TWM414261U - Low pressure distillation equipment - Google Patents

Low pressure distillation equipment Download PDF

Info

Publication number
TWM414261U
TWM414261U TW100204457U TW100204457U TWM414261U TW M414261 U TWM414261 U TW M414261U TW 100204457 U TW100204457 U TW 100204457U TW 100204457 U TW100204457 U TW 100204457U TW M414261 U TWM414261 U TW M414261U
Authority
TW
Taiwan
Prior art keywords
tray
steaming
tower
liquid
pressure distillation
Prior art date
Application number
TW100204457U
Other languages
Chinese (zh)
Inventor
shi-yun Luo
Original Assignee
Re Sun Machinery Ind Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Re Sun Machinery Ind Co Ltd filed Critical Re Sun Machinery Ind Co Ltd
Priority to TW100204457U priority Critical patent/TWM414261U/en
Publication of TWM414261U publication Critical patent/TWM414261U/en

Links

Landscapes

  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)

Description

M414261 五、新型說明: 【新型所屬之技術領域】 本新型係關於一種蒸餾塔的技術領域’特別是適用於含水 的液態混合物’例如酒、生質酒精或糠醇等物質的提純蒸餾塔 及其蒸餾方式。 【先前技術】 生質物質中,只要含有可發酵性糖,如蔗糖、葡萄糖、麥 芽糖、果糖、藻多糖等的,皆可以用來製造生質酒精。因此擁 有可轉變為發酵性糖的原料,如甘蔗、甜菜、甜高粱等含糖作 物,或含澱粉質的原料,如玉米、小麥、大麥、稻米、高粱、 燕麥等糧麵,和甘H、樹薯、馬鈴薯料類,以及富含纖維 素的稻桿、稻殼、玉米稈、麥稈、蔑逢、廢木塊、林木廢棄物、 樹葉等’都可加以利用。透過蒸煮以破壞植物組織,釋放儲藏 在植物細胞内義粉粒,然後再經過糖化過程,把殿粉質原料 轉化為糖,之後進入糖蜜發酵製程,再經由生物分解發酵、蒸 餾、脫水,便能產製成酒精。 ” -般生質物質直接轉销發㈣成約的含水 生質酒精’再經過蒸峨高濃度到9G%〜95%。傳統的方式 是藉由多個蒸顧塔相連’並依序進行第一次蒸顧、第二次蒸餘 及/或第三次蒸解。其所需設備較多,設備成本高、佔用較 大空間,而且需要較長的蒸餾時間。 中國專利⑽0945377揭示—種高效節能蒸潑塔組,包 3 M414261 括兩個或兩個以上的蒸娜、塔間冷卻塔和加熱導熱油的鍋 爐;所述的蒸鱗包括塔身、塔膽蒸顧裝置和塔底加熱裝置。 其雖然增加了 _原料與加絲置的接觸面積,使酒精原料得 以充分加絲發,提高蒸率,但其賴是多鱗體的組 CT所以蒸鶴设傷所需要的空間大,而且蒸餘時間長。 又中國專利CN2197364揭示-種工業用的酒精蒸館塔, 其包括塔殼體、位於塔殼體上的酒汽出口管、原料進料管、蒸 汽輸入管和排液管,其關鍵在於所述的塔殼體是由鐵板焊接成 的整體結構’在塔殼體上設有人孔,在塔殼體内壁上設有若干 個上下間格財❹職< 塔板,在細塔板的邊緣上均設有通 至其下一個塔板面上的順流板。在順流板的下端對著的塔板處 »又有盛液盤,塔板、順流板和盛液盤均架設在架上。此設計所 蒸館得到的酒精會先留置於盛液盤’且溢滿後攤流在相鄰的塔 板上。 台灣專利529632本創作系關於一種酒精蒸餾器結構,係 包括蒸發槽、第一冷卻系統、第二冷卻系統、氣水分離裝置及 收集槽等構成,其主要為使蒸發槽所蒸發之蒸氣經由第一冷卻 系統及氣水分離裝置來收集比重較輕的醛類或其他雜質物,而 於第一冷卻系統中未凝結之蒸氣則由第二冷卻系統冷凝收集 之’藉以去除蒸餾酒液中之醛類或其他雜質物者。 【新型内容】 β 本新型的目的係在提供一種低壓蒸餾設備,其具有在單一 4 塔體的作職得高濃度蒸舰的功效。 7動另_目_、在提供—種賴聽方法,其能夠在 體峽行混合細,藉此在較短科間下取得高濃度的 4根據上述的目的與功效,本新型所揭示的蒸館設備包含一 蒸潑塔加解元配置在該驗_部;—賴槽位在該墓 館塔—側,並且用關置待驗㈣;—連接管穿過該預熱 槽’且-端連接該蒸麟的蒸館出σ;—供液管—端連接於該 預熱槽,另一端伸入該塔體内。 而搭配上it細設騎使输的驗方法為在—預熱槽 内注入待麵液n ;接著將部份待蒸舰脸人細塔内使 其受熱汽化上升;而完成蒸餾的高溫氣體可被導入預熱槽内, 藉此提高待蒸餾液體的溫度;然後再將已提高溫度的待蒸餾液 體注入蒸德塔内與高溫的酒水蒸餾氣體混合並一同進行蒸餘。 以下即根據本新型的目的、功效及結構組態,舉出較佳實 施例,並配合圖式詳細說明。 【實施方式】 請參閱第1圖’圖中揭示蒸餘設備包含一蒸館塔1〇、一 預熱槽20、一冷凝器30及一暫存槽40。 蒸德塔1〇具有一塔體12,且在該塔體12的頂端設有一 蒸餾出口 14。其次塔體12的内部組設有複數個塔盤16,且這 些塔盤16分層地組設在塔體12的軸向。 M414261 又-加熱單元18配置在組設在塔體12内部下方;該加数 單元18可歧高溫蒸氣歧其他形式賭媒。—般而言,加 熱單元18可提供1〇〇度C以上的溫度。 ° 預熱槽20位在蒸德塔1〇的一側,其可用以容納待蒸館液 體22,例如酒、生質酒精或是糠醇等含水的混合物。‘、 一連接管24係穿過預熱槽2G,林—端連接蒸娜1〇 的蒸餾出口 14。