TWI664387B - 熱交換器，包含該熱交換器之反應器配置，及控制反應器溫度的方法 - Google Patents
熱交換器，包含該熱交換器之反應器配置，及控制反應器溫度的方法 Download PDFInfo
- Publication number
- TWI664387B TWI664387B TW104108662A TW104108662A TWI664387B TW I664387 B TWI664387 B TW I664387B TW 104108662 A TW104108662 A TW 104108662A TW 104108662 A TW104108662 A TW 104108662A TW I664387 B TWI664387 B TW I664387B
- Authority
- TW
- Taiwan
- Prior art keywords
- heat exchanger
- transfer medium
- reactor
- heat transfer
- heat
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract description 18
- 238000012546 transfer Methods 0.000 claims abstract description 128
- 239000007788 liquid Substances 0.000 claims abstract description 60
- 238000007789 sealing Methods 0.000 claims abstract description 6
- 238000006243 chemical reaction Methods 0.000 claims description 24
- 150000003839 salts Chemical class 0.000 claims description 15
- 230000003647 oxidation Effects 0.000 claims description 14
- 238000007254 oxidation reaction Methods 0.000 claims description 14
- HGINCPLSRVDWNT-UHFFFAOYSA-N Acrolein Chemical compound C=CC=O HGINCPLSRVDWNT-UHFFFAOYSA-N 0.000 claims description 8
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical group CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims description 4
- 125000005641 methacryl group Chemical group 0.000 claims description 4
- 238000001816 cooling Methods 0.000 claims description 3
- 238000007599 discharging Methods 0.000 claims description 3
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 2
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 2
- VQTUBCCKSQIDNK-UHFFFAOYSA-N Isobutene Chemical group CC(C)=C VQTUBCCKSQIDNK-UHFFFAOYSA-N 0.000 claims description 2
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 claims description 2
- 229940078552 o-xylene Drugs 0.000 claims description 2
- LGRFSURHDFAFJT-UHFFFAOYSA-N phthalic anhydride Chemical compound C1=CC=C2C(=O)OC(=O)C2=C1 LGRFSURHDFAFJT-UHFFFAOYSA-N 0.000 claims description 2
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 claims description 2
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 claims description 2
- 241000270295 Serpentes Species 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 17
- 239000002826 coolant Substances 0.000 description 9
- 239000000203 mixture Substances 0.000 description 6
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 description 4
- LPXPTNMVRIOKMN-UHFFFAOYSA-M sodium nitrite Chemical compound [Na+].[O-]N=O LPXPTNMVRIOKMN-UHFFFAOYSA-M 0.000 description 4
- 238000013461 design Methods 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 239000003054 catalyst Substances 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 230000002706 hydrostatic effect Effects 0.000 description 2
- 239000000155 melt Substances 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 235000010333 potassium nitrate Nutrition 0.000 description 2
- 239000004323 potassium nitrate Substances 0.000 description 2
- VWDWKYIASSYTQR-UHFFFAOYSA-N sodium nitrate Chemical compound [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 description 2
- 235000010288 sodium nitrite Nutrition 0.000 description 2
- 230000008016 vaporization Effects 0.000 description 2
- 238000009834 vaporization Methods 0.000 description 2
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 229910001963 alkali metal nitrate Inorganic materials 0.000 description 1
- -1 alkali metal nitrite Chemical class 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- JHIWVOJDXOSYLW-UHFFFAOYSA-N butyl 2,2-difluorocyclopropane-1-carboxylate Chemical compound CCCCOC(=O)C1CC1(F)F JHIWVOJDXOSYLW-UHFFFAOYSA-N 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 235000012489 doughnuts Nutrition 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 239000000374 eutectic mixture Substances 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 230000010412 perfusion Effects 0.000 description 1
- ZLMJMSJWJFRBEC-OUBTZVSYSA-N potassium-40 Chemical compound [40K] ZLMJMSJWJFRBEC-OUBTZVSYSA-N 0.000 description 1
- 230000003449 preventive effect Effects 0.000 description 1
- 239000012429 reaction media Substances 0.000 description 1
- 230000003134 recirculating effect Effects 0.000 description 1
- 238000012552 review Methods 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 235000010344 sodium nitrate Nutrition 0.000 description 1
- 239000004317 sodium nitrate Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F28—HEAT EXCHANGE IN GENERAL
- F28D—HEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
