US1181976A - Fireproof lubricating-oil. - Google Patents
Fireproof lubricating-oil. Download PDFInfo
- Publication number
- US1181976A US1181976A US8281316A US8281316A US1181976A US 1181976 A US1181976 A US 1181976A US 8281316 A US8281316 A US 8281316A US 8281316 A US8281316 A US 8281316A US 1181976 A US1181976 A US 1181976A
- Authority
- US
- United States
- Prior art keywords
- ounces
- oil
- lubricating
- graphite
- soda
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000010687 lubricating oil Substances 0.000 title description 18
- 239000003921 oil Substances 0.000 description 22
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 21
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 15
- 239000010439 graphite Substances 0.000 description 14
- 229910002804 graphite Inorganic materials 0.000 description 14
- 239000000126 substance Substances 0.000 description 10
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 9
- 239000004254 Ammonium phosphate Substances 0.000 description 9
- 229940037003 alum Drugs 0.000 description 9
- 229910000148 ammonium phosphate Inorganic materials 0.000 description 9
- 235000019289 ammonium phosphates Nutrition 0.000 description 9
- MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 description 9
- 238000000034 method Methods 0.000 description 9
- 230000008569 process Effects 0.000 description 9
- PBYZMCDFOULPGH-UHFFFAOYSA-N tungstate Chemical compound [O-][W]([O-])(=O)=O PBYZMCDFOULPGH-UHFFFAOYSA-N 0.000 description 8
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 description 7
- 229910052921 ammonium sulfate Inorganic materials 0.000 description 7
- 235000011130 ammonium sulphate Nutrition 0.000 description 7
- 229910052799 carbon Inorganic materials 0.000 description 7
- 238000005461 lubrication Methods 0.000 description 7
- 230000009471 action Effects 0.000 description 6
- 239000002184 metal Substances 0.000 description 6
- 229910052751 metal Inorganic materials 0.000 description 6
- 239000000203 mixture Substances 0.000 description 5
- 230000003647 oxidation Effects 0.000 description 5
- 238000007254 oxidation reaction Methods 0.000 description 5
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- 239000000314 lubricant Substances 0.000 description 4
- 150000002739 metals Chemical class 0.000 description 4
- 238000011282 treatment Methods 0.000 description 4
- 230000003137 locomotive effect Effects 0.000 description 3
- 238000012856 packing Methods 0.000 description 3
- 241000506680 Haemulon melanurum Species 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 2
- 235000019647 acidic taste Nutrition 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 230000005484 gravity Effects 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 230000002265 prevention Effects 0.000 description 2
- 239000010959 steel Substances 0.000 description 2
- 238000005496 tempering Methods 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- 229910001369 Brass Inorganic materials 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 241000234435 Lilium Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 239000010951 brass Substances 0.000 description 1
- 150000001722 carbon compounds Chemical class 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000001050 lubricating effect Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000009877 rendering Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M125/00—Lubricating compositions characterised by the additive being an inorganic material
- C10M125/24—Compounds containing phosphorus, arsenic or antimony
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M125/00—Lubricating compositions characterised by the additive being an inorganic material
- C10M125/02—Carbon; Graphite
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M125/00—Lubricating compositions characterised by the additive being an inorganic material
- C10M125/10—Metal oxides, hydroxides, carbonates or bicarbonates
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M125/00—Lubricating compositions characterised by the additive being an inorganic material
- C10M125/20—Compounds containing nitrogen
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M125/00—Lubricating compositions characterised by the additive being an inorganic material
- C10M125/22—Compounds containing sulfur, selenium or tellurium
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/04—Elements
- C10M2201/041—Carbon; Graphite; Carbon black
Landscapes
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Lubricants (AREA)
Description
UNITED STATES PATENT OFFICE.
ROBERT R. GRAF, OF BALTIMORE, MARYLAND.
FIREPROOF LUBRICATING-OIL.
No Drawing.