M414261 V. New description: [New technical field] The present invention relates to a technical field of distillation towers, in particular to a purified distillation column suitable for aqueous liquid mixtures such as wine, bio-alcohol or sterol, and distillation thereof. the way. [Prior Art] Biomass can be used to produce bio-alcohol as long as it contains fermentable sugars such as sucrose, glucose, maltose, fructose, algal polysaccharides and the like. Therefore, there are raw materials that can be converted into fermentable sugar, such as sugar cane, sugar beet, sweet sorghum and other sugary crops, or raw materials containing starch, such as corn, wheat, barley, rice, sorghum, oats, etc., and Gan H, The cassava, potato, and cellulose-rich rice straw, rice husks, corn stalks, wheat straw, stalks, waste wood, forest waste, leaves, etc. can all be utilized. By cooking to destroy the plant tissue, releasing the stored particles in the plant cells, and then undergoing the saccharification process, converting the powdery raw materials into sugar, and then entering the molasses fermentation process, and then through biodegradation fermentation, distillation, and dehydration, Produced into alcohol. - The general biomass is directly transferred to the hair (four) into the relevant hydrous biomass alcohol 'after the high concentration of steamed sputum to 9G% ~ 95%. The traditional way is to connect by multiple steam towers ' and sequentially first The second steaming, the second steaming and/or the third steaming. It requires more equipment, high equipment cost, occupies a large space, and requires a long distillation time. Chinese Patent (10) 0945377 discloses a kind of high-efficiency steaming Pagoda group, package 3 M414261 comprises two or more steaming towers, an inter-column cooling tower and a boiler for heating heat transfer oil; the steaming scale comprises a tower body, a tower bile distillation device and a bottom heating device. Although the contact area between the raw material and the wire is increased, the alcohol raw material can be fully added and the steaming rate is increased. However, it depends on the multi-scale group CT, so the space required for steaming the crane is large, and the steaming The Chinese patent CN2197364 discloses an industrial alcohol steaming tower, which comprises a tower shell, a wine steam outlet pipe on the tower shell, a raw material feeding pipe, a steam inlet pipe and a drain pipe, the key The tower housing is welded by iron plates. The whole structure 'has a manhole on the tower shell, and there are several upper and lower compartments on the inner wall of the tower shell. The tray is provided on the edge of the thin tray to the next tray. The downstream plate on the surface. At the lower end of the downstream plate, there is a liquid tray, and the tray, the downstream plate and the liquid tray are erected on the frame. The alcohol obtained in the steaming hall of the design will be retained first. After the liquid tray is filled and spread over the adjacent trays, Taiwan Patent 529632 is based on an alcohol distiller structure including an evaporation tank, a first cooling system, a second cooling system, and gas-water separation. The device and the collecting