- F28D7/00—Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall
- F28D7/16—Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall the conduits being arranged in parallel spaced relation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
- B01J8/067—Heating or cooling the reactor
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F28—HEAT EXCHANGE IN GENERAL
- F28F—DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
- F28F27/00—Control arrangements or safety devices specially adapted for heat-exchange or heat-transfer apparatus
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00106—Controlling the temperature by indirect heat exchange
- B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
- B01J2208/00212—Plates; Jackets; Cylinders
- B01J2208/00221—Plates; Jackets; Cylinders comprising baffles for guiding the flow of the heat exchange medium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00106—Controlling the temperature by indirect heat exchange
- B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
- B01J2208/00256—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles in a heat exchanger for the heat exchange medium separate from the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00106—Controlling the temperature by indirect heat exchange
- B01J2208/00265—Part of all of the reactants being heated or cooled outside the reactor while recycling
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F28—HEAT EXCHANGE IN GENERAL
- F28D—HEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
- F28D21/00—Heat-exchange apparatus not covered by any of the groups F28D1/00 - F28D20/00
- F28D2021/0019—Other heat exchangers for particular applications; Heat exchange systems not otherwise provided for
- F28D2021/0022—Other heat exchangers for particular applications; Heat exchange systems not otherwise provided for for chemical reactors
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F28—HEAT EXCHANGE IN GENERAL
- F28D—HEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
- F28D21/00—Heat-exchange apparatus not covered by any of the groups F28D1/00 - F28D20/00
- F28D2021/0019—Other heat exchangers for particular applications; Heat exchange systems not otherwise provided for
- F28D2021/0061—Other heat exchangers for particular applications; Heat exchange systems not otherwise provided for for phase-change applications
- F28D2021/0064—Vaporizers, e.g. evaporators
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F28—HEAT EXCHANGE IN GENERAL
- F28F—DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
- F28F2265/00—Safety or protection arrangements; Arrangements for preventing malfunction
- F28F2265/12—Safety or protection arrangements; Arrangements for preventing malfunction for preventing overpressure
Landscapes
- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Heat-Exchange Devices With Radiators And Conduit Assemblies (AREA)
- Details Of Heat-Exchange And Heat-Transfer (AREA)
- Structure Of Emergency Protection For Nuclear Reactors (AREA)
- Heat-Pump Type And Storage Water Heaters (AREA)
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201461954669P | 2014-03-18 | 2014-03-18 | |
| US61/954,669 | 2014-03-18 | ||
| ??102014103691.3 | 2014-03-18 | ||
| DE102014103691.3A DE102014103691A1 (de) | 2014-03-18 | 2014-03-18 | Wärmetauscher, Reaktoranordnung umfassend diesen Wärmetauscher und Verfahren zum Temperieren eines Reaktors |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| TW201544784A TW201544784A (zh) | 2015-12-01 |
| TWI664387B true TWI664387B (zh) | 2019-07-01 |
Family
ID=54053408
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| TW104108662A TWI664387B (zh) | 2014-03-18 | 2015-03-18 | 熱交換器，包含該熱交換器之反應器配置，及控制反應器溫度的方法 |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US9797657B2 (enExample) |
| EP (1) | EP3120099B1 (enExample) |
| JP (1) | JP6429895B2 (enExample) |
| KR (1) | KR102364341B1 (enExample) |
| CN (1) | CN106104188B (enExample) |
| BR (1) | BR112016021210B1 (enExample) |
| DE (1) | DE102014103691A1 (enExample) |
| MY (1) | MY182526A (enExample) |
| RU (1) | RU2676167C2 (enExample) |
| SG (1) | SG11201607209UA (enExample) |
| TW (1) | TWI664387B (enExample) |
| WO (1) | WO2015140009A2 (enExample) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102014114193A1 (de) | 2014-09-30 | 2015-08-13 | Basf Se | Verfahren und Anlage zur Rückgewinnung von Acrylsäure |