1 '0 all whom it may concern:
Be it known that I, Rom-arr R. Gum, a citizen of the United States, residing at No. 114 East Lombard street, in the city of Baltimore and the State of Maryland, have invented new and useful Fireproof Lubricating-Oils, of which the following is a specification. s
The object of my invention is the production of fire proof lubricating oils, for high speed machinery, journals, bearings, friction surfaces, clutches, locomotive and car axles where cotton wick packings are used, and all other mechanical parts vwhere friction, heating and oxidation; caused by heat and friction thus permitting of perfect lubrication, (1) by increasing the flashing (ignition) point to such a high degree of temperature as to prevent the burning of the oil. (2) by maintaining normal oil temperature upon the surface Where lubrication is required. lily process further renders oils fire proof in the use of the art of tempering metals, case hardening of iron and steel and all oil treatments of metals in oil, since they must be thrust into the oil in a highly heated state and therein allowed to remain until cold, all danger of fire and burning of the oil so treated by my new and improved process for fire proof oils is fully overcome, thereby making complete, the process of tempering, cooling and technical treatment of such metals.
My new and improved process for the making of fire proof lubricating oils overcomes all dangers of fires, hotboxes, heated axles and journals or bearings of locomotives and railway coaches where cotton wicking or waste packings are charged with a quantity of lubricating oilto be supplied to the journals and axles as required, and so frequently take fire, because of the heat generated from friction due to the low point of flashing (ignition) causing the oil to leave the friction parts, due to a lighter gravity produced by heat. All power of lubrication is lost, causing great heat, fires, change in the crystalline form of the metal, with ultimate ruin and breakage of the parts.
My formula consists of 6 ounces of tungstate of soda, 5 ounces of ammonium muriate, 6 ounces of ammonium phosphate, 16 ounces of sal soda, 5 ounces of graphite, ounce of alum, and 6 ounces of ammonium sulfate, all of which I mix together in the finest powder form and add to one gallon Specification of Letters Patent.
- minutes.
Patented May 2, 1916.
Application filed March 8, 1916. Serial No. 82,813.
of lubricating oil and boil for thirty (30) This treatment of lubricating oil will at once cause it to offer great resistance to heat, increase viscosity and prevent the oxidation of carbon properties in the oil, thus producing such a high flashing (ignition) point as to render said oil incapable of burning or being excluded from the friction parts by the action of heat. Since various oils have different densities, boil at various degrees of heat, my process can be applied to meet the requirements of the particular oil to be treated; as proven by me in the many uses of the various oils treated by my new and improved process for the making of fire proof lubricating oils.
The advantages of the combination as herein set forth, are as follows:
(1) With the addition of 5 ounces of graphite and ounce of alum combined with (3 ounces of tungstate of soda, 5 ounces of ammonium muriate. 6 ounces of ammonium phosphate, 16 ounces of sal soda and (3 ounces of ammonium sulfate, I can better control carbon oxidation and combustion and prevent the absorption of heat, both of which are the essential parts to perfect lubrication.
(2) (a) Prevention of the emulsion of oils due to heat. friction and agitation, thereby increasing the viscosity or power of lubrication, (1)) the keeping oil cool and preventing it from reaching its flashing point from the aforesaid actions and conditions. (0) changing to a lighter density and thereby forced from the friction parts.
(3) That graphite can only be suspended in the ordinary lubricating oils, while the said oils remain at their normal temperature. (a) the power of lubrication of graphite depends upon the constant application of it to the friction parts in a suspended state inoil of a uniform temperature. (b) its power combined in a viscous medium renders it the ideal lubricant in this state.
(4) The combination and proportions of the various ingredients as named by me in my new and improved process for the making of fire proof lubricating oils overcome acidities that arise either in or created by heat and molecular action on carbon.
(5) That all danger of fire in locomotive and car axles, pulley hangers, friction clutches, high speed machinery, gas and gas fuel engines where oil is either stored in cotton wick or waste packings, or containers to be consumed by the bearings as required 1 a better combination is had between the oil and the remainder of the chemicals as used by me, namely-5 ounces of ammonium muriate and 6 ounces of ammonium phosphate combined with 5 ounces of graphite. (a) when mixed in the above proportions, by their combined chemical action create a chemical combination in the presence of ounce of alum; which better incorporates the oil aml chemicals uscdt l)) by increasing viscosity, to) preventing the oxidation of carbon, (1!) creating a chemical cooling condition preventing the heating and changing of lubricating oils to a lighter gravity.