tank are mainly configured to collect vapors evaporated by the evaporation tank through the first cooling system and the gas-water separation device to collect aldehydes or other impurities having a relatively small specific gravity, and are not condensed in the first cooling system. The vapor is collected by the second cooling system to remove the aldehydes or other impurities in the distilled liquor. [New content] β The purpose of the novel is to provide a low-pressure distillation apparatus having a single 4-tower body. High job The effect of steaming ships. 7 moving another _ _ _, in the provision of a kind of listening method, which can be mixed in the body gorge, thereby achieving a high concentration of 4 in a shorter section, according to the above purposes and effects, The steaming museum apparatus disclosed in the present invention comprises a steaming tower plus a solution element disposed in the inspection section; the shelf is located on the side of the tomb tower, and is closed (4); the connecting pipe passes through the The hot chute 'and-end is connected to the steaming kiln of the steaming kiln; the liquid supply pipe end is connected to the preheating tank, and the other end is extended into the tower body. In order to inject the surface liquid n into the preheating tank; then, some of the steam towers are steamed and heated to rise; and the high temperature gas that completes the distillation can be introduced into the preheating tank, thereby increasing the temperature to be distilled. The temperature of the liquid; then the liquid to be distilled having an increased temperature is injected into the steaming tower and mixed with the high-temperature distilled liquor of the wine and steamed together. DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS In the following, the preferred embodiments of the present invention will be described in detail with reference to the drawings. [Embodiment] Please refer to Fig. 1 to show that the steaming equipment includes a steaming tower 1 , a preheating tank 20, a condenser 30 and a temporary storage tank 40. The steam tower 1 has a column body 12, and a distillation outlet 14 is provided at the top end of the column body 12. Secondly, the inner portion of the tower body 12 is provided with a plurality of trays 16, and these trays 16 are layered in the axial direction of the tower body 12. M414261 Again, the heating unit 18 is disposed below the interior of the tower body 12; the adder unit 18 can distinguish between other forms of gambling media. In general, the heating unit 18 can provide a temperature above 1 degree C. ° The preheating tank 20 is located on the side of the steaming tower 1 ,, which can be used to accommodate the liquid to be steamed, such as wine, bio-alcohol or sterol. ‘, a connecting pipe 24 is passed through the preheating tank 2G, and the forest end is connected to the distillation outlet 14 of the steaming water.

