dioxide
- bath
- bicarbonate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title description 11
- 238000009987 spinning Methods 0.000 title description 11
- 229920002955 Art silk Polymers 0.000 title description 6
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 20
- 229910002092 carbon dioxide Inorganic materials 0.000 description 10
- 239000001569 carbon dioxide Substances 0.000 description 10
- BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical class OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 description 8
- 229920002678 cellulose Polymers 0.000 description 7
- 239000001913 cellulose Substances 0.000 description 7
- 230000001376 precipitating effect Effects 0.000 description 5
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 4
- 239000002253 acid Substances 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 2
- 235000017557 sodium bicarbonate Nutrition 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical group [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 150000001340 alkali metals Chemical class 0.000 description 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 1
- -1 alkaline earth metal bicarbonates Chemical class 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 229910000000 metal hydroxide Inorganic materials 0.000 description 1
- 150000004692 metal hydroxides Chemical class 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F2/00—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof
- D01F2/02—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof from solutions of cellulose in acids, bases or salts
- D01F2/04—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof from solutions of cellulose in acids, bases or salts from cuprammonium solutions
Definitions
- HERMANN SCHMIDT OF WIESDORF-ON-THE-BHINE, AND EMIL HUBERT, F ELBER- FELD, GERKANY, ASSIGNOIQS TO I. G. FARBENINDUSTBIE AKTIENGESELLSCHAFT, 0F FBANKFORT-ON-TEE-KAIN, GERMANY.
- This invention relates to a new method of spinning artificial silk fromcuprammonium cellulose solutions and involves the use of an aqueous precipitating bath containing dis- 5 solved carbon dioxide or carbonic acid or its chemical equivalent, a soluble bicarbonand elasticity than silk produced by spin-.
- the aqueous precipitating bath may contain carbon dioxide dissolved therein and chemically combined with water as thehypothetical acid H 00 or chemi-- cally com med with metals as bior acid carbonates as NaHCO
- the bicarbonate may be added to the bath as such, for ininstance, as sodium bicarbonate or formed in the bath by treating a solution of a metal hydroxide or carbonate with carbon dioxide. It will be further understood that in the vention threads is then effected according tp the cusfrom cuprammoniumcellulose appended claims where reference is made to dissolved carbon dioxide, carbonic acid and acid carbonates are embraced.
- Emmple 2.-Cuprammonium cellulose solution is precipitated. in water containing approximately 2 grams of sodium bicarbonate per liter'in a spinning vessel, for examleaccording to the process of German Pat.
- Process for the manufacture of artificial silk which comprises spinning a cuprammonium cellulose solution into an aqueous precipitating bath containing a bicarbonate in solution.
- Process for. the manufacture of artificial silk which comprises spimiing a cuprammonium cellulose solution into an aqueous precipitating bath containing a bicarbonate of an alkali iorming metal in solution.
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Artificial Filaments (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE1689895X | 1926-06-11 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US1689895A true US1689895A (en) | 1928-10-30 |
Family
ID=7739477
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US180994A Expired - Lifetime US1689895A (en) | 1926-06-11 | 1927-04-04 | Method of spinning artificial silk |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US1689895A (en, 2012) |
| BE (1) | BE342824A (en, 2012) |
| FR (1) | FR635774A (en, 2012) |
| NL (2) | NL23476C (en, 2012) |
-
0
- BE BE342824D patent/BE342824A/xx unknown
- NL NL21377D patent/NL21377C/xx active
- NL NL23476D patent/NL23476C/xx active
-
1927
- 1927-04-04 US US180994A patent/US1689895A/en not_active Expired - Lifetime
- 1927-06-10 FR FR635774D patent/FR635774A/fr not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| FR635774A (fr) | 1928-03-24 |
| NL21377C (en, 2012) | |
| NL23476C (en, 2012) | |
| BE342824A (en, 2012) |
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