(7) The chemicals named in the aforesaid formula consisting of 6 ounces of tungstate of soda, 5 ounces of ammonium muriate, 6 ounces of ammonium phosphate, 16 ounces of sal soda, 5 ounces of graphite, one half ounce of alum and 6 ounces of ammonium sulfate all combined in a finely powdered form and added to one gallon of lubricating oil and boiled for thirty minutes, will not in any way injure, corrode or change the character. condition, substance or structure of any steel, iron, brass or other metal parts upon which they are used; and on the contrary will preserve from the action of heat, oxidation of carbon, acidities, prevention of fires and add longer life to the lubricated parts.
(8) That 6 ounces of tungstate of soda, 5 ounces of ammonium muriate, 6 ounces of ammonium phosphate, 16 ounces of sal soda, 5 ounces of graphite, ounce of alum, and 6 ounces of ammonium sulfate all of which I mix together in the finest powder form and add to one gallon of lubricating oil and boil for thirty minutes is an improvement over my previous patent of February 10th, 1891, as a new and useful combination for a fireproof lubricating oil, for the lubrication of machinery or in the use of the techni all treatment of metals.
(9) -My object in the use, of 5 ounces of graphite combined with 6 ounces of tungstate of soda, 5 ounces of ammonium muriate, 6 ounces of ammonium phosphate, 16 ounces of sal soda, one half ounce of alum, and 6 ounces of ammonium sulfate, all of which I mix together in a finely powdered form and add to one gallon of lubricating oil and boil for thirty minutes. (a) that the use of the same (graphite) is demanded as a lubricant, (b) that the success of its use depends upon its suspension in a cool lubricant: since in the absence of the same it produces friction and heat. (0) -by the combination of one half ounce. of alum, graphite shows greater aliinity for the oil and other chemicals as used by me in my fornulla consisting of 6 ounces of tungstate of soda, 5 ounces of ammonium muriate, 6 ounces of ammonium phosphate, 16 ounces of sal soda. 5 ounces of graphite, -3 ounce of alum, and 6 ounces of ammonium sulfate, all of which I mix together in the finest powdered form and add to one gallon of lubricating oil and boil for thirty minutes. ((1) I further add 6 ounces of tungstate of soda, 5 ounces of ammonium muriate and 6 ounces of ammonium phosphate in the aforesaid proportions as mentioned in my formula and process for a new and improved lubricating oil for the purpose of rendering carbon or compounds of carbon incapable of taking fire by lessening molecular action of graphite in the presence of carbon compounds and oxygensucli as is required of perfect lubricating oils.
Having fully described my process and product, I claim,
An oil adapted to form a lubricant ofiering great resistance to heat, comprising an unctuous substance as a base, graphite and a mixture of chemical salts, namely, 6 ounces of tungstate of soda. 5 ounces of ammonium muriate, 6 ounces of ammonium phosphate, 16 ounces of sal soda, 5 ounces of graphite, 9 ounce of alum and 6 ounces of ammonium sulfate, mixed to one gallon of lubricating oil and boiled for one half hour.
ROBERT R. GRAF.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US8281316A US1181976A (en) | 1916-03-08 | 1916-03-08 | Fireproof lubricating-oil. |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US8281316A US1181976A (en) | 1916-03-08 | 1916-03-08 | Fireproof lubricating-oil. |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US1181976A true US1181976A (en) | 1916-05-02 |
Family
ID=3249949
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US8281316A Expired - Lifetime US1181976A (en) | 1916-03-08 | 1916-03-08 | Fireproof lubricating-oil. |
Country Status (1)
| Country | Link |
|---|---|
| US (1) | US1181976A (en) |
-
1916
- 1916-03-08 US US8281316A patent/US1181976A/en not_active Expired - Lifetime
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