一供液管26係-端連接預熱槽2〇,另一端伸入蒸館塔川 的塔體12内。 其次,冷凝器30的入口端係用以結合連接管24,或壯人 穿過預熱㈣的賴管;暫細4G肋結合綠^ %的出 口端。 清參閱第2圖,塔盤16係具有複數個貫穿構造的穿孔 他’而且在每-穿孔16的—側(如謝的上方)具有一擔面 脱。由於擋面咐與塔盤16表面相離,所以塔盤Μ表面與 擋面脱之間形成侧向通孔16e。其次,在塔盤16的側邊可 開設一個貫__執16d ;該空孔 穿孔16a。 狀於 而穿孔16a與空孔i6d皆形 上述的塔盤16是單一片體; 成於該片體上。 6 M414261 穿孔16a,且對各穿孔16a形成有擋面⑽。以各子板17组成 塔片16,其可使各子板17方便崎於塔體内。 至於塔盤16上的空孔16d則可藉由在適當位置不配置子 板17的方式而形成(如圖中處線所示)。 請參閱第4圖,以糖化發酵所製得之生質酒精作為待基館 液體22為例,其含有約12%至2〇%的酒精濃度,並 熱槽20内。 、 *當待蒸舰體22注入蒸鱗1〇内受加熱單元ΐδ加熱而 蒸發後,高溫的蒸賊體會朝著蒸邮口 14的方向移動。 由於在塔體U内配置有複數片的塔盤16,所以高 儲氣體的上升雜,會逐—通過其上升路徑巾每—塔盤Μ: 的穿孔16a。特別是’高溫蒸館氣體與塔盤16會不斷的產生 碰撞且需由穿孔16a通過,所以塔盤16可以有效的降緩高溫 氣體的上升速度以及有效地增加蒸域體留置在難塔1〇内 _間;進而由細出π 14可峰得的具有較高酒精濃度的 高溫酒水蒸餾氣體。 值得注意的是,高溫蒸餾氣體係流入連接管24内,而且 該連接管24可以穿過預熱槽20内部;因此高溫蒸館氣體可透 過連接管24與預熱槽20内的待蒸餾液體22進行熱交換,以 提高待蒸餾液體22的溫度。此方式可以讓預熱槽2〇無需搭配 額外的加熱元件而能提高待蒸餾液體22的溫度,達到預熱效 果。此外在進行蒸餾的過程中,因加熱單元18持續提供加熱 7 M414261 作用,所以塔體12内為高溫高壓的狀態。 接著將已提高溫度的待蒸餾液體22由供液管26注入塔體 12内,使待蒸餾液體22與塔體12内的高溫的酒水蒸餾氣體 混合。此時可以降低塔體12内的溫度與壓力。 更重要的是,酒精的汽化溫度約在78.3度C,水的汽化 溫度為100度C,而加熱單元18可以提供超過1〇〇度c的溫 度,所以先前塔體12内部的溫度可升至約1〇〇度c,此時酒 精與水皆可成汽化狀態;但當待蒸餾液體22注入高溫狀態的 塔體12且與酒水蒸餾氣體混合後,先前的酒水蒸餾氣體的溫 度可降至約90纟C(或更低),此時酒精仍為汽化狀態,而大部 份的水氣會凝結成水滴而落下,進而促使酒精與水分離;此時 由蒸顧出口 14所祕的高溫酒水蒸館氣體再經冷凝器3〇凝結 成液態補’可觀存在暫存槽4㈣,其鋪濃度可達9〇% ; 雖未達到無水_的程度,但已具有高的產糊用價值,且可 以降低再精顧成無水酒精的困難度。 此外由於待蒸顧液體22已具有較高溫度,所以後續進行 蒸館時可以麟蒸舰體22在短咖隨高至高溫汽化狀 態,所以可縮短蒸館時間。 請參閱第5圖’由於塔盤16上的穿孔收上方具有一指 面脱,所以高溫蒸館氣體通過穿孔恤時,其可受到撞面^ 的阻擋然後再由側邊的側向通孔16c穿出;如此不但可以使蒸 館氣體分散及均勻化,還可以有效地延緩蒸織體上升速度, 8 M414261 以及提高受熱蒸餾時間,以有助於提高蒸餾氣體中的酒 請再參閱第4圖,若塔盤16的穿孔i6a受阻塞,而導致 蒸餾氣體無法通過穿孔16a,則蒸餾氣體可以穿過空孔. 且因為相鄰塔盤16的空孔l6d係對應成相錯狀,所以可増加 蒸餾氣體的行進路程,以提高蒸餾效果。 請參閱第6圖,本新型可在塔盤16的一侧配置一幹板 ® 且檔板19的一端高於塔盤16的表面。 在一般穿孔16a呈現暢通的狀態下,擋板19具有局部限 制酒水蒸餾氣體通過空孔16d;然而當穿孔16a阻塞時,高溫 的酒水蒸餾氣體便可通過擋板19下緣的間隙19a,然後再上 升通過空孔16d。是以配設擋板19可以增加高溫難氣體與 塔盤16的碰撞機率與次數,並據此增加蒸餾時間及提高蒸餾 • 效果。此外擋板19搭配空孔脱的設計,可在穿孔16a受阻 塞時’使蒸餾塔仍保持可以正常運作。 另外、纟£適冨6十算後’本新型的穿孔16a孔徑與孔數的搭 配可使待蒸顧液22流落到塔板16上時,逐漸累積成一酒水液 體層,如此咼溫酒水蒸餾氣體在通過穿孔16a與酒水液體層 時,可以提絲精與水分的分離效果;而擋板19 一端高於塔 盤16表面,則有助於酒水液體層的形成。 由以上所說明結構及其使用狀態可知,本新型所揭示的蒸 餾設備因預熱後的待蒸餾液體22加入塔體12内並與塔體 9 12内部的高溫氣體混合以進行麟,同時降低論氣體的溫 又及塔體12内賴力,藉此使酒精與水分離,以形成低壓蒸 德效果’並取得高酒精濃度的蒸餾氣體。 而根據本新型的使用狀態,可進一步歸納其蒸館方法包含 以下步驟: 請參閱第7圖,步驟S51係於一前述的預熱槽内注入待蒸 顧液體,該待蒸館液體為含水的混合物,例如酒、生質酒精戈 糖醇等。本件酬書以生質蹄為實施例。 步驟S52係將部份待蒸餾液體注入前述的蒸餾塔内,使其 夂熱汽化上升;此時含酒精及水的蒸餾氣體呈現高溫狀態,而 且不斷的與蒸餾塔内的塔盤碰撞而均勻化。 步驟S53是將完成蒸_高溫氣體導入預熱槽,藉此提高 待蒸鶴液翻溫度;注縣意的是,「將高溫紐導人預熱槽」 可以是利用前述的連接管穿過預熱槽的結構形式,使高溫蒸氣 體與待蒸舰體進行熱交換,也可以將部份的高溫細氣體混 入待蒸館細喊麵槽人。無論那-獅Μ無需以加熱器 或加熱設備對該待蒸餾液體進行加熱,故可以達到節省能源的 效果。 步驟S54可再將已提高溫度的待蒸餾液體注入蒸餾塔内 與尚溫的蒸德氣體混合並一同進行蒸館;由於酒精的汽化溫度 低·於水,所以若蒸餾氣體的溫度低於水的汽化溫度,且高於酒 精的汽化溫度,則蒸餾氣體中大部份的水會凝結落下,如此在 蒸餾出口所取到的蒸餾氣體中便會含有較高比例的酒精濃度。 使用者可以重覆進行步驟S53及步驟S54以取得更多的高 濃度蒸餾氣體。 步驟S55是將取自蒸館出口的高溫蒸館氣體導向一冷凝 器以進行液化收集;而且所取到的液體可以存置在適當的暫存 槽。 以上乃本新型之較佳實施例以及設計圖式,惟較佳實施例 以及設計圖式僅是舉例說明,並非用於限制本新型技藝之權利 範圍,凡以均等之技藝手段、或為下述r申請專利範圍」内容 所涵蓋之權利範圍而實施者,均不脫離本新型之範疇而為申請 人之權利範圍。 【圖式簡單說明】 第1圖係本新型的結構示意圖。 第2圖係本新型塔盤結構示意圖。 第3圖係本新型塔盤的另一結構示意圖。 第4圖係本新型使用狀態示意圖。 第5圖係本新型蒸餾氣體通過塔盤受阻的狀態示意圖。 第6圖係本新型之塔盤配置擋板及蒸餾氣體運動狀態示意圖。 第7圖係本新型蒸餾方法的步驟方塊圖蒸餾。 【主要元件符號說明】 10蒸餾塔 12塔體 14蒸餾出口 16塔盤 M414261 16a穿孔 16b擋面 16c側向通孔 16d空孔 17子板 18加熱單元 19擋板 19a間隙 20預熱槽 22待蒸餾液體 24連接管 26供液管 30冷凝器 40暫存槽A liquid supply pipe 26 is connected to the preheating tank 2 at the end of the liquid supply pipe 26, and the other end is inserted into the tower body 12 of the steaming tower. Secondly, the inlet end of the condenser 30 is used to join the connecting pipe 24, or to pass through the preheating (four) sluice pipe; the temporary fine 4G rib is combined with the green terminal. Referring to Fig. 2, the tray 16 has a plurality of perforations in the through-structure and has a face-off on the side of each perforation 16 (as above). Since the face 咐 is separated from the surface of the tray 16, a lateral through hole 16e is formed between the surface of the tray and the surface. Next, a __16d can be opened on the side of the tray 16; the hole is perforated 16a. The perforations 16a and the holes i6d are both shaped. The tray 16 described above is a single sheet; formed on the sheet. 