| US20170356701A1 (en) * | 2016-06-13 | 2017-12-14 | Chevron U.S.A. Inc. | Apparatus, systems and methods for protection against high pressure gas intrusion in shell and tube heat exchangers |
| EA202091052A1 (ru) | 2017-10-27 | 2020-06-11 | Стамикарбон Б.В. | Карбаматный конденсатор высокого давления |
| EP3534100A1 (en) * | 2018-02-28 | 2019-09-04 | Valeo Autosystemy SP. Z.O.O. | A heat exchanger |
| JP2024524123A (ja) | 2021-06-16 | 2024-07-05 | ベーアーエスエフ・エスエー | 触媒気相反応のための管状反応器を停止および加熱するためのプロセス |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20080023175A1 (en) * | 2006-07-27 | 2008-01-31 | Manfred Lehr | Method of varying the temperature of a tube bundle reactor |
| CN102455139A (zh) * | 2011-10-18 | 2012-05-16 | 张周卫 | 一种带真空绝热的双股流低温螺旋缠绕管式换热器 |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE898917C (de) * | 1942-09-20 | 1953-12-07 | Aenne Maria Luise Moos | Allseitig geschlossener Solekuehler |
| DE1057623B (de) * | 1955-02-08 | 1959-05-21 | Foster Wheeler Ltd | Zum Waermeaustausch zwischen einer Fluessigkeit und einem anderen Medium dienender Waermeaustauscher |
| BE795180A (fr) * | 1972-02-16 | 1973-05-29 | Deggendorfer Werft Eisenbau | Groupe refroidisseur destine a des appareils pour la realisation de reactions chimiques exothermiques |
| US4511432A (en) * | 1982-09-07 | 1985-04-16 | Sephton Hugo H | Feed distribution method for vertical tube evaporation |
| ZA200004211B (en) * | 1999-08-31 | 2001-02-14 | Nippon Catalytic Chem Ind | Method for catalytic gas phase oxidation. |
| DE102004041777A1 (de) * | 2004-08-28 | 2006-03-02 | Bayer Materialscience Ag | Verfahren und Vorrichtung zur Herstellung von Phosgen |
| JP2009513921A (ja) * | 2005-10-26 | 2009-04-02 | ベール ゲーエムベーハー ウント コー カーゲー | 熱交換器、および熱交換器を製造するための方法 |
| DK2237869T3 (da) * | 2008-01-25 | 2011-12-05 | Basf Se | Reaktor til gennemførelse af højtryksreaktioner, fremgangsmåde til ibrugtagning samt fremgangsmåde til gennemførelse af en reaktion |
| DE102008048405B3 (de) * | 2008-09-23 | 2010-04-22 | Alstom Technology Ltd. | Rohrbündel-Wärmetauscher zur Regelung eines breiten Leistungsbereiches |
| CN201444004U (zh) * | 2009-06-22 | 2010-04-28 | 大连优力特换热设备制造有限公司 | 一种可拆卸板式换热器 |
| JP2012149871A (ja) * | 2010-12-28 | 2012-08-09 | Sumitomo Chemical Co Ltd | 多管式熱交換構造 |
| RU134687U1 (ru) * | 2013-04-08 | 2013-11-20 | Федеральное государственное бюджетное образовательное учреждение высшего профессионального образования "Санкт-Петербургский государственный морской технический университет" | Система пассивного отвода тепла реакторной установки |
| CN203349689U (zh) * | 2013-05-16 | 2013-12-18 | 江苏昊隆换热器有限公司 | 一种新型板式换热器 |
-
2014
- 2014-03-18 DE DE102014103691.3A patent/DE102014103691A1/de not_active Withdrawn
-
2015
- 2015-03-10 JP JP2016558126A patent/JP6429895B2/ja active Active
- 2015-03-10 KR KR1020167028745A patent/KR102364341B1/ko active Active
- 2015-03-10 CN CN201580014566.2A patent/CN106104188B/zh active Active
- 2015-03-10 WO PCT/EP2015/054962 patent/WO2015140009A2/de not_active Ceased
- 2015-03-10 RU RU2016140695A patent/RU2676167C2/ru active
- 2015-03-10 MY MYPI2016001659A patent/MY182526A/en unknown
- 2015-03-10 BR BR112016021210-0A patent/BR112016021210B1/pt active IP Right Grant
- 2015-03-10 SG SG11201607209UA patent/SG11201607209UA/en unknown
- 2015-03-10 EP EP15710466.2A patent/EP3120099B1/de active Active
- 2015-03-18 US US14/661,408 patent/US9797657B2/en active Active
- 2015-03-18 TW TW104108662A patent/TWI664387B/zh active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20080023175A1 (en) * | 2006-07-27 | 2008-01-31 | Manfred Lehr | Method of varying the temperature of a tube bundle reactor |
| CN102455139A (zh) * | 2011-10-18 | 2012-05-16 | 张周卫 | 一种带真空绝热的双股流低温螺旋缠绕管式换热器 |
Also Published As
| Publication number | Publication date |
|---|---|
| KR102364341B1 (ko) | 2022-02-17 |
| RU2016140695A3 (enExample) | 2018-10-24 |
| MY182526A (en) | 2021-01-25 |
| EP3120099B1 (de) | 2019-06-12 |
| JP6429895B2 (ja) | 2018-11-28 |
| CN106104188A (zh) | 2016-11-09 |
| DE102014103691A1 (de) | 2015-09-24 |
| US9797657B2 (en) | 2017-10-24 |
| CN106104188B (zh) | 2018-10-09 |
| BR112016021210B1 (pt) | 2020-12-29 |
| WO2015140009A2 (de) | 2015-09-24 |
| EP3120099A2 (de) | 2017-01-25 |
| KR20160133544A (ko) | 2016-11-22 |
| SG11201607209UA (en) | 2016-10-28 |
| RU2016140695A (ru) | 2018-04-18 |
| TW201544784A (zh) | 2015-12-01 |
| WO2015140009A3 (de) | 2016-03-10 |
| JP2017510783A (ja) | 2017-04-13 |
| RU2676167C2 (ru) | 2018-12-26 |
| US20150267967A1 (en) | 2015-09-24 |
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