6 M414261 The perforations 16a are formed with a stop surface (10) for each of the perforations 16a. Each of the sub-boards 17 is composed of a tray 16, which allows each of the sub-boards 17 to be easily accommodated in the tower body. As for the hole 16d in the tray 16, it can be formed by not arranging the sub-board 17 at an appropriate position (as shown by the line in the figure). Referring to Fig. 4, the raw alcohol prepared by the saccharification fermentation is taken as an example of the liquid 22 to be used, which contains an alcohol concentration of about 12% to 2%, and is contained in the hot water tank 20. * When the steamed hull 22 is injected into the steaming scale 1 and heated by the heating unit ΐδ, the high-temperature steamed thief moves toward the steaming port 14. Since a plurality of trays 16 are disposed in the tower U, the rise of the high-storage gas will pass through the perforations 16a of the trays. In particular, the 'high-temperature steaming gas and the tray 16 will continuously collide and pass through the perforations 16a, so the tray 16 can effectively slow down the rising speed of the high-temperature gas and effectively increase the steaming body to remain in the difficult tower. _Intermediate; and further, a high-temperature distilled water gas having a higher alcohol concentration which is obtained by pulsing π 14 . It should be noted that the high temperature distillation gas system flows into the connecting pipe 24, and the connecting pipe 24 can pass through the inside of the preheating tank 20; therefore, the high temperature steaming gas can pass through the connecting pipe 24 and the liquid to be distilled in the preheating tank 20 Heat exchange is performed to increase the temperature of the liquid 22 to be distilled. This method allows the preheating tank 2 to increase the temperature of the liquid to be distilled 22 without the need for additional heating elements to achieve a preheating effect. Further, in the process of performing the distillation, since the heating unit 18 continuously supplies the heating 7 M414261, the inside of the tower body 12 is in a state of high temperature and high pressure. Next, the temperature-reduced liquid 22 to be distilled is injected into the column body 12 from the liquid supply pipe 26, and the liquid to be distilled 22 is mixed with the high-temperature wine distilled gas in the column body 12. At this time, the temperature and pressure in the tower body 12 can be lowered. More importantly, the vaporization temperature of alcohol is about 78.3 degrees C, the vaporization temperature of water is 100 degrees C, and the heating unit 18 can provide a temperature of more than 1 degree c, so the temperature inside the tower 12 can be raised to At about 1 degree c, both alcohol and water can be vaporized; however, when the liquid to be distilled 22 is injected into the column 12 in a high temperature state and mixed with the distilled liquor of the wine, the temperature of the previous distilled water of the wine can be reduced to about 90纟C (or lower), at this time, the alcohol is still vaporized, and most of the water will condense into water droplets and fall, which will promote the separation of alcohol and water. At this time, the high-temperature wine secreted by the steam outlet 14 The steaming hall gas is condensed into a liquid replenishment through the condenser 3〇, and there is a temporary storage tank 4 (four), and the paving concentration can reach 9〇%; although it does not reach the degree of anhydrous _, it has a high value for producing paste, and can Reduce the difficulty of refining into anhydrous alcohol. In addition, since the liquid to be distilled 22 already has a relatively high temperature, the steaming hull 22 can be vaporized from a short coffee to a high temperature at a subsequent steaming, so that the steaming time can be shortened. Please refer to Fig. 5 'Because the perforation on the tray 16 has a finger-off surface, the high-temperature steaming gas passes through the perforated shirt, which can be blocked by the collision surface and then by the side lateral through holes 16c. It can not only disperse and homogenize the vaporizer gas, but also effectively delay the rising speed of the steamed fabric, 8 M414261 and increase the heated distillation time to help improve the alcohol in the distilled gas. Please refer to Figure 4 again. If the perforation i6a of the tray 16 is blocked, and the distillation gas cannot pass through the perforations 16a, the distillation gas can pass through the pores. And since the pores 16d of the adjacent trays 16 are corresponding to the phase error, they can be added. The travel of the distillation gas to improve the distillation effect. Referring to Fig. 6, the present invention can be provided with a dry plate ® on one side of the tray 16 and one end of the baffle 19 is higher than the surface of the tray 16. In a state where the general perforation 16a is unobstructed, the baffle 19 has a partial restriction of the distilled water of the wine through the void 16d; however, when the perforation 16a is clogged, the high-temperature distilled alcohol gas can pass through the gap 19a of the lower edge of the baffle 19, and then Rise through the hole 16d. It is possible to increase the collision probability and the number of times of high-temperature difficult gas and the tray 16 by arranging the baffle 19, thereby increasing the distillation time and improving the distillation effect. In addition, the baffle 19 is designed with a hollow hole to allow the distillation column to remain in operation when the perforation 16a is blocked. In addition, after the 冨60 算 算 ' ' ' ' 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 本 ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' When passing through the perforation 16a and the wine liquid layer, the separation effect of the silk and the moisture can be improved; and the end of the baffle 19 is higher than the surface of the tray 16, which contributes to the formation of the liquid layer of the wine. It can be seen from the structure and the state of use described above that the distillation apparatus disclosed in the present invention is added to the tower body 12 by the preheated liquid 22 to be distilled and mixed with the high temperature gas inside the tower body 9 12 to carry out the lining, and at the same time reduce the theory. The temperature of the gas and the internal force of the tower body 12, thereby separating the alcohol from the water to form a low pressure steaming effect 'and obtaining a high alcohol concentration of the distillation gas. According to the state of use of the present invention, it can be further summarized that the steaming method comprises the following steps: Referring to FIG. 7, step S51 is to inject a liquid to be distilled in a preheating tank, and the liquid to be steamed is water-containing. Mixtures such as wine, bio-alcohol, and so on. This remuneration book uses the raw hoof as an example. Step S52 is: injecting a portion of the liquid to be distilled into the distillation column to cause the vaporization of the vapor to rise; at this time, the distilled gas containing alcohol and water exhibits a high temperature state, and continuously collides with the tray in the distillation tower to be uniformized. . Step S53 is to introduce the steaming_high temperature gas into the preheating tank, thereby increasing the temperature of the liquid to be steamed; the county intention is that the "high temperature lead conductor preheating tank" may be passed through the aforementioned connecting pipe. The structure of the hot trough allows the high-temperature vapor to exchange heat with the body to be steamed, and it is also possible to mix some of the high-temperature fine gas into the steaming chamber. No matter that - the Griffin does not need to heat the liquid to be distilled by a heater or a heating device, so that energy saving effect can be achieved. Step S54 can further inject the liquid to be distilled with the increased temperature into the distillation tower and mix with the steaming gas of the temperature and carry out the steaming together; since the vaporization temperature of the alcohol is low in water, if the temperature of the distilled gas is lower than that of water When the vaporization temperature is higher than the vaporization temperature of the alcohol, most of the water in the distillation gas will condense, so that the distillation gas taken at the distillation outlet will contain a higher proportion of alcohol. The user can repeat steps S53 and S54 to obtain more high-concentration distillation gas. In step S55, the high-temperature steaming gas taken from the steaming station outlet is directed to a condenser for liquefaction collection; and the taken liquid can be stored in an appropriate temporary storage tank. The above is a preferred embodiment and a design of the present invention. The preferred embodiments and the drawings are merely illustrative and not intended to limit the scope of the present invention. The scope of the rights covered by the content of the application for patents is not within the scope of this new type and is the scope of the applicant's rights. [Simple description of the drawing] Fig. 1 is a schematic view of the structure of the present invention. Figure 2 is a schematic view of the structure of the novel tray. Figure 3 is a schematic view of another structure of the novel tray. Figure 4 is a schematic diagram of the state of use of the present invention. Fig. 5 is a schematic view showing the state in which the distillation gas of the present invention is blocked by the tray. Fig. 6 is a schematic view showing the movement state of the baffle plate and the distillation gas of the present invention. Figure 7 is a block diagram of the distillation of the novel distillation process. [Main component symbol description] 10 distillation column 12 tower body 14 distillation outlet 16 tray M414261 16a perforation 16b stop surface 16c lateral through hole 16d hole 17 sub-plate 18 heating unit 19 baffle 19a gap 20 preheating tank 22 to be distilled Liquid 24 connection pipe 26 supply pipe 30 condenser 40 temporary storage tank

1212

Claims (1)

六、申請專利範圍: L —種低壓蒸餾設備,其包含: -蒸餘塔’係具有-塔體,該塔體的頂端為蒸館出口,該塔 _内部組設有複數個塔盤,且每一個塔盤皆具有魏個穿孔; 一加熱單元,係配置在該蒸餾塔内部; 一預熱槽’触在該細塔_側,_預置待細液體; 一連接管’係穿過該預熱槽内部,且_端連接該蒸館出口; 一供液管,係一端連接於該預熱槽,另一端伸入該塔體内; 其中,由該蒸餾出口流出的高溫蒸餾氣體藉該連接管與預熱槽 内的待蒸館液體形成熱交換,藉此提高待蒸鶴液體的溫度。 2·如申請專利範圍第1項所述之低壓蒸餾設備,更包含一冷凝 器及一暫存槽,其中該冷凝器連接該連接管,且該暫存槽連 接該冷凝器。 3.如申請專利範圍第1項所述之低壓蒸餾設備,其中該塔盤上 的每一穿孔皆具有一擋面,且該擋面與該穿孔間具有側向通 孔。 4·如申請專利範圍第3項所述之低壓蒸餾設備,其中該塔盤與 該擋面係為一體。 5. 如申請專利範圍第1項所述之低壓蒸餾設備,其中該塔盤上 具有空孔’該空孔的孔徑大於該穿孔,且相鄰塔盤的空孔成 相錯排列。 6. 如申請專利範圍第1項所述之低壓蒸餾設備,其中該塔盤的 13 M414261 一側配置有一擋板。 7.如申請專利範圍第6項所述之低壓蒸餾設備,其中該擋板的 一端高於塔盤的表面。Sixth, the scope of application for patents: L - a low-pressure distillation equipment, comprising: - a steaming tower " has a - tower body, the top of the tower is a steaming hall outlet, the tower _ internal group is provided with a plurality of trays, and Each tray has a perforation; a heating unit is disposed inside the distillation column; a preheating tank 'touches the thin tower_side, _presets a liquid to be fined; a connecting tube' passes through the pre- The inside of the heat sink, and the _ end is connected to the steaming gallery outlet; a liquid supply pipe is connected at one end to the preheating tank and the other end is inserted into the tower body; wherein the high temperature distillation gas flowing out from the distillation outlet is connected by the connection The tube forms a heat exchange with the liquid to be steamed in the preheating tank, thereby increasing the temperature of the liquid to be steamed. 2. The low-pressure distillation apparatus of claim 1, further comprising a condenser and a temporary storage tank, wherein the condenser is connected to the connection pipe, and the temporary storage tank is connected to the condenser. 3. The low pressure distillation apparatus of claim 1, wherein each of the perforations on the tray has a stop face and the through face has a lateral through hole therebetween. 4. The low pressure distillation apparatus of claim 3, wherein the tray is integral with the stop surface. 5. The low pressure distillation apparatus of claim 1, wherein the tray has a void having a larger diameter than the perforation, and the pores of the adjacent tray are arranged in a phase error. 6. The low pressure distillation apparatus of claim 1, wherein a baffle is disposed on a side of the 13 M414261 of the tray. 7. The low pressure distillation apparatus of claim 6, wherein one end of the baffle is higher than a surface of the tray.
TW100204457U 2011-03-14 2011-03-14 Low pressure distillation equipment TWM414261U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
TW100204457U TWM414261U (en) 2011-03-14 2011-03-14 Low pressure distillation equipment

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
TW100204457U TWM414261U (en) 2011-03-14 2011-03-14 Low pressure distillation equipment

Publications (1)

Publication Number Publication Date
TWM414261U true TWM414261U (en) 2011-10-21

Family

ID=46422240

Family Applications (1)

Application Number Title Priority Date Filing Date
TW100204457U TWM414261U (en) 2011-03-14 2011-03-14 Low pressure distillation equipment

Country Status (1)

Country Link
TW (1) TWM414261U (en)

Similar Documents

Publication Publication Date Title
US9345987B2 (en) Stripping absorption module
WO2019062816A1 (en) Continuous distillation process
CN201299982Y (en) Series-connected multi-level rectification solvent recovery device
US9360252B2 (en) Process and apparatus for removing heat and water from flue gas
CN104832938B (en) High-temperature flue gas recovery and heat energy utilization device and method for bamboo charcoal pyrolysis process
WO2015018196A1 (en) Continuous solid separation device and process for preparing fuel ethanol
CN107418979A (en) A kind of alcohol fuel energy-saving clean production method
CN106635709A (en) Brewing distillation device
CN202590405U (en) Triple effect concentration evaporator
CN205295296U (en) Split type white spirit distiller
CN102260314A (en) Betulin extraction method and device thereof
TWM414261U (en) Low pressure distillation equipment
CN205832658U (en) A kind of waste heat recycling device in xylose production process
TW201237161A (en) Low pressure distillation apparatus and distillation method thereof
CN107779370A (en) A kind of distilling device for producing white spirit
CN105214333B (en) The method of the efficiently purifying device and purification plant extract of one Plant Extracts
CN102094045A (en) Process and device for continuously separating ethanol from solid state fermentation materials
CN206252859U (en) A kind of concentrator based on steam heating power gain techniques
CN204447369U (en) A kind of tandem heater of acrylic acid dehydrating tower
CN206157127U (en) Evaporate wine and use wooden zhen zi
CN209010457U (en) A kind of refining system of biology vinegar liquid
CN102992952B (en) Alcohol differential pressure distillation production unit
CN207632774U (en) A kind of horizontal distilling apparatus and brewing device of making wine
CN206902116U (en) Efficient energy-saving brewing device
CN101612487A (en) The extraction of effective components of Chinese medicinal and concentrator and extraction and method for concentration

Legal Events

Date Code Title Description
MM4K Annulment or lapse of a utility model due to non-payment of fees